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WO2018070247A1 - Polariseur, lame polarisante et dispositif de formation d'image - Google Patents

Polariseur, lame polarisante et dispositif de formation d'image Download PDF

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Publication number
WO2018070247A1
WO2018070247A1 PCT/JP2017/034967 JP2017034967W WO2018070247A1 WO 2018070247 A1 WO2018070247 A1 WO 2018070247A1 JP 2017034967 W JP2017034967 W JP 2017034967W WO 2018070247 A1 WO2018070247 A1 WO 2018070247A1
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WO
WIPO (PCT)
Prior art keywords
polarizer
cutting
polarizing plate
film
face
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/JP2017/034967
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English (en)
Japanese (ja)
Inventor
正寛 市原
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sumitomo Chemical Co Ltd
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Sumitomo Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sumitomo Chemical Co Ltd filed Critical Sumitomo Chemical Co Ltd
Priority to CN201780063310.XA priority Critical patent/CN109844582B/zh
Priority to KR1020197013185A priority patent/KR102410190B1/ko
Publication of WO2018070247A1 publication Critical patent/WO2018070247A1/fr
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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    • G—PHYSICS
    • G02—OPTICS
    • G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B5/00—Optical elements other than lenses
    • G02B5/30—Polarising elements
    • G02B5/3025—Polarisers, i.e. arrangements capable of producing a definite output polarisation state from an unpolarised input state
    • G02B5/3033—Polarisers, i.e. arrangements capable of producing a definite output polarisation state from an unpolarised input state in the form of a thin sheet or foil, e.g. Polaroid
    • G—PHYSICS
    • G02—OPTICS
    • G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
    • G02B1/04—Optical elements characterised by the material of which they are made; Optical coatings for optical elements made of organic materials, e.g. plastics
    • G—PHYSICS
    • G02—OPTICS
    • G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
    • G02B1/10—Optical coatings produced by application to, or surface treatment of, optical elements
    • G02B1/14—Protective coatings, e.g. hard coatings

Definitions

  • the present invention relates to a polarizer, a polarizing plate, and an image display device.
  • the polarizer for the image display device is also formed into a thin film. Since a film-like polarizer is brittle and easily torn, in order to protect the polarizer, protective films are bonded to both sides of the polarizer in the production of a polarizing plate. In the production of a polarizing plate, in order to increase the dimensional accuracy of the polarizing plate, an end portion of a laminate composed of a protective film, a polarizer and the like is polished (for example, see Patent Document 1).
  • the frame of the image display device is required to be narrow in order to improve the design.
  • high dimensional accuracy is also required at the end of the polarizing plate.
  • a load is more likely to be applied to the end face of the polarizer during cutting, and the end face of the polarizer tends to be rougher than a polarizer in which a protective film overlaps on both sides.
  • the roughness of this end face causes a crack in the polarizer accompanying a temperature change.
  • it has been found that cracks are more likely to occur on the end face of the polarizer located on the surface side where there is no protective film than on the end face of the polarizer located on the surface side where the protective film overlaps.
  • the present invention has been made in view of the above circumstances, and has a high dimensional accuracy and is unlikely to generate cracks due to temperature changes, a polarizing plate including the polarizing plate, and an image display device including the polarizing plate.
  • the purpose is to provide.
  • the polarizer according to one aspect of the present invention is a film-like polarizer, and the average height Rc of the roughness curve element at the end face of the polarizer is 0.05 to 1.7 ⁇ m.
  • the average height Rc may be 0.05 to 0.28 ⁇ m.
  • a polarizing plate includes the above polarizer and a first optical film that overlaps one surface of the polarizer.
  • the first side of the sides surrounding one end surface of the polarizer is adjacent to the first optical film, and the second side of the sides surrounding the end surface is located on the opposite side of the first side.
  • the root mean square roughness Rq in the end surface along the second side may be 0.03 to 0.15 ⁇ m.
  • the first optical film may be a protective film.
  • the polarizing plate according to one aspect of the present invention may further include an adhesive layer that overlaps the other surface of the polarizer and a second optical film that overlaps the adhesive layer.
  • the polarizing plate according to one aspect of the present invention may further include a pressure-sensitive adhesive layer that overlaps the first optical film and a second optical film that overlaps the pressure-sensitive adhesive layer.
  • the second optical film may be a reflective polarizer.
  • An image display device includes the above polarizing plate.
  • a polarizer that has high dimensional accuracy and is less likely to crack due to temperature change
  • a polarizing plate that includes the polarizer
  • an image display device that includes the polarizing plate
  • FIG. 1 is a schematic perspective view of a polarizing plate according to an embodiment of the present invention
  • FIG. 1 is an end face of the polarizing plate shown in (a) in FIG. It is a typical enlarged view of a part (part b).
  • It is a side view of the cutting tool used for manufacture of the polarizing plate concerning one embodiment of the present invention.
  • It is a front view of the cutting tool shown in FIG.
  • It is a schematic diagram which shows the position of the cutting tool shown in FIG. 2, and the laminated body comprised from a some polarizing plate.
  • FIG. 3 shows the position of the cutting tool shown in FIG.
  • X, Y, and Z shown in each figure mean three coordinate axes orthogonal to each other.
  • the direction indicated by each coordinate axis is common to all drawings.
  • the illustrated dimensions and ratios of dimensions do not necessarily match the actual ones.
  • a polarizing plate 1 includes a film-like polarizer 2, a first optical film (3) that overlaps one surface of the polarizer 2, and a polarization.
  • the pressure sensitive adhesive layer 5 which overlaps the other surface of the child 2 and the second optical film (4) which overlaps the pressure sensitive adhesive layer 5 are provided.
  • the first optical film is, for example, the protective film 3.
  • the second optical film is, for example, a reflective polarizer 4.
  • the polarizer 2 included in the polarizing plate 1 and all of the optical film and the layer may be transparent.
  • the optical film (first optical film) is in direct contact with the polarizer 2 via the adhesive layer without the pressure-sensitive adhesive layer only on one side of the polarizer 2. is doing.
