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WO2019045397A2 - Composition cosmétique contenant une teneur élevée en composant huileux et masque en tissu l'utilisant - Google Patents

Composition cosmétique contenant une teneur élevée en composant huileux et masque en tissu l'utilisant Download PDF

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Publication number
WO2019045397A2
WO2019045397A2 PCT/KR2018/009884 KR2018009884W WO2019045397A2 WO 2019045397 A2 WO2019045397 A2 WO 2019045397A2 KR 2018009884 W KR2018009884 W KR 2018009884W WO 2019045397 A2 WO2019045397 A2 WO 2019045397A2
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WO
WIPO (PCT)
Prior art keywords
cosmetic composition
oil
bio
sheet mask
cellulose
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/KR2018/009884
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English (en)
Korean (ko)
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WO2019045397A3 (fr
Inventor
정주아
박창현
이은지
임재민
최양규
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Amorepacific Corp
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Amorepacific Corp
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Publication date
Application filed by Amorepacific Corp filed Critical Amorepacific Corp
Priority to CN201880070574.2A priority Critical patent/CN111343960A/zh
Publication of WO2019045397A2 publication Critical patent/WO2019045397A2/fr
Publication of WO2019045397A3 publication Critical patent/WO2019045397A3/fr
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0212—Face masks
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/731—Cellulose; Quaternized cellulose derivatives
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/41—Particular ingredients further characterized by their size
    • A61K2800/413—Nanosized, i.e. having sizes below 100 nm
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof

Definitions

  • the present invention relates to a cosmetic composition containing a high-content oil component and a sheet mask using the same
  • An aqueous emulsion containing a high content of an oil component is prepared as a nanoparticulate cosmetic composition by using a high pressure emulsification method so that a large amount of an emulsified preparation containing oil or wax, When applied to a sheet mask, it can be uniformly dispersed and filled in a sheet mask even though it contains a large amount of oil components.
  • the present invention relates to a cosmetic composition containing a high-content oil component capable of adjusting the use time by specific color development, and a sheet mask using the same.
  • the mask pack is applied to the skin and allowed to stand for a predetermined time and then removed.
  • the mask pack is classified into various kinds according to its formulation and use method.
  • the sheet mask is a product in which a cosmetic solution containing a moisturizing agent, a whitening agent, a wrinkle remover, and other functional cosmetic ingredients is impregnated in a sheet-like base material, and is used in such a manner that it is attached to the user's skin for a certain period of time and removed.
  • the sheet mask is one of the most common forms of mask packs because it has excellent portability and ease of use, and research and development is continuously carried out to meet various needs of consumers.
  • Such cosmetic lotion or cosmetic liquid is a product in which the content is made mainly of a solubilized formulation, which is mostly water, and has an immediate moisturizing effect.
  • a solubilized formulation which is mostly water
  • it has a problem of being dried quickly after use, pulling on skin, and low in persistence of moisturizing.
  • the sheet mask since the sheet mask has a different attachment time depending on the type of product, and moisture adheres to the skin when it is adhered for too long, it is preferable that the user informs the desorption timing in advance in order to optimally use the sheet mask .
  • a pattern layer coated with a thermosensitive dye is formed so that the hue of the pattern is changed by the temperature, thereby determining the optimal sheet desorption time through the change of the color of the sheet-
  • an additional step of forming a pattern using a thermosensitive dye on the surface of the sheet mask is required, which lowers economical efficiency in the manufacturing process.
  • the dye used for pattern formation absorbs There are problems such as causing skin trouble due to harmful components of human body contained in the dye.
  • Patent Document 1 Korean Patent No. 10-1633639 (name: emulsion of cell membrane-like structure of nanogel type using the self-assembled gel property and cosmetic composition using the same, date of registration: 2016.06.21)
  • Patent Document 2 Korean Registered Patent No. 10-1561180 (Name: functional mask sheet whose color changes according to temperature)
  • the present inventors have found that, by containing a high amount of an oil component, the present invention can provide a sheet mask with a uniform moisture content, And a sheet mask using the same.
