WO2023032902A1 - Non-alcoholic beer-flavored beverage - Google Patents
Non-alcoholic beer-flavored beverage Download PDFInfo
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- WO2023032902A1 WO2023032902A1 PCT/JP2022/032377 JP2022032377W WO2023032902A1 WO 2023032902 A1 WO2023032902 A1 WO 2023032902A1 JP 2022032377 W JP2022032377 W JP 2022032377W WO 2023032902 A1 WO2023032902 A1 WO 2023032902A1
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
Definitions
- the present invention relates to a non-alcoholic beer-taste beverage and a method for producing the same.
- Patent Document 1 describes a non-fermented beer-taste beverage with very little astringency that remains afterward despite the high total polyphenol content and a sharp aftertaste, with a total polyphenol content of 100 ppm or more.
- cyclodextrins and thaumatin characterized by containing one or more masking materials.
- non-alcoholic beer-taste beverages are required to have a stimulating feeling, and adding carbon dioxide gas is known as a method of imparting a stimulating feeling.
- the present invention relates to providing a new non-alcoholic beer-taste beverage that is refreshing and stimulating, and a method for producing the same.
- "Shimari” means that the aftertaste is sharp and the taste is unified.
- stimulation means that the oral cavity and throat are stimulated with a tingling sensation, and the taste is felt three-dimensionally to give a satisfying feeling to the drink.
- the present invention relates to the following [1] to [3].
- [1] A non-alcoholic beer-taste beverage having an acetic acid content of 90 to 320 mass ppm and a pH of 2.8 to 4.2.
- [2] A method for producing a non-alcoholic beer-taste beverage having a pH of 2.8 to 4.2, including a step of containing 90 to 320 ppm by mass of acetic acid.
- [3] A method of imparting a refreshing or irritating feeling to a non-alcoholic beer-taste beverage having a pH of 2.8 to 4.2, comprising the step of containing 90 to 320 ppm by mass of acetic acid.
- a stimulating feeling can be obtained by containing a specific amount of acetic acid in a non-alcoholic beer-taste beverage, and that a beer-taste beverage derived from acetic acid by setting it to a specific pH. It was newly found that it is excellent in simplicity while suppressing the negative sour smell for the flavor.
- acetic acid quickly evaporates in the oral cavity and irritates the oral cavity and throat as acid gas.
- sourness gives sharpness to the aftertaste and makes the taste more cohesive, and by making the pH, which is a substitute index for sourness, acidic, it is possible to impart a crispness.
- the non-alcoholic beer-taste beverage of the present invention contains acetic acid.
- the content of acetic acid in the non-alcoholic beer-taste beverage of the present invention is 90 mass ppm or more, preferably 95 mass ppm or more, more preferably 100 mass ppm or more, still more preferably 105 mass ppm, from the viewpoint of imparting a stimulating feeling. Above, more preferably 115 mass ppm or more, still more preferably 120 mass ppm or more, still more preferably 125 mass ppm or more.
- the Mass ppm or less more preferably 180 mass ppm or less, more preferably 170 mass ppm or less, still more preferably 160 mass ppm or less, still more preferably 150 mass ppm or less, still more preferably 140 mass ppm or less, still more preferably 130 mass ppm It is below. Also, a range in which these values are arbitrarily combined can be used.
- the non-alcoholic beer-taste beverage of the present invention can contain acetates such as sodium acetate.
- the content of acetic acid when containing acetate is the total amount of acetic acid and acetate.
- the amount of acetic acid in the non-alcoholic beer-taste beverage of the present invention can be adjusted by producing it by fermentation during the production process, or by adding acetic acid or a material containing acetic acid, and gives the viewpoint of suppressing sour odor and swelling. From the point of view, it is preferable to ferment raw materials such as food to produce brewed vinegar, or to add brewed vinegar for adjustment.
- brewed vinegar refers to acetic acid produced (brewed) by microorganisms such as yeast, acetic acid bacteria, and lactic acid bacteria.
- brewed vinegar can also be said to be the brewed vinegar in the present invention.
- brewed vinegar mixed with food materials such as sugars and plant extracts, nucleic acids / organic acids, or food additives such as their salts (salts such as sodium, potassium, calcium, magnesium, etc.) Suitable as vinegar.
- salts salts such as sodium, potassium, calcium, magnesium, etc.
- vinegar a non-alcoholic beer-taste beverage containing brewed vinegar
- adding brewed vinegar in the manufacturing process refer to a mode in which brewed vinegar is used at least in part.
- brewed vinegar when adding as a mixture of brewed vinegar and ingredients other than brewed vinegar, "brewed vinegar”
- brewed vinegar Non-alcoholic beer-taste beverages including” and "adding brewed vinegar”.
- glacial acetic acid which does not contain acetic acid produced by brewing, or synthetic acetic acid produced by chemical synthesis, may be used in combination with brewed vinegar.
- the proportion of brewed vinegar in acetic acid is preferably 10% by mass or more, more preferably 20% by mass or more, still more preferably 30% by mass or more, still more preferably 40% by mass, from the viewpoint of suppressing sour odor and imparting swelling.
- % by mass or more more preferably 50% by mass or more, more preferably 60% by mass or more, still more preferably 70% by mass or more, still more preferably 80% by mass or more, still more preferably 90% by mass or more, most preferably 100% by mass is.
- the acidity of the brewed vinegar is not limited, but may be, for example, 0.5 or more, 1.0 or more, 1.2 or more, 1.4 or more, 1.6 or more, 1.8 or more, or 8.0 or less, 7.0 or more. 5 or less, 7.0 or less, or 6.5 or less. Also, a range in which these values are arbitrarily combined can be used. In addition, from the viewpoint of suppressing sour odor, it is preferable to use brewed vinegar with a large amount of sodium.
- Sodium as used in the present invention also includes those present in the form of sodium ions, sodium salts, and the like.
- the content of sodium in brewed vinegar is preferably 100 mass ppm or more, more preferably 200 mass ppm or more, still more preferably 300 mass ppm or more, still more preferably 400 mass ppm or more, still more preferably 450 mass ppm or more, and further It is preferably 500 mass ppm or more, more preferably 550 mass ppm or more, still more preferably 600 mass ppm or more.
- it is preferably 1000 mass ppm or less, more preferably 900 mass ppm or less, still more preferably 800 mass ppm or less, and still more preferably 700 mass ppm or less.
- the acidity of beer-taste beverages is defined as "8.6" in the revised BCOJ beer analysis method (published by the Brewing Association of Japan, edited by the International Technical Committee of Beer Brewers Association [Analysis Committee], revised in 2013). acidity”.
- the content of sodium in brewed vinegar is described in (https://www.fukushihoken.metro.tokyo.lg.jp/shokuhin/hyouji/kyouzai/files/eiyouseibun_handbook.pdf) p.13. Measured by atomic absorption spectrophotometry.
- the pH of the non-alcoholic beer-taste beverage of the present invention is preferably pH 2.8 or higher, more preferably pH 2.9 or higher, still more preferably pH 3.0 or higher, and still more preferably pH 3.0 or higher, from the viewpoint of imparting shimmer and suppressing acid odor.
- pH 3.1 or higher more preferably pH 3.2 or higher, more preferably pH 3.3 or higher, still more preferably pH 3.4 or higher, and still more preferably pH 3.5 or higher.
- it is preferably pH 4.2 or less, more preferably pH 4.1 or less, still more preferably pH 4.0 or less, still more preferably pH 3.9 or less, still more preferably pH 3.8 or less.
- Adjustment of pH is the amount of acetic acid, addition of diluted water or carbonated water, type of raw materials (malt, corn grits, sugar solution, etc.), amount of raw materials, type of enzyme, amount of enzyme added, timing of enzyme addition, preparation Saccharification time in the tank, protein decomposition time in the brewing tank, pH in the brewing tank, pH in the brewing process (wort manufacturing process from malt input to yeast addition), type of acid used for pH adjustment ( lactic acid, phosphoric acid, malic acid, tartaric acid, citric acid, etc.), the amount of acid used for pH adjustment, the timing of pH adjustment (at the time of preparation, at the time of fermentation, at the completion of fermentation, before beer filtration, after beer filtration, etc.) ), set temperature and holding time for each temperature range when preparing wort (including during saccharification), original extract concentration in pre-fermentation liquid, original extract concentration in fermentation process, fermentation conditions (oxygen concentration, aeration conditions, yeast Variety, amount of yeast added, yeast growth number, yeast removal
- the pH of the non-alcoholic beer-taste beverage is the revised BCOJ beer analysis method (published by the Brewing Association of Japan, Beer Brewers Association International Technical Committee [Analysis Committee] edited by the 2013 enlarged revision of 8.7 pH Measured by the method described in
- beer-taste beverage refers to an alcohol-containing or non-alcoholic carbonated beverage with a beer-like flavor. That is, the beer-taste beverages of the present specification include all beer-flavored carbonated beverages unless otherwise specified. Among these, the present invention relates to a "non-alcoholic beer-taste beverage". As used herein, a “non-alcoholic beer-taste beverage” is a beer-taste beverage having an alcohol content of less than 1 v/v%. Unless otherwise specified, the non-alcoholic beer-taste beverage of the present invention includes any non-alcoholic carbonated beverage having a beer flavor, regardless of the presence or absence of a yeast fermentation process.
- the non-alcoholic beer-taste beverage of the present invention may be a fermented non-alcoholic beer-taste beverage or a non-fermented non-alcoholic beer-taste beverage as long as the ethanol content in the final product is less than 1 v/v%.
- the fermented non-alcoholic beer-taste beverage may be a top-fermented non-alcoholic beer-taste beverage brewed through a fermentation process using top-fermenting yeast, or a bottom-fermented non-alcoholic beer-taste beverage brewed through a fermentation process using bottom-fermenting yeast. It may be a beer-taste beverage.
- alcohol-producing yeast Sacharomyces
- wild yeast Bacteria and the like may also be used.
- Bacteria and the like may also be used.
- fermented non-alcoholic beer-taste beverages it is manufactured by adding yeast to stop fermentation so that it becomes less than 1 v / v%, or by a method that makes it less than 1 v / v% through a dealcoholization process after fermentation.
- the raw wort extract (O-Ex) concentration in the non-alcoholic beer-taste beverage of the present invention is preferably 14.0 w/w% or less, more preferably 13.5 w/w% or less, still more preferably 13.0 w/w. % or less, more preferably 12.5 w/w% or less, more preferably 12.0 w/w% or less, even more preferably 11.5 w/w% or less, even more preferably 11.0 w/w% or less, still more preferably 10.5 w/w% or less, more preferably 10.0 w/w% or less, more preferably 9.5 w/w% or less, still more preferably 9.0 w/w% or less, and preferably 4 .0 w/w% or more, more preferably 4.5 w/w% or more, still more preferably 5.0 w/w% or more, still more preferably 5.5 w/w% or more, still more preferably 6.0 w/w% or more , More preferably 6.5 w/
- the original wort extract (O-Ex) concentration is described in the revised BCOJ beer analysis method (published by the Brewing Association of Japan, Beer Brewers Association International Technical Committee [Analysis Committee] edited 2013 supplementary revision.
- the original wort extract (O-Ex) concentration is adjusted by adding diluted water or carbonated water, the type of raw materials (malt, corn grits, sugar solution, etc.), the amount of raw materials, and the wort filtration. time, pH of wort filtration, boiling time, boiling temperature, etc. can be appropriately set.
- the final appearance fermentation degree (LA) in the non-alcoholic beer-taste beverage of the present invention is 80% or less, 75% or less, 70% or less, 68% or less, 66% or less, 64% or less, 62% or less, 60% or less, 58 % or less, 56% or less, 54% or less, 53% or less, or 52% or less. 20% or more, 22% or more, 23% or more, 24% or more, 26% or more, 28% or more, 30% or more, 32% or more, 34% or more, 36% or more, 38% or more, 40% or more, It can be 42% or more, 44% or more, 46% or more.
- the final appearance fermentation degree (LA) is described in the revised BCOJ beer analysis method (published by the Brewing Association of Japan, Beer Brewers Association International Technical Committee [Analysis Committee] edited 2013 supplementary revision.
- the final appearance fermentation degree (LA) is adjusted by the type of raw materials (malt, corn grits, sugar solution, etc.), the amount of raw materials, the type of enzyme, enzymes (sugar degrading enzymes, isomerases, etc.). ) addition amount, timing of enzyme addition, saccharification time, pH during saccharification, pH in the preparation process (wort manufacturing process from malt input to before yeast addition), wort filtration time, wort preparation
- the set temperature, holding time, and the like for each temperature range during (including during saccharification) can be appropriately set.
- the alcohol content (alcohol content) of the non-alcoholic beer-taste beverage of the present invention is preferably less than 1.0 v/v%, more preferably 0.95 v/v% or less, still more preferably 0.90 v/v% or less, More preferably 0.85 v/v% or less, more preferably 0.80 v/v% or less, still more preferably 0.75 v/v% or less, still more preferably 0.70 v/v% or less, still more preferably 0.60 v /v% or less, more preferably 0.50v/v% or less, more preferably 0.40v/v% or less, still more preferably 0.30v/v% or less, still more preferably 0.20v/v% or less, and further It is preferably 0.10 v/v % or less, more preferably 0.05 v/v % or less.
- alcohol content is described in the revised BCOJ beer analysis method (published by the Brewing Association of Japan, Beer Brewers Association International Technical Committee [Analysis Committee] edited 2013 supplementary revision.
- the alcohol content is adjusted by appropriately setting the addition of diluted water or carbonated water, the sugar composition of the pre-fermentation liquid, the type of yeast, the amount of yeast, the addition of brewer's alcohol, the addition of distilled alcohol, etc. be able to.
- the chromaticity of the non-alcoholic beer-taste beverage of the present invention is, for example, 1.0 EBC or more, 3.0 EBC or more, 5.0 EBC or more, 6.0 EBC or more, 7.0 EBC or more, 8.0 EBC or more, 9.0 EBC or more, It can be 10.0 EBC or more, 15.0 EBC or more, or 20.0 EBC or more, and can be 40.0 EBC or less, or 30.0 EBC or less.
- chromaticity is described in the revised BCOJ beer analysis method (Published by the Brewing Association of Japan, Beer Brewers Association International Technical Committee [Analysis Committee] Edited 2013 Supplementary Revision 8.8 Chromaticity Adjustment of chromaticity is done by adding diluted water or carbonated water, types of raw materials (malt, corn grits, sugar solution, etc.), amount of raw materials, temperature during mashing, pH during mashing, and mashing time. , Wort filtration time, pH of wort filtration, boiling time, boiling temperature, amount of pigment components such as caramel pigment, beer filtration type (diatomaceous earth filtration, various membrane filtration, etc.), beer filtration amount, etc. can be set.
- the bitterness value of the non-alcoholic beer-taste beverage of the present invention can be, for example, 5 BUs or more, 10 BUs or more, 15 BUs or more, 18 BUs or more, 20 BUs or more, 23 BUs or more, 25 BUs or more, or 40 BUs or less, 35 BUs or less, or 32 BUs. 30 BUs, 28 BUs or less.
- the bitterness value is measured according to the method described in the section "BCOJ Beer Analysis Method (2004.11.1 Revised Edition) 8.15 Bitterness Value".
- bitterness value depends on the content of iso-alpha acids contained in the beverage. Iso- ⁇ -acids are obtained by isomerizing ⁇ -acids contained in hops.
- hop varieties To control the amount of iso- ⁇ -acids, hop varieties, amount of hops used, timing of hop addition, temperature when hops were added and holding time in that temperature range, pH when hops were added, original pre-fermentation solution Extract concentration, original extract concentration in the fermentation process, fermentation conditions (oxygen concentration, aeration conditions, yeast variety, yeast addition amount, yeast growth number, yeast removal timing, fermentation temperature, fermentation time, pressure setting, carbon dioxide concentration, etc.) ), etc., can be adjusted by the conditions of beer filtration, the addition of dilution water, the addition of carbonated water, and the like.
- hop processed products such as iso- ⁇ acid
- Original extract concentration, original extract concentration in the fermentation process, fermentation conditions oxygen concentration, aeration conditions, yeast variety, yeast addition amount, yeast growth number, yeast removal timing, fermentation temperature, fermentation time, pressure setting, carbon dioxide concentration etc.
- Hops may be pelleted hops, extract hops, or hop bracts. Hops and hop processed products may be used alone or in combination.
- the total nitrogen content in the non-alcoholic beer-taste beverage of the present invention is, for example, 10 mg/100 mL or more, 15 mg/100 mL or more, 20 mg/100 mL or more, 25 mg/100 mL or more, 30 mg/100 mL or more, 35 mg/100 mL or more, 40 mg/100 mL or more.
- the total nitrogen content is the total amount of all nitrogen compounds such as proteins and amino acids.
- Adjustment of the total nitrogen content is done by adding diluted water or carbonated water, type of raw materials (malt, corn grits, sugar solution, etc.), amount of raw materials, type of enzyme, amount of enzyme (including proteolytic enzyme, etc.) added, enzyme Temperature during reaction, timing of enzyme addition, proteolysis time in the brewing tank, pH in the brewing tank, temperature in the brewing tank, pH in the brewing process (wort production process from malt input to yeast addition) , temperature in the preparation process, temperature at the time of wort filtration, time of wort filtration, pH at the time of wort filtration, amount of sparging water used at the time of wort filtration, each temperature range when preparing wort Set temperature and holding time, boiling time and pH in the boiling process, original extract concentration in the pre-fer
- the total amount of polyphenols in the non-alcoholic beer-taste beverage of the present invention is 10 mass ppm or more, 20 mass ppm or more, 30 mass ppm or more, 40 mass ppm or more, 50 mass ppm or more, 60 mass ppm or more, 70 mass ppm or more, 80 It can be 90 mass ppm or more, and can be 200 mass ppm or less, 180 mass ppm or less, 150 mass ppm or less, 140 mass ppm or less, 130 mass ppm or less, and 120 mass ppm or less. .
- the amount of total polyphenols is described in the revised BCOJ beer analysis method (published by the Brewing Association of Japan, Beer Brewers Association International Technical Committee [Analysis Committee] edited 2013 supplementary revision) 8.19 total polyphenols measured by the method
- the amount of total polyphenols can be adjusted by adding diluted water or carbonated water, the type of raw materials (raw materials containing polyphenols such as malt), the amount of raw materials, the type of enzyme, the amount of enzyme added, the timing of enzyme addition, and the brewing tank.
- Aeration time (mash aeration, etc.), pH in the brewing tank, pH in the brewing process (from malt input to wort production process before yeast addition), wort filtration time, when preparing wort (including saccharification) ), the set temperature and holding time for each temperature range, the concentration of the original extract in the pre-fermentation solution, the concentration of the original extract in the fermentation process, the fermentation conditions (oxygen concentration, ventilation conditions, yeast variety, amount of yeast added, yeast growth number, yeast removal timing, fermentation temperature, fermentation time, pressure setting, carbon dioxide concentration, etc.) can be set appropriately.
