MX2019011612A - Metodo para producir acido acetico. - Google Patents
Metodo para producir acido acetico.Info
- Publication number
- MX2019011612A MX2019011612A MX2019011612A MX2019011612A MX2019011612A MX 2019011612 A MX2019011612 A MX 2019011612A MX 2019011612 A MX2019011612 A MX 2019011612A MX 2019011612 A MX2019011612 A MX 2019011612A MX 2019011612 A MX2019011612 A MX 2019011612A
- Authority
- MX
- Mexico
- Prior art keywords
- removal
- acetaldehyde
- acetic acid
- mass
- concentration
- Prior art date
Links
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 title abstract 9
- 238000000034 method Methods 0.000 title abstract 3
- IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 abstract 8
- 239000008346 aqueous phase Substances 0.000 abstract 3
- 238000009835 boiling Methods 0.000 abstract 3
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 abstract 2
- KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 abstract 2
- 238000004519 manufacturing process Methods 0.000 abstract 2
- 238000005810 carbonylation reaction Methods 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 238000001704 evaporation Methods 0.000 abstract 1
- 230000008020 evaporation Effects 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 239000012074 organic phase Substances 0.000 abstract 1
- 239000012286 potassium permanganate Substances 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C53/00—Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
- C07C53/08—Acetic acid
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/10—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
- C07C51/12—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Se proporciona un método que permite la producción industrialmente eficiente de ácido acético de alta calidad con un buen valor de prueba de permanganato de potasio y un bajo contenido de impureza sin un costo elevado; el método para producir ácido acético de acuerdo con la presente invención tiene un paso de reacción de carbonilación, un paso de evaporación y un paso de eliminación del componente con punto de ebullición inferior, y en donde con calentamiento del evaporador, (i) una concentración del acetaldehído en la fase acuosa de un condensado superior en una columna de eliminación del componente con punto de ebullición inferior se controla a no menos de 2340 ppm en masa; y/o (ii) una concentración de acetato de metilo en la fase acuosa se controla a menos de 19.0% en masa, y/o; (iii) una concentración de acetato de metilo en la fase orgánica del condensado superior en la columna de eliminación del componente con punto de ebullición inferior se controla a menos de 38.0% en masa, y luego por lo menos una porción de la fase acuosa se trata en el paso de eliminación y separación del acetaldehído para reciclar un líquido residual después de la separación y eliminación del acetaldehído al recipiente de reacción y/o el paso de eliminación o separación del acetaldehído y/u otros procesos.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2017062764 | 2017-03-28 | ||
| PCT/JP2017/019579 WO2018179457A1 (ja) | 2017-03-28 | 2017-05-25 | 酢酸の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2019011612A true MX2019011612A (es) | 2019-11-18 |
| MX375788B MX375788B (es) | 2025-03-07 |
Family
ID=60037537
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2019011612A MX375788B (es) | 2017-03-28 | 2017-05-25 | Metodo para producir acido acetico |
Country Status (13)
| Country | Link |
|---|---|
| EP (1) | EP3401303B1 (es) |
| JP (1) | JP6481043B1 (es) |
| KR (1) | KR102328843B1 (es) |
| CN (1) | CN110191874A (es) |
| AR (1) | AR111174A1 (es) |
| BR (1) | BR112019018754A2 (es) |
| ES (1) | ES2779805T3 (es) |
| MX (1) | MX375788B (es) |
| MY (1) | MY189357A (es) |
| PH (1) | PH12019550201A1 (es) |
| SG (1) | SG11201908151VA (es) |