  • the present invention has been completed based on this finding.
  • a sheet mask in which a cosmetic composition containing a high content of an oil component is applied to a sheet mask to provide a sheet mask having improved moisturizing durability and a sheet mask capable of informing the timing of removal / The purpose is to provide.
  • the present invention provides a cosmetic composition
  • a cosmetic composition comprising an emulsion containing an oil component as a nanoparticle; And bio-cellulose into which the cosmetic composition is impregnated.
  • the present invention provides nanoparticulate cosmetic compositions from a water-in-oil type emulsion containing a high amount of oil component by using high pressure emulsification technology, It is possible to improve the moisture retention ability of the sheet mask.
  • FIG. 1 is a comparative photograph showing the state of a dried sheet when a sheet mask according to the present invention and a sheet mask impregnated with a solubilized formulation are subjected to color change after skin adhesion and removal.
  • FIG. 2 is a graph showing the results of evaluation of skin moisturization over time.
  • the present invention relates to a cosmetic composition containing a high-content oil component and a sheet mask using the same, and more particularly to a cosmetic composition containing a high-content oil component and an oil-in-water (O / W) emulsion containing a high-
  • the present invention is characterized by providing a cosmetic composition containing a large amount of an oil component by making nanoparticles and impregnating the composition with a sheet mask to provide a sheet mask excellent in moisturizing durability.
  • the present invention is applicable to a bio-cellulosic sheet in which the nanoparticulate cosmetic composition is applied to a bio-cellulose sheet using the high-pressure emulsification method, which is capable of imparting an informing function that the absorbed moisture is reversed to a transparent color after the moisture contained in the bio-cellulose sheet and the skin effective ingredient is absorbed by the skin, And a mask is provided.
  • the cosmetic composition according to the present invention is an emulsion of an oil-in-water (O / W) emulsion containing a large amount of oil component, which is made into a nanoparticle by a high-pressure emulsification method. May be contained in an amount of 10 to 60% by weight, and preferably 20 to 40% by weight.
  • a commonly used sheet mask is a product in which the contents are made mainly of a solubilized formulation in which most of the water is carried. This results in an instant moisturizing effect, but it has the disadvantage that the moisturizing effect is quickly lowered after removing the mask.
  • the present invention provides a cosmetic composition that is nanoparticle-formed by using a high-pressure emulsification method, thereby increasing the content of the oil component by several times to several tens of times, So that it can be filled evenly on the sheet substrate of the mask.
  • the cosmetic composition according to the present invention is an emulsion of an oil-in-water (O / W) emulsion containing a large amount of oil components, which is obtained by nanoparticle formation through a high-pressure emulsification method. So that it can be filled evenly on the sheet substrate.
  • O / W oil-in-water
  • the sheet mask according to the present invention using the above-mentioned cosmetic composition can prevent the moisture content and the skin active ingredient from being impregnated into the sheet by a large amount of the nano-particle oil component contained in the cosmetic composition, And at the same time, it has an advantage of improving moisture retention and allowing smooth removal without skin irritation even during drying.
  • the nano-granulated oil component has an advantage of improving feeling of use of the sheet mask by providing a light and refreshing feeling by improving a somewhat heavy use feeling of a sheet mask containing a large amount of oil component.
  • the cosmetic composition according to the present invention may be impregnated on various kinds of sheet materials.
  • sheet materials For example, nonwoven fabric, woven fabric, paper, foam or sponge may be used.
  • the material may be viscose rayon, modal, (PE), polypropylene (PP), polyethylene terephthalate (PET), polyvinyl alcohol (PVA), polyvinyl chloride (PVC), polyacrylonitrile (PAN) , Polyamide, polyurethane (PU), polylactic acid (PLA), nylon, cotton, hemp, pulp, cellulose and bio-cellulose, but the present invention is not limited thereto.
