MX2014002274A - Procedimiento para preparar [3-[(6-cloro-3-piridinil)metil]-2-tiaz olidiniliden]cianamida. - Google Patents
Procedimiento para preparar [3-[(6-cloro-3-piridinil)metil]-2-tiaz olidiniliden]cianamida.Info
- Publication number
- MX2014002274A MX2014002274A MX2014002274A MX2014002274A MX2014002274A MX 2014002274 A MX2014002274 A MX 2014002274A MX 2014002274 A MX2014002274 A MX 2014002274A MX 2014002274 A MX2014002274 A MX 2014002274A MX 2014002274 A MX2014002274 A MX 2014002274A
- Authority
- MX
- Mexico
- Prior art keywords
- pridinyl
- cyanamide
- chlor
- methyl
- producing
- Prior art date
Links
- XZMCDFZZKTWFGF-UHFFFAOYSA-N Cyanamide Chemical compound NC#N XZMCDFZZKTWFGF-UHFFFAOYSA-N 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 title abstract 2
- SKCNYHLTRZIINA-UHFFFAOYSA-N 2-chloro-5-(chloromethyl)pyridine Chemical compound ClCC1=CC=C(Cl)N=C1 SKCNYHLTRZIINA-UHFFFAOYSA-N 0.000 abstract 1
- UFULAYFCSOUIOV-UHFFFAOYSA-N cysteamine Chemical compound NCCS UFULAYFCSOUIOV-UHFFFAOYSA-N 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D417/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and sulfur atoms as the only ring hetero atoms, not provided for by group C07D415/00
- C07D417/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and sulfur atoms as the only ring hetero atoms, not provided for by group C07D415/00 containing two hetero rings
- C07D417/06—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and sulfur atoms as the only ring hetero atoms, not provided for by group C07D415/00 containing two hetero rings linked by a carbon chain containing only aliphatic carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D417/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and sulfur atoms as the only ring hetero atoms, not provided for by group C07D415/00
- C07D417/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and sulfur atoms as the only ring hetero atoms, not provided for by group C07D415/00 containing two hetero rings
- C07D417/04—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and sulfur atoms as the only ring hetero atoms, not provided for by group C07D415/00 containing two hetero rings directly linked by a ring-member-to-ring-member bond
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Plural Heterocyclic Compounds (AREA)
- Thiazole And Isothizaole Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Procedimiento para preparar [3-[(6-cloro-3-piridinil)metil]-2-tiaz olidiniliden]cianamida, que comprende las siguientes etapas: (i) reacción de N-cianocarbonimidoditiocarbonato de dimetilo y 2-aminoetanetiol o una sal del mismo en presencia de una base; (ii) reacción de la mezcla de reacción con 5-clorometil-2-cloropir idina. que no necesita ninguna purificación del intermedio de la cianimino-1,3-tiazolidina.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP11179883 | 2011-09-02 | ||
| PCT/EP2012/066602 WO2013030152A1 (de) | 2011-09-02 | 2012-08-27 | Verfahren zum herstellen von [3-[(6-chlor-3-pridinyl)methyl]-2-thiazolidinyliden] cyanamid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2014002274A true MX2014002274A (es) | 2014-03-31 |
| MX357595B MX357595B (es) | 2018-07-16 |
Family
ID=46785401
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2014002274A MX357595B (es) | 2011-09-02 | 2012-08-27 | Procedimiento para preparar [3-[(6-cloro-3-piridinil)metil]-2-tiaz olidiniliden]cianamida. |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US20150005502A1 (es) |
| EP (1) | EP2751100B1 (es) |
| JP (1) | JP2014525422A (es) |