- the total polyphenol content of the beer-taste beverage of the present invention can be controlled by adjusting the amount of raw materials with a high polyphenol content, such as barley malt and malt husks. Specifically, the total amount of polyphenols can be increased by increasing the amount of raw materials such as malt with a high polyphenol content.
- the content of free amino nitrogen (FAN) in the non-alcoholic beer-taste beverage of the present invention is 1.0 mg/100 mL or more, 2.0 mg/100 mL or more, 3.0 mg/100 mL or more, 4.0 mg/100 mL or more, 5 0 mg/100 mL or more, 6.0 mg/100 mL or more, 7.0 mg/100 mL or more, 8.0 mg/100 mL or more, 9.0 mg/100 mL or more, 10.0 mg/100 mL or more; 0 mg/100 mL or less, 19.0 mg/100 mL or less, 18.0 mg/100 mL or less, 17.0 mg/100 mL or less, 16.0 mg/100 mL or less, 15.0 mg/100 mL or less, 14.0 mg/100 mL or less can.
- the content of FAN is based on the revised BCOJ beer analysis method (published by the Brewing Association of Japan, Beer Brewers Association International Technical Committee [Analysis Committee] edited by the 2013 supplementary revision 8.18 free amino nitrogen
- the FAN content is adjusted by adding diluted water or carbonated water, the type of raw materials (malt, corn grits, sugar solution, etc.), the amount of raw materials, the type of enzyme, the enzyme (protein (including degrading enzymes, etc.), timing of enzyme addition, protein decomposition time in the brewing tank, pH in the brewing tank, pH in the brewing process (wort manufacturing process from the addition of malt to the addition of yeast), Time of wort filtration, set temperature and holding time for each temperature range when preparing wort, boiling time and pH in the boiling process, original extract concentration in the pre-fermentation liquid, original extract concentration in the fermentation process, fermentation conditions (Oxygen concentration, aeration conditions, yeast variety, amount of yeast added, yeast growth number, yeast removal timing, fermentation temperature, fermentation time, pressure
- the content of iso- ⁇ acids in the non-alcoholic beer-taste beverage of the present invention is 2.0 mass ppm or more, 4.0 mass ppm or more, 6.0 mass ppm or more, 7.0 mass ppm or more, and 8.0 mass ppm. Above, 9.0 mass ppm or more, 9.5 mass ppm or more, 10 mass ppm or more, and 40.0 mass ppm or less, 35.0 mass ppm or less, 30.0 mass ppm or less, 25 0 mass ppm or less, 20.0 mass ppm or less, or 15.0 mass ppm or less.
- the content of iso- ⁇ acids is determined by the revised BCOJ beer analysis method (published by the Brewing Association of Japan, Beer Brewers Association International Technical Committee [Analysis Committee] edited by the 2013 supplementary revision of 8.25 iso- ⁇ Acids and ⁇ -acids are measured by the method described in.
- the content of iso- ⁇ -acids can be adjusted by adjusting the hop variety, the amount of hops used, the timing of adding hops, the temperature at which hops are added, and the temperature range during which the hops are added.
- Time, pH at the time of hop addition, original extract concentration in the pre-fermentation liquid, original extract concentration in the fermentation process, fermentation conditions oxygen concentration, aeration conditions, yeast variety, amount of yeast added, yeast growth number, yeast removal timing, Fermentation temperature, fermentation time, pressure setting, carbon dioxide concentration, etc.
- fermentation conditions oxygen concentration, aeration conditions, yeast variety, amount of yeast added, yeast growth number, yeast removal timing, Fermentation temperature, fermentation time, pressure setting, carbon dioxide concentration, etc.
- beer filtration conditions addition of dilution water, addition of carbonated water, etc.
- commercially available hop processed products iso- ⁇ acid, etc.
- Hops may be pelleted pellet hops, extracted extract hops, or hop bracts.Hop and hop processing. Products may be used alone or in combination.
- the non-alcoholic beer-taste beverage of the present invention preferably contains ethyl acetate.
- the content of ethyl acetate is 0.1 mass ppm or more, 0.2 mass ppm or more, 0.3 mass ppm or more, 0.4 mass ppm or more, 0.5 mass ppm or more, 0.6 mass ppm or more, 0 .7 mass ppm or more, 0.8 mass ppm or more, 0.9 mass ppm or more, 1.0 mass ppm or more, 2.0 mass ppm or more, 3.0 mass ppm or more, 4.0 mass ppm or more; 0 mass ppm or more, 6.0 mass ppm or more, 7.0 mass ppm or more, 8.0 mass ppm or more, 9.0 mass ppm or more, 10.0 mass ppm or more, 11.0 mass ppm or more, 12.0 mass ppm or more, 13.0 mass ppm or more, 14.0 mass ppm or more, 15.0 mass ppm
- the content of ethyl acetate is measured by gas chromatography. Adjustment of the content of ethyl acetate can be done by adding diluted water or carbonated water, adding ethyl acetate-containing fragrance, amount of ethyl acetate-containing fragrance, amount of ethyl acetate-containing raw material, adding ethyl acetate-containing raw material, raw material containing ethyl acetate.
- the set temperature and holding time of each temperature range the original extract concentration of the pre-fermentation liquid, Original extract concentration in the fermentation process, fermentation conditions (oxygen concentration, ventilation conditions, yeast variety, yeast addition amount, yeast growth number, yeast removal timing, fermentation temperature, fermentation time, pressure setting, carbon dioxide concentration, etc.) It can be set appropriately.
- the content of isoamyl acetate in the non-alcoholic beer-taste beverage of the present invention is 0.01 mass ppm or more, 0.02 mass ppm or more, 0.03 mass ppm or more, 0.04 mass ppm or more, 0.05 mass ppm or more.
- 0.06 mass ppm or more 0.07 mass ppm or more, 0.08 mass ppm or more, 0.09 mass ppm or more, 0.1 mass ppm or more, 0.15 mass ppm or more, 0.20 mass ppm or more, 0.25 mass ppm or more, 0.30 mass ppm or more, 0.35 mass ppm or more, 0.40 mass ppm or more, 0.45 mass ppm or more, 0.50 mass ppm or more, 1.0 mass ppm or more, 2 0 mass ppm or more, 3.0 mass ppm or more, 4.0 mass ppm or more, 5.0 mass ppm or more, and 20.0 mass ppm or less, 15.0 mass ppm or less, and 10.0 mass ppm or more.
- the content of isoamyl acetate is measured by gas chromatography.
- the adjustment of the content of isoamyl acetate is carried out by adding diluent water or carbonated water, adding isoamyl acetate-containing fragrance, amount of isoamyl acetate-containing fragrance, amount of isoamyl acetate-containing raw material, addition of isoamyl acetate-containing raw material, raw material containing isoamyl acetate.
- the type of enzyme amount of substrate for isoamyl acetate, amount of raw material that is the substrate for isoamyl acetate, amount of raw material, type of raw material, type of enzyme, amount of enzyme added, timing of enzyme addition, saccharification time in the preparation tank, preparation Proteolysis time in the tank, pH in the brewing tank, pH in the brewing process (from malt input to the wort production process before adding yeast), amount of acid used for pH adjustment, timing of pH adjustment ( At the time of preparation, during fermentation, at the completion of fermentation, before beer filtration, after beer filtration, etc.), when preparing wort (including during saccharification), the set temperature and holding time of each temperature range, the original extract concentration of the pre-fermentation liquid, Original extract concentration in the fermentation process, fermentation conditions (oxygen concentration, ventilation conditions, yeast variety, yeast addition amount, yeast growth number, yeast removal timing, fermentation temperature, fermentation time, pressure setting, carbon dioxide concentration, etc.) It can be set appropriately.
- the content of isoamyl alcohol in the non-alcoholic beer-taste beverage of the present invention is 1.0 mass ppm or more, 2.0 mass ppm or more, 3.0 mass ppm or more, 4.0 mass ppm or more, 5.0 mass ppm or more.
- 6.0 mass ppm or more 7.0 mass ppm or more, 8.0 mass ppm or more, 9.0 mass ppm or more, 10.0 mass ppm or more, 15.0 mass ppm or more, 20.0 mass ppm or more, It can be 30.0 mass ppm or more, and 100.0 mass ppm or less, 90.0 mass ppm or less, 80.0 mass ppm or less, 70.0 mass ppm or less, 60.0 mass ppm or less, 50 0 mass ppm or less and 40.0 mass ppm or less.
- the content of isoamyl alcohol is measured by gas chromatography.
- the adjustment of the content of isoamyl alcohol includes addition of diluted water or carbonated water, addition of isoamyl alcohol-containing fragrance, amount of isoamyl alcohol-containing fragrance, amount of isoamyl alcohol-containing raw material, addition of isoamyl alcohol-containing raw material, raw material containing isoamyl alcohol type, amount of substrate for isoamyl alcohol, amount of raw material that is the substrate for isoamyl alcohol, amount of raw material, type of raw material, type of enzyme, amount of enzyme added, timing of enzyme addition, saccharification time in the preparation tank, preparation Proteolysis time in the tank, pH in the brewing tank, pH in the brewing process (from malt input to the wort production process before adding yeast), amount of acid used for pH adjustment, timing of pH adjustment ( At the time of preparation, during fermentation, at the completion of fermentation, before beer filtration, after beer filtration, etc.), when preparing wort (including during saccharification), the set temperature and holding time of each temperature range, the original extract concentration of the
- the content of ethyl caproate in the non-alcoholic beer-taste beverage of the present invention is 1.0 mass ppb or more, 2.0 mass ppb or more, 3.0 mass ppb or more, 4.0 mass ppb or more, and 5.0 mass ppb.
- the content of ethyl caproate is measured by gas chromatography.
- the content of ethyl caproate can be adjusted by adding diluted water or carbonated water, adding an ethyl caproate-containing fragrance, the amount of the ethyl caproate-containing fragrance, the amount of the ethyl caproate-containing raw material, the addition of the ethyl caproate-containing raw material, Type of raw material containing ethyl caproate, amount of substrate for ethyl caproate, amount of raw material serving as substrate for ethyl caproate, amount of raw material, type of raw material, type of enzyme, amount of enzyme added, timing of enzyme addition , saccharification time in the brewing tank, protein decomposition time in the brewing tank, pH in the brewing tank, pH in the brewing process (wort manufacturing process from malt input to yeast addition), acid used for pH adjustment addition amount, timing of pH adjustment (during preparation, fermentation, completion of fermentation, before beer filtration
- the content of 4-vinylguaiacol (4VG) in the non-alcoholic beer-taste beverage of the present invention is 1 ⁇ g/L or more, 5 ⁇ g/L or more, 7 ⁇ g/L or more, 10 ⁇ g/L or more, 10 ⁇ g/L or more, 15 ⁇ g/L or more. , 20 ⁇ g/L or more, and 500 ⁇ g/L or less, 450 ⁇ g/L or less, 400 ⁇ g/L or less, 350 ⁇ g/L or less, or 300 ⁇ g/L or less.
- the content of 4-vinylguaiacol is measured by gas chromatography.
- the content of 4-vinylguaiacol is adjusted by adding diluted water or carbonated water, adding a 4-vinylguaiacol-containing flavor, the amount of the 4-vinylguaiacol-containing flavor, the amount of the 4-vinylguaiacol-containing raw material, and the amount of the 4-vinylguaiacol.
- the main raw materials in the non-alcoholic beer-taste beverage of the present invention may be water and malt, or may be without malt. Furthermore, hops may be used, and preservatives, sweeteners, water-soluble dietary fibers, bittering agents or bitterness-imparting agents, antioxidants, flavors, acidulants, salts, spirits, and the like may also be used.
- Malt refers to the germinated, dried, and rooted barley seeds of barley, wheat, rye, oats, oats, pigeons, and oats. malted barley is preferred.
- Barley malt is one of the most commonly used malts as a raw material for Japanese beer-taste beverages.
- colored malt can also be used. When using colored malt, different types of colored malt may be appropriately combined and used, or one type of colored malt may be used.
- grains other than malt, protein, yeast extract, sugar solution, etc. may be used.
- Such grains include, for example, wheat that does not correspond to malt (barley, wheat, rye, oats, oats, pigeons, oats, etc.), rice (polished rice, brown rice, etc.), corn (corn grits, etc.), Koryan, potato, beans (soybeans, peas, etc.), buckwheat, sorghum, millet, barley, starches obtained therefrom, extracts thereof, and the like.
- corn corn (corn grits, etc.).
- proteins include soybean protein, pea protein, yeast extract, decomposition products thereof, and the like.
- non-alcoholic beer-taste beverages using liquid sugar containing a carbon source amino acid-containing materials such as the above-mentioned grains other than malt (for example, soybean protein, etc.) as a nitrogen source are mentioned. be done.
- Hops include, for example, pellet hops, powdered hops, and hop extracts. As the hops to be used, processed hops such as isoformed hops and reduced hops may be used.
- preservatives examples include benzoic acid; benzoates such as sodium benzoate; benzoate esters such as propyl parahydroxybenzoate and butyl parahydroxybenzoate; and dimethyl dicarbonate.
- a commercially available preparation such as Strong Samprezer (a mixture of sodium benzoate and butyl benzoate, manufactured by San-Eigen FFI Co., Ltd.) may be used.
- These preservatives may be used alone or in combination of two or more.
- the amount of the preservative is preferably 5 to 1200 mass ppm, more preferably 10 to 1100 mass ppm, still more preferably 15 to 1000 mass ppm, still more preferably 20 to 900 mass ppm.
- sweeteners include commercially available saccharified solutions obtained by decomposing grain-derived starch with acids or enzymes, sugars such as commercially available starch syrup, sugars of trisaccharides or higher, sugar alcohols, natural sweeteners such as stevia, and artificial sweeteners. mentioned.
- the form of these sugars may be liquid such as solution, or solid such as powder.
- sugars with a higher proportion of maltose may be used by appropriately setting conditions for hydrolysis with an enzyme or acid.
- sucrose, fructose, glucose, maltose, trehalose, maltotriose, solutions of these (sugar solutions), and the like can also be used.
- Isomerized sugars such as isomaltose and isomaltotriose can also be used.
- artificial sweeteners include aspartame, acesulfame potassium (acesulfame K), sucralose, and neotame. Sweeteners may be used alone or in combination of two or more.
- water-soluble dietary fiber examples include indigestible dextrin, polydextrose, soybean dietary fiber, guar gum decomposition product, pectin, glucomannan, alginic acid, laminarin, fucoidin, carrageenan, etc.
- Indigestible dextrin or polydextrose are preferred from a sexual point of view.
- the bittering agent or bitterness-imparting agent is not particularly limited, and other than hops, for example, Ganoderma lucidum, Ganoderma lucidum, Himejiko, Juniper nut, Sage, Astragalus, Ganoderma lucidum, Bay laurel, Quassin, Citrus extract, Nigaki extract coffee extract, tea extract, bitter gourd extract, lotus germ extract, aloe vera extract, stonecrop extract, litchi extract, laurel extract, sage extract, caraway extract, naringin, absinthine, wormwood, A wormwood extract etc. are mentioned.
- the antioxidant is not particularly limited, and those used as antioxidants in ordinary beer and low-malt beer can be used. Examples include ascorbic acid, erythorbic acid, tocopherols such as vitamin E, and catechins.
- Beer flavors are used to impart a beer-like flavor, and include brewing components and the like generated by fermentation. Beer flavors include esters, higher alcohols, and lactones such as isoamyl acetate, n-propanol, isobutanol, acetaldehyde, ethyl caproate, ethyl caprylate, isoamyl propionate, linalool, geraniol, citral, and 4-vinylguaiacol. (4-VG), 4-methyl-3-pentenoic acid, 2-methyl-2-pentenoic acid, 1,4-cineole, 1,8-cineole, 2,3-diethyl-5-methylpyrazine, ⁇ -decanolactone .
- the acidulant is not particularly limited as long as it is a substance having a sour taste, and examples thereof include tartaric acid, phosphoric acid, citric acid, gluconic acid, lactic acid, malic acid, phytic acid, succinic acid, gluconodeltalactone, and salts thereof. mentioned. Among these acidulants, tartaric acid, phosphoric acid, citric acid, gluconic acid, lactic acid, malic acid, phytic acid, succinic acid or salts thereof are preferred, and tartaric acid, phosphoric acid, citric acid, lactic acid or salts thereof are preferred. more preferred. These acidulants may be used alone or in combination of two or more.
- spirits are obtained by saccharifying grains such as wheat, rice, buckwheat, and corn using malt or, if necessary, using an enzyme agent, fermenting them using yeast, and then further distilling them. means liquor.
- wheat is preferred as a grain that is a raw material for spirits.
- One aspect of the non-alcoholic beer-taste beverage of the present invention includes an aspect of a packaged beverage.
- the container include bottles, PET bottles, cans, and barrels, and cans, bottles, and PET bottles are preferable from the viewpoint of being particularly easy to carry.
- a colorless and transparent bottle or PET bottle it is exposed to sunlight or fluorescent light, so a colored bottle, colored PET bottle, can or barrel is preferable.
- the malt ratio of the non-alcoholic beer-taste beverage of the present invention can be 20% or more, 25% or more, 30% or more, 35% or more, 40% or more, 42% or more, 45% or more, or 100%. 90% or less, 80% or less, 75% or less, 70% or less, 65% or less, 60% or less, 55% or less, 52% or less, or 50% or less.
- the malt ratio means a value calculated in accordance with the Liquor Tax Act and liquor administrative laws and regulations, etc., which are enforced on April 1, 2018.
- the amount of carbon dioxide in the non-alcoholic beer-taste beverage of the present invention is represented by the carbon dioxide pressure of the beverage.
- the upper limit of the carbon dioxide pressure of the beverage is 5.0 kg/cm 2 , 4.5 kg/cm 2 or 4.0 kg/cm 2 and the lower limit is 0.20 kg/cm 2 , 0.50 kg/cm 2 . cm 2 , or 1.0 kg/cm 2 , and any combination of these upper and lower limits may be used.
- the carbon dioxide pressure of the beverage is 0.20 kg/cm 2 or more and 5.0 kg/cm 2 or less, 0.50 kg/cm 2 or more and 4.5 kg/cm 2 or less, or 1.0 kg/cm 2 or more4.
- gas pressure refers to gas pressure within a container, except in special cases.
- To measure the pressure after fixing the sample heated to 20°C to the gas pressure gauge, open the stopcock of the gas pressure gauge once to release the gas, close the stopcock again, and shake the gas pressure gauge until the pointer reaches a fixed position. It is measured using a method of reading the value when it is reached or using a commercially available gas pressure measuring device.
- the non-alcoholic beer-taste beverage of the present invention may contain various additives as necessary.
- additives include, for example, colorants, foaming agents, fermentation accelerators, yeast extracts, protein substances such as peptide-containing substances, amino acids (glycine, proline, etc.), seasonings such as amino acids.
- Colorants are used to give beverages a beer-like color, and caramel pigments and the like can be used.