  • the polarizer 2, the first optical film (3), the pressure-sensitive adhesive layer 5 and the second optical film (4) are all rectangular having substantially the same dimensions.
  • the entire polarizing plate 1 is also a rectangular film.
  • each shape of the polarizer 2 and the polarizing plate 1 is not limited because it depends on the shape of the surface of the image display element to which the polarizing plate 1 is attached.
  • Each shape of the polarizer 2 and the polarizing plate 1 may be, for example, a polygon, a circle, or an ellipse. Part or all of the outlines of the polarizer 2 and the polarizing plate 1 may be straight lines or curved lines.
  • the image display device may be a liquid crystal display device or an organic EL display device, for example.
  • the liquid crystal display device may include, for example, a liquid crystal cell and a polarizing plate 1 attached to one surface or both surfaces of the liquid crystal cell.
  • the organic EL display device may include, for example, an organic EL element and a polarizing plate 1 attached to the surface of the organic EL element.
  • two polarizing plates are arranged in the liquid crystal cell.
  • the polarizer included in the polarizing plate disposed on the back side of the liquid crystal cell is more easily exposed to heat than the polarizer included in the polarizing plate disposed on the viewing side of the liquid crystal cell. Therefore, when the polarizing plate 1 including the polarizer 2 according to the present embodiment is disposed on the back side of the liquid crystal cell, cracks in the polarizer 2 due to temperature changes are suppressed. The reason will be described later.
  • the average height Rc of the roughness curve element at the end face 2a of the polarizer 2 is 0.05 to 1.7 ⁇ m.
  • the average height Rc may be 0.05 to 0.28 ⁇ m, 0.07 to 1.7 ⁇ m, 0.07 to 1.604 ⁇ m, 0.07 to 1.0 ⁇ m, or 0.07 to 0.28 ⁇ m. Good.
  • the average height Rc of the roughness curve element in the end surface 2a may be defined by the following formula 1, for example.
  • Rc is the average of the height Zt of the roughness curve element (contour curve element) at the reference length l.
  • i is a natural number of 1 or more and m or less, and m is a natural number of 2 or more.
  • Zti is the height of the i-th contour curve element at the reference length l.
  • the contour curve element is a set of adjacent peaks and valleys, and the height Zt of the contour curve element is the difference between the adjacent set of peaks (maximum value) and valleys (minimum value).
  • Rc may be measured on the end surface 2a of the polarizer 2 by, for example, a laser microscope.
  • the end face 2a is deformed non-uniformly and rapidly due to rapid expansion or contraction associated with heat shock.
  • the expansion or contraction of the polarizer 2 is anisotropic. Due to these factors, as the temperature of the polarizer 2 changes, cracks are likely to occur in the polarizer 2 starting from the end face 2a. For example, a crack is generated starting from a valley of a contour curve element (that is, a deep depression in the end face 2a).
  • the average height Rc of the roughness curve element at the end face 2a is 0.05 to 1.7 ⁇ m, the above-mentioned crack factors are reduced, and the polarizer accompanying the temperature change The occurrence of cracks 2 is suppressed.
  • the length of cracks formed on the end surface 2a having an average height Rc of 0.05 to 1.7 ⁇ m tends to be shorter than the length of cracks formed on the end surface 2a having an average height Rc of greater than 1.7 ⁇ m. There is.
  • the average height Rc of the roughness curve elements on the end surface 2a of the polarizer 2 is substantially uniform over the entire end surface 2a.
  • the average height Rc of the roughness curve element on the end surface 2a of the polarizer 2 is the interface (adhesive surface) between the polarizer 2 and the protective film.
  • the polarizer 2 is a stretched film, it is easy to tear, and the end face of the polarizer located on the surface side where there is no protective film is handled with a polishing blade and is easily roughened. Therefore, the average height Rc of the roughness curve element at the end face 2a of the polarizer 2 tends to increase as the distance from the interface between the polarizer 2 and the protective film increases.
  • the maximum value of the average height Rc of the roughness curve element measured at the end face 2a of the polarizer 2 is, for example, 0.1. It may be from 05 to 0.28 ⁇ m.
  • the length of the crack formed on the end face 2a having the maximum average height Rc of 0.05 to 0.28 ⁇ m is: There is a tendency that the maximum value of the average height Rc is shorter than the length of the crack formed in the end face 2a larger than 0.28 ⁇ m.
  • the average height Rc of the roughness curve element at the end face 2a of the polarizer 2 is not uniform, the number of cracks formed on the end face 2a having the maximum average height Rc of 0.05 to 0.28 ⁇ m is There is a tendency that the maximum value of the average height Rc is smaller than the number of cracks formed in the end face 2a larger than 0.28 ⁇ m.
  • the end face of the polarizer or the polarizing plate When the end face of the polarizer or the polarizing plate is not polished, the end face of the polarizer is not roughened by polishing. Therefore, the average height Rc of the end face of the polarizer is substantially zero, and cracks are hardly generated on the end face of the polarizer. In other words, the smaller the average height Rc of the end surface 2a, the less likely the cracks are generated on the end surface of the polarizer.
  • the accuracy of the dimension of the polarizer whose average height Rc of the end face 2a is less than 0.05 ⁇ m is inferior to the precision of the dimension of the polarizer whose average height Rc of the end face 2a is 0.05 ⁇ m or more.
  • the dimensional accuracy of a polarizer having a polished end surface is higher than the dimensional accuracy of a polarizer having an unpolished end surface.
  • the rectangular polarizer 2 has four end faces 2a.
  • the average height Rc of the roughness curve elements on a part of the end faces 2a may be 0.05 to 1.7 ⁇ m.
  • the average height Rc of the roughness curve elements on all the end faces 2a of the polarizer 2 may be 0.05 to 1.7 ⁇ m. The more end faces 2a having Rc of 0.05 to 1.7 ⁇ m, the more easily the occurrence of cracks in the polarizer 2 is suppressed.