| KR (1) | KR20140059206A (es) |
| CN (1) | CN103797008B (es) |
| BR (1) | BR112014004852A2 (es) |
| DK (1) | DK2751100T3 (es) |
| ES (1) | ES2556470T3 (es) |
| IL (1) | IL231022A (es) |
| MX (1) | MX357595B (es) |
| TW (1) | TWI527812B (es) |
| WO (1) | WO2013030152A1 (es) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107629045A (zh) * | 2017-11-10 | 2018-01-26 | 上海生农生化制品股份有限公司 | 一种噻虫啉的水相合成方法 |
| CN109354590B (zh) * | 2018-12-18 | 2020-06-23 | 山东省联合农药工业有限公司 | 一种噻虫啉的合成方法 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| HU188852B (en) * | 1983-03-16 | 1986-05-28 | Richter Gedeon Vegyeszeti Gyar Rt,Hu | Process for producing thiazolidine derivatives active against gastric ulcer and intestinal ulcer |
| JPH0717621B2 (ja) | 1986-03-07 | 1995-03-01 | 日本バイエルアグロケム株式会社 | 新規ヘテロ環式化合物 |
| US5219868A (en) * | 1990-12-10 | 1993-06-15 | Mitsui Toatsu Chemicals, Inc. | Imidazolidine derivatives, preparation thereof, insecticides containing same as an effective ingredient and intermediates therefor |
| DE4427569A1 (de) * | 1994-08-04 | 1996-02-08 | Bayer Ag | Verfahren zur Herstellung von Cyanimino-1,3-thiazolidin |
| DE19904310A1 (de) * | 1999-01-28 | 2000-08-03 | Bayer Ag | Verfahren zur Herstellung heterocyclischer Verbindungen |
| KR100676222B1 (ko) * | 1999-08-18 | 2007-01-30 | 바이엘 악티엔게젤샤프트 | 4,6-디클로로-5-플루오로피리미딘의 제조방법 |
| AU766982B2 (en) * | 2000-01-19 | 2003-10-30 | Bayer Intellectual Property Gmbh | Method for producing heterocyclic compounds |
| JP2005119992A (ja) * | 2003-10-15 | 2005-05-12 | Fuji Photo Film Co Ltd | ピリジンカルボン酸誘導体及びインドリルアザフタリド化合物の製造方法 |
| CN100567274C (zh) * | 2007-09-04 | 2009-12-09 | 中国农业大学 | [反]-β-法尼烯类似物及其制备方法与应用 |
| EP2042493A1 (de) * | 2007-09-14 | 2009-04-01 | Bayer CropScience AG | Verfahren zum Herstellen von Cyanimino-1,3-thiazolidinen |
| KR101348304B1 (ko) * | 2011-03-22 | 2014-01-20 | 동부팜한농 주식회사 | ((2Z)-3-[(6-메틸피리딘-3-일)메틸-1,3-티아졸리딘-2-이리덴]시아나미드, 티아클로프리드(Thiacloprid))의 제조방법 |
-
2012
- 2012-08-27 JP JP2014527614A patent/JP2014525422A/ja active Pending
- 2012-08-27 ES ES12753705.8T patent/ES2556470T3/es active Active
- 2012-08-27 BR BR112014004852A patent/BR112014004852A2/pt not_active Application Discontinuation
- 2012-08-27 MX MX2014002274A patent/MX357595B/es active IP Right Grant
- 2012-08-27 US US14/241,538 patent/US20150005502A1/en not_active Abandoned
- 2012-08-27 CN CN201280042379.1A patent/CN103797008B/zh not_active Expired - Fee Related
- 2012-08-27 EP EP12753705.8A patent/EP2751100B1/de active Active
- 2012-08-27 KR KR1020147005004A patent/KR20140059206A/ko not_active Ceased
- 2012-08-27 DK DK12753705.8T patent/DK2751100T3/en active
- 2012-08-27 WO PCT/EP2012/066602 patent/WO2013030152A1/de not_active Ceased
- 2012-08-31 TW TW101131668A patent/TWI527812B/zh not_active IP Right Cessation
-
2014
- 2014-02-18 IL IL231022A patent/IL231022A/en active IP Right Grant
Also Published As
| Publication number | Publication date |
|---|---|
| EP2751100A1 (de) | 2014-07-09 |
| IL231022A0 (en) | 2014-03-31 |
| US20150005502A1 (en) | 2015-01-01 |
| TW201323422A (zh) | 2013-06-16 |
| CN103797008A (zh) | 2014-05-14 |
| MX357595B (es) | 2018-07-16 |
| EP2751100B1 (de) | 2015-10-14 |
| TWI527812B (zh) | 2016-04-01 |
| BR112014004852A2 (pt) | 2017-04-04 |
| WO2013030152A1 (de) | 2013-03-07 |
| KR20140059206A (ko) | 2014-05-15 |
| JP2014525422A (ja) | 2014-09-29 |
| DK2751100T3 (en) | 2016-01-18 |
| ES2556470T3 (es) | 2016-01-18 |
| CN103797008B (zh) | 2016-08-17 |
| IL231022A (en) | 2016-04-21 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant or registration |