- the foam-forming agent is used to form a beer-like foam in a beverage or to retain the foam of the beverage.
- Proteins, peptide-containing substances such as collagen peptides, yeast extracts, and the like can be used as appropriate.
- Fermentation promoters are used to promote fermentation by yeast.
- yeast extract, bran ingredients such as rice and wheat, vitamins, minerals, etc. can be used alone or in combination.
- the non-alcoholic beer-taste beverage of the present invention has a step of containing acetic acid to 90 to 320 ppm by mass, and has a pH within the range of 2.8 to 4.2. It can be produced in the same manner as non-alcoholic beer-taste beverages.
- a method for producing a general non-alcoholic beer-taste beverage the production method using and not using malt as a raw material will be shown.
- a non-alcoholic beer-taste beverage manufactured using malt as a raw material is first prepared by adding raw materials such as grains, starch, sugars, bittering agents, or coloring agents and water as necessary, in addition to barley such as malt. If necessary, an enzyme such as amylase is added to the mixture containing the mixture for gelatinization and saccharification, followed by filtration to obtain a saccharified solution. If necessary, hops, bittering agents, etc. are added to the saccharified liquid and boiled, and solids such as coagulated proteins are removed in a clarifying tank. As an alternative to this saccharified solution, hops may be added to malt extract and warm water, and the mixture may be boiled. Hops may be mixed at any stage from the beginning of boiling to the end of boiling.
- Known conditions may be used for the conditions in the saccharification step, the boiling step, the solid content removal step, and the like.
- the wort After boiling, the wort is cooled. Flavors, acidulants, pigments such as caramel pigments, antioxidants, bittering agents, sweeteners, amino acid raw materials, etc. are added to the wort obtained. Add gas. Then, it is filled into a container and sterilized to obtain the desired non-alcoholic beer-taste beverage.
- acetic acid is added as a step in the production method of the present invention, it is preferably added before filtration immediately before packaging.
- liquid sugar containing a carbon source, a nitrogen source as an amino acid-containing material other than wheat or malt, hops, pigments, etc. are mixed with warm water. and make a liquid sugar solution.
- the liquid sugar solution is boiled.
- hops may be mixed into the liquid sugar solution during boiling rather than before the start of boiling.
- the wort is cooled, flavoring agents, acidulants, pigments such as caramel pigments, antioxidants, bittering agents, sweeteners, amino acid raw materials, etc. are added to the wort obtained, and filtered. Add carbon dioxide gas. Then, it is filled into a container and sterilized to obtain the desired non-alcoholic beer-taste beverage.
- acetic acid is added as a step in the production method of the present invention, it is preferably added before filtration immediately before packaging.
- the non-alcoholic beer-taste beverage obtained by the production method of the present invention is excellent in refreshing and stimulating feeling. Accordingly, the present invention also provides a method for improving the flavor of non-alcoholic beer-taste beverages by imparting sharpness and stimulation. The details of the steps in the flavor improving method of the present invention are the same as those of the production method of the present invention.
- Yeast was added, fermentation was performed, and the alcohol concentration was adjusted as shown in Tables 1 and 2.
- Synthetic acetic acid was added so that the concentrations shown in Tables 1 and 2 were obtained, a filtration step, beer flavoring were added, carbonation was performed, and bottling was performed to obtain a non-alcoholic beer-taste beverage.
- Examples 12-24 A non-alcoholic beer-taste beverage was prepared in the same manner as in Example 1, except that the above-prepared brewed vinegar was added in place of the synthetic acetic acid to give the composition shown in Table 4. The same evaluations as in Example 1 were also made for staining, irritating feeling, and sour odor. Table 4 shows the results.
- Non-alcoholic beer-taste beverages were prepared by adding synthetic acetic acid or brewed vinegar to the commercially available non-alcoholic beer-taste beverages (Reference Examples 1 and 2) so that the amounts of acetic acid shown in Table 6 were obtained. In the same manner as described above, evaluations were made for spotting, irritation, sour odor, and swelling. Table 6 shows the results.
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Abstract
Description
本発明は、ノンアルコールビールテイスト飲料及びその製造方法に関する。 The present invention relates to a non-alcoholic beer-taste beverage and a method for producing the same.
近年の消費者の嗜好の多様化にともなって、様々な香味特徴をもつノンアルコールビールテイスト飲料の開発が望まれている。例えば、特許文献1には、ポリフェノールの総含有量が高いにもかかわらず、後に残る渋味が非常に少なく、後キレのよい非発酵ビールテイスト飲料として、ポリフェノールの総含有量が100ppm以上であり、シクロデキストリン及びソーマチンからなる群より選択される1種以上のマスキング素材を含有することを特徴とする、非発酵ビールテイスト飲料が開示されている。また、ノンアルコールビールテイスト飲料に刺激感が求められる場合もあり、刺激感を付与する方法として炭酸ガスを加えることが知られている。 With the diversification of consumer tastes in recent years, the development of non-alcoholic beer-taste beverages with various flavor characteristics is desired. For example, Patent Document 1 describes a non-fermented beer-taste beverage with very little astringency that remains afterward despite the high total polyphenol content and a sharp aftertaste, with a total polyphenol content of 100 ppm or more. , cyclodextrins and thaumatin, characterized by containing one or more masking materials. In some cases, non-alcoholic beer-taste beverages are required to have a stimulating feeling, and adding carbon dioxide gas is known as a method of imparting a stimulating feeling.
しかしながら、特許文献1の飲料においては、後キレを付与するためにシクロデキストリンやソーマチンのようなマスキング素材を添加する必要があり、そのようなマスキング素材を用いる必要のない新たな技術が求められる。また、刺激感を付与するために炭酸ガス圧を高くすると、炭酸によりお腹が膨らんでしまうなどの問題もあるため、刺激感付与についてもさらなる改良が望まれる。 However, in the beverage of Patent Document 1, it is necessary to add a masking material such as cyclodextrin or thaumatin in order to give it a sharp aftertaste, and a new technology that does not require the use of such a masking material is required. Further, if the carbon dioxide gas pressure is increased in order to impart a stimulating feeling, there is a problem that the stomach swells due to the carbonic acid.
本発明は、シマリ及び刺激感に優れる新たなノンアルコールビールテイスト飲料及びその製造方法を提供することに関する。ここで、「シマリ」とは後味がキレて、味がまとまることを指す。また、「刺激感」とは口腔内やのどをピリピリと刺激し、味が立体的に感じて飲み応えを与えることを指す。 The present invention relates to providing a new non-alcoholic beer-taste beverage that is refreshing and stimulating, and a method for producing the same. Here, "Shimari" means that the aftertaste is sharp and the taste is unified. In addition, the term “stimulation” means that the oral cavity and throat are stimulated with a tingling sensation, and the taste is felt three-dimensionally to give a satisfying feeling to the drink.
本発明は、下記[1]~[3]に関する。
[1]酢酸の含有量が90~320質量ppmであり、pHが2.8~4.2である、ノンアルコールビールテイスト飲料。
[2]酢酸を90~320質量ppmとなるように含有させる工程を含む、pHが2.8~4.2のノンアルコールビールテイスト飲料の製造方法。
[3]酢酸を90~320質量ppmとなるように含有させる工程を含む、pHが2.8~4.2のノンアルコールビールテイスト飲料にシマリ又は刺激感を付与する方法。
The present invention relates to the following [1] to [3].
[1] A non-alcoholic beer-taste beverage having an acetic acid content of 90 to 320 mass ppm and a pH of 2.8 to 4.2.
[2] A method for producing a non-alcoholic beer-taste beverage having a pH of 2.8 to 4.2, including a step of containing 90 to 320 ppm by mass of acetic acid.
[3] A method of imparting a refreshing or irritating feeling to a non-alcoholic beer-taste beverage having a pH of 2.8 to 4.2, comprising the step of containing 90 to 320 ppm by mass of acetic acid.
本発明によれば、シマリ及び刺激感に優れる新たなノンアルコールビールテイスト飲料及びその製造方法を提供することができる。 According to the present invention, it is possible to provide a new non-alcoholic beer-taste beverage that is refreshing and has excellent stimulation, and a method for producing the same.
本発明者らが、前記課題について鋭意検討したところ、ノンアルコールビールテイスト飲料において酢酸を特定量含有させることで刺激感が得られること、及び特定のpHとすることで酢酸に由来するビールテイスト飲料の香味にとってネガティブな酸臭を抑制しつつシマリに優れることを新たに見出した。このメカニズムは定かではないが酢酸は口腔内ですぐに蒸発し、酸の気体として口腔内や喉などを刺激することが知られている。酸味は後味にキレを与えてまとまりのある味わいにできることが知られており、酸味の代用指標となるpHを酸性にすることでシマリ感を付与できる。さらにpHは酢酸濃度と同様に酢酸の揮発効率も変化することが知られている。以上から、溶液中の酢酸量を特定量含有させること、および溶液を特定のpHとすることで酢酸による嫌な酸臭を抑制しつつ、刺激感やシマリを付与できたと推定される。 As a result of intensive studies on the above-mentioned problems, the present inventors found that a stimulating feeling can be obtained by containing a specific amount of acetic acid in a non-alcoholic beer-taste beverage, and that a beer-taste beverage derived from acetic acid by setting it to a specific pH. It was newly found that it is excellent in simplicity while suppressing the negative sour smell for the flavor. Although the mechanism is not clear, it is known that acetic acid quickly evaporates in the oral cavity and irritates the oral cavity and throat as acid gas. It is known that sourness gives sharpness to the aftertaste and makes the taste more cohesive, and by making the pH, which is a substitute index for sourness, acidic, it is possible to impart a crispness. Furthermore, it is known that the pH changes the acetic acid volatilization efficiency as well as the acetic acid concentration. From the above, it is presumed that by containing a specific amount of acetic acid in the solution and by setting the solution to a specific pH, it was possible to impart an irritating feeling and shimmer while suppressing the unpleasant sour odor due to acetic acid.
本発明のノンアルコールビールテイスト飲料は、酢酸を含有する。本発明のノンアルコールビールテイスト飲料中の酢酸の含有量は、刺激感を付与する観点から、90質量ppm以上、好ましくは95質量ppm以上、より好ましくは100質量ppm以上、更に好ましくは105質量ppm以上、更に好ましくは115質量ppm以上、更に好ましくは120質量ppm以上、更に好ましくは125質量ppm以上である。また、酸臭を抑制する観点から、320質量ppm以下、好ましくは310質量ppm以下、より好ましくは300質量ppm以下、更に好ましくは250質量ppm以下、更に好ましくは200質量ppm以下、更に好ましくは190質量ppm以下、更に好ましくは180質量ppm以下、更に好ましくは170質量ppm以下、更に好ましくは160質量ppm以下、更に好ましくは150質量ppm以下、更に好ましくは140質量ppm以下、更に好ましくは130質量ppm以下である。また、これらの値を任意に組み合わせた範囲とすることができる。本発明のノンアルコールビールテイスト飲料は、酢酸ナトリウムなどの酢酸塩を含むことができる。酢酸塩を含む場合における酢酸の含有量は、酢酸及び酢酸塩の合計量である。 The non-alcoholic beer-taste beverage of the present invention contains acetic acid. The content of acetic acid in the non-alcoholic beer-taste beverage of the present invention is 90 mass ppm or more, preferably 95 mass ppm or more, more preferably 100 mass ppm or more, still more preferably 105 mass ppm, from the viewpoint of imparting a stimulating feeling. Above, more preferably 115 mass ppm or more, still more preferably 120 mass ppm or more, still more preferably 125 mass ppm or more. In addition, from the viewpoint of suppressing sour odor, the Mass ppm or less, more preferably 180 mass ppm or less, more preferably 170 mass ppm or less, still more preferably 160 mass ppm or less, still more preferably 150 mass ppm or less, still more preferably 140 mass ppm or less, still more preferably 130 mass ppm It is below. Also, a range in which these values are arbitrarily combined can be used. The non-alcoholic beer-taste beverage of the present invention can contain acetates such as sodium acetate. The content of acetic acid when containing acetate is the total amount of acetic acid and acetate.
本発明のノンアルコールビールテイスト飲料における酢酸量は、製造工程中に発酵による生成、または酢酸や酢酸を含む素材を添加することなどにより調整することができ、酸臭を抑制する観点及び膨らみを付与する観点から、食品などの素材を発酵することにより醸造酢を生成させることや、醸造酢を添加して調整することが好ましい。本明細書において「醸造酢」とは、酵母、酢酸菌、乳酸菌などの微生物により生成(醸造)した酢酸を含むものを指す。例えば、日本農林規格(JAS)昭和五十四年六月八日農林水産省告第八百一号(最終改正:平成二十年十月十六日農林水産省告示第千五百六号)に記載の醸造酢、食酢の表示に関する公正競争規約及び施行規則(平成30 年5 月18 日施行)に記載の醸造酢などが挙げられ、穀物酢、果実酢、米酢、米黒酢、りんご酢、ぶどう酢なども醸造酢に該当するがこれに限らない。酵母、酢酸菌、乳酸菌などの微生物により生成(醸造)した酢酸を一部でも含めばよく、製造工程中で酢酸菌や乳酸菌などを用いて生成した酢酸も含むが、一般的なビールの製造方法(酵母による発酵)により生成した酢酸は本発明における醸造酢には含まない。またこれら醸造酢に、水や他の食品や素材などを混合したものも、本発明における醸造酢といえる。たとえば、糖類や植物エキスなどの食品素材や、核酸類・有機酸類、またはそれらの塩(ナトリウム、カリウム、カルシウム、マグネシウムなどの塩)などの食品添加物を混合した醸造酢も、本発明における醸造酢として好適である。また、「膨らみ」とは口に含んで飲み込み、味がキレるまでの香味総量を指す。なお、本明細書において「醸造酢を含むノンアルコールビールテイスト飲料」や、製造工程において「醸造酢を添加する」とは、少なくとも一部に醸造酢を用いている態様を指すものである。即ち、食品などの素材を発酵することにより生成された醸造酢や、醸造酢を添加する場合の他に、醸造酢と醸造酢以外の成分との混合物として添加する場合についても、「醸造酢を含むノンアルコールビールテイスト飲料」、「醸造酢を添加する」に該当するものとする。例えば、醸造により生成した酢酸を全く含まない、いわゆる氷酢酸や化学合成により製造された合成酢酸と、醸造酢とを併用する場合などが考えられる。 The amount of acetic acid in the non-alcoholic beer-taste beverage of the present invention can be adjusted by producing it by fermentation during the production process, or by adding acetic acid or a material containing acetic acid, and gives the viewpoint of suppressing sour odor and swelling. From the point of view, it is preferable to ferment raw materials such as food to produce brewed vinegar, or to add brewed vinegar for adjustment. As used herein, "brewed vinegar" refers to acetic acid produced (brewed) by microorganisms such as yeast, acetic acid bacteria, and lactic acid bacteria. For example, Japanese Agricultural Standards (JAS) June 8, 1979 Ministry of Agriculture, Forestry and Fisheries Notification No. 801 (final revision: October 16, 2008 Ministry of Agriculture, Forestry and Fisheries Notification No. 1506) Brewed vinegar described in , and brewed vinegar described in the Fair Competition Code and Enforcement Regulations Concerning Labeling of Vinegar (enforced on May 18, 2018), grain vinegar, fruit vinegar, rice vinegar, rice black vinegar, apple Vinegar, grape vinegar, and the like also correspond to brewed vinegar, but are not limited to this. Acetic acid produced (brewed) by microorganisms such as yeast, acetic acid bacteria, and lactic acid bacteria may be included, even if only partially, and acetic acid produced using acetic acid bacteria and lactic acid bacteria during the manufacturing process is also included, but general beer production methods Acetic acid produced by (fermentation with yeast) is not included in the brewed vinegar in the present invention. A mixture of these brewed vinegars with water, other foodstuffs, materials, etc. can also be said to be the brewed vinegar in the present invention. For example, brewed vinegar mixed with food materials such as sugars and plant extracts, nucleic acids / organic acids, or food additives such as their salts (salts such as sodium, potassium, calcium, magnesium, etc.) Suitable as vinegar. In addition, "bulging" refers to the total amount of flavor until the taste is sharp after being swallowed in the mouth. In this specification, "a non-alcoholic beer-taste beverage containing brewed vinegar" and "adding brewed vinegar" in the manufacturing process refer to a mode in which brewed vinegar is used at least in part. In other words, in addition to the case of adding brewed vinegar produced by fermenting materials such as foods, and the case of adding brewed vinegar, when adding as a mixture of brewed vinegar and ingredients other than brewed vinegar, "brewed vinegar" Non-alcoholic beer-taste beverages including" and "adding brewed vinegar". For example, so-called glacial acetic acid, which does not contain acetic acid produced by brewing, or synthetic acetic acid produced by chemical synthesis, may be used in combination with brewed vinegar.
酢酸中の醸造酢の割合は、酸臭を抑制する観点及び膨らみを付与する観点から、好ましくは10質量%以上、より好ましくは20質量%以上、更に好ましくは30質量%以上、更に好ましくは40質量%以上、更に好ましくは50質量%以上、更に好ましくは60質量%以上、更に好ましくは70質量%以上、更に好ましくは80質量%以上、更に好ましくは90質量%以上、最も好ましくは100質量%である。 The proportion of brewed vinegar in acetic acid is preferably 10% by mass or more, more preferably 20% by mass or more, still more preferably 30% by mass or more, still more preferably 40% by mass, from the viewpoint of suppressing sour odor and imparting swelling. % by mass or more, more preferably 50% by mass or more, more preferably 60% by mass or more, still more preferably 70% by mass or more, still more preferably 80% by mass or more, still more preferably 90% by mass or more, most preferably 100% by mass is.
