MX2018000198A - Procedimiento para la preparacion de un derivado de furfural que comprende neutralizar una mezcla de reaccion acida. - Google Patents
Procedimiento para la preparacion de un derivado de furfural que comprende neutralizar una mezcla de reaccion acida.Info
- Publication number
- MX2018000198A MX2018000198A MX2018000198A MX2018000198A MX2018000198A MX 2018000198 A MX2018000198 A MX 2018000198A MX 2018000198 A MX2018000198 A MX 2018000198A MX 2018000198 A MX2018000198 A MX 2018000198A MX 2018000198 A MX2018000198 A MX 2018000198A
- Authority
- MX
- Mexico
- Prior art keywords
- reaction mixture
- acid reaction
- furfural derivative
- neutralizing
- chemical formula
- Prior art date
Links
- 239000011541 reaction mixture Substances 0.000 title abstract 7
- 239000002253 acid Substances 0.000 title abstract 5
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical class O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 3
- 230000003472 neutralizing effect Effects 0.000 title abstract 2
- 239000000126 substance Substances 0.000 abstract 3
- 150000001875 compounds Chemical class 0.000 abstract 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 2
- 239000007788 liquid Substances 0.000 abstract 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 abstract 1
- 239000003377 acid catalyst Substances 0.000 abstract 1
- 125000002252 acyl group Chemical group 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 239000008103 glucose Substances 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
- C07D307/48—Furfural
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Furan Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Un derivado de furfural que tiene la fórmula química (1), en donde R representa hidrógeno, un grupo alquilo o un grupo acilo, se prepara en un procedimiento, tal procedimiento comprende hacer reaccionar un material de partida que contiene fructosa y/o glucosa con un compuesto que contiene un grupo hidroxilo líquido de fórmula R-OH en presencia de un catalizador ácido a una temperatura de reacción en el intervalo de 150 a 300 °C para producir una mezcla de reacción ácida primaria que comprende el derivado de furfural de fórmula química (1); separar parte del compuesto que contiene un grupo hidroxilo líquido de la mezcla de reacción ácida primaria para producir una mezcla de reacción ácida secundaria; neutralizar la mezcla de reacción ácida secundaria a un valor de pH de al menos 3 para obtener una mezcla de reacción neutralizada; y purificar la mezcla de reacción neutralizada para recuperar el derivado de furfural de la fórmula química (1).
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL2015066 | 2015-07-01 | ||
| PCT/NL2016/050470 WO2017003294A1 (en) | 2015-07-01 | 2016-07-01 | Process for the preparation of a furfural derivative comprising neutralizing an acid reaction mixture |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX2018000198A true MX2018000198A (es) | 2018-04-11 |
Family
ID=53783874
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2018000198A MX2018000198A (es) | 2015-07-01 | 2016-07-01 | Procedimiento para la preparacion de un derivado de furfural que comprende neutralizar una mezcla de reaccion acida. |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US10266508B2 (es) |
| EP (1) | EP3317262B1 (es) |
| CN (1) | CN107848996B (es) |
| BR (1) | BR112017028433B1 (es) |
| CA (1) | CA2990588C (es) |
| ES (1) | ES2806988T3 (es) |
| MX (1) | MX2018000198A (es) |
| WO (1) | WO2017003294A1 (es) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2017003293A1 (en) * | 2015-07-01 | 2017-01-05 | Furanix Technologies B.V. | Process for the preparation of a furfural derivative |
| WO2023066577A1 (en) | 2021-10-21 | 2023-04-27 | Furanix Technologies B.V. | Process for the preparation of a furfural derivative |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3290263A (en) * | 1962-08-02 | 1966-12-06 | Colonial Sugar Refining Co | Process of reacting sugars with reagents wherein the sugar is dissolved in monohydric alcohols containing grouping |
| DE3601281A1 (de) * | 1986-01-17 | 1987-07-23 | Sueddeutsche Zucker Ag | Verfahren zur herstellung von 5-hydroxymethylfurfural einschliesslich eines kristallinen produktes unter ausschliesslicher verwendung von wasser als loesungsmittel |
| US7317116B2 (en) | 2004-12-10 | 2008-01-08 | Archer-Daniels-Midland-Company | Processes for the preparation and purification of hydroxymethylfuraldehyde and derivatives |