  • one end face 2a of the polarizer 2 is surrounded by a first side S1, a second side S2, a third side S3, and a fourth side S4.
  • the peripheral edge of the end face 2a is composed of the first side S1, the second side S2, the third side S3, and the fourth side S4.
  • the first side S1 is adjacent to the protective film 3 (first optical film).
  • the second side S2 is located on the opposite side of the first side S1.
  • the second side S ⁇ b> 2 is adjacent to the pressure-sensitive adhesive layer 5.
  • the second side S ⁇ b> 2 is a side that is not adjacent to the protective film 3.
  • the root mean square roughness Rq in a portion (2as) along the second side S2 of the end face 2a may be 0.03 to 0.50 ⁇ m.
  • side S2 among the end surfaces 2a may be described as "the side part 2as" of the end surface 2a.
  • the root mean square roughness Rq may be 0.03 to 0.466 ⁇ m, 0.03 to 0.30 ⁇ m, 0.03 to 0.15 ⁇ m, or 0.031 to 0.081 ⁇ m.
  • the root mean square roughness Rq at the side 2as of the end face 2a may be defined by the following formula 2, for example.
  • l (alphabet L) is a reference length in the side portion 2as of the end face 2a.
  • Z (x) is the height of the roughness curve at an arbitrary position x on the reference length l.
  • Rq may be measured at the side portion 2as of the end surface 2a by, for example, a laser microscope. In other words, Rq may be measured along the second side S2 of the end face 2a of the polarizer 2.
  • the width of the side portion 2as in the thickness direction (Z-axis direction) of the polarizer 2 may be narrow as long as Rq can be measured.
  • the width of the side portion 2as in the thickness direction (Z-axis direction) of the polarizer 2 may be less than or equal to half the thickness of the polarizer 2.
  • the width of the side portion 2as in the thickness direction (Z-axis direction) of the polarizer 2 may be substantially the same as the spot diameter of the laser used for measuring Rq.
  • the width of the side portion 2as in the thickness direction (Z-axis direction) of the polarizer 2 may be a width corresponding to the Rq measurement limit using a laser microscope.
  • the rougher the side portion 2as the more easily the side portion 2as is deformed unevenly due to expansion or contraction associated with a temperature change.
  • the side portion 2as is likely to be unevenly and rapidly deformed due to rapid expansion or contraction accompanying heat shock.
  • the expansion or contraction of the polarizer 2 is anisotropic. Due to these factors, as the temperature of the polarizer 2 changes, cracks are likely to occur in the polarizer 2 starting from the side 2as. In other words, as the temperature of the polarizer 2 changes, cracks are likely to occur in the portion along the second side S2 that is not adjacent to the protective film in the end face 2a.
  • cracks are likely to occur starting from a valley of the roughness curve (that is, a deep depression in the side portion 2as).
  • Rq in the side part 2as located on the second side S2 side without the protective film 3 is reduced, The various factors of cracks as described above are easily reduced, and the occurrence of cracks in the polarizer 2 due to temperature changes is easily suppressed. That is, when Rq in side part 2as located in the 2nd side S2 side without protective film 3 is small, generation
  • the root mean square roughness Rq is 0.03 to 0.15 ⁇ m
  • the occurrence of cracks in the side portion 2as located on the second side S2 side is easily suppressed.
  • the end face of the polarizer or the polarizing plate is not polished, the end face of the polarizer is not roughened by polishing. Therefore, the root mean square roughness Rq is substantially zero, and cracks are hardly generated on the end face of the polarizer.
  • the end face of the polarizer or the polarizing plate is not polished, it is difficult to adjust the size of the polarizer or the polarizing plate to a desired value (for example, a tolerance range of the product standard) with high accuracy.
  • the accuracy of the dimension of the polarizer whose root mean square roughness Rq is less than 0.03 ⁇ m tends to be lower than the precision of the dimension of a polarizer whose root mean square roughness Rq is 0.03 ⁇ m or more.
  • the rectangular polarizer 2 has four end faces 2a.
  • the root mean square roughness Rq at the side 2as of some of the end faces 2a may be 0.03 to 0.15 ⁇ m.
  • the root mean square roughness Rq at the side portions 2as of all the end faces 2a of the polarizer 2 may be 0.03 to 0.15 ⁇ m.
  • the end face 2a having the side portion 2as having Rq of 0.03 to 0.15 ⁇ m increases, the occurrence of cracks on the second side S2 side of the polarizer 2 is more easily suppressed.
  • the resin constituting the polarizer 2 may be, for example, a polyvinyl alcohol resin, a polyvinyl acetate resin, an ethylene / vinyl acetate copolymer resin (EVA) resin, a polyamide resin, or a polyester resin.
  • the polarizer 2 may be stretched in a uniaxial direction or a biaxial direction.
  • the polarizer 2 may be dyed with iodine or a dichroic dye.
  • the dyed polarizer 2 may be treated with boric acid.
  • the polarizer 2 may be one in which iodine is adsorbed and oriented on a polyvinyl alcohol film.
  • the thickness of the polarizer 2 may be, for example, 2 to 30 ⁇ m, 2 to 15 ⁇ m, or 2 to 10 ⁇ m.
  • the thinner the polarizer the easier it is for cracks to occur in the polarizer.
  • cracks in the polarizer 2 can be suitably suppressed even when the thickness of the polarizer 2 is 10 ⁇ m or less.
  • the protective film 3 includes, for example, a cellulose resin (such as triacetyl cellulose), a polyolefin resin (such as a polypropylene resin), a cyclic olefin resin (such as a norbornene resin), an acrylic resin (such as a polymethyl methacrylate resin), Alternatively, it may be a polyester resin (polyethylene terephthalate resin or the like).
  • a cellulose resin such as triacetyl cellulose
  • a polyolefin resin such as a polypropylene resin
  • a cyclic olefin resin such as a norbornene resin
  • an acrylic resin such as a polymethyl methacrylate resin
  • it may be a polyester resin (polyethylene terephthalate resin or the like).