醸造酢の酸度は限定されないが、例えば、0.5以上、1.0以上、1.2以上、1.4以上、1.6以上、1.8以上、また、8.0以下、7.5以下、7.0以下、6.5以下のものが挙げられる。また、これらの値を任意に組み合わせた範囲とすることができる。また、酸臭の抑制する観点から、ナトリウム量の多い醸造酢を用いることが好ましい。本発明でいうナトリウムは、ナトリウムイオン、ナトリウム塩などの形で存在するものも含む。醸造酢中のナトリウムの含有量は、好ましくは100質量ppm以上、より好ましくは200質量ppm以上、更に好ましくは300質量ppm以上、更に好ましくは400質量ppm以上、更に好ましくは450質量ppm以上、更に好ましくは500質量ppm以上、更に好ましくは550質量ppm以上、更に好ましくは600質量ppm以上である。また、多量に添加すると渋みや硬さを付与してしまう観点から、好ましくは1000質量ppm以下、より好ましくは900質量ppm以下、更に好ましくは800質量ppm以下、更に好ましくは700質量ppm以下である。また、これらの値を任意に組み合わせた範囲とすることができる。本明細書において、ビールテイスト飲料の酸度は、改訂BCOJビール分析法(公益財団法人日本醸造協会発行、ビール酒造組合国際技術委員会〔分析委員会〕編集、2013年増補改訂)の「8.6 酸度」に記載の方法によって測定する。本明細書において、醸造酢中のナトリウムの含有量は、(https://www.fukushihoken.metro.tokyo.lg.jp/shokuhin/hyouji/kyouzai/files/eiyouseibun_handbook.pdf)p.13に記載される原子吸光光度法により測定する。 The acidity of the brewed vinegar is not limited, but may be, for example, 0.5 or more, 1.0 or more, 1.2 or more, 1.4 or more, 1.6 or more, 1.8 or more, or 8.0 or less, 7.0 or more. 5 or less, 7.0 or less, or 6.5 or less. Also, a range in which these values are arbitrarily combined can be used. In addition, from the viewpoint of suppressing sour odor, it is preferable to use brewed vinegar with a large amount of sodium. Sodium as used in the present invention also includes those present in the form of sodium ions, sodium salts, and the like. The content of sodium in brewed vinegar is preferably 100 mass ppm or more, more preferably 200 mass ppm or more, still more preferably 300 mass ppm or more, still more preferably 400 mass ppm or more, still more preferably 450 mass ppm or more, and further It is preferably 500 mass ppm or more, more preferably 550 mass ppm or more, still more preferably 600 mass ppm or more. In addition, from the viewpoint of imparting astringency and hardness when added in a large amount, it is preferably 1000 mass ppm or less, more preferably 900 mass ppm or less, still more preferably 800 mass ppm or less, and still more preferably 700 mass ppm or less. . Also, a range in which these values are arbitrarily combined can be used. In this specification, the acidity of beer-taste beverages is defined as "8.6" in the revised BCOJ beer analysis method (published by the Brewing Association of Japan, edited by the International Technical Committee of Beer Brewers Association [Analysis Committee], revised in 2013). acidity”. In this specification, the content of sodium in brewed vinegar is described in (https://www.fukushihoken.metro.tokyo.lg.jp/shokuhin/hyouji/kyouzai/files/eiyouseibun_handbook.pdf) p.13. Measured by atomic absorption spectrophotometry.
本発明のノンアルコールビールテイスト飲料に醸造酢を含有させること、特にナトリウム量の多い醸造酢を含有させることで酸臭の抑制を付与できるメカニズムは定かではないが、ナトリウムはpHの緩衝作用があるため、ナトリウムを含んだ溶液は口腔内でのpH変化が起こりにくく酢酸の過剰な揮発を抑制して酸臭を抑制できたと推定される。 The mechanism by which acid odor can be suppressed by including brewed vinegar in the non-alcoholic beer-taste beverage of the present invention, particularly by including brewed vinegar with a large amount of sodium, is not clear, but sodium has a pH buffering effect. Therefore, it is presumed that the pH of the solution containing sodium is less likely to change in the oral cavity, suppressing excessive volatilization of acetic acid and suppressing the sour odor.
本発明のノンアルコールビールテイスト飲料におけるpHは、シマリを付与し酸臭を抑制する観点から、好ましくはpH2.8以上、より好ましくはpH2.9以上、更に好ましくはpH3.0以上、更に好ましくはpH3.1以上、更に好ましくはpH3.2以上、更に好ましくはpH3.3以上、更に好ましくはpH3.4以上、更に好ましくはpH3.5以上である。また、シマリ付与効果が低下する観点から、好ましくはpH4.2以下、より好ましくはpH4.1以下、更に好ましくはpH4.0以下、更に好ましくはpH3.9以下、更に好ましくはpH3.8以下である。pHの調整は、酢酸の量、希釈水または炭酸水の添加、原材料(麦芽、コーングリッツ、糖液等)の種類、原材料の量、酵素の種類、酵素の添加量、酵素の添加のタイミング、仕込槽で糖化時間、仕込槽でのタンパク分解時間、仕込槽でのpH、仕込工程(麦芽投入から酵母添加前での麦汁製造工程)でのpH、pH調整の際に使用する酸の種類(乳酸、リン酸、リンゴ酸、酒石酸、クエン酸など)、pH調整の際に使用する酸の添加量、pH調整のタイミング(仕込時、発酵時、発酵完了時、ビール濾過前、ビール濾過後など)、麦汁を調製する際(糖化時含む)の各温度領域の設定温度及び保持時間、発酵前液のオリジナルエキス濃度、発酵工程でのオリジナルエキス濃度、発酵条件(酸素濃度、通気条件、酵母品種、酵母の添加量、酵母増殖数、酵母の除去タイミング、発酵温度、発酵時間、圧力設定、二酸化炭素濃度等)等を適宜設定して行うことができる。本明細書において、ノンアルコールビールテイスト飲料のpHは、改訂BCOJビール分析法(公益財団法人日本醸造協会発行、ビール酒造組合国際技術委員会〔分析委員会〕編集2013年増補改訂の8.7 pHに記載されている方法によって測定する。 The pH of the non-alcoholic beer-taste beverage of the present invention is preferably pH 2.8 or higher, more preferably pH 2.9 or higher, still more preferably pH 3.0 or higher, and still more preferably pH 3.0 or higher, from the viewpoint of imparting shimmer and suppressing acid odor. pH 3.1 or higher, more preferably pH 3.2 or higher, more preferably pH 3.3 or higher, still more preferably pH 3.4 or higher, and still more preferably pH 3.5 or higher. In addition, from the viewpoint of reducing the effect of imparting shimmer, it is preferably pH 4.2 or less, more preferably pH 4.1 or less, still more preferably pH 4.0 or less, still more preferably pH 3.9 or less, still more preferably pH 3.8 or less. be. Adjustment of pH is the amount of acetic acid, addition of diluted water or carbonated water, type of raw materials (malt, corn grits, sugar solution, etc.), amount of raw materials, type of enzyme, amount of enzyme added, timing of enzyme addition, preparation Saccharification time in the tank, protein decomposition time in the brewing tank, pH in the brewing tank, pH in the brewing process (wort manufacturing process from malt input to yeast addition), type of acid used for pH adjustment ( lactic acid, phosphoric acid, malic acid, tartaric acid, citric acid, etc.), the amount of acid used for pH adjustment, the timing of pH adjustment (at the time of preparation, at the time of fermentation, at the completion of fermentation, before beer filtration, after beer filtration, etc.) ), set temperature and holding time for each temperature range when preparing wort (including during saccharification), original extract concentration in pre-fermentation liquid, original extract concentration in fermentation process, fermentation conditions (oxygen concentration, aeration conditions, yeast Variety, amount of yeast added, yeast growth number, yeast removal timing, fermentation temperature, fermentation time, pressure setting, carbon dioxide concentration, etc.) can be set appropriately. In this specification, the pH of the non-alcoholic beer-taste beverage is the revised BCOJ beer analysis method (published by the Brewing Association of Japan, Beer Brewers Association International Technical Committee [Analysis Committee] edited by the 2013 enlarged revision of 8.7 pH Measured by the method described in
本明細書における「ビールテイスト飲料」とは、ビール様の風味をもつアルコール含有またはノンアルコールの炭酸飲料をいう。つまり、本明細書のビールテイスト飲料は、特に断わりがない場合、ビール風味の炭酸飲料を全て包含する。本発明はこのうち、「ノンアルコールビールテイスト飲料」に関する。本明細書において「ノンアルコールビールテイスト飲料」とは、アルコール度数が1v/v%未満のビールテイスト飲料である。本発明のノンアルコールビールテイスト飲料は、特に断りがない場合、酵母による発酵工程の有無に拘わらず、ビール風味を有するいずれのノンアルコールの炭酸飲料をも包含する。即ち、本発明のノンアルコールビールテイスト飲料は、最終製品中のエタノール含有量が1v/v%未満であれば発酵ノンアルコールビールテイスト飲料であってもよいし、非発酵ノンアルコールビールテイスト飲料であってもよい。発酵ノンアルコールビールテイスト飲料は上面発酵酵母を用いた発酵工程を経て醸造された上面発酵ノンアルコールビールテイスト飲料であってもよく、下面発酵酵母を用いた発酵工程を経て醸造された下面発酵ノンアルコールビールテイスト飲料であってもよい。発酵にはアルコールを生成する酵母(サッカロマイセス)や野生酵母(ブレタノマイセスなど)を用いても良いし、アルコールを生成しない酵母(サッカロマイセスなど)、野生酵母(ブレタノマイセスなど)、乳酸発酵やグルコン酸発酵を行う菌などを用いても良い。発酵ノンアルコールビールテイスト飲料の場合は、酵母を添加し1v/v%未満になるように発酵を停止させる方法や、発酵後に脱アルコール工程を経て1v/v%未満になるような方法で製造してもよい。 The term "beer-taste beverage" as used herein refers to an alcohol-containing or non-alcoholic carbonated beverage with a beer-like flavor. That is, the beer-taste beverages of the present specification include all beer-flavored carbonated beverages unless otherwise specified. Among these, the present invention relates to a "non-alcoholic beer-taste beverage". As used herein, a "non-alcoholic beer-taste beverage" is a beer-taste beverage having an alcohol content of less than 1 v/v%. Unless otherwise specified, the non-alcoholic beer-taste beverage of the present invention includes any non-alcoholic carbonated beverage having a beer flavor, regardless of the presence or absence of a yeast fermentation process. That is, the non-alcoholic beer-taste beverage of the present invention may be a fermented non-alcoholic beer-taste beverage or a non-fermented non-alcoholic beer-taste beverage as long as the ethanol content in the final product is less than 1 v/v%. may The fermented non-alcoholic beer-taste beverage may be a top-fermented non-alcoholic beer-taste beverage brewed through a fermentation process using top-fermenting yeast, or a bottom-fermented non-alcoholic beer-taste beverage brewed through a fermentation process using bottom-fermenting yeast. It may be a beer-taste beverage. For fermentation, alcohol-producing yeast (Saccharomyces) or wild yeast (Brettanomyces, etc.) may be used, or non-alcohol-producing yeast (Saccharomyces, etc.), wild yeast (Brettanomyces, etc.), lactic acid fermentation, or gluconic acid fermentation may be used. Bacteria and the like may also be used. In the case of fermented non-alcoholic beer-taste beverages, it is manufactured by adding yeast to stop fermentation so that it becomes less than 1 v / v%, or by a method that makes it less than 1 v / v% through a dealcoholization process after fermentation. may
本発明のノンアルコールビールテイスト飲料における原麦汁エキス(O-Ex)濃度は、好ましくは14.0w/w%以下、より好ましくは13.5w/w%以下、更に好ましくは13.0w/w%以下、更に好ましくは12.5w/w%以下、更に好ましくは12.0w/w%以下、更に好ましくは11.5w/w%以下、更に好ましくは11.0w/w%以下、更に好ましくは10.5w/w%以下、更に好ましくは10.0w/w%以下、更に好ましくは9.5w/w%以下、更に好ましくは9.0w/w%以下とすることができ、また好ましくは4.0w/w%以上、より好ましくは4.5w/w%以上、更に好ましくは5.0w/w%以上、更に好ましくは5.5w/w%以上、更に好ましくは6.0w/w%以上、更に好ましくは6.5w/w%以上、更に好ましくは7.0w/w%以上、更に好ましくは7.5w/w%以上、更に好ましくは8.0w/w%以上、更に好ましくは8.5w/w%以上である。本明細書において、原麦汁エキス(O-Ex)濃度は、改訂BCOJビール分析法(公益財団法人日本醸造協会発行、ビール酒造組合国際技術委員会〔分析委員会〕編集2013年増補改訂に記載されている方法によって測定する。原麦汁エキス(O-Ex)濃度の調整は、希釈水または炭酸水の添加、原材料(麦芽、コーングリッツ、糖液等)の種類、原材料の量、麦汁濾過の時間、麦汁濾過のpH、煮沸時間、煮沸温度等を適宜設定して行うことができる。 The raw wort extract (O-Ex) concentration in the non-alcoholic beer-taste beverage of the present invention is preferably 14.0 w/w% or less, more preferably 13.5 w/w% or less, still more preferably 13.0 w/w. % or less, more preferably 12.5 w/w% or less, more preferably 12.0 w/w% or less, even more preferably 11.5 w/w% or less, even more preferably 11.0 w/w% or less, still more preferably 10.5 w/w% or less, more preferably 10.0 w/w% or less, more preferably 9.5 w/w% or less, still more preferably 9.0 w/w% or less, and preferably 4 .0 w/w% or more, more preferably 4.5 w/w% or more, still more preferably 5.0 w/w% or more, still more preferably 5.5 w/w% or more, still more preferably 6.0 w/w% or more , More preferably 6.5 w/w% or more, more preferably 7.0 w/w% or more, still more preferably 7.5 w/w% or more, still more preferably 8.0 w/w% or more, still more preferably 8.0 w/w% or more. 5 w/w% or more. In this specification, the original wort extract (O-Ex) concentration is described in the revised BCOJ beer analysis method (published by the Brewing Association of Japan, Beer Brewers Association International Technical Committee [Analysis Committee] edited 2013 supplementary revision. The original wort extract (O-Ex) concentration is adjusted by adding diluted water or carbonated water, the type of raw materials (malt, corn grits, sugar solution, etc.), the amount of raw materials, and the wort filtration. time, pH of wort filtration, boiling time, boiling temperature, etc. can be appropriately set.
本発明のノンアルコールビールテイスト飲料における最終外観発酵度(LA)は80%以下、75%以下、70%以下、68%以下、66%以下、64%以下、62%以下、60%以下、58%以下、56%以下、54%以下、53%以下、52%以下にすることができる。また、20%以上、22%以上、23%以上、24%以上、26%以上、28%以上、30%以上、32%以上、34%以上、36%以上、38%以上、40%以上、42%以上、44%以上、46%以上にすることができる。本明細書において、最終外観発酵度(LA)は、改訂BCOJビール分析法(公益財団法人日本醸造協会発行、ビール酒造組合国際技術委員会〔分析委員会〕編集2013年増補改訂に記載されている方法によって測定する。最終外観発酵度(LA)の調整は、原材料(麦芽、コーングリッツ、糖液等)の種類、原材料の量、酵素の種類、酵素(糖質分解酵素、異性化酵素等も含む)の添加量、酵素の添加のタイミング、糖化時間、糖化時のpH、仕込工程(麦芽投入から酵母添加前までの麦汁製造工程)でのpH、麦汁濾過の時間、麦汁を調製する際(糖化時含む)の各温度領域の設定温度及び保持時間等を適宜設定して行うことができる。 The final appearance fermentation degree (LA) in the non-alcoholic beer-taste beverage of the present invention is 80% or less, 75% or less, 70% or less, 68% or less, 66% or less, 64% or less, 62% or less, 60% or less, 58 % or less, 56% or less, 54% or less, 53% or less, or 52% or less. 20% or more, 22% or more, 23% or more, 24% or more, 26% or more, 28% or more, 30% or more, 32% or more, 34% or more, 36% or more, 38% or more, 40% or more, It can be 42% or more, 44% or more, 46% or more. In this specification, the final appearance fermentation degree (LA) is described in the revised BCOJ beer analysis method (published by the Brewing Association of Japan, Beer Brewers Association International Technical Committee [Analysis Committee] edited 2013 supplementary revision. The final appearance fermentation degree (LA) is adjusted by the type of raw materials (malt, corn grits, sugar solution, etc.), the amount of raw materials, the type of enzyme, enzymes (sugar degrading enzymes, isomerases, etc.). ) addition amount, timing of enzyme addition, saccharification time, pH during saccharification, pH in the preparation process (wort manufacturing process from malt input to before yeast addition), wort filtration time, wort preparation The set temperature, holding time, and the like for each temperature range during (including during saccharification) can be appropriately set.
本発明のノンアルコールビールテイスト飲料におけるアルコール度数(アルコール含有量)は、好ましくは1.0v/v%未満、より好ましくは0.95v/v%以下、更に好ましくは0.90v/v%以下、更に好ましくは0.85v/v%以下、更に好ましくは0.80v/v%以下、更に好ましくは0.75v/v%以下、更に好ましくは0.70v/v%以下、更に好ましくは0.60v/v%以下、更に好ましくは0.50v/v%以下、更に好ましくは0.40v/v%以下、更に好ましくは0.30v/v%以下、更に好ましくは0.20v/v%以下、更に好ましくは0.10v/v%以下、更に好ましくは0.05v/v%以下である。本明細書において、アルコール度数(アルコール含有量)は、改訂BCOJビール分析法(公益財団法人日本醸造協会発行、ビール酒造組合国際技術委員会〔分析委員会〕編集2013年増補改訂に記載されている方法によって測定する。アルコール度数の調整は、希釈水または炭酸水の添加、発酵前液の糖組成、酵母の種類、酵母の量、醸造アルコールの添加、蒸留アルコールの添加等を適宜設定して行うことができる。 The alcohol content (alcohol content) of the non-alcoholic beer-taste beverage of the present invention is preferably less than 1.0 v/v%, more preferably 0.95 v/v% or less, still more preferably 0.90 v/v% or less, More preferably 0.85 v/v% or less, more preferably 0.80 v/v% or less, still more preferably 0.75 v/v% or less, still more preferably 0.70 v/v% or less, still more preferably 0.60 v /v% or less, more preferably 0.50v/v% or less, more preferably 0.40v/v% or less, still more preferably 0.30v/v% or less, still more preferably 0.20v/v% or less, and further It is preferably 0.10 v/v % or less, more preferably 0.05 v/v % or less. In this specification, the alcohol content (alcohol content) is described in the revised BCOJ beer analysis method (published by the Brewing Association of Japan, Beer Brewers Association International Technical Committee [Analysis Committee] edited 2013 supplementary revision. The alcohol content is adjusted by appropriately setting the addition of diluted water or carbonated water, the sugar composition of the pre-fermentation liquid, the type of yeast, the amount of yeast, the addition of brewer's alcohol, the addition of distilled alcohol, etc. be able to.
本発明のノンアルコールビールテイスト飲料における色度は、例えば、1.0EBC以上、3.0EBC以上、5.0EBC以上、6.0EBC以上、7.0EBC以上、8.0EBC以上、9.0EBC以上、10.0EBC以上、15.0EBC以上、20.0EBC以上とすることができ、また、40.0EBC以下、30.0EBC以下とすることができる。本明細書において、色度は、改訂BCOJビール分析法(公益財団法人日本醸造協会発行、ビール酒造組合国際技術委員会〔分析委員会〕編集2013年増補改訂の8.8 色度に記載されている方法によって測定する。色度の調整は、希釈水または炭酸水の添加、原材料(麦芽、コーングリッツ、糖液等)の種類、原材料の量、マッシング時の温度、マッシング時のpH、マッシングの時間、麦汁濾過の時間、麦汁濾過のpH、煮沸時間、煮沸温度、カラメル色素などの色素成分の量、ビール濾過の形式(珪藻土濾過、各種膜ろ過など)、ビール濾過の濾過量等を適宜設定して行うことができる。 The chromaticity of the non-alcoholic beer-taste beverage of the present invention is, for example, 1.0 EBC or more, 3.0 EBC or more, 5.0 EBC or more, 6.0 EBC or more, 7.0 EBC or more, 8.0 EBC or more, 9.0 EBC or more, It can be 10.0 EBC or more, 15.0 EBC or more, or 20.0 EBC or more, and can be 40.0 EBC or less, or 30.0 EBC or less. In this specification, the chromaticity is described in the revised BCOJ beer analysis method (Published by the Brewing Association of Japan, Beer Brewers Association International Technical Committee [Analysis Committee] Edited 2013 Supplementary Revision 8.8 Chromaticity Adjustment of chromaticity is done by adding diluted water or carbonated water, types of raw materials (malt, corn grits, sugar solution, etc.), amount of raw materials, temperature during mashing, pH during mashing, and mashing time. , Wort filtration time, pH of wort filtration, boiling time, boiling temperature, amount of pigment components such as caramel pigment, beer filtration type (diatomaceous earth filtration, various membrane filtration, etc.), beer filtration amount, etc. can be set.