  • the sheet mask according to the present invention is manufactured by uniformly filling a nano-particle cosmetic composition containing the high-content oil component on a bio-cellulose sheet substrate through a general sheet mask manufacturing process. At this time, When applied to the skin, when the moisture and the skin effective ingredient impregnated in the sheet mask are absorbed into the skin, the skin is reversed from blue to transparent color, thereby enabling the alarm function to be completed.
  • the sheet mask impregnated with the cosmetic composition nanoparticles into the bio-cellulosic sheet material is blue due to light scattering by the moisture contained in the bio-cellulose and the oil component converted into the high-pressure emulsified toner nanoparticles, Thereafter, when the moisture and the skin effective component impregnated in the sheet mask are absorbed into the skin, only the nano-granulated oil component remains in the sheet mask, and the sheet mask is reversed from the blue color to the inherent transparent color of the bio- And an alarm function that the absorption of the skin effective component is completed can be performed.
  • the nano-granulated oil component remaining on the sheet mask prevents the bio-cellulose from being completely dried and strongly adhered to the skin, thereby allowing the sheet mask to be smoothly removed without skin irritation have.
  • the thickness of the bio-cellulose to which the nanoparticulate cosmetic composition is impregnated can be appropriately controlled so that the sheet mask according to the present invention can more effectively confirm discoloration of the sheet mask.
  • the thickness of the bio-cellulose can be controlled by adjusting the dry weight of the sheet per unit area due to the large thickness deviation.
  • the weight of the bio-cellulose is 100 mg / cm 2 and the weight after drying is 20 mg to 300 mg, the blending of the moisture contained in the bio-cellulose and the oil component converted into the nanoparticles by the high-pressure emulsification can be more clearly displayed.
  • the weight of the bio-cellulose after drying is 100 mg to 100 mg and the weight of the bio-cellulose is 50 mg to 150 mg.
  • bio-cellulose can be used without limitation in bio-celluloses produced in various ways through culturing the cells in a culture medium.
  • the production strains of bio-cellulose may be any kind of bio-celluloses known to be usable for the production of bio- The strain may also be used without limitation.
  • strains selected from the group consisting of Acetobacter genus, Rhizobium genus and Agrobacterium genus can be used, but the present invention is not limited thereto.
  • the cosmetic composition of the present invention uses a high-pressure emulsification method as one means for converting an oil-in-water type emulsion containing a large amount of oil components into nanoparticles.
  • the present invention is not limited to this,
  • various emulsions for nanoparticle formation such as a phase-inversion emulsification method, an inversion emulsification method, a D-phase emulsification method, a MPG (Micro Porous Glass) emulsification method, a liquid crystal emulsification method, a nano emulsification method, a multiple emulsification method,
  • a phase-inversion emulsification method an inversion emulsification method
  • a D-phase emulsification method a MPG (Micro Porous Glass) emulsification method
  • a liquid crystal emulsification method a nano emulsification method
  • a multiple emulsification method can be used.
  • the oil component used in the present invention is a mixture of an oil soluble component having a property of melting in oil, solvent, etc., without dissolving in water.
  • the oil component is a fat, wax, a higher alcohol, a higher fatty acid having a melting point of 30 ° C or higher and a solid state at room temperature, Solid phase components including hydrocarbons and the like; Or a liquid phase component comprising an oil, an ester, an ether, a hydrocarbon and the like.
  • examples of the solid phase component include fat such as shea butter, mango seed butter, and cacao butter; Waxes such as myristyl myristate, camellia sinensis leaf extract, jojoba, sunflower seed, carnauba wax, candelilla wax and beeswax; Higher alcohols such as cetyl alcohol, stearyl alcohol and behenyl alcohol; Higher fatty acids such as caprylic / capric triglyceride, lauric acid, myristic acid, palmitic acid and stearic acid; And hydrocarbons such as ceresin; And the like.
