MX2012002614A - Nuevo metodo para la preparacion de silice precipitado. - Google Patents
Nuevo metodo para la preparacion de silice precipitado.Info
- Publication number
- MX2012002614A MX2012002614A MX2012002614A MX2012002614A MX2012002614A MX 2012002614 A MX2012002614 A MX 2012002614A MX 2012002614 A MX2012002614 A MX 2012002614A MX 2012002614 A MX2012002614 A MX 2012002614A MX 2012002614 A MX2012002614 A MX 2012002614A
- Authority
- MX
- Mexico
- Prior art keywords
- precipitated silica
- novel method
- acid
- silicate
- preparing precipitated
- Prior art date
Links
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 2
- 239000000377 silicon dioxide Substances 0.000 title abstract 2
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 abstract 5
- 239000002253 acid Substances 0.000 abstract 4
- 239000012429 reaction media Substances 0.000 abstract 2
- 239000007858 starting material Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
- C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
- C01B33/193—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates of aqueous solutions of silicates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D37/00—Processes of filtration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Silicon Compounds (AREA)
Abstract
La invención es concerniente con un método para preparar sílice precipitada que consiste de: (i) formar un arrancador que tiene un pH entre 2 y 5; (ii) agregar simultáneamente sílice y ácido, de tal manera que el pH del medio de reacción es de entre 2 y 5; (iii) agregar silicato hasta que el pH es de entre 7 y 10; (iv) agregar simultáneamente silicato y ácido, de tal manera que el pH es de entre 7 y 10; (v) agregar ácido hasta que el pH de entre 2.5 y 5.3; (vi) traer el medio de reacción en contacto con el ácido y el silicato, de tal manera que el pH es de entre aproximadamente 2.5 y 5.3 y (vii) agregar silicato para incrementar el pH a un valor de entre 4.7 y 6.3.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR0904179A FR2949454B1 (fr) | 2009-09-03 | 2009-09-03 | Nouveau procede de preparation de silices precipitees |
| PCT/EP2010/062864 WO2011026895A1 (fr) | 2009-09-03 | 2010-09-02 | Nouveau procede de preparation de silices precipitees |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX2012002614A true MX2012002614A (es) | 2012-04-20 |
Family
ID=42104457
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2012002614A MX2012002614A (es) | 2009-09-03 | 2010-09-02 | Nuevo metodo para la preparacion de silice precipitado. |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US9567230B2 (es) |
| EP (1) | EP2473443B1 (es) |
| JP (1) | JP5628920B2 (es) |
| KR (1) | KR101426175B1 (es) |
| CN (1) | CN102548898B (es) |
| BR (1) | BR112012004842B1 (es) |
| ES (1) | ES2618805T3 (es) |
| FR (1) | FR2949454B1 (es) |
| MX (1) | MX2012002614A (es) |
| WO (1) | WO2011026895A1 (es) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MY180098A (en) * | 2011-12-23 | 2020-11-22 | Rhodia Operations | Novel process for preparing silicas |
| FR2985991B1 (fr) | 2012-01-25 | 2014-11-28 | Rhodia Operations | Nouveau procede de preparation de silices precipitees |
| FR2985992B1 (fr) * | 2012-01-25 | 2015-03-06 | Rhodia Operations | Nouveau procede de preparation de silices precitees |
| JP2015504843A (ja) * | 2013-01-23 | 2015-02-16 | ローディア オペレーションズ | 沈澱シリカの製造方法 |
| JP6204695B2 (ja) * | 2013-05-15 | 2017-09-27 | 株式会社トクヤマ | 金属酸化物ゾルの製造方法 |
| CN109626384A (zh) * | 2018-12-27 | 2019-04-16 | 通化双龙硅材料科技有限公司 | 一种牙膏用沉淀二氧化硅摩擦剂的制备方法 |