本発明のノンアルコールビールテイスト飲料における苦味価は、例えば、5BUs以上、10BUs以上、15BUs以上、18BUs以上、20BUs以上、23BUs以上、25BUs以上とすることができ、また、40BUs以下、35BUs以下、32BUs以下、30BUs、28BUs以下とすることができる。本明細書において、苦味価は、「BCOJビール分析法(2004.11.1 改訂版)8.15 苦味価」の項に記載の方法に従って測定する。具体的には、脱ガスしたサンプルに酸を加えた後イソオクタンで抽出し、得られたイソオクタン層の吸光度を、イソオクタンを対照にして275nmで計測し、ファクターを乗じて苦味価(BU)を得ることができる。苦味価は、飲料に含まれるイソα酸の含有量に依存する。ホップに含まれるα酸を異性化することによりイソα酸は得られる。イソα酸の量を制御するには、ホップ品種、ホップの使用量、ホップの添加タイミング、ホップの添加時の温度およびその温度帯での保持時間、ホップ添加時のpH、発酵前液のオリジナルエキス濃度、発酵工程でのオリジナルエキス濃度、発酵条件(酸素濃度、通気条件、酵母品種、酵母の添加量、酵母増殖数、酵母の除去タイミング、発酵温度、発酵時間、圧力設定、二酸化炭素濃度等)等、ビール濾過の条件、希釈水の添加、炭酸水の添加等により調整することができる。また、市販のホップ加工品(イソα酸など)などでも調整することができ、量、種類、添加タイミング、添加時の温度およびその温度帯での保持時間、添加時のpH、発酵前液のオリジナルエキス濃度、発酵工程でのオリジナルエキス濃度、発酵条件(酸素濃度、通気条件、酵母品種、酵母の添加量、酵母増殖数、酵母の除去タイミング、発酵温度、発酵時間、圧力設定、二酸化炭素濃度等)等、ビール濾過の条件、希釈水の添加、炭酸水の添加等により調整することができる。ホップはペレットにしたペレットホップを用いてもよく、エキス化したエキスホップを用いてもよく、ホップ苞を用いてもよい。ホップおよびホップ加工品は単独で使用してもよく、併用してもよい。 The bitterness value of the non-alcoholic beer-taste beverage of the present invention can be, for example, 5 BUs or more, 10 BUs or more, 15 BUs or more, 18 BUs or more, 20 BUs or more, 23 BUs or more, 25 BUs or more, or 40 BUs or less, 35 BUs or less, or 32 BUs. 30 BUs, 28 BUs or less. In this specification, the bitterness value is measured according to the method described in the section "BCOJ Beer Analysis Method (2004.11.1 Revised Edition) 8.15 Bitterness Value". Specifically, acid is added to the degassed sample, followed by extraction with isooctane, the absorbance of the resulting isooctane layer is measured at 275 nm against isooctane, and multiplied by a factor to obtain the bitterness value (BU). be able to. The bitterness value depends on the content of iso-alpha acids contained in the beverage. Iso-α-acids are obtained by isomerizing α-acids contained in hops. To control the amount of iso-α-acids, hop varieties, amount of hops used, timing of hop addition, temperature when hops were added and holding time in that temperature range, pH when hops were added, original pre-fermentation solution Extract concentration, original extract concentration in the fermentation process, fermentation conditions (oxygen concentration, aeration conditions, yeast variety, yeast addition amount, yeast growth number, yeast removal timing, fermentation temperature, fermentation time, pressure setting, carbon dioxide concentration, etc.) ), etc., can be adjusted by the conditions of beer filtration, the addition of dilution water, the addition of carbonated water, and the like. In addition, commercially available hop processed products (such as iso-α acid) can also be adjusted, and the amount, type, addition timing, temperature at the time of addition and retention time in that temperature range, pH at the time of addition, pre-fermentation solution Original extract concentration, original extract concentration in the fermentation process, fermentation conditions (oxygen concentration, aeration conditions, yeast variety, yeast addition amount, yeast growth number, yeast removal timing, fermentation temperature, fermentation time, pressure setting, carbon dioxide concentration etc.) can be adjusted by the conditions of beer filtration, the addition of dilution water, the addition of carbonated water, and the like. Hops may be pelleted hops, extract hops, or hop bracts. Hops and hop processed products may be used alone or in combination.
本発明のノンアルコールビールテイスト飲料における全窒素量は、例えば、10mg/100mL以上、15mg/100mL以上、20mg/100mL以上、25mg/100mL以上、30mg/100mL以上、35mg/100mL以上、40mg/100mL以上、45mg/100mL以上、50mg/100mL以上とすることができ、また、100mg/100mL以下、95mg/100mL以下、90mg/100mL以下、85mg/100mL以下、80mg/100mL以下、75mg/100mL以下、70mg/100mL以下とすることができる。全窒素量はタンパク質、アミノ酸等の全ての窒素化合物の総量である。本明細書において、全窒素量は、改訂BCOJビール分析法(公益財団法人日本醸造協会発行、ビール酒造組合国際技術委員会〔分析委員会〕編集2013年増補改訂)8.9 全窒素に記載されている方法によって測定する。全窒素量の調整は、希釈水または炭酸水の添加、原材料(麦芽、コーングリッツ、糖液等)の種類、原材料の量、酵素の種類、酵素(タンパク分解酵素等も含む)の添加量、酵素反応時の温度、酵素の添加のタイミング、仕込槽でのタンパク分解時間、仕込槽でのpH、仕込槽での温度、仕込工程(麦芽投入から酵母添加前までの麦汁製造工程)でのpH、仕込工程での温度、麦汁濾過時の温度、麦汁濾過の時間、麦汁濾過時のpH、麦汁濾過の際に使用するスパージング水の量、麦汁を調製する際の各温度領域の設定温度及び保持時間、煮沸工程での煮沸時間及びpH、発酵前液のオリジナルエキス濃度、発酵工程でのオリジナルエキス濃度、発酵条件(酸素濃度、通気条件、酵母品種、酵母の添加量、酵母増殖数、酵母の除去タイミング、発酵温度、発酵時間、圧力設定、二酸化炭素濃度等)等、ビール濾過の条件を適宜設定して行うことができる。 The total nitrogen content in the non-alcoholic beer-taste beverage of the present invention is, for example, 10 mg/100 mL or more, 15 mg/100 mL or more, 20 mg/100 mL or more, 25 mg/100 mL or more, 30 mg/100 mL or more, 35 mg/100 mL or more, 40 mg/100 mL or more. , 45 mg / 100 mL or more, 50 mg / 100 mL or more, and 100 mg / 100 mL or less, 95 mg / 100 mL or less, 90 mg / 100 mL or less, 85 mg / 100 mL or less, 80 mg / 100 mL or less, 75 mg / 100 mL or less, 70 mg / It can be 100 mL or less. The total nitrogen content is the total amount of all nitrogen compounds such as proteins and amino acids. In this specification, the total nitrogen content is described in the revised BCOJ beer analysis method (published by the Brewing Association of Japan, Beer Brewers Association International Technical Committee [Analysis Committee] edited 2013 supplementary revision) 8.9 total nitrogen measured by the method Adjustment of the total nitrogen content is done by adding diluted water or carbonated water, type of raw materials (malt, corn grits, sugar solution, etc.), amount of raw materials, type of enzyme, amount of enzyme (including proteolytic enzyme, etc.) added, enzyme Temperature during reaction, timing of enzyme addition, proteolysis time in the brewing tank, pH in the brewing tank, temperature in the brewing tank, pH in the brewing process (wort production process from malt input to yeast addition) , temperature in the preparation process, temperature at the time of wort filtration, time of wort filtration, pH at the time of wort filtration, amount of sparging water used at the time of wort filtration, each temperature range when preparing wort Set temperature and holding time, boiling time and pH in the boiling process, original extract concentration in the pre-fermentation solution, original extract concentration in the fermentation process, fermentation conditions (oxygen concentration, aeration conditions, yeast variety, amount of yeast added, yeast Conditions for beer filtration, such as growth number, yeast removal timing, fermentation temperature, fermentation time, pressure setting, carbon dioxide concentration, etc., can be appropriately set.
本発明のノンアルコールビールテイスト飲料における総ポリフェノール量は、10質量ppm以上、20質量ppm以上、30質量ppm以上、40質量ppm以上、50質量ppm以上、60質量ppm以上、70質量ppm以上、80質量ppm以上、90質量ppm以上とすることができ、また、200質量ppm以下、180質量ppm以下、150質量ppm以下、140質量ppm以下、130質量ppm以下、120質量ppm以下とすることができる。本明細書において、総ポリフェノール量は、改訂BCOJビール分析法(公益財団法人日本醸造協会発行、ビール酒造組合国際技術委員会〔分析委員会〕編集2013年増補改訂)8.19 総ポリフェノールに記載されている方法によって測定する。総ポリフェノール量の調整は、希釈水または炭酸水の添加、原材料(麦芽等のポリフェノールを含む原料)の種類、原材料の量、酵素の種類、酵素の添加量、酵素の添加のタイミング、仕込槽で通気時間(マッシュエアレーションなど)、仕込槽でのpH、仕込工程(麦芽投入から酵母添加前での麦汁製造工程)でのpH、麦汁濾過の時間、麦汁を調製する際(糖化時含む)の各温度領域の設定温度及び保持時間、発酵前液のオリジナルエキス濃度、発酵工程でのオリジナルエキス濃度、発酵条件(酸素濃度、通気条件、酵母品種、酵母の添加量、酵母増殖数、酵母の除去タイミング、発酵温度、発酵時間、圧力設定、二酸化炭素濃度等)等を適宜設定して行うことができる。また、本発明のビールテイスト飲料の総ポリフェノール量は、例えば、大麦麦芽、麦芽のハスク(穀皮)などのポリフェノール含有量の多い原材料の使用量を調整することによって制御できる。具体的には、ポリフェノール含有量の多い麦芽等の原材料の使用量を増やすことにより総ポリフェノール量を増加させることができる。 The total amount of polyphenols in the non-alcoholic beer-taste beverage of the present invention is 10 mass ppm or more, 20 mass ppm or more, 30 mass ppm or more, 40 mass ppm or more, 50 mass ppm or more, 60 mass ppm or more, 70 mass ppm or more, 80 It can be 90 mass ppm or more, and can be 200 mass ppm or less, 180 mass ppm or less, 150 mass ppm or less, 140 mass ppm or less, 130 mass ppm or less, and 120 mass ppm or less. . In this specification, the amount of total polyphenols is described in the revised BCOJ beer analysis method (published by the Brewing Association of Japan, Beer Brewers Association International Technical Committee [Analysis Committee] edited 2013 supplementary revision) 8.19 total polyphenols measured by the method The amount of total polyphenols can be adjusted by adding diluted water or carbonated water, the type of raw materials (raw materials containing polyphenols such as malt), the amount of raw materials, the type of enzyme, the amount of enzyme added, the timing of enzyme addition, and the brewing tank. Aeration time (mash aeration, etc.), pH in the brewing tank, pH in the brewing process (from malt input to wort production process before yeast addition), wort filtration time, when preparing wort (including saccharification) ), the set temperature and holding time for each temperature range, the concentration of the original extract in the pre-fermentation solution, the concentration of the original extract in the fermentation process, the fermentation conditions (oxygen concentration, ventilation conditions, yeast variety, amount of yeast added, yeast growth number, yeast removal timing, fermentation temperature, fermentation time, pressure setting, carbon dioxide concentration, etc.) can be set appropriately. In addition, the total polyphenol content of the beer-taste beverage of the present invention can be controlled by adjusting the amount of raw materials with a high polyphenol content, such as barley malt and malt husks. Specifically, the total amount of polyphenols can be increased by increasing the amount of raw materials such as malt with a high polyphenol content.
本発明のノンアルコールビールテイスト飲料における遊離アミノ態窒素(FAN)の含有量は、1.0mg/100mL以上、2.0mg/100mL以上、3.0mg/100mL以上、4.0mg/100mL以上、5.0mg/100mL以上、6.0mg/100mL以上、7.0mg/100mL以上、8.0mg/100mL以上、9.0mg/100mL以上、10.0mg/100mL以上とすることができ、また、20.0mg/100mL以下、19.0mg/100mL以下、18.0mg/100mL以下、17.0mg/100mL以下、16.0mg/100mL以下、15.0mg/100mL以下、14.0mg/100mL以下とすることができる。本明細書において、FANの含有量は、改訂BCOJビール分析法(公益財団法人日本醸造協会発行、ビール酒造組合国際技術委員会〔分析委員会〕編集2013年増補改訂の8.18 遊離アミノ態窒素に記載されている方法によって測定する。FANの含有量の調整は、希釈水または炭酸水の添加、原材料(麦芽、コーングリッツ、糖液等)の種類、原材料の量、酵素の種類、酵素(タンパク分解酵素等も含む)の添加量、酵素の添加のタイミング、仕込槽でのタンパク分解時間、仕込槽でのpH、仕込工程(麦芽投入から酵母添加前までの麦汁製造工程)でのpH、麦汁濾過の時間、麦汁を調製する際の各温度領域の設定温度及び保持時間、煮沸工程での煮沸時間及びpH、発酵前液のオリジナルエキス濃度、発酵工程でのオリジナルエキス濃度、発酵条件(酸素濃度、通気条件、酵母品種、酵母の添加量、酵母増殖数、酵母の除去タイミング、発酵温度、発酵時間、圧力設定、二酸化炭素濃度等)等を適宜設定して行うことができる。 The content of free amino nitrogen (FAN) in the non-alcoholic beer-taste beverage of the present invention is 1.0 mg/100 mL or more, 2.0 mg/100 mL or more, 3.0 mg/100 mL or more, 4.0 mg/100 mL or more, 5 0 mg/100 mL or more, 6.0 mg/100 mL or more, 7.0 mg/100 mL or more, 8.0 mg/100 mL or more, 9.0 mg/100 mL or more, 10.0 mg/100 mL or more; 0 mg/100 mL or less, 19.0 mg/100 mL or less, 18.0 mg/100 mL or less, 17.0 mg/100 mL or less, 16.0 mg/100 mL or less, 15.0 mg/100 mL or less, 14.0 mg/100 mL or less can. In this specification, the content of FAN is based on the revised BCOJ beer analysis method (published by the Brewing Association of Japan, Beer Brewers Association International Technical Committee [Analysis Committee] edited by the 2013 supplementary revision 8.18 free amino nitrogen The FAN content is adjusted by adding diluted water or carbonated water, the type of raw materials (malt, corn grits, sugar solution, etc.), the amount of raw materials, the type of enzyme, the enzyme (protein (including degrading enzymes, etc.), timing of enzyme addition, protein decomposition time in the brewing tank, pH in the brewing tank, pH in the brewing process (wort manufacturing process from the addition of malt to the addition of yeast), Time of wort filtration, set temperature and holding time for each temperature range when preparing wort, boiling time and pH in the boiling process, original extract concentration in the pre-fermentation liquid, original extract concentration in the fermentation process, fermentation conditions (Oxygen concentration, aeration conditions, yeast variety, amount of yeast added, yeast growth number, yeast removal timing, fermentation temperature, fermentation time, pressure setting, carbon dioxide concentration, etc.) can be set appropriately.
本発明のノンアルコールビールテイスト飲料におけるイソα酸の含有量は、2.0質量ppm以上、4.0質量ppm以上、6.0質量ppm以上、7.0質量ppm以上、8.0質量ppm以上、9.0質量ppm以上、9.5質量ppm以上、10質量ppm以上とすることができ、また、40.0質量ppm以下、35.0質量ppm以下、30.0質量ppm以下、25.0質量ppm以下、20.0質量ppm以下、15.0質量ppm以下とすることができる。本明細書において、イソα酸の含有量は、改訂BCOJビール分析法(公益財団法人日本醸造協会発行、ビール酒造組合国際技術委員会〔分析委員会〕編集2013年増補改訂の8.25 イソα酸、α酸に記載されている方法によって測定する。イソα酸の含有量の調整は、ホップ品種、ホップの使用量、ホップの添加タイミング、ホップの添加時の温度およびその温度帯での保持時間、ホップ添加時のpH、発酵前液のオリジナルエキス濃度、発酵工程でのオリジナルエキス濃度、発酵条件(酸素濃度、通気条件、酵母品種、酵母の添加量、酵母増殖数、酵母の除去タイミング、発酵温度、発酵時間、圧力設定、二酸化炭素濃度等)等、ビール濾過の条件、希釈水の添加、炭酸水の添加等により調整することができる。また、市販のホップ加工品(イソα酸など)などでも調整することができ、量、種類、添加タイミング、添加時の温度およびその温度帯での保持時間、添加時のpH、発酵前液のオリジナルエキス濃度、発酵工程でのオリジナルエキス濃度、発酵条件(酸素濃度、通気条件、酵母品種、酵母の添加量、酵母増殖数、酵母の除去タイミング、発酵温度、発酵時間、圧力設定、二酸化炭素濃度等)等、ビール濾過の条件、希釈水の添加、炭酸水の添加等により調整することができる。ホップはペレットにしたペレットホップを用いてもよく、エキス化したエキスホップを用いてもよく、ホップ苞を用いてもよい。ホップおよびホップ加工品は単独で使用してもよく、併用しても良い。 The content of iso-α acids in the non-alcoholic beer-taste beverage of the present invention is 2.0 mass ppm or more, 4.0 mass ppm or more, 6.0 mass ppm or more, 7.0 mass ppm or more, and 8.0 mass ppm. Above, 9.0 mass ppm or more, 9.5 mass ppm or more, 10 mass ppm or more, and 40.0 mass ppm or less, 35.0 mass ppm or less, 30.0 mass ppm or less, 25 0 mass ppm or less, 20.0 mass ppm or less, or 15.0 mass ppm or less. In this specification, the content of iso-α acids is determined by the revised BCOJ beer analysis method (published by the Brewing Association of Japan, Beer Brewers Association International Technical Committee [Analysis Committee] edited by the 2013 supplementary revision of 8.25 iso-α Acids and α-acids are measured by the method described in. The content of iso-α-acids can be adjusted by adjusting the hop variety, the amount of hops used, the timing of adding hops, the temperature at which hops are added, and the temperature range during which the hops are added. Time, pH at the time of hop addition, original extract concentration in the pre-fermentation liquid, original extract concentration in the fermentation process, fermentation conditions (oxygen concentration, aeration conditions, yeast variety, amount of yeast added, yeast growth number, yeast removal timing, Fermentation temperature, fermentation time, pressure setting, carbon dioxide concentration, etc.) can be adjusted by beer filtration conditions, addition of dilution water, addition of carbonated water, etc. In addition, commercially available hop processed products (iso-α acid, etc.) can be adjusted. ), etc., the amount, type, addition timing, temperature at the time of addition and retention time in that temperature range, pH at the time of addition, original extract concentration in the pre-fermentation liquid, original extract concentration in the fermentation process, Fermentation conditions (oxygen concentration, ventilation conditions, yeast variety, amount of yeast added, yeast growth number, yeast removal timing, fermentation temperature, fermentation time, pressure setting, carbon dioxide concentration, etc.), beer filtration conditions, dilution water It can be adjusted by addition, addition of carbonated water, etc. Hops may be pelleted pellet hops, extracted extract hops, or hop bracts.Hop and hop processing. Products may be used alone or in combination.