| EP1834950A1 (en) * | 2006-03-10 | 2007-09-19 | Avantium International B.V. | Method for the synthesis of 5-alkoxymethylfurfural ethers and their use |
| EP2050742B1 (en) | 2006-03-10 | 2010-07-07 | Furanix Technologies B.V | Use of an organic acid esters of 5-hydroxymethylfurfural |
| EP2197867B1 (en) | 2007-09-07 | 2016-03-02 | Furanix Technologies B.V | Hydroxymethylfurfural ethers from sugars or hmf and branched alcohols |
| NL2005928C2 (en) | 2010-12-28 | 2012-07-02 | Furanix Technologies Bv | Process for the conversion of a carbohydrate-containing feedstock. |
| WO2013043131A1 (en) | 2011-09-23 | 2013-03-28 | Agency For Science, Technology And Research | Method of producing 5-hydroxymethylfurfural from carbohydrates |
| CN103159707A (zh) | 2011-12-09 | 2013-06-19 | 中国科学院大连化学物理研究所 | 一种生物质催化转化制备呋喃衍生物的方法 |
| WO2016207025A1 (de) * | 2015-06-24 | 2016-12-29 | Basf Se | Verfahren zum herstellen und abtrennen von hmf |
| WO2017003293A1 (en) * | 2015-07-01 | 2017-01-05 | Furanix Technologies B.V. | Process for the preparation of a furfural derivative |
-
2016
- 2016-07-01 CN CN201680039049.5A patent/CN107848996B/zh active Active
- 2016-07-01 US US15/736,037 patent/US10266508B2/en active Active
- 2016-07-01 BR BR112017028433-2A patent/BR112017028433B1/pt active IP Right Grant
- 2016-07-01 CA CA2990588A patent/CA2990588C/en active Active
- 2016-07-01 ES ES16745529T patent/ES2806988T3/es active Active
- 2016-07-01 MX MX2018000198A patent/MX2018000198A/es unknown
- 2016-07-01 WO PCT/NL2016/050470 patent/WO2017003294A1/en not_active Ceased
- 2016-07-01 EP EP16745529.4A patent/EP3317262B1/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN107848996A (zh) | 2018-03-27 |
| EP3317262B1 (en) | 2020-04-22 |
| CA2990588A1 (en) | 2017-01-05 |
| CA2990588C (en) | 2020-04-14 |
| US20180186761A1 (en) | 2018-07-05 |
| EP3317262A1 (en) | 2018-05-09 |
| BR112017028433A2 (pt) | 2018-08-28 |
| BR112017028433B1 (pt) | 2022-02-08 |
| CN107848996B (zh) | 2021-07-27 |
| ES2806988T3 (es) | 2021-02-19 |
| WO2017003294A1 (en) | 2017-01-05 |
| US10266508B2 (en) | 2019-04-23 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| AR072447A1 (es) | Proceso para preparar 2- alcoximetilen-4,4-difluoro-3-oxobutiratos de alquilo | |
| MX2023013444A (es) | Deshidrohalogenacion de hidroclorofluorocarburos. | |
| MX2018000196A (es) | Procedimiento para la preparacion de un derivado de furfural. | |
| EP4296365A3 (en) | Processes for conversion of biologically derived mevalonic acid | |
| MX377644B (es) | 6.7.beta-epóxidos esteroideos como intermedios químicos. | |
| AR116423A1 (es) | Un proceso de fabricación de compuestos heterocíclicos de 2-nitroimino | |
| EA201890795A1 (ru) | Способ прямого получения диметилового эфира гликоля и совместного получения этиленгликоля из монометилового эфира этиленгликоля | |
| AU2020298092A8 (en) | Process for the preparation of CIC-1 chloride channel inhibitors | |
| MX2018000198A (es) | Procedimiento para la preparacion de un derivado de furfural que comprende neutralizar una mezcla de reaccion acida. | |
| MX2020010773A (es) | Metodo para la preparacion del compuesto de pirroloaminopiridazino na y sus intermedios. | |
| MX381350B (es) | Proceso para la preparacion de 1,4-bis (etoximetil) ciclohexano. | |
| MY182164A (en) | Process for producing acetic acid by introducing a lithium compound | |
| BR112021018733A2 (pt) | Composições de d-metirosina e métodos para preparar as mesmas | |
| PL422926A1 (pl) | Oksym 7-propoksynaringeniny i sposób otrzymywania oksymu 7-propoksynaringeniny | |
| PL422932A1 (pl) | Oksym 7-izopropoksynaringeniny i sposób otrzymywania oksymu 7-izopropoksynaringeniny | |
| MX2018007379A (es) | Proceso para la purificacion de metacrilato de metilo. | |
| WO2014087431A8 (en) | One pot process for the conversion of aroyl chlorides to acyl thioureas | |
| BR112017003121A2 (pt) | método para a síntese de um óxido de fosfina de hidrogênio heterocíclico | |
| MX2013006954A (es) | Proceso para preparar oxidos de divinilareno. | |
| EA201791358A1 (ru) | Способ получения блокированного на обоих концах простого эфира этиленгликоля | |
| MX376346B (es) | Proceso para preparar trifluoroacetofenonas sustituidas con un grupo de tipo halo. | |
| AR093947A1 (es) | Un proceso mejorado para la eliminacion del paladio desde 4-amino-3-halo-5-fluor-6-(aril)piridina-2-carboxilatos y 4-amino-3-halo-6-(aril)piridina-2-carboxilatos | |
| PL411433A1 (pl) | Sposób wytwarzania 5-alkilosalicylaldoksymów i zastosowanie | |
| EA027932B1 (ru) | Способ получения 2-алкил-3-бутин-2-олов | |
| PL407902A1 (pl) | Nowe P-winylobenzyle oraz sposób ich otrzymywania |