WO2012019420A1 - Method for improving tobacco stem quality through combing steam explosion and enzyme treatment technology - Google Patents
Method for improving tobacco stem quality through combing steam explosion and enzyme treatment technology Download PDFInfo
- Publication number
- WO2012019420A1 WO2012019420A1 PCT/CN2011/000778 CN2011000778W WO2012019420A1 WO 2012019420 A1 WO2012019420 A1 WO 2012019420A1 CN 2011000778 W CN2011000778 W CN 2011000778W WO 2012019420 A1 WO2012019420 A1 WO 2012019420A1
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- WO
- WIPO (PCT)
- Prior art keywords
- tobacco stem
- steam
- tobacco
- quality
- stem
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/18—Other treatment of leaves, e.g. puffing, crimpling, cleaning
- A24B3/182—Puffing
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/20—Biochemical treatment
Definitions
- the invention relates to a method for improving the quality of tobacco stems by combining steam explosion with enzyme treatment technology, and belongs to the field of tobacco processing. Background technique
- Tobacco stems are an important part of tobacco leaves and generally account for about 1/4 of the quality of whole tobacco leaves.
- the cell wall material content of cellulose, hemicellulose, lignin and pectin in the stem is about 43.8% of the dry matter mass. High content of cellulose, hemicellulose, lignin and pectin, resulting in strong irritant stems, heavy gas, odor, cough, gargle, less aroma, restricting the cut stem in the cigarette formula Use ratio.
- the object of the present invention is achieved by a method for improving the quality of tobacco stems by combining steam explosion with enzyme treatment technology, which can combine steam explosion with enzyme treatment technology for treating tobacco stems and improving tobacco use for tobacco stems. Quality, the method includes the following steps:
- the added tobacco stems are treated under constant temperature and constant humidity conditions, and the treatment temperature is maintained at 30 to 35.
- C relative humidity is 90%;
- the stem is subjected to low-temperature dehydration and drying treatment, so that the water content is controlled to be about 20 ⁇ 30%;
- the above steam blasting method is: using saturated steam as a working medium, and fully blasting the stem by adjusting the saturated steam pressure and the pressure action time.
- the steam explosion pressure is 0. 8 ⁇ 1. OMPa, the steam holding time is 20 ⁇ 40 seconds.
- the treatment temperature is 35 ° C, and the relative humidity is 90%; in the d step, the suspension drying is used for dehydration treatment, so that the water content is maintained at about 30%.
- the basic guarantee for realizing the method is to first perform steam explosion on the tobacco stem, and then carry out enzymatic treatment on the tobacco stem after the explosion, and the constant temperature and constant humidity conditions in the enzyme treatment process can improve the treatment effect.
- the beneficial effects of the invention are that - steam explosion is the use of high pressure steam to infiltrate between the cellulose and lignin macromolecules in the structure of the stem, and the instantaneous release of high pressure steam between the tissues is realized by the rapid pressure loss outside the stem.
- the stalk is broken to promote the separation of the lignocellulosic structure, which makes the structure of the stem after fluffing fluffy, which is beneficial to the osmotic activity of ligninase and cellulase during the subsequent enzyme treatment, and strengthens the enzyme treatment effect.
- the high pressure and high temperature environment of steam explosion can also Effectively realize the conversion of cellulose, semi-fibres and pectin in tobacco stems, and improve the reducing sugar content in the stems.
- ligninase and cellulase to treat the stems after steam explosion can further reduce the lignin and cellulose in the stems, reduce the content of lignin and cellulose in the stems, and reduce the stems. Woody gas and coughing caused by lignin and cellulose.
- the combination of steam explosion and enzyme treatment to treat tobacco stems can effectively improve the quality of tobacco stems and increase the amount of tobacco stems added in cigarette production, which is of great significance for reducing cigarette production costs.
- the stems are dried by the enzyme-killing, and the shreds are processed according to the cigarette formula, and the amount of cut stems can be increased by more than 5%.
- Sensory evaluation showed that the sensory quality of the cut tobacco after steam blasting and enzyme treatment was increased by 5%, and the sensory quality of the cigarette was consistent with the original formula.
- the steam pressure is gauge pressure
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
Description
说 明 书 应用蒸汽爆破与酶处理技术相结合改善烟梗质量的方法 技术领域 Description of the method for improving the quality of tobacco stems by combining steam explosion with enzyme treatment technology
本发明涉及一种应用蒸汽爆破与酶处理技术相结合改善烟梗质量的方法,属 于烟草加工领域。 背景技术 The invention relates to a method for improving the quality of tobacco stems by combining steam explosion with enzyme treatment technology, and belongs to the field of tobacco processing. Background technique
烟梗是烟叶的重要组成部分, 一般占到整片烟叶质量的约 1/4。 烟梗中纤维 素、 半纤维素、 木质素和果胶等细胞壁物质含量约占干物质质量的 43. 8%。 纤维 素、 半纤维素、 木质素和果胶含量较高, 致使烟梗具有强烈的刺激性, 杂气重、 吸味呛咳、 涩口, 香气量少, 制约了梗丝在卷烟配方中的使用比例。 Tobacco stems are an important part of tobacco leaves and generally account for about 1/4 of the quality of whole tobacco leaves. The cell wall material content of cellulose, hemicellulose, lignin and pectin in the stem is about 43.8% of the dry matter mass. High content of cellulose, hemicellulose, lignin and pectin, resulting in strong irritant stems, heavy gas, odor, cough, gargle, less aroma, restricting the cut stem in the cigarette formula Use ratio.