| TW (1) | TWI701234B (es) |
| WO (1) | WO2018179457A1 (es) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB202015833D0 (en) * | 2020-10-06 | 2020-11-18 | Bp Chem Int Ltd | Separation process and apparatus |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3244350B2 (ja) | 1993-07-08 | 2002-01-07 | ダイセル化学工業株式会社 | 高純度酢酸の製造方法 |
| TW283702B (es) * | 1993-07-08 | 1996-08-21 | Daicel Chem | |
| US5625095A (en) * | 1994-06-15 | 1997-04-29 | Daicel Chemical Industries, Ltd. | Process for producing high purity acetic acid |
| IN192600B (es) | 1996-10-18 | 2004-05-08 | Hoechst Celanese Corp | |
| US7485749B2 (en) * | 2006-08-22 | 2009-02-03 | Lyondell Chemical Technology, L.P. | Preparation of acetic acid |
| US7619113B2 (en) * | 2007-09-27 | 2009-11-17 | Celanese International Corporation | Method and apparatus for making acetic acid with improved purification |
| US7820855B2 (en) | 2008-04-29 | 2010-10-26 | Celanese International Corporation | Method and apparatus for carbonylating methanol with acetic acid enriched flash stream |
| US8586789B2 (en) * | 2009-03-30 | 2013-11-19 | Lyondell Chemical Technology, L.P. | Removing hydrocarbon impurities from acetic acid production intermediate |
| JP5837576B2 (ja) * | 2010-05-18 | 2015-12-24 | セラニーズ・インターナショナル・コーポレーション | 過マンガン酸塩還元性化合物を除去することによって酢酸流を精製する方法 |
| US8940932B2 (en) * | 2010-10-06 | 2015-01-27 | Daicel Corporation | Process for producing acetic acid |
| WO2012081418A1 (ja) * | 2010-12-15 | 2012-06-21 | 株式会社ダイセル | 酢酸の製造方法 |
| TWI547477B (zh) * | 2012-03-14 | 2016-09-01 | 大賽璐股份有限公司 | 醋酸之製造方法 |
| MX356188B (es) * | 2012-12-21 | 2018-05-16 | Daicel Corp | Procedimiento para producir acido acetico. |
| US9233907B1 (en) * | 2014-11-14 | 2016-01-12 | Celanese International Corporation | Reducing hydrogen iodide content in carbonylation processes |
| US9512056B2 (en) * | 2015-02-04 | 2016-12-06 | Celanese International Corporation | Process to control HI concentration in residuum stream |
| WO2016194850A1 (ja) * | 2015-06-01 | 2016-12-08 | 株式会社ダイセル | 酢酸の製造方法 |
| US9302974B1 (en) * | 2015-07-01 | 2016-04-05 | Celanese International Corporation | Process for producing acetic acid |
-
2017
- 2017-05-25 JP JP2017536046A patent/JP6481043B1/ja active Active
- 2017-05-25 CN CN201780083025.4A patent/CN110191874A/zh active Pending
- 2017-05-25 KR KR1020197030525A patent/KR102328843B1/ko active Active
- 2017-05-25 MY MYPI2019005733A patent/MY189357A/en unknown
- 2017-05-25 MX MX2019011612A patent/MX375788B/es active IP Right Grant
- 2017-05-25 ES ES17737197T patent/ES2779805T3/es active Active
- 2017-05-25 EP EP17737197.8A patent/EP3401303B1/en active Active
- 2017-05-25 BR BR112019018754A patent/BR112019018754A2/pt not_active IP Right Cessation
- 2017-05-25 SG SG11201908151V patent/SG11201908151VA/en unknown
- 2017-05-25 WO PCT/JP2017/019579 patent/WO2018179457A1/ja not_active Ceased
- 2017-06-22 TW TW106120838A patent/TWI701234B/zh active
-
2018
- 2018-03-12 AR ARP180100567A patent/AR111174A1/es unknown
-
2019
- 2019-09-25 PH PH12019550201A patent/PH12019550201A1/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| WO2018179457A1 (ja) | 2018-10-04 |
| MY189357A (en) | 2022-02-07 |
| EP3401303B1 (en) | 2020-02-12 |
| KR20190127857A (ko) | 2019-11-13 |
| AR111174A1 (es) | 2019-06-12 |
| EP3401303A1 (en) | 2018-11-14 |
| JP6481043B1 (ja) | 2019-03-13 |
| KR102328843B1 (ko) | 2021-11-19 |
| TW201840522A (zh) | 2018-11-16 |
| PH12019550201A1 (en) | 2020-07-06 |
| SG11201908151VA (en) | 2019-10-30 |
| BR112019018754A2 (pt) | 2020-04-07 |
| EP3401303A4 (en) | 2018-11-14 |
| TWI701234B (zh) | 2020-08-11 |
| MX375788B (es) | 2025-03-07 |
| ES2779805T3 (es) | 2020-08-19 |
| CN110191874A (zh) | 2019-08-30 |
| JPWO2018179457A1 (ja) | 2019-04-04 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant or registration |