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MX2009004262A - Proceso para la sulfinilacion de un derivado de pirazol. - Google Patents

Proceso para la sulfinilacion de un derivado de pirazol.

Info

Publication number
MX2009004262A
MX2009004262A MX2009004262A MX2009004262A MX2009004262A MX 2009004262 A MX2009004262 A MX 2009004262A MX 2009004262 A MX2009004262 A MX 2009004262A MX 2009004262 A MX2009004262 A MX 2009004262A MX 2009004262 A MX2009004262 A MX 2009004262A
Authority
MX
Mexico
Prior art keywords
acid
sulfinylation
pyrazole derivative
amine
pyrazole
Prior art date
Application number
MX2009004262A
Other languages
English (en)
Inventor
Michael Keil
Oliver Kuhn
Martin Sukopp
Carsten Groening
Jon J Longlet
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of MX2009004262A publication Critical patent/MX2009004262A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/44—Oxygen and nitrogen or sulfur and nitrogen atoms
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00—Medicinal preparations containing organic active ingredients
    • A61K31/33—Heterocyclic compounds
    • A61K31/395—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins
    • A61K31/41—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having five-membered rings with two or more ring hetero atoms, at least one of which being nitrogen, e.g. tetrazole
    • A61K31/415—1,2-Diazoles
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P33/00—Antiparasitic agents

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • Medicinal Chemistry (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Plant Pathology (AREA)
  • Wood Science & Technology (AREA)
  • Tropical Medicine & Parasitology (AREA)
  • Epidemiology (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Oncology (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • Communicable Diseases (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Catalysts (AREA)

Abstract

Un proceso para la sulfinilación de un derivado de pirazol, caracterizado porque se hace reaccionar 5-amino-1-[2,6-dicloro-4-( trifluorometil)fenil]-1H-pirazol-3-carbonitrilo (II) con un agente de sulfinilación seleccionado de ácido trifluorometilsulfínico, anhídrido de ácido trifluorometilsulfínic o y una sal de metal trifluorometilsulfinato alcalino o alcalinotérreo y mezclas del ácido y/o de la(s) sal(es), en presencia de al menos un complejo de amina ácida, en donde la(s) amina(s) es/son seleccionada(s) de aminas terciarias y el/los acido(s) es/son seleccionado(s) de acido fluorhídrico, clorhídrico, bromhídrico y yodhídrico, y derivados del ácido sulfónico, y con la adición de un agente halogenante.
MX2009004262A 2006-11-10 2007-11-05 Proceso para la sulfinilacion de un derivado de pirazol. MX2009004262A (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US86517806P 2006-11-10 2006-11-10
US91361707P 2007-04-24 2007-04-24
PCT/EP2007/061891 WO2008055877A1 (en) 2006-11-10 2007-11-05 Process for the sulfinylation of a pyrazole derivative

Publications (1)

Publication Number Publication Date
MX2009004262A true MX2009004262A (es) 2009-05-05

Family

ID=39167843

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2009004262A MX2009004262A (es) 2006-11-10 2007-11-05 Proceso para la sulfinilacion de un derivado de pirazol.

Country Status (22)

Country Link
US (2) US8263783B2 (es)
EP (1) EP2081908B1 (es)
JP (1) JP5450077B2 (es)
KR (1) KR20090083453A (es)
CN (1) CN102746233A (es)
AR (1) AR063646A1 (es)
AU (1) AU2007316718B2 (es)
BR (1) BRPI0718774A2 (es)
CA (1) CA2667559A1 (es)
DK (1) DK2081908T3 (es)
EA (1) EA200900629A1 (es)
ES (1) ES2422296T3 (es)
HR (1) HRP20130582T1 (es)
IL (1) IL198259A (es)
MA (1) MA30917B1 (es)
MX (1) MX2009004262A (es)
NZ (1) NZ576594A (es)
PL (1) PL2081908T3 (es)
PT (1) PT2081908E (es)
TW (1) TWI413498B (es)
WO (1) WO2008055877A1 (es)
ZA (1) ZA200903968B (es)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8440709B2 (en) 2005-12-14 2013-05-14 Makhteshim Chemical Works Ltd. Polymorphs and amorphous forms of 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(trifluoromethyl)sulfinyl]-1H-pyrazole-3-carbonitrile
US8629287B2 (en) 2006-11-10 2014-01-14 Basf Se Process for the sulfinylation of a pyrazole derivative
WO2010037693A1 (de) * 2008-10-02 2010-04-08 Basf Se Verfahren zur herstellung und aufreinigung von trifluormethansulfinsäure
EP3412658A1 (en) * 2017-06-09 2018-12-12 Solvay Sa Processes for the manufacture of sulfur-substitued pyrazole derivatives
EP3412659A1 (en) * 2017-06-09 2018-12-12 Solvay Sa Processes for the manufacture of sulfur-substituted pyrazole derivatives
WO2020188376A1 (en) * 2019-03-19 2020-09-24 Gharda Chemicals Limited A process for synthesis of fipronil