  • the thickness of the protective film 3 may be 5 to 90 ⁇ m, 5 to 80 ⁇ m, or 5 to 50 ⁇ m.
  • the protective film 3 may be bonded to the surface of the polarizer 2 through an adhesive layer. You may form the protective film directly on the surface of the polarizer 2 by apply
  • the resin constituting the adhesive layer may be, for example, an epoxy resin.
  • the epoxy resin may be, for example, a hydrogenated epoxy resin, an alicyclic epoxy resin, or an aliphatic epoxy resin.
  • a polymerization initiator photo cationic polymerization initiator, thermal cationic polymerization initiator, photo radical polymerization initiator, thermal radical polymerization initiator, etc.
  • other additives such as sensitizer, etc.
  • the resin constituting the adhesive layer may be, for example, an acrylic resin such as acrylamide, acrylate, urethane acrylate, and epoxy acrylate.
  • a water-based adhesive containing a polyvinyl alcohol-based resin may be used for the adhesive layer.
  • the resin constituting the pressure-sensitive adhesive layer 5 may be, for example, an acrylic resin, a silicone resin, polyester, polyurethane, or polyether. You may form the pressure-sensitive adhesive layer 5 by apply
  • the thickness of the pressure-sensitive adhesive layer 5 may be, for example, 2 to 500 ⁇ m, 2 to 200 ⁇ m, or 2 to 50 ⁇ m.
  • the pressure-sensitive adhesive layer 5 formed on the separator may be transferred to the surface of the polarizer 2.
  • the separator is attached to the polarizer 2 or other optical film for the purpose of protecting the pressure-sensitive adhesive layer or preventing the adhesion of foreign substances.
  • the separator is a peelable film. For example, when sticking the polarizing plate 1 to an image display element, a separator is peeled off and a pressure-sensitive adhesive layer is exposed.
  • the separator may be temporarily used in the manufacturing process of the polarizing plate 1 and then peeled off from the polarizing plate 1.
  • the resin constituting the separator may be, for example, a polyethylene resin, a polypropylene resin, or a polyester tree (such as polyethylene terephthalate).
  • the thickness of the separator may be, for example, 2 to 500 ⁇ m, 2 to 200 ⁇ m, or 2 to 100 ⁇ m.
  • the reflective polarizer 4 (second optical film) may be a multilayer film made of polycarbonate or the like, for example.
  • the thickness of the reflective polarizer 4 may be, for example, 15 to 200 ⁇ m.
  • the total thickness of the polarizing plate 1 may be, for example, 10 to 500 ⁇ m, 10 to 300 ⁇ m, or 10 to 200 ⁇ m.
  • the average height Rc of the roughness curve element on the end surface 2a of the polarizer 2 provided in the polarizing plate 1 is controlled within the range of 0.05 to 1.7 ⁇ m by cutting the end portion of the polarizing plate 1 described below. can do.
  • the root mean square roughness Rq at the side portion 2as of the end face 2a of the polarizer 2 provided in the polarizing plate 1 can be controlled within the range of 0.03 to 0.15 ⁇ m by the cutting process described below. .
  • the cutting process will be described in detail with reference to FIGS.
  • a plurality of polarizing plates 1A having the same laminated structure as the polarizing plate 1 according to the present embodiment are produced.
  • Each polarizing plate 1A is the same as the polarizing plate 1 according to the present embodiment except that the end face is not cut. Since the end surface 2a of the polarizing plate 1A that has not been cut is not rough, the Rc of the end surface 2a of the polarizer 2 included in each polarizing plate 1A is less than 0.05. Moreover, Rq in side part 2as of the end surface 2a of each polarizing plate 1A which is not cut is less than 0.03.
  • a stacked body 100 is formed by stacking a plurality of polarizing plates 1 ⁇ / b> A.
  • each polarizing plate 1 ⁇ / b> A The dimensions of each polarizing plate 1 ⁇ / b> A are exactly the same, and the entire surface of each polarizing plate 1 ⁇ / b> A completely overlaps each other in the laminate 100.
  • An end surface 100 a of the laminate 100 illustrated in FIG. 4 is a surface including the end surface of the polarizer 2. That is, the end surfaces of the polarizers 2 included in each polarizing plate 1 ⁇ / b> A are aligned within the end surface 100 a of the laminate 100.
  • the end surface 100 a of the laminate 100 faces the cutting surface S of the cutting tool 10 and contacts the cutting blade on the cutting surface S.
  • the laminate 100 is composed of four polarizing plates 1A, but the number of polarizing plates 1A constituting the laminate 100 is not particularly limited.
  • the cutting tool 10 is fixed to a support 10a (arbor).
  • the cutting tool 10 rotates with respect to the rotation axis A.
  • the rotational speed (rotational speed) of the cutting tool 10 is freely adjusted.
  • the cutting tool 10 has a disk shape.
  • the rotation axis A of the cutting tool 10 is orthogonal to the end surface 100a of the laminated body 100 to be cut (that is, the end surface of each polarizer 2).
  • the number of rotations of the cutting tool 10 per unit time affects the average height Rc of the roughness curve element on the end surface 2 a of the polarizer 2.
  • the number of rotations of the cutting tool 10 per unit time also affects the root mean square roughness Rq at the side portion 2as of the end face 2a of the polarizer 2.
  • the number of rotations of the cutting tool 10 per unit time may be, for example, 3.5 to 14 times, or 5.6 to 10.2.
  • the average height Rc of the roughness curve element at the end face 2a of the polarizer 2 is easily controlled to 0.05 to 1.7 ⁇ m.
  • the root mean square roughness Rq at the side 2as of the end face 2a of the polarizer 2 is easily controlled to 0.03 to 0.15.
