MX2019003391A - Produccion continua de materiales en capas 2d exfoliados mediante flujo de compresion. - Google Patents
Produccion continua de materiales en capas 2d exfoliados mediante flujo de compresion.Info
- Publication number
- MX2019003391A MX2019003391A MX2019003391A MX2019003391A MX2019003391A MX 2019003391 A MX2019003391 A MX 2019003391A MX 2019003391 A MX2019003391 A MX 2019003391A MX 2019003391 A MX2019003391 A MX 2019003391A MX 2019003391 A MX2019003391 A MX 2019003391A
- Authority
- MX
- Mexico
- Prior art keywords
- exfoliated
- continuous production
- layered
- layered materials
- compressive flow
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B9/00—Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00
- B32B9/04—Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00 comprising such particular substance as the main or only constituent of a layer, which is next to another layer of the same or of a different material
- B32B9/041—Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00 comprising such particular substance as the main or only constituent of a layer, which is next to another layer of the same or of a different material of metal
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/40—Compounds of aluminium
- C09C1/42—Clays
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/182—Graphene
- C01B32/184—Preparation
- C01B32/19—Preparation by exfoliation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
- B05B1/00—Nozzles, spray heads or other outlets, with or without auxiliary devices such as valves, heating means
- B05B1/02—Nozzles, spray heads or other outlets, with or without auxiliary devices such as valves, heating means designed to produce a jet, spray, or other discharge of particular shape or nature, e.g. in single drops, or having an outlet of particular shape
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
- B05B1/00—Nozzles, spray heads or other outlets, with or without auxiliary devices such as valves, heating means
- B05B1/02—Nozzles, spray heads or other outlets, with or without auxiliary devices such as valves, heating means designed to produce a jet, spray, or other discharge of particular shape or nature, e.g. in single drops, or having an outlet of particular shape
- B05B1/04—Nozzles, spray heads or other outlets, with or without auxiliary devices such as valves, heating means designed to produce a jet, spray, or other discharge of particular shape or nature, e.g. in single drops, or having an outlet of particular shape in flat form, e.g. fan-like, sheet-like
- B05B1/044—Slits, e.g. narrow openings defined by two straight and parallel lips; Elongated outlets for producing very wide discharges, e.g. fluid curtains
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B33/00—Layered products characterised by particular properties or particular surface features, e.g. particular surface coatings; Layered products designed for particular purposes not covered by another single class
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y40/00—Manufacture or treatment of nanostructures
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
- C01B21/064—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with boron
- C01B21/0648—After-treatment, e.g. grinding, purification
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/182—Graphene
- C01B32/194—After-treatment
