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MX2019002738A - Procedimiento para producir sulfato de potasio a partir de cloruro de potasio y acido sulfurico. - Google Patents

Procedimiento para producir sulfato de potasio a partir de cloruro de potasio y acido sulfurico.

Info

Publication number
MX2019002738A
MX2019002738A MX2019002738A MX2019002738A MX2019002738A MX 2019002738 A MX2019002738 A MX 2019002738A MX 2019002738 A MX2019002738 A MX 2019002738A MX 2019002738 A MX2019002738 A MX 2019002738A MX 2019002738 A MX2019002738 A MX 2019002738A
Authority
MX
Mexico
Prior art keywords
sulfuric acid
potassium chloride
potassium
hydrochloric acid
potassium sulfate
Prior art date
Application number
MX2019002738A
Other languages
English (en)
Inventor
Bessenet Sebastien
Le Flammec Didier
Original Assignee
Veolia Water Tech Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Veolia Water Tech Inc filed Critical Veolia Water Tech Inc
Publication of MX2019002738A publication Critical patent/MX2019002738A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D5/00—Sulfates or sulfites of sodium, potassium or alkali metals in general
    • C01D5/04—Preparation of sulfates with the aid of sulfurous acid or sulfites, e.g. Hargreaves process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0018—Evaporation of components of the mixture to be separated
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/004—Fractional crystallisation; Fractionating or rectifying columns
    • B01D9/0045—Washing of crystals, e.g. in wash columns
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/01—Chlorine; Hydrogen chloride
    • C01B7/03—Preparation from chlorides
    • C01B7/035—Preparation of hydrogen chloride from chlorides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/01—Chlorine; Hydrogen chloride
    • C01B7/07—Purification ; Separation
    • C01B7/0706—Purification ; Separation of hydrogen chloride
    • C01B7/0718—Purification ; Separation of hydrogen chloride by adsorption
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D5/00—Sulfates or sulfites of sodium, potassium or alkali metals in general
    • C01D5/02—Preparation of sulfates from alkali metal salts and sulfuric acid or bisulfates; Preparation of bisulfates

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

Se proporciona un proceso para producir sulfato de potasio a partir de cloruro de potasio y ácido sulfúrico. El proceso implica mezclar cloruro de potasio con el agua para formar una suspensión de cloruro de potasio que se mezcla con ácido sulfúrico reciclado para formar una mezcla de ácidos de K+, Cl-, SO42-. Esta mezcla se somete a un proceso de cristalización que produce cristales de sulfato de potasio y un vapor de ácido clorhídrico-agua. El ácido clorhídrico se separa del vapor de ácido clorhídrico-agua para formar una solución de ácido clorhídrico.
MX2019002738A 2016-09-13 2017-09-06 Procedimiento para producir sulfato de potasio a partir de cloruro de potasio y acido sulfurico. MX2019002738A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201662393934P 2016-09-13 2016-09-13
PCT/US2017/050156 WO2018052767A1 (en) 2016-09-13 2017-09-06 Method for producing potassium sulfate from potassium chloride and sulfuric acid

Publications (1)

Publication Number Publication Date
MX2019002738A true MX2019002738A (es) 2019-05-09

Family

ID=60022152

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2019002738A MX2019002738A (es) 2016-09-13 2017-09-06 Procedimiento para producir sulfato de potasio a partir de cloruro de potasio y acido sulfurico.

Country Status (12)

Country Link
US (1) US10773968B2 (es)
EP (1) EP3512805B1 (es)
CN (1) CN109906200B (es)
AU (1) AU2017325967B2 (es)
BR (1) BR112019004697B1 (es)
CA (1) CA3035969C (es)
CL (1) CL2019000620A1 (es)
IL (1) IL265137B2 (es)
JO (1) JOP20170077B1 (es)
MX (1) MX2019002738A (es)
RU (1) RU2708204C1 (es)
WO (1) WO2018052767A1 (es)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112158871B (zh) * 2020-10-14 2021-12-07 青岛碱业钾肥科技有限公司 一种混酸的处理方法及处理系统
CN112794345B (zh) * 2021-01-20 2022-12-27 宁夏中泰富瑞科技有限公司 一种氯化钾制硫酸钾设备及其制造工艺
CN114288841A (zh) * 2021-12-31 2022-04-08 山东三方化工集团有限公司 曼海姆法硫酸钾尾气处理系统

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3998935A (en) 1975-01-30 1976-12-21 Pennzoil Company Manufacture of potassium sulfate
US4045543A (en) 1975-11-12 1977-08-30 Pennzoil Company Production of potassium sulfate and hydrogen chloride
JPS58161917A (ja) 1982-03-19 1983-09-26 Onoda Kagaku Kogyo Kk 硫酸カリウムの製造方法
US4588573A (en) * 1983-09-27 1986-05-13 Prodeco, Inc. Method for the production of potassium sulfate using sulfuric acid and potassium chloride
SU1527143A1 (ru) * 1987-06-11 1989-12-07 Казанский Химико-Технологический Институт Им.С.М.Кирова Способ получени сол ной кислоты и бисульфата кали
US6767528B2 (en) * 1997-07-01 2004-07-27 John E. Stauffer Manufacture of hydrogen chloride from salt and sulfuric acid
CN1067657C (zh) 1998-07-17 2001-06-27 金作美 循环硫酸氢钾分解氯化钾制造硫酸钾的方法
AU2002247943A1 (en) 2002-03-07 2003-09-16 Visweswara Rao Abburi A cyclic process for continuously producing potassium sulphate and potassium sulphate produced thereby
US8551429B2 (en) 2011-11-14 2013-10-08 Intercontinental Potash Corp. (Usa) Methods of processing polyhalite ore, methods of producing potassium sulfate, and related systems
RU2548959C2 (ru) * 2013-08-23 2015-04-20 Андрей Вилорьевич Доронин Способ производства двойного сульфата и раствора хлористого водорода
CN104876248B (zh) * 2015-05-15 2016-09-14 中南大学 一种制备硫酸钾并联产氯化铵的方法

Also Published As

Publication number Publication date
CL2019000620A1 (es) 2019-06-14
IL265137B2 (en) 2024-06-01
CN109906200A (zh) 2019-06-18
WO2018052767A1 (en) 2018-03-22
JOP20170077B1 (ar) 2021-08-17
EP3512805A1 (en) 2019-07-24
IL265137B1 (en) 2024-02-01
US20200071176A1 (en) 2020-03-05
CN109906200B (zh) 2022-09-20
US10773968B2 (en) 2020-09-15
BR112019004697B1 (pt) 2023-01-10
RU2708204C1 (ru) 2019-12-04
CA3035969C (en) 2021-05-25
IL265137A (es) 2019-04-30
BR112019004697A2 (pt) 2019-05-28
CA3035969A1 (en) 2018-03-22
AU2017325967A1 (en) 2019-03-28
EP3512805B1 (en) 2026-01-28
AU2017325967B2 (en) 2019-11-28

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