  • the cutting tool 10 has a cutting surface S perpendicular to the rotation axis A. Therefore, the cutting surface S is parallel to the end surface 100a of the laminated body 100 to be cut. In other words, the cutting surface S is parallel to the end surface 2a of the polarizer 2 to be cut. As shown in FIG. 2 and FIG. 3, on the cutting surface S, a first cutting portion group consisting of cutting portions 11a, 11b and 11c and a second cutting consisting of cutting portions 11d, 11e and 11f. A group is provided on the cutting surface S. Each cutting part has the cutting blade B for scraping off an end surface. The cutting parts are arranged around the rotation axis A at substantially equal intervals.
  • Each cutting part protrudes from the cutting surface S toward the end surface 100a of the laminated body 100 to be cut.
  • the cutting blade B is disposed on the protruding top surface of each cutting portion.
  • the cutting blade B which each cutting part has is arrange
  • FIG. In other words, the cutting blade B included in each cutting unit is arranged so as to extend in parallel to the end surface 2 a of each polarizer 2 in the laminate 100.
  • each cutting portion provided on the cutting surface S of the cutting tool 10 is omitted, but all of the cutting tools 10 shown in FIGS. 2 to 5 are the same. .
  • the cutting portions 11a, 11b and 11c abut against the end surface 100a of the laminate 100 in this order, and the end surfaces 100a (each The end face 2a) of the polarizer 2 is cut.
  • the distance from the cutting surface S to the cutting blade B of the cutting part 11a is smaller than the distance from the cutting surface S to the cutting blade B of the cutting part 11b.
  • the distance from the cutting surface S to the cutting blade B of the cutting part 11b is smaller than the distance from the cutting surface S to the cutting blade B of the cutting part 11c.
  • the protruding height of the cutting blade B of the cutting portion 11b is higher than the protruding height of the cutting blade B of the cutting portion 11a
  • the protruding height of the cutting blade B of the cutting portion 11c is the protruding height of the cutting blade B of the cutting portion 11b. Higher than height.
  • the cutting portions 11d, 11e, and 11f abut against the end surface 100a of the laminated body 100 in this order, and cut the end surface 100a (end surface 2a of each polarizer 2).
  • the distance from the cutting surface S to the cutting blade B of the cutting part 11d is smaller than the distance from the cutting surface S to the cutting blade B of the cutting part 11e.
  • the distance from the cutting surface S to the cutting blade B of the cutting part 11e is smaller than the distance from the cutting surface S to the cutting blade B of the cutting part 11f.
  • the protruding height of the cutting blade B of the cutting portion 11e is higher than the protruding height of the cutting blade B of the cutting portion 11d
  • the protruding height of the cutting blade B of the cutting portion 11f is the protruding height of the cutting blade B of the cutting portion 11e. Higher than height.
  • the distance from the rotation axis A to the cutting blade B of the cutting part 11b is shorter than the distance from the rotation axis A to the cutting blade B of the cutting part 11a.
  • the distance from the rotation axis A to the cutting blade B of the cutting part 11c is shorter than the distance from the rotation axis A to the cutting blade B of the cutting part 11b.
  • the distance from the rotation axis A to the cutting blade B of the cutting part 11e is shorter than the distance from the rotation axis A to the cutting blade B of the cutting part 11d.
  • the distance from the rotation axis A to the cutting blade B of the cutting part 11f is shorter than the distance from the cutting part 11e to the cutting blade B.
  • the cutting portions 11a, 11b, 11d, and 11e are for rough cutting, and these cutting blades B are made of, for example, polycrystalline diamond.
  • the cutting parts 11c and 11f located at the tail end in each cutting part group are for finishing, and these cutting blades B are made of, for example, single crystal diamond.
  • the material of each cutting blade B is not limited.
  • the circle drawn by each cutting portion by the rotation of the cutting tool 10 intersects the surface of each polarizer 2 in the laminate 100 (the surface of each polarizer 2 facing the Z-axis direction) substantially perpendicularly.
  • the circle drawn by each cutting blade B of the cutting portions 11 c and 11 f having the shortest distance from the rotation axis A intersects the surface of each polarizer 2 in the laminate 100 substantially perpendicularly.
  • the approach angle ⁇ of each cutting blade B with respect to the surface of each polarizer 2 is preferably closer to 90 °.
  • the approach angle ⁇ of each cutting blade B with respect to the surface of the laminate 100 facing the Z-axis direction is preferably closer to 90 °.
  • the approach angle ⁇ of each cutting blade B of the cutting portions 11c and 11f having the shortest distance from the rotation axis A is preferably closer to 90 °.
  • the diameter of the cutting surface S of the cutting tool 10 is preferably larger than the thickness of the laminate 100.
  • the diameter of the cutting surface S of the cutting tool 10 is large enough to cut the end surfaces of all the stacked polarizing plates 1A uniformly. As shown in FIGS.
  • the height at which the laminate 100 is disposed is preferably substantially the same as the height of the rotation axis A of the cutting tool 10.
  • the position of the laminate 100 in the direction parallel to the end face 2a of each polarizer 2 is preferably substantially the same as the position of the rotation axis A of the cutting tool 10 in the same direction.
  • the position of the laminated body 100 in the direction parallel to the end surface 100a of the laminated body 100 is preferably substantially the same as the position of the rotation axis A of the cutting tool 10 in the same direction.
  • the thickness of the laminate 100 may be adjusted.
  • the number of polarizing plates 1A constituting the laminate 100 may be adjusted.
  • the approach angle ⁇ of the cutting blade B approaches 90 °.
  • the thickness of the laminate 100 may be adjusted for the purpose of adjusting the relative positional relationship between the laminate 100 and the rotation axis A of the cutting tool 10.
  • the number of polarizing plates 1A constituting the laminate 100 may be adjusted.
  • the entrance angle ⁇ of each cutting blade B is adjusted to be substantially vertical, the position of the laminated body 100 and the position of the rotation axis A of the cutting tool 10 are matched, and the rotation speed of the cutting tool 10 is appropriately set.
  • the average height Rc of the roughness curve element at the end face 2a of the polarizer 2 included in the polarizing plate 1 can be easily controlled within the range of 0.05 to 1.7 ⁇ m.