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/20—Graphite
- C01B32/21—After-treatment
- C01B32/22—Intercalation
- C01B32/225—Expansion; Exfoliation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G39/00—Compounds of molybdenum
- C01G39/06—Sulfides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
- C01P2002/82—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by IR- or Raman-data
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
- C01P2002/84—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by UV- or VIS- data
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/20—Particle morphology extending in two dimensions, e.g. plate-like
- C01P2004/24—Nanoplates, i.e. plate-like particles with a thickness from 1-100 nanometer
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/26—Electron or ion microscopes; Electron or ion diffraction tubes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Nanotechnology (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Ceramic Engineering (AREA)
- Dispersion Chemistry (AREA)
- General Physics & Mathematics (AREA)
- Manufacturing & Machinery (AREA)
- Crystallography & Structural Chemistry (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- Developing Agents For Electrophotography (AREA)
- Prostheses (AREA)
- Nozzles (AREA)
- Carbon And Carbon Compounds (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Disintegrating Or Milling (AREA)
- Adornments (AREA)
- Preparation Of Clay, And Manufacture Of Mixtures Containing Clay Or Cement (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
Se describen en la presente métodos para la producción continua de un material bidimensional (2D) exfoliado que comprende pasar una mezcla de material 2D a través de una boquilla convergente y divergente, la mezcla de material 2D comprende un material en capas 2D y un fluido comprimible. El método de la presente descripción emplea compresión y expansión física de un flujo de gases a alta presión, lo cual deja el material en capas 2D prácticamente sin defectos para producir un material en capas 2D exfoliado de una manera simple, continua y ecológica.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201662402591P | 2016-09-30 | 2016-09-30 | |
| PCT/US2017/053691 WO2018064152A1 (en) | 2016-09-30 | 2017-09-27 | Continuous production of exfoliated 2d layered materials by compressive flow |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX2019003391A true MX2019003391A (es) | 2019-06-06 |
Family
ID=61756903
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2019003391A MX2019003391A (es) | 2016-09-30 | 2017-09-27 | Produccion continua de materiales en capas 2d exfoliados mediante flujo de compresion. |
Country Status (11)
| Country | Link |
|---|---|
| US (2) | US10882276B2 (es) |
| EP (1) | EP3490717B1 (es) |
| JP (1) | JP7094024B2 (es) |
| KR (1) | KR102498683B1 (es) |
| CN (2) | CN109803768A (es) |
| AU (1) | AU2017335685B2 (es) |
| CA (1) | CA3036086A1 (es) |
| IL (1) | IL265404B2 (es) |
| MX (1) | MX2019003391A (es) |
| TW (1) | TWI743215B (es) |
| WO (1) | WO2018064152A1 (es) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109803768A (zh) * | 2016-09-30 | 2019-05-24 | 加利福尼亚大学董事会 | 通过压缩流连续产生剥离型2d层状材料 |
| CN111377436A (zh) * | 2018-12-31 | 2020-07-07 | 浙江工业大学 | 一种气体驱动的层状材料剥离装置及剥离方法 |
| US11581430B2 (en) * | 2019-08-22 | 2023-02-14 | Globalfoundries U.S. Inc. | Planar transistor device comprising at least one layer of a two-dimensional (2D) material and methods for making such transistor devices |