发明内容 Summary of the invention
本发明的目的是提供一种应用蒸汽爆破与酶处理技术相结合改善烟梗质量 的方法, 以提高烟梗的烟用质量。 It is an object of the present invention to provide a method for improving the quality of tobacco stems by combining steam explosion with enzyme treatment techniques to improve the quality of tobacco stems.
本发明的目的是这样实现的:一种应用蒸汽爆破与酶处理技术相结合改善烟 梗质量的方法, 能将蒸汽爆破与酶处理技术相结合用于处理烟梗, 改善了烟梗的 烟用质量, 该方法包括以下步骤: The object of the present invention is achieved by a method for improving the quality of tobacco stems by combining steam explosion with enzyme treatment technology, which can combine steam explosion with enzyme treatment technology for treating tobacco stems and improving tobacco use for tobacco stems. Quality, the method includes the following steps:
a )、 使用蒸汽爆破机将润湿后的烟梗进行蒸汽爆破; a), using a steam blasting machine to steam blast the wetted stem;
b )、 将爆破后的烟梗添加木质素酶和纤维素酶; b) adding ligninase and cellulase to the blasted stem;
c )、 将加酶后的烟梗在恒温、 恒湿条件下进行处理, 保持处理温度为 30〜 35。C, 相对湿度为 90%; c), the added tobacco stems are treated under constant temperature and constant humidity conditions, and the treatment temperature is maintained at 30 to 35. C, relative humidity is 90%;
d )、 将酶处理后烟梗进行低温脱水干燥处理, 使其含水率控制在 20〜30 % 左右; d), after the enzyme treatment, the stem is subjected to low-temperature dehydration and drying treatment, so that the water content is controlled to be about 20~30%;
e )、 最后将脱水后的烟梗进行切丝处理用于卷烟生产。 e) Finally, the dehydrated stems are subjected to shredding for cigarette production.
上述蒸汽爆破方法是: 使用饱和水蒸汽作为工作介质, 通过调整饱和蒸汽压 力和压力作用时间实现对烟梗的充分爆破。 The above steam blasting method is: using saturated steam as a working medium, and fully blasting the stem by adjusting the saturated steam pressure and the pressure action time.
上述蒸汽爆破压力为 0. 8〜1. OMPa, 蒸汽保压时间为 20〜40秒。 The steam explosion pressure is 0. 8~1. OMPa, the steam holding time is 20~40 seconds.
上述 c步中处理温度为 35°C, 相对湿度为 90%; d步中使用悬浮式干燥进行 脱水处理, 使其含水率保持在 30%左右。 实现所述方法的基本保证是先对烟梗进行蒸汽爆破,然后再对爆破后的烟梗 进行酶处理处理, 酶处理过程中恒温和恒湿条件可提高处理效果。 In the above step c, the treatment temperature is 35 ° C, and the relative humidity is 90%; in the d step, the suspension drying is used for dehydration treatment, so that the water content is maintained at about 30%. The basic guarantee for realizing the method is to first perform steam explosion on the tobacco stem, and then carry out enzymatic treatment on the tobacco stem after the explosion, and the constant temperature and constant humidity conditions in the enzyme treatment process can improve the treatment effect.
本发明的有益效果是- 蒸汽爆破是利用高压蒸汽渗透于烟梗结构组织中的纤维素、木质素大分子之 间,通过烟梗外部的快速失压使组织间的高压蒸汽的瞬间释放实现烟梗进行破碎 促使木质纤维素结构分离, 使爆破后烟梗结构蓬松, 有利于后继酶处理时木质素 酶和纤维素酶的渗透作用, 强化了酶处理效果; 同时蒸汽爆破的高压高温环境还 可以有效实现烟梗中纤维素、半纤维和果胶质等物质的转化, 提高烟梗爆出物中 还原糖含量。 The beneficial effects of the invention are that - steam explosion is the use of high pressure steam to infiltrate between the cellulose and lignin macromolecules in the structure of the stem, and the instantaneous release of high pressure steam between the tissues is realized by the rapid pressure loss outside the stem. The stalk is broken to promote the separation of the lignocellulosic structure, which makes the structure of the stem after fluffing fluffy, which is beneficial to the osmotic activity of ligninase and cellulase during the subsequent enzyme treatment, and strengthens the enzyme treatment effect. At the same time, the high pressure and high temperature environment of steam explosion can also Effectively realize the conversion of cellulose, semi-fibres and pectin in tobacco stems, and improve the reducing sugar content in the stems.