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2716453B1 (fr) 1994-02-22 1996-03-29 Rhone Poulenc Agrochimie Procédé de sulfinylation de composés hétérocycliques.
DE3568455D1 (en) 1984-05-23 1989-04-06 Rhone Poulenc Chimie Detergent compositions containing copolymers based on polyoxyethylene and polyoxyalkylene used as antisoil redeposition agents, and process for their preparation
GB8713768D0 (en) * 1987-06-12 1987-07-15 May & Baker Ltd Compositions of matter
RU2192414C2 (ru) 1996-08-01 2002-11-10 Родиа Шими Способ введения замещенной дифторметильной группы
JPH11246555A (ja) * 1997-10-31 1999-09-14 Sumitomo Chem Co Ltd フッ素置換ベンゾヘテロ環化合物
DE69720082T2 (de) 1997-12-22 2003-12-11 Minnesota Mining & Manufacturing Company, St. Paul Verfahren zur herstellung von fluorierten sulfinaten
DE19853560A1 (de) 1998-11-20 2000-05-25 Bayer Ag Verfahren zur Herstellung von 5-Amino-3-(thio)carbamoylpyrazolen
BR9917518B1 (pt) 1999-10-22 2009-08-11 processos para a preparação de pesticidas 1-arilpirazóis e seus intermediários.
JP2001220386A (ja) * 1999-11-30 2001-08-14 Takeda Chem Ind Ltd オキサジアゾリン誘導体の製造方法
JP2002020364A (ja) 2000-07-06 2002-01-23 Konica Corp スルフィン酸ナトリウム、スルフィン酸カリウムの製造方法およびそれらを用いた写真用カプラーの製造方法
EP1331222A1 (en) * 2002-01-28 2003-07-30 Virbac S.A. Environment friendly reagents and process for halogenoalkylsulfinylation of organic compounds
CN1176078C (zh) * 2002-03-27 2004-11-17 江苏省农药研究所 带三氟甲基亚磺酰基的吡唑类化合物的亚磺酰化方法
US8629287B2 (en) 2006-11-10 2014-01-14 Basf Se Process for the sulfinylation of a pyrazole derivative
AU2007316721B2 (en) 2006-11-10 2013-05-09 Basf Se Process for the sulfinylation of a pyrazole derivative
FR2924115B1 (fr) 2007-11-27 2010-02-26 Rhodia Operations Procede de preparation d'un acide trifluoromethanesulfinique
WO2010037693A1 (de) 2008-10-02 2010-04-08 Basf Se Verfahren zur herstellung und aufreinigung von trifluormethansulfinsäure

Also Published As

Publication number Publication date
IL198259A0 (en) 2009-12-24
CA2667559A1 (en) 2008-05-15
CN102746233A (zh) 2012-10-24
PL2081908T3 (pl) 2013-09-30
JP5450077B2 (ja) 2014-03-26
ES2422296T3 (es) 2013-09-10
MA30917B1 (fr) 2009-11-02
NZ576594A (en) 2011-12-22
TWI413498B (zh) 2013-11-01
HRP20130582T1 (en) 2013-08-31
US20100137395A1 (en) 2010-06-03
IL198259A (en) 2013-10-31
DK2081908T3 (da) 2013-07-29
WO2008055877A1 (en) 2008-05-15
PT2081908E (pt) 2013-06-28
JP2010509271A (ja) 2010-03-25
KR20090083453A (ko) 2009-08-03
AU2007316718B2 (en) 2013-03-28
AU2007316718A1 (en) 2008-05-15
TW200829169A (en) 2008-07-16
BRPI0718774A2 (pt) 2013-12-03
EA200900629A1 (ru) 2009-10-30
EP2081908B1 (en) 2013-04-24
EP2081908A1 (en) 2009-07-29
US20120309806A1 (en) 2012-12-06
US8263783B2 (en) 2012-09-11
AR063646A1 (es) 2009-02-04
ZA200903968B (en) 2012-02-29

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