本発明のノンアルコールビールテイスト飲料において酢酸エチルを含有することが好ましい。酢酸エチルの含有量としては0.1質量ppm以上、0.2質量ppm以上、0.3質量ppm以上、0.4質量ppm以上、0.5質量ppm以上、0.6質量ppm以上、0.7質量ppm以上、0.8質量ppm以上、0.9質量ppm以上、1.0質量ppm以上、2.0質量ppm以上、3.0質量ppm以上、4.0質量ppm以上、5.0質量ppm以上、6.0質量ppm以上、7.0質量ppm以上、8.0質量ppm以上、9.0質量ppm以上、10.0質量ppm以上、11.0質量ppm以上、12.0質量ppm以上、13.0質量ppm以上、14.0質量ppm以上、15.0質量ppm以上とすることができ、また、60.0質量ppm以下、50.0質量ppm以下、45.0質量ppm以下、40.0質量ppm以下とすることができる。本明細書において、酢酸エチルの含有量は、ガスクロマトグラフィーによって測定する。酢酸エチルの含有量の調整は、希釈水または炭酸水の添加、酢酸エチル含有香料の添加、酢酸エチル含有香料の量、酢酸エチル含有原料の量、酢酸エチル含有原料の添加、酢酸エチルを含む原材料の種類、酢酸エチルの基質の量、酢酸エチルの基質となる原材料の量、原材料の量、原材料の種類、酵素の種類、酵素の添加量、酵素の添加のタイミング、仕込槽で糖化時間、仕込槽でのタンパク分解時間、仕込槽でのpH、仕込工程(麦芽投入から酵母添加前での麦汁製造工程)でのpH、pH調整の際に使用する酸の添加量、pH調整のタイミング(仕込時、発酵時、発酵完了時、ビール濾過前、ビール濾過後など)、麦汁を調製する際(糖化時含む)の各温度領域の設定温度及び保持時間、発酵前液のオリジナルエキス濃度、発酵工程でのオリジナルエキス濃度、発酵条件(酸素濃度、通気条件、酵母品種、酵母の添加量、酵母増殖数、酵母の除去タイミング、発酵温度、発酵時間、圧力設定、二酸化炭素濃度等)等を適宜設定して行うことができる。 The non-alcoholic beer-taste beverage of the present invention preferably contains ethyl acetate. The content of ethyl acetate is 0.1 mass ppm or more, 0.2 mass ppm or more, 0.3 mass ppm or more, 0.4 mass ppm or more, 0.5 mass ppm or more, 0.6 mass ppm or more, 0 .7 mass ppm or more, 0.8 mass ppm or more, 0.9 mass ppm or more, 1.0 mass ppm or more, 2.0 mass ppm or more, 3.0 mass ppm or more, 4.0 mass ppm or more; 0 mass ppm or more, 6.0 mass ppm or more, 7.0 mass ppm or more, 8.0 mass ppm or more, 9.0 mass ppm or more, 10.0 mass ppm or more, 11.0 mass ppm or more, 12.0 mass ppm or more, 13.0 mass ppm or more, 14.0 mass ppm or more, 15.0 mass ppm or more, and 60.0 mass ppm or less, 50.0 mass ppm or less, 45.0 mass ppm ppm or less and 40.0 mass ppm or less. As used herein, the content of ethyl acetate is measured by gas chromatography. Adjustment of the content of ethyl acetate can be done by adding diluted water or carbonated water, adding ethyl acetate-containing fragrance, amount of ethyl acetate-containing fragrance, amount of ethyl acetate-containing raw material, adding ethyl acetate-containing raw material, raw material containing ethyl acetate. amount of ethyl acetate substrate, amount of raw material that is the substrate for ethyl acetate, amount of raw material, type of raw material, type of enzyme, amount of enzyme added, timing of enzyme addition, saccharification time in the brewing tank, preparation Proteolysis time in the tank, pH in the brewing tank, pH in the brewing process (from malt input to the wort production process before adding yeast), amount of acid used for pH adjustment, timing of pH adjustment ( At the time of preparation, during fermentation, at the completion of fermentation, before beer filtration, after beer filtration, etc.), when preparing wort (including during saccharification), the set temperature and holding time of each temperature range, the original extract concentration of the pre-fermentation liquid, Original extract concentration in the fermentation process, fermentation conditions (oxygen concentration, ventilation conditions, yeast variety, yeast addition amount, yeast growth number, yeast removal timing, fermentation temperature, fermentation time, pressure setting, carbon dioxide concentration, etc.) It can be set appropriately.
本発明のノンアルコールビールテイスト飲料における酢酸イソアミルの含有量は、0.01質量ppm以上、0.02質量ppm以上、0.03質量ppm以上、0.04質量ppm以上、0.05質量ppm以上、0.06質量ppm以上、0.07質量ppm以上、0.08質量ppm以上、0.09質量ppm以上、0.1質量ppm以上、0.15質量ppm以上、0.20質量ppm以上、0.25質量ppm以上、0.30質量ppm以上、0.35質量ppm以上、0.40質量ppm以上、0.45質量ppm以上、0.50質量ppm以上、1.0質量ppm以上、2.0質量ppm以上、3.0質量ppm以上、4.0質量ppm以上、5.0質量ppm以上とすることができ、また、20.0質量ppm以下、15.0質量ppm以下、10.0質量ppm以下とすることができる。本明細書において、酢酸イソアミルの含有量は、ガスクロマトグラフィーによって測定する。酢酸イソアミルの含有量の調整は、希釈水または炭酸水の添加、酢酸イソアミル含有香料の添加、酢酸イソアミル含有香料の量、酢酸イソアミル含有原料の量、酢酸イソアミル含有原料の添加、酢酸イソアミルを含む原材料の種類、酢酸イソアミルの基質の量、酢酸イソアミルの基質となる原材料の量、原材料の量、原材料の種類、酵素の種類、酵素の添加量、酵素の添加のタイミング、仕込槽で糖化時間、仕込槽でのタンパク分解時間、仕込槽でのpH、仕込工程(麦芽投入から酵母添加前での麦汁製造工程)でのpH、pH調整の際に使用する酸の添加量、pH調整のタイミング(仕込時、発酵時、発酵完了時、ビール濾過前、ビール濾過後など)、麦汁を調製する際(糖化時含む)の各温度領域の設定温度及び保持時間、発酵前液のオリジナルエキス濃度、発酵工程でのオリジナルエキス濃度、発酵条件(酸素濃度、通気条件、酵母品種、酵母の添加量、酵母増殖数、酵母の除去タイミング、発酵温度、発酵時間、圧力設定、二酸化炭素濃度等)等を適宜設定して行うことができる。 The content of isoamyl acetate in the non-alcoholic beer-taste beverage of the present invention is 0.01 mass ppm or more, 0.02 mass ppm or more, 0.03 mass ppm or more, 0.04 mass ppm or more, 0.05 mass ppm or more. , 0.06 mass ppm or more, 0.07 mass ppm or more, 0.08 mass ppm or more, 0.09 mass ppm or more, 0.1 mass ppm or more, 0.15 mass ppm or more, 0.20 mass ppm or more, 0.25 mass ppm or more, 0.30 mass ppm or more, 0.35 mass ppm or more, 0.40 mass ppm or more, 0.45 mass ppm or more, 0.50 mass ppm or more, 1.0 mass ppm or more, 2 0 mass ppm or more, 3.0 mass ppm or more, 4.0 mass ppm or more, 5.0 mass ppm or more, and 20.0 mass ppm or less, 15.0 mass ppm or less, and 10.0 mass ppm or more. It can be 0 mass ppm or less. As used herein, the content of isoamyl acetate is measured by gas chromatography. The adjustment of the content of isoamyl acetate is carried out by adding diluent water or carbonated water, adding isoamyl acetate-containing fragrance, amount of isoamyl acetate-containing fragrance, amount of isoamyl acetate-containing raw material, addition of isoamyl acetate-containing raw material, raw material containing isoamyl acetate. type of enzyme, amount of substrate for isoamyl acetate, amount of raw material that is the substrate for isoamyl acetate, amount of raw material, type of raw material, type of enzyme, amount of enzyme added, timing of enzyme addition, saccharification time in the preparation tank, preparation Proteolysis time in the tank, pH in the brewing tank, pH in the brewing process (from malt input to the wort production process before adding yeast), amount of acid used for pH adjustment, timing of pH adjustment ( At the time of preparation, during fermentation, at the completion of fermentation, before beer filtration, after beer filtration, etc.), when preparing wort (including during saccharification), the set temperature and holding time of each temperature range, the original extract concentration of the pre-fermentation liquid, Original extract concentration in the fermentation process, fermentation conditions (oxygen concentration, ventilation conditions, yeast variety, yeast addition amount, yeast growth number, yeast removal timing, fermentation temperature, fermentation time, pressure setting, carbon dioxide concentration, etc.) It can be set appropriately.
本発明のノンアルコールビールテイスト飲料におけるイソアミルアルコールの含有量は、1.0質量ppm以上、2.0質量ppm以上、3.0質量ppm以上、4.0質量ppm以上、5.0質量ppm以上、6.0質量ppm以上、7.0質量ppm以上、8.0質量ppm以上、9.0質量ppm以上、10.0質量ppm以上、15.0質量ppm以上、20.0質量ppm以上、30.0質量ppm以上とすることができ、また、100.0質量ppm以下、90.0質量ppm以下、80.0質量ppm以下、70.0質量ppm以下、60.0質量ppm以下、50.0質量ppm以下、40.0質量ppm以下とすることができる。本明細書において、イソアミルアルコールの含有量は、ガスクロマトグラフィーによって測定する。イソアミルアルコールの含有量の調整は、希釈水または炭酸水の添加、イソアミルアルコール含有香料の添加、イソアミルアルコール含有香料の量、イソアミルアルコール含有原料の量、イソアミルアルコール含有原料の添加、イソアミルアルコールを含む原材料の種類、イソアミルアルコールの基質の量、イソアミルアルコールの基質となる原材料の量、原材料の量、原材料の種類、酵素の種類、酵素の添加量、酵素の添加のタイミング、仕込槽で糖化時間、仕込槽でのタンパク分解時間、仕込槽でのpH、仕込工程(麦芽投入から酵母添加前での麦汁製造工程)でのpH、pH調整の際に使用する酸の添加量、pH調整のタイミング(仕込時、発酵時、発酵完了時、ビール濾過前、ビール濾過後など)、麦汁を調製する際(糖化時含む)の各温度領域の設定温度及び保持時間、発酵前液のオリジナルエキス濃度、発酵工程でのオリジナルエキス濃度、発酵条件(酸素濃度、通気条件、酵母品種、酵母の添加量、酵母増殖数、酵母の除去タイミング、発酵温度、発酵時間、圧力設定、二酸化炭素濃度等)等を適宜設定して行うことができる。 The content of isoamyl alcohol in the non-alcoholic beer-taste beverage of the present invention is 1.0 mass ppm or more, 2.0 mass ppm or more, 3.0 mass ppm or more, 4.0 mass ppm or more, 5.0 mass ppm or more. , 6.0 mass ppm or more, 7.0 mass ppm or more, 8.0 mass ppm or more, 9.0 mass ppm or more, 10.0 mass ppm or more, 15.0 mass ppm or more, 20.0 mass ppm or more, It can be 30.0 mass ppm or more, and 100.0 mass ppm or less, 90.0 mass ppm or less, 80.0 mass ppm or less, 70.0 mass ppm or less, 60.0 mass ppm or less, 50 0 mass ppm or less and 40.0 mass ppm or less. As used herein, the content of isoamyl alcohol is measured by gas chromatography. The adjustment of the content of isoamyl alcohol includes addition of diluted water or carbonated water, addition of isoamyl alcohol-containing fragrance, amount of isoamyl alcohol-containing fragrance, amount of isoamyl alcohol-containing raw material, addition of isoamyl alcohol-containing raw material, raw material containing isoamyl alcohol type, amount of substrate for isoamyl alcohol, amount of raw material that is the substrate for isoamyl alcohol, amount of raw material, type of raw material, type of enzyme, amount of enzyme added, timing of enzyme addition, saccharification time in the preparation tank, preparation Proteolysis time in the tank, pH in the brewing tank, pH in the brewing process (from malt input to the wort production process before adding yeast), amount of acid used for pH adjustment, timing of pH adjustment ( At the time of preparation, during fermentation, at the completion of fermentation, before beer filtration, after beer filtration, etc.), when preparing wort (including during saccharification), the set temperature and holding time of each temperature range, the original extract concentration of the pre-fermentation liquid, Original extract concentration in the fermentation process, fermentation conditions (oxygen concentration, ventilation conditions, yeast variety, yeast addition amount, yeast growth number, yeast removal timing, fermentation temperature, fermentation time, pressure setting, carbon dioxide concentration, etc.) It can be set appropriately.
本発明のノンアルコールビールテイスト飲料におけるカプロン酸エチルの含有量は、1.0質量ppb以上、2.0質量ppb以上、3.0質量ppb以上、4.0質量ppb以上、5.0質量ppb以上、6.0質量ppb以上、7.0質量ppb以上、8.0質量ppb以上、9.0質量ppb以上、10.0質量ppb以上、15.0質量ppb以上、20.0質量ppb以上、25.0質量ppb以上、30.0質量ppb以上、35.0質量ppb以上、40.0質量ppb以上、45.0質量ppb以上、50.0質量ppb以上とすることができ、また、900.0質量ppb以下、800.0質量ppb以下、700.0質量ppb以下、650.0質量ppb以下、600.0質量ppb以下、550.0質量ppb以下、500.0質量ppb以下、450.0質量ppb以下、400.0質量ppb以下とすることができる。本明細書において、カプロン酸エチルの含有量は、ガスクロマトグラフィーによって測定する。カプロン酸エチルの含有量の調整は、希釈水または炭酸水の添加、カプロン酸エチル含有香料の添加、カプロン酸エチル含有香料の量、カプロン酸エチル含有原料の量、カプロン酸エチル含有原料の添加、カプロン酸エチルを含む原材料の種類、カプロン酸エチルの基質の量、カプロン酸エチルの基質となる原材料の量、原材料の量、原材料の種類、酵素の種類、酵素の添加量、酵素の添加のタイミング、仕込槽で糖化時間、仕込槽でのタンパク分解時間、仕込槽でのpH、仕込工程(麦芽投入から酵母添加前での麦汁製造工程)でのpH、pH調整の際に使用する酸の添加量、pH調整のタイミング(仕込時、発酵時、発酵完了時、ビール濾過前、ビール濾過後など)、麦汁を調製する際(糖化時含む)の各温度領域の設定温度及び保持時間、発酵前液のオリジナルエキス濃度、発酵工程でのオリジナルエキス濃度、発酵条件(酸素濃度、通気条件、酵母品種、酵母の添加量、酵母増殖数、酵母の除去タイミング、発酵温度、発酵時間、圧力設定、二酸化炭素濃度等)等を適宜設定して行うことができる。 The content of ethyl caproate in the non-alcoholic beer-taste beverage of the present invention is 1.0 mass ppb or more, 2.0 mass ppb or more, 3.0 mass ppb or more, 4.0 mass ppb or more, and 5.0 mass ppb. 6.0 mass ppb or more, 7.0 mass ppb or more, 8.0 mass ppb or more, 9.0 mass ppb or more, 10.0 mass ppb or more, 15.0 mass ppb or more, 20.0 mass ppb or more , 25.0 mass ppb or more, 30.0 mass ppb or more, 35.0 mass ppb or more, 40.0 mass ppb or more, 45.0 mass ppb or more, 50.0 mass ppb or more, and 900.0 mass ppb or less, 800.0 mass ppb or less, 700.0 mass ppb or less, 650.0 mass ppb or less, 600.0 mass ppb or less, 550.0 mass ppb or less, 500.0 mass ppb or less, 450 0 mass ppb or less and 400.0 mass ppb or less. As used herein, the content of ethyl caproate is measured by gas chromatography. The content of ethyl caproate can be adjusted by adding diluted water or carbonated water, adding an ethyl caproate-containing fragrance, the amount of the ethyl caproate-containing fragrance, the amount of the ethyl caproate-containing raw material, the addition of the ethyl caproate-containing raw material, Type of raw material containing ethyl caproate, amount of substrate for ethyl caproate, amount of raw material serving as substrate for ethyl caproate, amount of raw material, type of raw material, type of enzyme, amount of enzyme added, timing of enzyme addition , saccharification time in the brewing tank, protein decomposition time in the brewing tank, pH in the brewing tank, pH in the brewing process (wort manufacturing process from malt input to yeast addition), acid used for pH adjustment addition amount, timing of pH adjustment (during preparation, fermentation, completion of fermentation, before beer filtration, after beer filtration, etc.), setting temperature and holding time for each temperature range when preparing wort (including during saccharification), Original extract concentration in the pre-fermentation liquid, original extract concentration in the fermentation process, fermentation conditions (oxygen concentration, ventilation conditions, yeast variety, amount of yeast added, yeast growth number, yeast removal timing, fermentation temperature, fermentation time, pressure setting , carbon dioxide concentration, etc.) can be set appropriately.