  • Waxes such as myristyl myristate, camellia sinensis leaf extract, jojoba, sunflower seed, carnauba wax, candelilla wax and beeswax
  • Higher alcohols such as cetyl alcohol, stearyl alcohol and behenyl alcohol
  • Higher fatty acids such as caprylic / capric triglyceride, lauric acid,
  • liquid phase component examples include natural oils such as meadowfoam seed oil, sunflower seed oil, macadamia seed oil, green tea seed oil, ginger oil, ginseng oil, coconut oil, olive oil and camellia oil; Esters such as phytosteryl / octyldodecylauroyl glutamate, isostearyl isostearate, methyl haptylisostearate, dicaprylyl carbonate and isopropyl palmitate; Ethers such as dicaprylyl ether; Silicone oils such as dimethicone, cyclopentasiloxane, cyclohexasiloxane, phenyltrimethicone, trisiloxane and methyltrimethicone; And hydrocarbons such as squalane.
  • natural oils such as meadowfoam seed oil, sunflower seed oil, macadamia seed oil, green tea seed oil, ginger oil, ginseng oil, coconut oil, olive oil and camellia oil
  • the cosmetic composition of the present invention can be used as a surfactant to stabilize the particles of the oil component nanoparticles formed by the high-pressure emulsification method.
  • the cosmetic composition of the present invention may contain a polyol, ethanol, Functional ingredients, pigments, fragrances, thickeners, preservatives, and the like.
  • the present invention provides nanoparticulate cosmetic compositions from a water-in-oil type emulsion containing a high content of oil components by using a high-pressure emulsification technique, It is possible to uniformly fill the sheet mask through the process, thereby improving the moisture holding performance of the sheet mask.
  • the moisture contained in the bio-cellulose and light scattered by the nanoparticles made of the high- And after the fluid is absorbed into the skin, the blue color is reversed to a transparent color, thereby giving a notification function that the absorption is completed.
  • Example 1 In-water type emulsions of Example 1 and Comparative Example 1 were prepared in accordance with the following production methods with the compositions shown in the following Table 1, respectively (unit: wt%).
  • Comparative Example 1 uses a solubilized formulation that does not contain an oil component and a surfactant.
  • Example 1 Comparative Example 1 One Purified water To 100 To 100 2 Polyglyceryl-3 methyl glucoside distearate 3.20 0 3 Methylglucose sesquistearate 0.40 0 4 Cetearyl glucoside 0.20 0 5 A mixture of oil-soluble components such as a hydrocarbon-based oil, an ester-based oil, a natural oil or a silicone- 25.00 0 6 antiseptic 0.20 0.20 7 Ethylhexyl glycerin 0.05 0.05 8 Polyol, ethanol 13.10 23.00 9 Spices 0.17 0.17
  • An underwater type emulsion is prepared using raw materials 1 to 9 in Table 1 above.
  • Example 2 the emulsion is deaerated and the final cosmetic composition is prepared by applying a pressure of 3 Cycle or more at 1,000 bar using M-110EH-30 Microfluidizer® Processor (Microfluidics).
  • Example 1 The composition of Example 1 and Comparative Example 1 was immersed in a circular biocellulose sheet having a diameter of 4 cm. As shown in FIG. 1, Example 1 exhibited a blue color due to scattering of light by nanoparticle oil components and moisture, Comparative Example 1 exhibited a transparent color, and after application of the skin, In Example 1, the blue color is inverted to a transparent color, whereas in Comparative Example 1, no color change is observed.
  • the sheet mask according to the present invention can adjust the use time by the expression of specific color without any additional constitution such as forming a certain pattern by using a dye containing human harmful component, and can smoothly remove .
  • Example 1 Comparative Example 1 Weight after drying (g) 36.03 15.20 Residual amount (%) 72.06 30.40
  • Example 1 As can be seen from the above Table 2, it can be seen that the moisture content of Example 1 is more than two times that of Comparative Example 1, which means that the nano-granulated oil component contained in Example 1 is oil And it is expected that the sheet mask according to the present invention is applied to the skin to reduce the dryness of the skin and improve the moisturizing effect.