  • the approach angle ⁇ of each cutting blade B is adjusted to be substantially vertical, the position of the laminate 100 and the position of the rotation axis A of the cutting tool 10 are matched, and the number of rotations of the cutting tool 10 is appropriately adjusted.
  • the root mean square roughness Rq at the side 2as of the polarizer 2 included in the polarizing plate 1 can be easily controlled within the range of 0.03 to 0.15 ⁇ m.
  • the number of rotations of the cutting tool 10 necessary for controlling each of Rc and Rq within the above ranges can be determined by preliminary experiments.
  • the cutting tool 10 in a direction parallel to the end surface 100a of the laminated body 100 (end surface 2a of each polarizer 2). May move freely.
  • the position of the cutting tool 10 may be freely adjusted in the Z-axis direction (vertical direction). In this case, the position of the stacked body 100 in the Z-axis direction may be fixed.
  • the laminate 100 may freely move.
  • the position of the stacked body 100 may be freely adjusted in the Z-axis direction (for example, the vertical direction).
  • the position of the cutting tool 10 in the Z-axis direction may be fixed.
  • each polarizing plate 1 ⁇ / b> A constituting the laminate 100 the polarizer 2 is preferably positioned above the protective film 3.
  • the elastic modulus of the protective film 3 is preferably higher than the elastic modulus of the polarizer 2.
  • each cutting blade B of the cutting tool 10 moves from the upper side to the lower side of the stacked body 100. Therefore, when the polarizer 2 is positioned above the protective film 3, each cutting blade B first contacts the polarizer 2 and then contacts the protective film 3. In other words, each cutting blade B enters from the polarizer 2 having a low elastic modulus, and subsequently enters the protective film 3 having a high elastic modulus.
  • the average height Rc of the roughness curve element on the end face 2a of the polarizer 2 can be easily controlled within the range of 0.05 to 1.7 ⁇ m. It is easy to control the root mean square roughness Rq at the side portion 2as of 2 within the range of 0.03 to 0.15 ⁇ m.
  • the rotating cutting tool 10 may be moved at a constant speed in a direction (Y direction) parallel to the end surface 100a of the laminate 100.
  • the end surface 100a of the laminated body 100 end surface 2a of each polarizer 2
  • the position of the stacked body 100 may be fixed.
  • the laminate 100 may be brought close to the cutting tool 10 at a constant speed.
  • the end surface 100a of the stacked body 100 the end surface 2a of each polarizer 2
  • the position of the cutting tool 10 may be fixed.
  • each polarizing plate 1A constituting the laminated body 100 it is possible to adjust the dimensions of each polarizing plate 1A constituting the laminated body 100 with high accuracy, compared to the conventional cutting of the laminated body 100 by laser.
  • the polarizing plate includes a polarizer, a first optical film (for example, a protective film) that overlaps the polarizer, a pressure-sensitive adhesive layer that overlaps the first optical film, and a second optical film that overlaps the pressure-sensitive adhesive layer (for example, a reflective polarizer).
  • a first optical film for example, a protective film
  • a pressure-sensitive adhesive layer that overlaps the first optical film
  • a second optical film that overlaps the pressure-sensitive adhesive layer
  • the first optical film or the second optical film is a film with an antiglare function, a film with a surface antireflection function, a reflection film, a transflective film, a viewing angle compensation film, a release film, an optical compensation layer, a touch sensor layer, a charging It may be a prevention layer or an antifouling layer.
  • the first optical film may be a reflective polarizer
  • the second optical film may be a protective film.
  • Example 1 (1) Production of polarizer A polyvinyl alcohol film having a thickness of 20 ⁇ m was prepared. The average degree of polymerization of this polyvinyl alcohol film was about 2400, and the degree of saponification was 99.9 mol% or more. The polyvinyl alcohol film was uniaxially stretched about 4 times by a dry method. While maintaining the stretched state of the polyvinyl alcohol film by stretching, the polyvinyl alcohol film was immersed in pure water at 40 ° C. for 1 minute. Next, the polyvinyl alcohol film was immersed in the first dyeing solution (aqueous solution) for 60 seconds. The temperature of the first staining liquid was adjusted to 28 ° C.
  • first dyeing solution aqueous solution
  • the mass ratio of iodine: potassium iodide: water in the first staining solution was 0.1: 5: 100.
  • the polyvinyl alcohol film was immersed in the second dyeing solution (aqueous solution) for 300 seconds. The temperature of the second staining solution was adjusted to 68 ° C.
  • the mass ratio of potassium iodide: boric acid: water in the second dyeing solution was 10.5: 7.5: 100.
  • the polyvinyl alcohol film was washed with pure water for 5 seconds. The temperature of pure water was adjusted to 5 ° C.
  • the polarizer which is a long strip
  • KC8UX2MW which is a triacetylcellulose film (TAC film) manufactured by Konica Minolta Opto Co., Ltd. was used.
  • the thickness of the release film was 80 ⁇ m.
  • the release film was not saponified.
  • the laminated film includes a polarizer, a water-based adhesive layer that overlaps one surface of the polarizer, a protective film that overlaps the water-based adhesive layer, a pure water layer that overlaps the other surface of the polarizer, and a pure water layer. And an overlapping release film.
  • the laminated film was transported to a drying device to dry the aqueous adhesive layer and volatilize and remove the pure water layer. The temperature in the drying apparatus was adjusted to 80 ° C. The drying time was 300 seconds.
  • a single-sided protective polarizing plate was obtained by peeling the release film from the dried laminate.
  • This single-sided protective polarizing plate includes a polarizer, a dry aqueous adhesive layer that overlaps one surface of the polarizer, and a protective film that overlaps the aqueous adhesive layer.
  • a brightness enhancement film is bonded to the surface of the polarizer provided in the above-mentioned single-side protective polarizing plate via a pressure-sensitive adhesive layer, and the polarizing plate with brightness enhancement film is obtained. Obtained.