| EP4045470A4 (en) * | 2019-10-14 | 2023-11-08 | C-crete Technologies, LLC | CEMENTITIOUS COMPOSITES PREPARED FROM CARBON-BASED NANOMATERIALS |
| CN110642295B (zh) * | 2019-10-25 | 2021-08-03 | 四川大学 | 基于固相力化学反应器的二硫化钼纳米片层剥离制备方法 |
| US11177182B2 (en) | 2020-01-30 | 2021-11-16 | Globalfoundries U.S. Inc. | Vertical transistor device comprising a two-dimensional (2D) material positioned in a channel region of the device and methods of making such vertical transistor devices |
| US11094791B1 (en) | 2020-01-30 | 2021-08-17 | Globalfoundries U.S. Inc. | Vertical transistor device with source/drain regions comprising a twi-dimensional (2D) material and methods of making such vertical transistor devices |
| GB2606689B (en) * | 2021-03-17 | 2024-12-11 | Qinetiq Ltd | Deposition method |
| KR20230033369A (ko) * | 2021-09-01 | 2023-03-08 | 주식회사 씨앤씨머티리얼즈 | 육방정 질화붕소 나노시트 분산 조성물 및 그 제조 방법 |
| KR102611645B1 (ko) * | 2023-05-03 | 2023-12-08 | 이승민 | 건식 박리를 통한 2차원 물질의 제조방법 및 이를 이용하여 제조된 2차원 물질 |
| JP2025098969A (ja) * | 2023-12-20 | 2025-07-02 | 国立研究開発法人農業・食品産業技術総合研究機構 | 遷移金属カルコゲニド薄膜の配向性制御方法、製造方法、製造装置、及び、フレキシブル基板 |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5549162A (en) | 1978-10-03 | 1980-04-09 | Ikeuchi:Kk | Mist producting device |
| KR0137839B1 (ko) | 1994-06-10 | 1998-06-15 | 석진철 | 동기형 모터의 스테이터 구조 |
| JP2000015126A (ja) | 1998-06-29 | 2000-01-18 | Minolta Co Ltd | 流動層型ジェット粉砕機 |
| US20020054995A1 (en) * | 1999-10-06 | 2002-05-09 | Marian Mazurkiewicz | Graphite platelet nanostructures |
| US7166657B2 (en) | 2002-03-15 | 2007-01-23 | Eastman Kodak Company | Article utilizing highly branched polymers to splay layered materials |
| US6863983B2 (en) | 2002-06-25 | 2005-03-08 | University Of Massachusetts | Layered silicate material and applications of layered materials with porous layers |
| US7105108B2 (en) | 2002-08-15 | 2006-09-12 | Advanced Energy Technology Inc. | Graphite intercalation and exfoliation process |
| US20050214474A1 (en) * | 2004-03-24 | 2005-09-29 | Taeyoung Han | Kinetic spray nozzle system design |
| US7754184B2 (en) | 2006-06-08 | 2010-07-13 | Directa Plus Srl | Production of nano-structures |
| US7785492B1 (en) | 2006-09-26 | 2010-08-31 | Nanotek Instruments, Inc. | Mass production of nano-scaled platelets and products |
| BE1017673A3 (fr) | 2007-07-05 | 2009-03-03 | Fib Services Internat | Procede et dispositif de projection de matiere pulverulente dans un gaz porteur. |
| US7790285B2 (en) | 2007-12-17 | 2010-09-07 | Nanotek Instruments, Inc. | Nano-scaled graphene platelets with a high length-to-width aspect ratio |
| US8696938B2 (en) | 2008-08-25 | 2014-04-15 | Nanotek Instruments, Inc. | Supercritical fluid process for producing nano graphene platelets |
| WO2011020035A2 (en) * | 2009-08-14 | 2011-02-17 | Northwestern University | Sorting two-dimensional nanomaterials by thickness |
| US8414799B2 (en) | 2010-06-18 | 2013-04-09 | National Defense University | Method for manufacturing graphene |
| JP5877590B2 (ja) | 2010-12-22 | 2016-03-08 | プラズマ技研工業株式会社 | コールドスプレー用ノズル及びそのコールドスプレー用ノズルを用いたコールドスプレー装置 |
| US9914108B2 (en) * | 2011-07-19 | 2018-03-13 | The Australian National University | Exfoliating laminar material by ultrasonication in surfactant |
| US8734683B2 (en) | 2011-11-29 | 2014-05-27 | Xerox Corporation | Graphene nano-sheets and methods for making the same |