  • Example 1 The amount of skin moisturizing over time in Example 1 and Comparative Example 1 was measured to evaluate the moisturizing duration.
  • test site of the forearm was measured, and 300 ⁇ l / cm 2 of the sample of Example 1 and Comparative Example 1 were applied to the test site, and the sample was absorbed for 30 minutes. After 3 hours of application, After the lapse of time, the test site of the forearm was measured three times, and the average value was evaluated.
  • the evaluation result is shown in Fig. 2.
  • the measured value is high when the moisture content is high, and the measured value is low when it is low.
  • the moisturizing amount was continuously decreased with time after the moisturizing amount greatly increased immediately after the application, and the moisturizing amount after 3 hours of application was reduced to about 1/2 of that after the application, After 6 hours of application, the amount of moisture decreased to about 1/4 of the level immediately after application.
  • Example 1 the moisturizing amount immediately after application was not higher than that in Comparative Example 1, but the moisturizing amount was steadily increased immediately after application, and the moisturizing amount after 3 hours of application was increased to more than twice that of Comparative Example 1, The moisturizing amount was slightly higher than that of Comparative Example 1 after 6 hours of application, and the amount of moisture was about 3 times higher than that of Comparative Example 1, 1, it was evaluated that the persistence of moisturizing was remarkably high.
  • the sheet mask according to the present invention can suppress the evaporation of moisture and skin active ingredients impregnated into the sheet by a large amount of nano-particle oil components contained in the cosmetic composition, thereby providing a balance of water content to the skin, .
  • the present invention can uniformly fill the sheet mask through the conventional general sheet mask manufacturing process by manufacturing the nanoparticulate cosmetic composition from the underwater type emulsion containing a high amount of oil component by using the high pressure emulsification technique,
  • the nanoparticulate cosmetic composition from the underwater type emulsion containing a high amount of oil component by using the high pressure emulsification technique.
  • it is blue due to light scattering by nanoparticles made of moisture and high-pressure emulsions contained in bio-cellulose, Thereafter, the blue color is reversed to a transparent color, thereby giving a notification function that the absorption is completed.

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
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  • Veterinary Medicine (AREA)
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  • Oil, Petroleum & Natural Gas (AREA)
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Abstract

La présente invention concerne une composition cosmétique contenant une teneur élevée en un composant huileux et un masque en tissu l'utilisant. Plus particulièrement, la présente invention concerne une composition cosmétique contenant une teneur élevée en un composant huileux et un masque en tissu l'utilisant, une émulsion de type huile-dans-l'eau qui contient une teneur élevée en un composant huileux étant préparée sous la forme d'une composition cosmétique nanoparticulaire à l'aide d'un procédé d'émulsification haute pression, il est possible qu'elle contienne une grande quantité d'une formulation émulsifiée comprenant de l'huile ou de la cire tout en ayant une fluidité comme une formulation solubilisée, de telle sorte que, lorsqu'elle est appliquée à un masque en tissu, l'émulsion de type huile-dans-l'eau est uniformément dispersée et imprégnée dans le masque en tissu même si l'émulsion contient une grande quantité de composant huileux ; et il est possible non seulement de produire un masque en tissu ayant une sensation rafraîchissante et une excellente rétention de l'humidité mais aussi d'être capable d'ajuster le temps d'utilisation au moyen d'un développement de couleur spécifique lors d'une application à la bio-cellulose.
PCT/KR2018/009884 2017-08-28 2018-08-28 Composition cosmétique contenant une teneur élevée en composant huileux et masque en tissu l'utilisant Ceased WO2019045397A2 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201880070574.2A CN111343960A (zh) 2017-08-28 2018-08-28 含有高含量油成分的化妆品组合物及使用其的片状面膜

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KR10-2017-0108460 2017-08-28
KR1020170108460A KR20190023153A (ko) 2017-08-28 2017-08-28 고함량 오일성분이 포함된 화장료 조성물 및 이를 이용한 시트 마스크

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