  • the orientations of the single-sided protective polarizing plate and the brightness enhancement film were adjusted so that the stretching direction of the polarizer was parallel to the stretching axis of the brightness enhancement film.
  • An acrylic resin was used for the pressure-sensitive adhesive layer.
  • “APF” which is a reflective polarizer manufactured by 3M Corporation was used.
  • the polarizing plate with a separator includes a polarizer, a water-based adhesive layer that overlaps one surface of the polarizer, a protective film (first optical film) that overlaps the water-based adhesive layer, and a first layer that overlaps the other surface of the polarizer.
  • the polarizing plate with a separator was cut into a size of 120 mm x 70 mm to obtain 100 polarizing plates.
  • a super cutter was used for cutting.
  • the structure, composition and dimensions of the 100 polarizing plates were the same.
  • a laminate was obtained by aligning the four sides of 100 polarizing plates and stacking 100 polarizing plates.
  • a laminate including 100 polarizing plates is identified with the laminate 100 illustrated in FIGS. 4 and 5.
  • the four end faces 100a of the laminate 100 were cut.
  • the method of cutting the four end faces 100a was exactly the same.
  • the cutting tool used in the example was the same as the cutting tool 10 shown in FIGS.
  • each of the first cutting part group and the second cutting part group had five cutting parts.
  • the cutting tool used in the embodiment is identified with the cutting tool 10 shown in FIGS.
  • the Z-axis direction in each figure is regarded as the upward direction
  • the X-axis direction and the Y-axis direction are regarded as the horizontal direction.
  • the five cutting blades B of each cutting section group are arranged on the cutting surface S so that the protruding heights of the five cutting blades B gradually increase along the direction opposite to the rotation direction of the cutting tool 10. It was. Further, along the direction opposite to the rotation direction of the cutting tool 10, the five cutting parts of each cutting part group have the cutting surface S so that the distance from the rotation axis A to the cutting blade B of the cutting part gradually decreases. Had been placed on top. A total of ten cutting parts constituting the first cutting part group and the second cutting part group were arranged at equal intervals so as to surround the rotation axis A. The height of the pair of cutting blades B that face each other via the rotation axis A was the same.
  • each cutting blade group of the cutting tool 10 has five cutting blades B having different heights, one rotation of the cutting tool 10 corresponds to five stages of cutting with different depths.
  • a pair of cutting tools 10 were used in cutting the end surface 100a of the laminate 100.
  • the cutting surfaces S of the pair of cutting tools 10 faced each other.
  • the interval between the pair of cutting tools 10 was adjusted so that the laminate 100 was accommodated between the pair of cutting tools 10.
  • the orientation of the cutting tool 10 was adjusted so that the rotation axis A of the cutting tool 10 was horizontal.
  • the position of each cutting tool 10 was fixed, and each cutting tool 10 was rotated about the rotation axis A.
  • the orientation of the end surface 100a of the stacked body 100 was adjusted so that the end surface 100a of the stacked body 100 was perpendicular to the rotation axis A of the cutting tool 10 (the normal line of the cutting surface S).
  • the direction of the laminated body 100 was adjusted so that the surface of the laminated body 100 might become horizontal.
  • a synthetic resin plate having the same thickness as the laminated body 100 and slightly smaller than the laminated body 100 was placed under the laminated body 100 to adjust the height at which the laminated body 100 was placed. As shown in FIGS. 4 and 5, by adjusting the height at which the laminated body 100 is arranged, the approach angle ⁇ of each cutting blade B with respect to the surface of each polarizer 2 in the laminated body 100 becomes substantially vertical, The height at which the body 100 is disposed is substantially the same as the height of the rotation axis A of the cutting tool 10. The thickness of the synthetic resin plate used for adjusting the height at which the laminated body 100 is arranged was 60 mm.
  • the height at which the laminate 100 is arranged was kept constant.
  • the laminated body 100 was moved at a constant speed in the horizontal direction (Y-axis direction), and the laminated body 100 was gradually introduced between the pair of rotating cutting tools 10. That is, one end surface 100a of the laminate 100 is gradually cut by the cutting surface S of one cutting tool 10, and at the same time, the other end surface 100a of the laminate 100 is gradually cut by the cutting surface S of the other cutting tool 10. .
  • the laminated body 100 was continuously moved in the horizontal direction (Y-axis direction) until the entire end surface 100a of the laminated body 100 was cut.
  • each polarizing plate 1 the polarizer 2 is disposed on the protective film 3, so that each cutting blade B of the cutting tool 10 is first turned into each polarizer 2 in the laminate 100 by one rotation of the cutting tool 10. Then, the end face of each protective film 3 adjacent to each polarizer 2 was cut.
  • the average height Rc of the roughness curve element on the end surface 2a of the polarizer 2 included in the polarizing plate 1 of Example 1 was measured by the following procedure.
  • the end surface 2 a of the polarizer 2 to be measured means an end surface that has been cut by the cutting tool 10.
  • a 3D measurement laser microscope “OLS4100” manufactured by Olympus Corporation was used for the measurement of Rc. Five polarizing plates 1 were randomly extracted from 100 polarizing plates of Example 1.
  • the Rc of the two end faces 2a perpendicular to the direction of the drawing axis of the polarizer 2 is measured, and the average value of Rc of the two end faces 2a is measured. Calculated.
  • the average value of Rc of each of the polarizers 2 included in the five polarizing plates 1 was calculated, and the average value of these five types of Rc was further averaged.
  • the Rc of Example 1 calculated by the above procedure was 0.07 ⁇ m.
  • the root-mean-square roughness Rq at the side portion 2as of the end face 2a of the polarizer 2 included in the polarizing plate 1 of Example 1 was measured by the following procedure.
  • the end surface 2 a of the polarizer 2 to be measured means an end surface that has been cut by the cutting tool 10.
  • a 3D measurement laser microscope “OLS4100” manufactured by Olympus Corporation was used for the measurement of Rq. Five polarizing plates 1 were randomly extracted from 100 polarizing plates of Example 1.