本発明のノンアルコールビールテイスト飲料における4-ビニルグアイアコール(4VG)の含有量は、1μg/L以上、5μg/L以上、7μg/L以上、10μg/L以上、μg/L以上、15μg/L以上、20μg/L以上、とすることができ、また、500μg/L以下、450μg/L以下、400μg/L以下、350μg/L以下、300μg/L以下とすることができる。本明細書において、4-ビニルグアイアコールの含有量は、ガスクロマトグラフィーによって測定する。4-ビニルグアイアコールの含有量の調整は、希釈水または炭酸水の添加、4-ビニルグアイアコール含有香料の添加、4-ビニルグアイアコール含有香料の量、4-ビニルグアイアコール含有原料の量、4-ビニルグアイアコール含有原料の添加、4-ビニルグアイアコールを含む原材料の種類、4-ビニルグアイアコールの基質(フェルラ酸など)の量、4-ビニルグアイアコールの基質(フェルラ酸など)となる原材料の量、原材料の量、原材料の種類、酵素の種類、酵素の添加量、酵素の添加のタイミング、仕込槽で糖化時間、仕込槽でのタンパク分解時間、仕込槽でのpH、仕込工程(麦芽投入から酵母添加前での麦汁製造工程)でのpH、pH調整の際に使用する酸の添加量、pH調整のタイミング(仕込時、発酵時、発酵完了時、ビール濾過前、ビール濾過後など)、麦汁を調製する際(糖化時含む)の各温度領域の設定温度及び保持時間、発酵前液のオリジナルエキス濃度、発酵工程でのオリジナルエキス濃度、発酵条件(酸素濃度、通気条件、酵母品種、酵母の添加量、酵母増殖数、酵母の除去タイミング、発酵温度、発酵時間、圧力設定、二酸化炭素濃度等)等を適宜設定して行うことができる。 The content of 4-vinylguaiacol (4VG) in the non-alcoholic beer-taste beverage of the present invention is 1 μg/L or more, 5 μg/L or more, 7 μg/L or more, 10 μg/L or more, 10 μg/L or more, 15 μg/L or more. , 20 μg/L or more, and 500 μg/L or less, 450 μg/L or less, 400 μg/L or less, 350 μg/L or less, or 300 μg/L or less. As used herein, the content of 4-vinylguaiacol is measured by gas chromatography. The content of 4-vinylguaiacol is adjusted by adding diluted water or carbonated water, adding a 4-vinylguaiacol-containing flavor, the amount of the 4-vinylguaiacol-containing flavor, the amount of the 4-vinylguaiacol-containing raw material, and the amount of the 4-vinylguaiacol. Addition of contained raw materials, types of raw materials containing 4-vinyl guaiacol, amount of 4-vinyl guaiacol substrate (ferulic acid, etc.), amount of raw materials serving as 4-vinyl guaiacol substrate (ferulic acid, etc.), amount of raw materials, The type of raw material, the type of enzyme, the amount of enzyme added, the timing of enzyme addition, the saccharification time in the brewing tank, the protein decomposition time in the brewing tank, the pH in the brewing tank, the brewing process (from the addition of malt to the addition of yeast) wort production process), the amount of acid used for pH adjustment, the timing of pH adjustment (at the time of preparation, during fermentation, at the end of fermentation, before beer filtration, after beer filtration, etc.), and preparing wort Set temperature and holding time for each temperature range (including during saccharification), original extract concentration in pre-fermentation solution, original extract concentration in fermentation process, fermentation conditions (oxygen concentration, aeration conditions, yeast variety, amount of yeast added) , yeast growth number, yeast removal timing, fermentation temperature, fermentation time, pressure setting, carbon dioxide concentration, etc.) can be set appropriately.
本発明のノンアルコールビールテイスト飲料における主な原材料は、水と共に麦芽を用いてもよく、また、麦芽を用いなくてもよい。さらにホップを用いてもよく、その他に、保存料、甘味料、水溶性食物繊維、苦味料又は苦味付与剤、酸化防止剤、香料、酸味料、塩類、スピリッツ等を用いてもよい。 The main raw materials in the non-alcoholic beer-taste beverage of the present invention may be water and malt, or may be without malt. Furthermore, hops may be used, and preservatives, sweeteners, water-soluble dietary fibers, bittering agents or bitterness-imparting agents, antioxidants, flavors, acidulants, salts, spirits, and the like may also be used.
麦芽とは、大麦、小麦、ライ麦、カラス麦、オート麦、ハト麦、エン麦などの麦類の種子を発芽させて乾燥させ、除根したものをいい、産地や品種は、いずれのものであってもよく、大麦麦芽が好ましい。大麦麦芽は、日本のビールテイスト飲料の原料として最も一般的に用いられる麦芽の1つである。大麦には、二条大麦、六条大麦などの種類があるが、いずれを用いてもよい。さらに、通常麦芽のほか、色麦芽なども用いることができる。なお、色麦芽を用いる際には、種類の異なる色麦芽を適宜組み合わせて用いてもよいし、一種類の色麦芽を用いてもよい。 Malt refers to the germinated, dried, and rooted barley seeds of barley, wheat, rye, oats, oats, pigeons, and oats. malted barley is preferred. Barley malt is one of the most commonly used malts as a raw material for Japanese beer-taste beverages. There are two kinds of barley, such as two-rowed barley and six-rowed barley, and any of them may be used. In addition to normal malt, colored malt can also be used. When using colored malt, different types of colored malt may be appropriately combined and used, or one type of colored malt may be used.
また、麦芽と共に、麦芽以外の穀物、タンパク、酵母エキス、糖液等を用いてもよい。そのような穀物としては、例えば、麦芽には該当しない麦(大麦、小麦、ライ麦、カラス麦、オート麦、ハト麦、エン麦等)、米(白米、玄米等)、トウモロコシ(コーングリッツ等)、こうりゃん、ばれいしょ、豆(大豆、えんどう豆等)、そば、ソルガム、粟、ひえ、およびそれらから得られたデンプン、これらの抽出物(エキス)等が挙げられる。これらの中でも、トウモロコシ(コーングリッツ等)を用いることが好ましい。また、タンパクとしては、大豆タンパク、エンドウ豆タンパク、酵母エキス、これらの分解物等が挙げられる。 In addition to malt, grains other than malt, protein, yeast extract, sugar solution, etc. may be used. Such grains include, for example, wheat that does not correspond to malt (barley, wheat, rye, oats, oats, pigeons, oats, etc.), rice (polished rice, brown rice, etc.), corn (corn grits, etc.), Koryan, potato, beans (soybeans, peas, etc.), buckwheat, sorghum, millet, barley, starches obtained therefrom, extracts thereof, and the like. Among these, it is preferable to use corn (corn grits, etc.). Examples of proteins include soybean protein, pea protein, yeast extract, decomposition products thereof, and the like.
なお、麦芽を用いない場合には、炭素源を含有する液糖、麦芽以外の上述の穀物等のアミノ酸含有材料(例えば、大豆たんぱく等)としての窒素源を用いたノンアルコールビールテイスト飲料が挙げられる。 In addition, when malt is not used, non-alcoholic beer-taste beverages using liquid sugar containing a carbon source, amino acid-containing materials such as the above-mentioned grains other than malt (for example, soybean protein, etc.) as a nitrogen source are mentioned. be done.
ホップとしては、例えば、ペレットホップ、粉末ホップ、ホップエキス等が挙げられる。また、用いるホップは、イソ化ホップ、還元ホップ等のホップ加工品を用いてもよい。 Hops include, for example, pellet hops, powdered hops, and hop extracts. As the hops to be used, processed hops such as isoformed hops and reduced hops may be used.
保存料としては、例えば、安息香酸;安息香酸ナトリウム等の安息香酸塩;パラオキシ安息香酸プロピル、パラオキシ安息香酸ブチル等の安息香酸エステル;二炭酸ジメチル等が挙げられる。また、保存料としては、強力サンプレザー(三栄源エフ・エフ・アイ株式会社製、安息香酸ナトリウムと安息香酸ブチルの混合物)等の市販の製剤を用いてもよい。これらの保存料は、単独で用いてもよく、2種以上を併用してもよい。保存料の配合量は、好ましくは5~1200質量ppm、より好ましくは10~1100質量ppm、更に好ましくは15~1000質量ppm、より更に好ましくは20~900質量ppmである。 Examples of preservatives include benzoic acid; benzoates such as sodium benzoate; benzoate esters such as propyl parahydroxybenzoate and butyl parahydroxybenzoate; and dimethyl dicarbonate. Moreover, as a preservative, a commercially available preparation such as Strong Samprezer (a mixture of sodium benzoate and butyl benzoate, manufactured by San-Eigen FFI Co., Ltd.) may be used. These preservatives may be used alone or in combination of two or more. The amount of the preservative is preferably 5 to 1200 mass ppm, more preferably 10 to 1100 mass ppm, still more preferably 15 to 1000 mass ppm, still more preferably 20 to 900 mass ppm.
甘味料としては、穀物由来のデンプンを酸または酵素等で分解した市販の糖化液、市販の水飴等の糖類、三糖類以上の糖、糖アルコール、ステビア等の天然甘味料、人工甘味料等が挙げられる。これらの糖類の形態は、溶液等の液体であってもよく、粉末等の固体であってもよい。また、デンプンの原料穀物の種類、デンプンの精製方法、および酵素や酸による加水分解等の処理条件についても特に制限はない。例えば、酵素や酸による加水分解の条件を適宜設定することにより、マルトースの比率を高めた糖類を用いてもよい。その他、スクロース、フルクトース、グルコース、マルトース、トレハロース、マルトトリオースおよびこれらの溶液(糖液)等を用いることもできる。イソマルトース、イソマルトトリオ―スなどの異性化した糖なども用いることができる。また、人工甘味料としては、例えば、アスパルテーム、アセスルファムカリウム(アセスルファムK)、スクラロース、ネオテーム等が挙げられる。甘味料は単独で使用しても良いし、2種以上を併用しても良い。 Examples of sweeteners include commercially available saccharified solutions obtained by decomposing grain-derived starch with acids or enzymes, sugars such as commercially available starch syrup, sugars of trisaccharides or higher, sugar alcohols, natural sweeteners such as stevia, and artificial sweeteners. mentioned. The form of these sugars may be liquid such as solution, or solid such as powder. In addition, there are no particular restrictions on the type of starch raw material grains, the method of purifying starch, and the treatment conditions such as hydrolysis with enzymes or acids. For example, sugars with a higher proportion of maltose may be used by appropriately setting conditions for hydrolysis with an enzyme or acid. In addition, sucrose, fructose, glucose, maltose, trehalose, maltotriose, solutions of these (sugar solutions), and the like can also be used. Isomerized sugars such as isomaltose and isomaltotriose can also be used. Examples of artificial sweeteners include aspartame, acesulfame potassium (acesulfame K), sucralose, and neotame. Sweeteners may be used alone or in combination of two or more.
水溶性食物繊維としては、例えば、難消化性デキストリン、ポリデキストロース、大豆食物繊維、グアーガム分解物、ペクチン、グルコマンナン、アルギン酸、ラミナリン、フコイジン、カラギーナン等が挙げられ、安定性や安全性等の汎用性の観点から、難消化性デキストリンまたはポリデキストロースが好ましい。 Examples of water-soluble dietary fiber include indigestible dextrin, polydextrose, soybean dietary fiber, guar gum decomposition product, pectin, glucomannan, alginic acid, laminarin, fucoidin, carrageenan, etc. Indigestible dextrin or polydextrose are preferred from a sexual point of view.
苦味料または苦味付与剤としては、特に限定されず、ホップの他に、例えば、マンネンロウ、レイシ、姫茴香、杜松実、セージ、迷迭香、マンネンタケ、月桂樹、クワシン、柑橘抽出物、ニガキ抽出物、コーヒー抽出物、茶抽出物、ゴーヤ抽出物、ハス胚芽抽出物、キダチアロエ抽出物、マンネンロウ抽出物、レイシ抽出物、ローレル抽出物、セージ抽出物、キャラウェイ抽出物、ナリンギン、アブシンチン、ニガヨモギ、ニガヨモギ抽出物等が挙げられる。 The bittering agent or bitterness-imparting agent is not particularly limited, and other than hops, for example, Ganoderma lucidum, Ganoderma lucidum, Himejiko, Juniper nut, Sage, Astragalus, Ganoderma lucidum, Bay laurel, Quassin, Citrus extract, Nigaki extract coffee extract, tea extract, bitter gourd extract, lotus germ extract, aloe vera extract, stonecrop extract, litchi extract, laurel extract, sage extract, caraway extract, naringin, absinthine, wormwood, A wormwood extract etc. are mentioned.
酸化防止剤としては、特に限定されず、通常のビールや発泡酒に酸化防止剤として用いられるものが使用でき、例えば、アスコルビン酸、エリソルビン酸、ビタミンEなどのトコフェロール類およびカテキン等が挙げられる。 The antioxidant is not particularly limited, and those used as antioxidants in ordinary beer and low-malt beer can be used. Examples include ascorbic acid, erythorbic acid, tocopherols such as vitamin E, and catechins.
香料としては、特に限定されず、一般的なビール香料を用いることができる。ビール香料は、ビール様の風味付けのために用いるものであり、発酵により発生する醸造成分等が含まれる。ビール香料としては、エステルや高級アルコールやラクトン類、例えば、酢酸イソアミル、n-プロパノール、イソブタノール、アセトアルデヒド、カプロン酸エチル、カプリル酸エチル、イソアミルプロピオネート、リナロール、ゲラニオール、シトラール、4-ビニルグアイアコール(4-VG)、4-メチル-3-ペンテン酸、2-メチル-2-ペンテン酸、1,4-シネオール、1,8-シネオール、2,3-ジエチル-5-メチルピラジン、γ-デカノラクトン、γ-ウンデカラクトン、ヘキサン酸エチル、2-メチル酪酸エチル、n-酪酸エチル、ミルセン等を含むビール香料(ビール様の香りを想起させる香料))などが挙げられる。 The flavor is not particularly limited, and general beer flavor can be used. Beer flavors are used to impart a beer-like flavor, and include brewing components and the like generated by fermentation. Beer flavors include esters, higher alcohols, and lactones such as isoamyl acetate, n-propanol, isobutanol, acetaldehyde, ethyl caproate, ethyl caprylate, isoamyl propionate, linalool, geraniol, citral, and 4-vinylguaiacol. (4-VG), 4-methyl-3-pentenoic acid, 2-methyl-2-pentenoic acid, 1,4-cineole, 1,8-cineole, 2,3-diethyl-5-methylpyrazine, γ-decanolactone .
酸味料としては、酸味を有する物質であれば特に限定されないが、例えば、酒石酸、リン酸、クエン酸、グルコン酸、乳酸、リンゴ酸、フィチン酸、コハク酸、グルコノデルタラクトンまたはそれらの塩が挙げられる。これらの酸味料の中でも、酒石酸、リン酸、クエン酸、グルコン酸、乳酸、リンゴ酸、フィチン酸、コハク酸またはそれらの塩が好ましく、酒石酸、リン酸、クエン酸、乳酸、またはそれらの塩がより好ましい。これらの酸味料は、単独で用いてもよく、2種以上を併用してもよい。 The acidulant is not particularly limited as long as it is a substance having a sour taste, and examples thereof include tartaric acid, phosphoric acid, citric acid, gluconic acid, lactic acid, malic acid, phytic acid, succinic acid, gluconodeltalactone, and salts thereof. mentioned. Among these acidulants, tartaric acid, phosphoric acid, citric acid, gluconic acid, lactic acid, malic acid, phytic acid, succinic acid or salts thereof are preferred, and tartaric acid, phosphoric acid, citric acid, lactic acid or salts thereof are preferred. more preferred. These acidulants may be used alone or in combination of two or more.
本明細書において、スピリッツとは、麦、米、そば、トウモロコシ等の穀物を原料として、麦芽または必要により酵素剤を用いて糖化し、酵母を用いて発酵させた後、更に蒸留して得られる酒類を意味する。スピリッツの原材料である穀物としては、麦が好ましい。 As used herein, spirits are obtained by saccharifying grains such as wheat, rice, buckwheat, and corn using malt or, if necessary, using an enzyme agent, fermenting them using yeast, and then further distilling them. means liquor. Wheat is preferred as a grain that is a raw material for spirits.
本発明のノンアルコールビールテイスト飲料の一態様として、容器詰飲料の態様が挙げられる。容器の例としては、ビン、ペットボトル、缶、または樽が挙げられるが、特に持ち運びが容易であるとの観点から、缶、ビン、ペットボトルが好ましい。なお、無色透明のビンやペットボトルを使用する場合、太陽光や蛍光灯の光にさらされることになるため、有色のビン、有色のペットボトル、缶、または樽が好ましい。 One aspect of the non-alcoholic beer-taste beverage of the present invention includes an aspect of a packaged beverage. Examples of the container include bottles, PET bottles, cans, and barrels, and cans, bottles, and PET bottles are preferable from the viewpoint of being particularly easy to carry. When using a colorless and transparent bottle or PET bottle, it is exposed to sunlight or fluorescent light, so a colored bottle, colored PET bottle, can or barrel is preferable.
本発明のノンアルコールビールテイスト飲料の麦芽比率は、20%以上、25%以上、30%以上、35%以上、40%以上、42%以上、45%以上とすることができ、また、100%以下、90%以下、80%以下、75%以下、70%以下、65%以下、60%以下、55%以下、52%以下、50%以下とすることができる。本明細書において、麦芽比率とは平成30年4月1日が施行日の酒税法および酒類行政関係法令等解釈通達に従って計算された値を意味する。 The malt ratio of the non-alcoholic beer-taste beverage of the present invention can be 20% or more, 25% or more, 30% or more, 35% or more, 40% or more, 42% or more, 45% or more, or 100%. 90% or less, 80% or less, 75% or less, 70% or less, 65% or less, 60% or less, 55% or less, 52% or less, or 50% or less. In the present specification, the malt ratio means a value calculated in accordance with the Liquor Tax Act and liquor administrative laws and regulations, etc., which are enforced on April 1, 2018.
本発明のノンアルコールビールテイスト飲料の炭酸ガスの量は、飲料の炭酸ガス圧によって表される。典型的には、飲料の炭酸ガス圧の上限は5.0kg/cm2、4.5kg/cm2、または4.0kg/cm2であり、下限は0.20kg/cm2、0.50kg/cm2、または1.0kg/cm2であり、これらの上限および下限のいずれを組み合わせてもよい。例えば、飲料の炭酸ガス圧は、0.20kg/cm2以上5.0kg/cm2以下、0.50kg/cm2以上4.5kg/cm2以下、または、1.0kg/cm2以上4.0kg/cm2以下であってよい。本明細書において、ガス圧とは、特別な場合を除き、容器内におけるガス圧をいう。圧力の測定は、20℃にした試料をガス内圧計に固定した後、一度ガス内圧計の活栓を開いてガスを抜き、再び活栓を閉じ、ガス内圧計を振り動かして指針が一定の位置に達したときの値を読み取る方法を用いて、または市販のガス圧測定装置を用いて測定する。 The amount of carbon dioxide in the non-alcoholic beer-taste beverage of the present invention is represented by the carbon dioxide pressure of the beverage. Typically, the upper limit of the carbon dioxide pressure of the beverage is 5.0 kg/cm 2 , 4.5 kg/cm 2 or 4.0 kg/cm 2 and the lower limit is 0.20 kg/cm 2 , 0.50 kg/cm 2 . cm 2 , or 1.0 kg/cm 2 , and any combination of these upper and lower limits may be used. For example, the carbon dioxide pressure of the beverage is 0.20 kg/cm 2 or more and 5.0 kg/cm 2 or less, 0.50 kg/cm 2 or more and 4.5 kg/cm 2 or less, or 1.0 kg/cm 2 or more4. It may be 0 kg/cm 2 or less. In the present specification, gas pressure refers to gas pressure within a container, except in special cases. To measure the pressure, after fixing the sample heated to 20°C to the gas pressure gauge, open the stopcock of the gas pressure gauge once to release the gas, close the stopcock again, and shake the gas pressure gauge until the pointer reaches a fixed position. It is measured using a method of reading the value when it is reached or using a commercially available gas pressure measuring device.