| CN112250074B (zh) * | 2020-10-26 | 2021-05-07 | 广州市飞雪材料科技有限公司 | 一种高吸油高比表面积的二氧化硅的制备方法及其应用 |
| US20240409418A1 (en) | 2021-10-26 | 2024-12-12 | Evonik Operations Gmbh | Precipitated silica, process for production thereof and use thereof |
| CN114132938B (zh) * | 2021-12-08 | 2022-05-24 | 金三江(肇庆)硅材料股份有限公司 | 一种高吸油值低比表面积二氧化硅及其制备方法 |
| JP2025501077A (ja) | 2021-12-23 | 2025-01-17 | ローディア オペレーションズ | 沈降シリカ及びその製造方法 |
| WO2023118283A1 (en) | 2021-12-23 | 2023-06-29 | Rhodia Operations | Precipitated silica and process for its manufacture |
| US20250382188A1 (en) * | 2022-06-24 | 2025-12-18 | Rhodia Operations | Method For Recovering Silicate from Polymeric Composition Comprising Silica |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3034914A (en) * | 1959-05-05 | 1962-05-15 | Pittsburgh Plate Glass Co | Preparation of siliceous products |
| FR2710629B1 (fr) * | 1993-09-29 | 1995-12-29 | Rhone Poulenc Chimie | Nouveau procédé de préparation de silice précipitée, nouvelles silices précipitées et leur utilisation au renforcement des élastomères. |
| FR2732328B1 (fr) * | 1995-03-29 | 1997-06-20 | Rhone Poulenc Chimie | Nouveau procede de preparation de silice precipitee, nouvelles silices precipitees contenant de l'aluminium et leur utilisation au renforcement des elastomeres |
| JP4515761B2 (ja) * | 2001-08-13 | 2010-08-04 | ロディア・シミ | シリカの製造方法、特定の細孔寸法及び／又は粒度分布を有するシリカ並びにそれらの特に重合体強化のための使用 |
| EP1423459B1 (fr) * | 2001-08-13 | 2008-02-27 | Société de Technologie Michelin | Composition de caoutchouc dienique pour pneumatique comprenant une silice specifique comme charge renforcante |
| FR2910459B1 (fr) * | 2006-12-22 | 2010-09-17 | Rhodia Recherches & Tech | Nouveau procede de preparation de silices precipitees par mise en oeuvre d'un melangeur rapide |
| FR2928363B1 (fr) * | 2008-03-10 | 2012-08-31 | Rhodia Operations | Nouveau procede de preparation de silices precipitees, silices precipitees a morphologie, granulometrie et porosite particulieres et leurs utilisations, notamment pour le renforcement de polymeres |
-
2009
- 2009-09-03 FR FR0904179A patent/FR2949454B1/fr not_active Expired - Fee Related
-
2010
- 2010-09-02 EP EP10747873.7A patent/EP2473443B1/fr not_active Not-in-force
- 2010-09-02 BR BR112012004842-2A patent/BR112012004842B1/pt not_active IP Right Cessation
- 2010-09-02 US US13/394,320 patent/US9567230B2/en not_active Expired - Fee Related
- 2010-09-02 KR KR1020127005584A patent/KR101426175B1/ko not_active Expired - Fee Related
- 2010-09-02 CN CN201080046751.7A patent/CN102548898B/zh not_active Expired - Fee Related
- 2010-09-02 WO PCT/EP2010/062864 patent/WO2011026895A1/fr not_active Ceased
- 2010-09-02 ES ES10747873.7T patent/ES2618805T3/es active Active
- 2010-09-02 MX MX2012002614A patent/MX2012002614A/es active IP Right Grant
- 2010-09-02 JP JP2012527318A patent/JP5628920B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| US9567230B2 (en) | 2017-02-14 |
| JP5628920B2 (ja) | 2014-11-19 |
| KR20120041236A (ko) | 2012-04-30 |
| CN102548898B (zh) | 2015-01-14 |
| BR112012004842A2 (pt) | 2016-03-15 |
| FR2949454A1 (fr) | 2011-03-04 |
| US20120263638A1 (en) | 2012-10-18 |
| EP2473443B1 (fr) | 2016-12-21 |
| CN102548898A (zh) | 2012-07-04 |
| FR2949454B1 (fr) | 2011-09-16 |
| WO2011026895A1 (fr) | 2011-03-10 |
| ES2618805T3 (es) | 2017-06-22 |
| JP2013503806A (ja) | 2013-02-04 |
| BR112012004842B1 (pt) | 2019-07-09 |
| EP2473443A1 (fr) | 2012-07-11 |
| KR101426175B1 (ko) | 2014-08-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant or registration |