  • Heat Shock Test A heat shock test using a single polarizing plate of Example 1 (polarizing plate after cutting) was performed in the following procedure.
  • the separator was peeled off from the polarizing plate with a separator, and the polarizing plate was attached to an alkali-free glass plate via an adhesive layer to obtain a test sample.
  • alkali-free glass plate “Eagle-XG” manufactured by Corning was used.
  • the sample was confined in an autoclave for 20 minutes and subjected to pressure treatment.
  • the temperature in the autoclave was maintained at 50 ° C.
  • the pressure in the autoclave was maintained at 5 MPa.
  • the sample after the pressure treatment was left for 1 day in an atmosphere having a temperature of 23 ° C. and a relative humidity of 60%.
  • Step 1 maintaining the temperature in the test chamber at ⁇ 40 ° C. for 30 minutes.
  • Step 2 A step of maintaining the temperature in the test chamber at 23 ° C. for 5 minutes after Step 1.
  • Step 3 A step of maintaining the temperature in the test chamber at 85 ° C. for 30 minutes after Step 2.
  • the sample was taken out from the test tank. Next, the edge of the sample was observed with an optical microscope, and the presence or absence of cracks in the end surface 2a of the polarizer 2 was examined. As the optical microscope, “VHX-5000” manufactured by Keyence Corporation was used. The number of cracks per unit length on the end face 2a of the polarizer 2 was determined.
  • the “unit length” is a line segment in the end face of the polarizer, perpendicular to the thickness direction of the polarizer, and having a length of 10 mm.
  • the “number of cracks per unit length” means the number of cracks that intersect the unit length on the end face of the polarizer. The number of cracks in Example 1 was zero.
  • Examples 2 to 9 In Examples 2 to 9, the number of rotations of the cutting tool 10 per unit time was adjusted to the values shown in Table 1 below.
  • the synthetic resin plate was not disposed under the laminate 100. That is, in each of the cutting processes of Examples 5 to 7 and 9, the height at which the laminate 100 was disposed was lower than that of Example 1. Therefore, in each of the cutting operations in Examples 5 to 7 and 9, the approach angle ⁇ of each cutting blade B with respect to the surface of each polarizer 2 in the laminate 100 was not vertical. Further, in each of the cutting operations of Examples 5 to 7 and 9, the height at which the laminated body 100 was arranged was not substantially the same as the height of the rotation axis A of the cutting tool 10.
  • the polarizing plates of Examples 2 to 9 were prepared in the same manner as in Example 1 except for the above items related to cutting. In the same manner as in Example 1, Rc and Rq of each of Examples 2 to 9 were measured. The Rc and Rq of each of Examples 2 to 9 are shown in Table 1 below. In the same manner as in Example 1, the number of cracks in each of Examples 2 to 9 was measured. When a crack was formed on the end face of the polarizer, the length of the crack was also measured. The length of the crack is a distance from the end of the crack located on the end face of the polarizer to the end of the other crack. Table 1 below shows the number of cracks and the length of each of Examples 2 to 9.
  • the length of the crack shown in Table 1 is the length of the longest crack among the cracks formed on the end face of each polarizer.
  • the dimensional accuracy of each polarizing plate in Examples 2 to 9 was evaluated.
  • the accuracy of the dimensions of the polarizing plates in Examples 2 to 9 is shown in Table 1 below.
  • a polarizing plate of Comparative Example 1 was produced in the same manner as in Example 1 except for the above items related to cutting.
  • Rc and Rq in Comparative Example 1 were measured.
  • Rc and Rq of Comparative Example 1 are shown in Table 1 below.
  • the number of cracks and the crack length of Comparative Example 1 were measured.
  • the number of cracks and crack length in Comparative Example 1 are shown in Table 1 below.
  • the dimensional accuracy of the polarizing plate of Comparative Example 1 was evaluated. The accuracy of the dimensions of the polarizing plate of Comparative Example 1 is shown in Table 1 below.
  • Comparative Example 2 A polarizing plate of Comparative Example 2 was produced in the same manner as in Example 1 except that the cutting process was not performed. In the same manner as in Example 1, Rc and Rq in Comparative Example 2 were measured. Rc and Rq of Comparative Example 2 are shown in Table 1 below. In the same manner as in Example 1, the number of cracks in Comparative Example 2 was measured. The number of cracks in Comparative Example 2 is shown in Table 1 below. In the same manner as in Example 1, the dimensional accuracy of the polarizing plate of Comparative Example 2 was evaluated. The measured value of the length of one side of the polarizing plate of Comparative Example 2 was out of the tolerance range of the target value ⁇ 50 ⁇ m. That is, it was confirmed that the dimensional accuracy of the polarizing plate of Comparative Example 2 was low.
  • the polarizing plate according to the present invention is applied to, for example, a liquid crystal cell or an organic EL element, and is applied as an optical component constituting an image display device such as a liquid crystal television, an organic EL television, or a smartphone.
  • SYMBOLS 1 Polarizing plate, 2 ... Film-like polarizer, 2a ... End face of polarizer, 2as ... Side part of end face (part along end side of end face), 3 ... Protective film (first optical film), 4 ... reflective polarizer (second optical film), 5 ... pressure sensitive adhesive layer, S1 ... first side, S2 ... second side, S3 ... third side, S4 ... fourth side.

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  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Optics & Photonics (AREA)
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  • Liquid Crystal (AREA)

Abstract

L'objectif de la présente invention est de fournir un polariseur qui ne présente qu'un risque peu probable d'une fissure due à un changement de température. A cet effet, la hauteur moyenne Rc d'un élément de courbe de rugosité dans une section transversale 2a d'un polariseur 2 ayant une forme de film correspond à 0,05-1,7 µm.
PCT/JP2017/034967 2016-10-14 2017-09-27 Polariseur, lame polarisante et dispositif de formation d'image Ceased WO2018070247A1 (fr)

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JP6201025B1 (ja) 2017-09-20
KR102410190B1 (ko) 2022-06-20

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