本発明のノンアルコールビールテイスト飲料は、必要に応じて、様々な添加物を含有してもよい。そのような添加物としては、例えば、着色料、泡形成剤、発酵促進剤、酵母エキス、ペプチド含有物等のタンパク質系物質、アミノ酸(グリシン、プロリンなど)、アミノ酸等の調味料が挙げられる。 The non-alcoholic beer-taste beverage of the present invention may contain various additives as necessary. Such additives include, for example, colorants, foaming agents, fermentation accelerators, yeast extracts, protein substances such as peptide-containing substances, amino acids (glycine, proline, etc.), seasonings such as amino acids.
着色料は、飲料にビール様の色を与えるために使用するものであり、カラメル色素などを用いることができる。 Colorants are used to give beverages a beer-like color, and caramel pigments and the like can be used.
泡形成剤は、飲料にビール様の泡を形成させるため、あるいは飲料の泡を保持させるために使用するものであり、大豆サポニン、キラヤサポニン等の植物抽出サポニン系物質、コーン、大豆などの植物タンパク、およびコラーゲンペプチド等のペプチド含有物、酵母エキスなどを適宜使用することができる。 The foam-forming agent is used to form a beer-like foam in a beverage or to retain the foam of the beverage. Proteins, peptide-containing substances such as collagen peptides, yeast extracts, and the like can be used as appropriate.
発酵促進剤は、酵母による発酵を促進させるために使用するものであり、例えば、酵母エキス、米や麦などの糠成分、ビタミン、ミネラル剤などを単独または組み合わせて使用することができる。 Fermentation promoters are used to promote fermentation by yeast. For example, yeast extract, bran ingredients such as rice and wheat, vitamins, minerals, etc. can be used alone or in combination.
本発明のノンアルコールビールテイスト飲料は、酢酸を90~320質量ppmとなるように含有させる工程を有し、pHを2.8~4.2の範囲内とする以外は、いずれも一般的なノンアルコールビールテイスト飲料と同様にして製造できる。以下に、一般的なノンアルコールビールテイスト飲料の製造方法として、麦芽を原料として使用する場合と使用しない場合の製造方法を示す。 The non-alcoholic beer-taste beverage of the present invention has a step of containing acetic acid to 90 to 320 ppm by mass, and has a pH within the range of 2.8 to 4.2. It can be produced in the same manner as non-alcoholic beer-taste beverages. Below, as a method for producing a general non-alcoholic beer-taste beverage, the production method using and not using malt as a raw material will be shown.
麦芽を原料として使用して製造されるノンアルコールビールテイスト飲料は、まず、麦芽等の麦の他、必要に応じて他の穀物、でんぷん、糖類、苦味料、又は着色料などの原料及び水を含む混合物に、必要に応じてアミラーゼなどの酵素を添加し、糊化、糖化を行なわせ、ろ過し、糖化液とする。必要に応じてホップや苦味料などを糖化液に加えて煮沸し、清澄タンクにて凝固タンパク質などの固形分を取り除く。この糖化液の代替として、麦芽エキスに温水を加えたものにホップを加えて煮沸してもよい。ホップは煮沸開始から煮沸終了前のどの段階で混合してもよい。糖化工程、煮沸工程、固形分除去工程などにおける条件は、知られている条件を用いればよい。煮沸後、冷却し、得られた麦汁に香料、酸味料、カラメル色素などの色素、酸化防止剤、苦味料、甘味料、アミノ酸原料などを添加し、濾過し、得られた濾過液に炭酸ガスを加える。その後、容器に充填し殺菌工程を経て目的のノンアルコールビールテイスト飲料を得る。本発明の製造方法における工程として酢酸を添加する態様においては、容器詰めする直前のろ過の前に添加することが好ましい。 A non-alcoholic beer-taste beverage manufactured using malt as a raw material is first prepared by adding raw materials such as grains, starch, sugars, bittering agents, or coloring agents and water as necessary, in addition to barley such as malt. If necessary, an enzyme such as amylase is added to the mixture containing the mixture for gelatinization and saccharification, followed by filtration to obtain a saccharified solution. If necessary, hops, bittering agents, etc. are added to the saccharified liquid and boiled, and solids such as coagulated proteins are removed in a clarifying tank. As an alternative to this saccharified solution, hops may be added to malt extract and warm water, and the mixture may be boiled. Hops may be mixed at any stage from the beginning of boiling to the end of boiling. Known conditions may be used for the conditions in the saccharification step, the boiling step, the solid content removal step, and the like. After boiling, the wort is cooled. Flavors, acidulants, pigments such as caramel pigments, antioxidants, bittering agents, sweeteners, amino acid raw materials, etc. are added to the wort obtained. Add gas. Then, it is filled into a container and sterilized to obtain the desired non-alcoholic beer-taste beverage. In the embodiment in which acetic acid is added as a step in the production method of the present invention, it is preferably added before filtration immediately before packaging.
麦芽を原料として使用しないノンアルコールビールテイスト飲料を製造する場合には、まず、炭素源を含有する液糖、麦又は麦芽以外のアミノ酸含有材料としての窒素源、ホップ、色素等を、温水と共に混合し、液糖溶液とする。該液糖溶液は、煮沸する。原料としてホップを用いる場合、ホップは煮沸開始前ではなく、煮沸中に、該液糖溶液に混合してもよい。煮沸後、冷却し、得られた麦汁に香料、酸味料、カラメル色素などの色素、酸化防止剤、苦味料、甘味料、アミノ酸原料などを添加し、濾過し、得られた液糖溶液に対して、炭酸ガスを加える。その後、容器に充填し殺菌工程を経て目的のノンアルコールビールテイスト飲料を得る。本発明の製造方法における工程として酢酸を添加する態様においては、容器詰めする直前のろ過の前に添加することが好ましい。 When producing a non-alcoholic beer-taste beverage that does not use malt as a raw material, first, liquid sugar containing a carbon source, a nitrogen source as an amino acid-containing material other than wheat or malt, hops, pigments, etc. are mixed with warm water. and make a liquid sugar solution. The liquid sugar solution is boiled. When hops are used as a raw material, the hops may be mixed into the liquid sugar solution during boiling rather than before the start of boiling. After boiling, the wort is cooled, flavoring agents, acidulants, pigments such as caramel pigments, antioxidants, bittering agents, sweeteners, amino acid raw materials, etc. are added to the wort obtained, and filtered. Add carbon dioxide gas. Then, it is filled into a container and sterilized to obtain the desired non-alcoholic beer-taste beverage. In the embodiment in which acetic acid is added as a step in the production method of the present invention, it is preferably added before filtration immediately before packaging.
また、本発明の製造方法で得られたノンアルコールビールテイスト飲料は、シマリ及び刺激感に優れるものである。従って、本発明はノンアルコールビールテイスト飲料のシマリ及び刺激感を付与する香味向上方法についても提供するものである。なお、本発明の香味向上方法における工程の詳細は、本発明の製造方法と同様である。 In addition, the non-alcoholic beer-taste beverage obtained by the production method of the present invention is excellent in refreshing and stimulating feeling. Accordingly, the present invention also provides a method for improving the flavor of non-alcoholic beer-taste beverages by imparting sharpness and stimulation. The details of the steps in the flavor improving method of the present invention are the same as those of the production method of the present invention.
以下、実施例を示して本発明を具体的に説明するが、本発明は下記実施例に制限されるものではない。 The present invention will be specifically described below with reference to examples, but the present invention is not limited to the following examples.
<ノンアルコールビールテイスト飲料の調製>
実施例1~11、比較例1~6
水及び麦芽を仕込槽に投入して約45℃のマッシュを調製し、そのマッシュを75~85℃の範囲まですみやかに昇温した後、昇温後の所定の温度で一定時間保持、攪拌した後、麦汁濾過槽に移して濾過を行って麦汁を得た。得られた麦汁に温水を加えて希釈し、ホップ、乳酸、水あめを投入し、煮沸釜を用いて100℃で煮沸処理を行った。煮沸処理後に、ワールプールタンクに移送して、麦汁オリを除去し、約1~6℃まで冷却し、冷却液を得た。酵母を添加し、発酵を行い、表1~2に記載のアルコール濃度になるように調整した。表1~2に記載の濃度となるように合成酢酸を添加し、濾過工程、ビール香料を添加し、炭酸ガス付けを実施し、瓶詰を実施して、ノンアルコールビールテイスト飲料を得た。
<Preparation of non-alcoholic beer-taste beverage>
Examples 1-11, Comparative Examples 1-6
Water and malt were added to the preparation tank to prepare mash at about 45°C, and the temperature of the mash was quickly raised to the range of 75 to 85°C. After that, the wort was transferred to a wort filtration tank and filtered to obtain wort. Hot water was added to the obtained wort to dilute it, hops, lactic acid, and starch syrup were added, and the wort was boiled at 100°C using a boiling kettle. After the boiling treatment, the wort was transferred to a whirlpool tank to remove the wort pellets and cooled to about 1 to 6°C to obtain a cooling liquid. Yeast was added, fermentation was performed, and the alcohol concentration was adjusted as shown in Tables 1 and 2. Synthetic acetic acid was added so that the concentrations shown in Tables 1 and 2 were obtained, a filtration step, beer flavoring were added, carbonation was performed, and bottling was performed to obtain a non-alcoholic beer-taste beverage.
<シマリ>
各実施例・比較例のノンアルコールビールテイスト飲料を4℃まで冷却した後、「シマリ」について、2点の飲料を用意して、評価基準を統一した。スコア化は0.5刻みで実施し、専門パネリスト5名のスコアの平均点を算出した。結果を表1~2に示す。
(シマリの評価基準)
「1」:不適
「2」:合格
「3」:好ましい
<Simari>
After cooling the non-alcoholic beer-taste beverage of each example and comparative example to 4° C., two beverages were prepared for “Shimari” and the evaluation criteria were unified. Scoring was performed in increments of 0.5, and the average score of five expert panelists was calculated. The results are shown in Tables 1-2.
(Evaluation criteria for simplicity)
"1": Unsuitable "2": Passed "3": Favorable
<刺激感>
各実施例・比較例のノンアルコールビールテイスト飲料を4℃まで冷却した後、「刺激感」について、2点の飲料を用意して、評価基準を統一した。スコア化は0.5刻みで実施し、専門パネリスト5名のスコアの平均点を算出した。結果を表1~2に示す。
(刺激感の評価基準)
「1」:不適
「2」:合格
「3」:好ましい
<Stimulation>
After cooling the non-alcoholic beer-taste beverages of each example and comparative example to 4° C., two beverages were prepared for “irritation” and the evaluation criteria were unified. Scoring was performed in increments of 0.5, and the average score of five expert panelists was calculated. The results are shown in Tables 1-2.
(Evaluation Criteria for Stimulation)
"1": Unsuitable "2": Passed "3": Favorable
<酸臭>
各実施例・比較例のノンアルコールビールテイスト飲料を4℃まで冷却した後、「酸臭」について、2点の飲料を用意して、評価基準を統一した。スコア化は0.5刻みで実施し、専門パネリスト5名のスコアの平均点を算出した。結果を表1~2に示す。
(酸臭の評価基準)
「1」:不適
「2」:合格
「3」:好ましい
<Sour odor>
After cooling the non-alcoholic beer-taste beverages of each example and comparative example to 4° C., two beverages were prepared for “acid odor” and the evaluation criteria were unified. Scoring was performed in increments of 0.5, and the average score of five expert panelists was calculated. The results are shown in Tables 1-2.
(Evaluation criteria for sour odor)
"1": Unsuitable "2": Passed "3": Favorable
表1に示すように、酢酸の含有量が90~320質量ppm、pHが2.8~4.2の実施例1~11ではいずれもシマリ、刺激感に優れるものであり、酸臭も抑制されていた。 As shown in Table 1, in Examples 1 to 11 with an acetic acid content of 90 to 320 ppm by mass and a pH of 2.8 to 4.2, all of them are excellent in shimmering and stimulating feeling, and also suppresses acid odor. It had been.
<醸造酢の調製>
大麦麦芽を用いて、仕込みを行い、得られた麦汁を酵母でアルコール発酵を行った。酵母を除去後、食酢、酢酸菌を添加して、酢酸発酵を行い、醸造酢を得た。そして、酢酸ナトリウムを用いてナトリウム含有量を調整し、表3に示す醸造酢A~Cを調製した。
<Preparation of brewed vinegar>
Barley malt was used for preparation, and the obtained wort was subjected to alcoholic fermentation with yeast. After removing the yeast, acetic acid fermentation was performed by adding vinegar and acetic acid bacteria to obtain brewed vinegar. Then, sodium acetate was used to adjust the sodium content, and brewed vinegars A to C shown in Table 3 were prepared.
実施例12~24
合成酢酸に代えて上記で調製した醸造酢を添加し、表4に示す組成とした以外は、実施例1と同様にノンアルコールビールテイスト飲料を調製した。シマリ、刺激感、酸臭についても実施例1と同様に評価を行った。結果を表4に示す。
Examples 12-24
A non-alcoholic beer-taste beverage was prepared in the same manner as in Example 1, except that the above-prepared brewed vinegar was added in place of the synthetic acetic acid to give the composition shown in Table 4. The same evaluations as in Example 1 were also made for staining, irritating feeling, and sour odor. Table 4 shows the results.
表4に示すように、合成酢酸に代えて醸造酢を用いた実施例12~24では、合成酢酸を用いた場合に比べて、酸臭の抑制に優れる傾向にあることが分かった。 As shown in Table 4, it was found that Examples 12 to 24, in which brewed vinegar was used instead of synthetic acetic acid, tended to be superior in suppressing sour odor compared to the case of using synthetic acetic acid.
<膨らみ>
実施例1、12、17、18、19、21、24のノンアルコールビールテイスト飲料を4℃まで冷却した後、「膨らみ」について、2点の飲料を用意して、評価基準を統一した。スコア化は0.5刻みで実施し、専門パネリスト5名のスコアの平均点を算出した。結果を表5に示す。
(膨らみの評価基準)
「1」:不適
「2」:合格
「3」:好ましい
<Swelling>
After cooling the non-alcoholic beer-taste beverages of Examples 1, 12, 17, 18, 19, 21, and 24 to 4° C., two beverages were prepared for “swelling” and the evaluation criteria were unified. Scoring was performed in increments of 0.5, and the average score of five expert panelists was calculated. Table 5 shows the results.
(Evaluation criteria for swelling)
"1": Unsuitable "2": Passed "3": Favorable
表5に示すように、合成酢酸に代えて醸造酢を用いた実施例12、17、18、19、21、24では、合成酢酸を用いた場合に比べて膨らみに優れる傾向にあることが分かった。 As shown in Table 5, in Examples 12, 17, 18, 19, 21, and 24, in which brewed vinegar was used instead of synthetic acetic acid, it was found that swelling tended to be superior to that in the case of using synthetic acetic acid. rice field.
実施例25~28
市販のノンアルコールビールテイスト飲料(参考例1、2)に対し、表6の酢酸量となるように合成酢酸又は醸造酢を添加して、ノンアルコールビールテイスト飲料を調製した。上記と同様にしてシマリ、刺激感、酸臭、膨らみについて評価を行った。結果を表6に示す。
Examples 25-28
Non-alcoholic beer-taste beverages were prepared by adding synthetic acetic acid or brewed vinegar to the commercially available non-alcoholic beer-taste beverages (Reference Examples 1 and 2) so that the amounts of acetic acid shown in Table 6 were obtained. In the same manner as described above, evaluations were made for spotting, irritation, sour odor, and swelling. Table 6 shows the results.
表6に示すように、市販品に酢酸を添加した場合でも、シマリ、刺激感に優れるものであり、酸臭も抑制されていたことが分かる。特に、醸造酢を添加した実施例26、28では、酸臭の抑制に優れ、且つ膨らみについても優れるものであった。 As shown in Table 6, even when acetic acid was added to the commercial product, it was found to be excellent in shimmering and irritating feeling, and to suppress the sour odor. In particular, Examples 26 and 28, in which brewed vinegar was added, were excellent in suppressing sour odor and also in swelling.
本発明によれば、シマリ、刺激感に優れる新たなテイストのノンアルコールビールテイスト飲料を提供できる。 According to the present invention, it is possible to provide a non-alcoholic beer-taste beverage with a new taste that is refreshing and stimulating.
Claims (10)
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2019118323A (en) * | 2018-01-09 | 2019-07-22 | アサヒビール株式会社 | Citrus fruit-like beverage, concentrate for citrus fruit-like beverage, and manufacturing method therefor |
| JP2020054236A (en) * | 2018-09-28 | 2020-04-09 | サッポロビール株式会社 | Beer taste beverage and method for producing the same |
| JP2020103209A (en) * | 2018-12-28 | 2020-07-09 | サントリーホールディングス株式会社 | Non-alcoholic beer taste beverage |
| JP2021003128A (en) * | 2020-09-30 | 2021-01-14 | サントリーホールディングス株式会社 | Beer-taste beverage |
| JP2021013347A (en) * | 2019-07-12 | 2021-02-12 | サントリーホールディングス株式会社 | Beer-taste beverages and manufacturing methods for beer-taste beverages |
| JP2022152782A (en) * | 2021-03-29 | 2022-10-12 | サッポロビール株式会社 | Method for producing beer-taste beverage |
-
2022
- 2022-08-29 WO PCT/JP2022/032377 patent/WO2023032902A1/en not_active Ceased
- 2022-08-31 TW TW111132909A patent/TW202327460A/en unknown
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2019118323A (en) * | 2018-01-09 | 2019-07-22 | アサヒビール株式会社 | Citrus fruit-like beverage, concentrate for citrus fruit-like beverage, and manufacturing method therefor |
| JP2020054236A (en) * | 2018-09-28 | 2020-04-09 | サッポロビール株式会社 | Beer taste beverage and method for producing the same |
| JP2020103209A (en) * | 2018-12-28 | 2020-07-09 | サントリーホールディングス株式会社 | Non-alcoholic beer taste beverage |
| JP2021013347A (en) * | 2019-07-12 | 2021-02-12 | サントリーホールディングス株式会社 | Beer-taste beverages and manufacturing methods for beer-taste beverages |
| JP2021003128A (en) * | 2020-09-30 | 2021-01-14 | サントリーホールディングス株式会社 | Beer-taste beverage |
| JP2022152782A (en) * | 2021-03-29 | 2022-10-12 | サッポロビール株式会社 | Method for producing beer-taste beverage |
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