| KR101387007B1 (ko) * | 2012-06-08 | 2014-04-18 | (주) 시온텍 | 그래핀의 제조방법 |
| JP2014104405A (ja) | 2012-11-27 | 2014-06-09 | Rix Corp | 凝集体の分散装置および分散方法 |
| KR101378734B1 (ko) * | 2013-01-22 | 2014-04-04 | 주식회사 제이오 | 고온-고압 매체를 이용한 그라파이트 박리 장치 및 방법 |
| GB201304770D0 (en) * | 2013-03-15 | 2013-05-01 | Provost Fellows Foundation Scholars And The Other Members Of Board Of | A scalable process for producing exfoliated defect-free, non-oxidised 2-dimens ional materials in large quantities |
| CN103350554B (zh) * | 2013-06-17 | 2015-11-04 | 南京科孚纳米技术有限公司 | 一种对流气体剪切剥离二维层状材料的方法 |
| FR3009298B1 (fr) | 2013-07-31 | 2018-06-08 | Univ Bordeaux 1 | Procede d'exfoliation de graphite assiste par reaction de diels-alder |
| GB201401715D0 (en) | 2014-01-31 | 2014-03-19 | Univ Manchester | Exfoliation |
| CN103977870B (zh) * | 2014-05-26 | 2016-03-30 | 北京航空航天大学 | 采用气流粉碎剥离工艺制备石墨烯前驱体二维纳米石墨粉的方法 |
| KR101625023B1 (ko) * | 2014-08-18 | 2016-05-27 | 조종수 | 그래핀 복합 유기용액의 제조방법 및 이 방법으로 제조한 그래핀 복합 유기용액 |
| KR101808230B1 (ko) * | 2015-10-13 | 2017-12-13 | 한국과학기술연구원 | 연속적인 전단응력과 유체충돌방식을 이용한 층상 구조 물질의 판상형 나노시트의 제조방법 |
| CN105540575A (zh) * | 2016-01-28 | 2016-05-04 | 成都新柯力化工科技有限公司 | 一种利用高压均质机剥离制备石墨烯的方法 |
| CA2972284C (en) | 2016-07-05 | 2019-05-14 | Vln Advanced Technologies Inc. | Apparatus and method for preparing graphene by exfoliation of graphite using a pulsed or cavitating waterjet |
| CN109803768A (zh) | 2016-09-30 | 2019-05-24 | 加利福尼亚大学董事会 | 通过压缩流连续产生剥离型2d层状材料 |
| JP6449390B1 (ja) | 2017-08-09 | 2019-01-09 | 住友理工株式会社 | 導電性膜の製造方法 |
| EP3636592A1 (en) | 2018-10-12 | 2020-04-15 | Advanced Material Development Limited | Liquid-exfoliated nanomaterials |
-
2017
- 2017-09-27 CN CN201780059878.4A patent/CN109803768A/zh active Pending
- 2017-09-27 EP EP17857322.6A patent/EP3490717B1/en active Active
- 2017-09-27 JP JP2019516104A patent/JP7094024B2/ja active Active
- 2017-09-27 MX MX2019003391A patent/MX2019003391A/es unknown
- 2017-09-27 AU AU2017335685A patent/AU2017335685B2/en active Active
- 2017-09-27 KR KR1020197009316A patent/KR102498683B1/ko active Active
- 2017-09-27 WO PCT/US2017/053691 patent/WO2018064152A1/en not_active Ceased
- 2017-09-27 CN CN202210999303.3A patent/CN115196624A/zh active Pending
- 2017-09-27 US US15/716,706 patent/US10882276B2/en active Active
- 2017-09-27 CA CA3036086A patent/CA3036086A1/en active Pending
- 2017-09-29 TW TW106133708A patent/TWI743215B/zh active
-
2019
- 2019-03-17 IL IL265404A patent/IL265404B2/en unknown
-
2020
- 2020-12-02 US US17/109,261 patent/US11472158B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| EP3490717B1 (en) | 2022-08-03 |
| US20180093454A1 (en) | 2018-04-05 |
| TW201813944A (zh) | 2018-04-16 |
| JP7094024B2 (ja) | 2022-07-01 |
| WO2018064152A1 (en) | 2018-04-05 |
| KR102498683B1 (ko) | 2023-02-09 |
| AU2017335685A1 (en) | 2019-05-02 |
| KR20190062417A (ko) | 2019-06-05 |
| CN109803768A (zh) | 2019-05-24 |
| US20210154977A1 (en) | 2021-05-27 |
| CA3036086A1 (en) | 2018-04-05 |
| EP3490717A1 (en) | 2019-06-05 |
| US10882276B2 (en) | 2021-01-05 |
| IL265404A (en) | 2019-05-30 |
| TWI743215B (zh) | 2021-10-21 |
| IL265404B2 (en) | 2023-07-01 |
| EP3490717A4 (en) | 2020-06-17 |
| JP2019532001A (ja) | 2019-11-07 |
| US11472158B2 (en) | 2022-10-18 |
| CN115196624A (zh) | 2022-10-18 |
| IL265404B1 (en) | 2023-03-01 |
| AU2017335685B2 (en) | 2022-09-29 |
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