使用木质素酶和纤维素酶对蒸汽爆破后的烟梗迸行处理可以使烟梗中的木 质素和纤维素达到进一步降解的目的, 减少烟梗中木质素和纤维素含量, 减少因 烟梗中木质素、 纤维素引起的木质气和呛咳性。 The use of ligninase and cellulase to treat the stems after steam explosion can further reduce the lignin and cellulose in the stems, reduce the content of lignin and cellulose in the stems, and reduce the stems. Woody gas and coughing caused by lignin and cellulose.
使用蒸汽爆破与酶处理相结合处理烟梗可以有效改善烟梗的烟用质量,提高 烟梗在卷烟生产中的添加量, 对于降低卷烟生产成本具有显著意义。 The combination of steam explosion and enzyme treatment to treat tobacco stems can effectively improve the quality of tobacco stems and increase the amount of tobacco stems added in cigarette production, which is of great significance for reducing cigarette production costs.
具体实施方式 detailed description
制备实施例: Preparation examples:
取经过调质、 醇化等正常处理工艺的烟梗 5kg, 使用清水快速冲洗去除表面 粘附灰尘, 晾置除去表面水分; 使用蒸汽爆破机对去除表面水分的烟梗进行爆破 处理, 爆破工作介质为饱和水蒸气, 爆破压力 0. 8MPa, 压力保留时间为 20秒。 烟梗蒸汽爆破后使用悬浮式鼓风干燥进行脱水干燥, 使其水分保持在 30%左右。 将木质素酶和纤维素酶活化后均勾添加后进行贮梗处理, 贮存装置温度设置为 35°C, 相对湿度设置为 90%, 避光处理 12〜24h。 酶处理后烟梗经灭酶烘干后进 行切丝, 按照卷烟配方进行卷烟加工, 梗丝添加量可提高 5%以上。 感官评吸表 明, 使用蒸汽爆破和酶处理加工后的梗丝在添加量提高 5%后, 卷烟感官质量与 原配方卷烟相一致。 Take 5k g of tobacco stems after normal treatment such as quenching and tempering, alcoholization, use water to quickly rinse off surface adhesion dust, and remove surface moisture by air; use steam blasting machine to blast the stems with surface moisture removal, blasting working medium The saturated water vapor has a bursting pressure of 0.8 MPa and a pressure retention time of 20 seconds. After the steam blasting of the stems, they are dehydrated and dried by suspension blast drying to keep the water content at about 30%. The ligninase and cellulase were activated and added to the stalk treatment. The temperature of the storage device was set to 35 ° C, the relative humidity was set to 90%, and the treatment was protected from light for 12 to 24 hours. After the enzyme treatment, the stems are dried by the enzyme-killing, and the shreds are processed according to the cigarette formula, and the amount of cut stems can be increased by more than 5%. Sensory evaluation showed that the sensory quality of the cut tobacco after steam blasting and enzyme treatment was increased by 5%, and the sensory quality of the cigarette was consistent with the original formula.
本文中蒸汽压力为表压。 In this paper, the steam pressure is gauge pressure.
Claims
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1020127017884A KR101256081B1 (en) | 2010-08-13 | 2011-05-03 | Method of improving quality of tobacco midrib by combining steam explosion and enzymatic treatment technology |
| GB1302998.8A GB2495893B (en) | 2010-08-13 | 2011-05-03 | Method for improving tobacco stem quality through combining steam explosion and enzyme treatment technology |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010102523941A CN101912149B (en) | 2010-08-13 | 2010-08-13 | Method for improving tobacco stalk quality by combining steam explosion and enzyme treatment technology |
| CN201010252394.1 | 2010-08-13 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| WO2012019420A1 true WO2012019420A1 (en) | 2012-02-16 |
Family
ID=43319941
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/CN2011/000778 Ceased WO2012019420A1 (en) | 2010-08-13 | 2011-05-03 | Method for improving tobacco stem quality through combing steam explosion and enzyme treatment technology |
Country Status (4)
| Country | Link |
|---|---|
| KR (1) | KR101256081B1 (en) |
| CN (1) | CN101912149B (en) |
| GB (1) | GB2495893B (en) |
| WO (1) | WO2012019420A1 (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2015108378A1 (en) | 2014-01-17 | 2015-07-23 | Samsung Electronics Co., Ltd. | Device to device communication method and apparatus |
| CN115067530A (en) * | 2022-06-23 | 2022-09-20 | 红云红河烟草(集团)有限责任公司 | A flexible silk-making process processing method for improving cigarette comfort |
| CN116509044A (en) * | 2023-02-15 | 2023-08-01 | 河南中烟工业有限责任公司 | Method for degrading lignin content of tobacco stems |
| CN116791389A (en) * | 2023-08-08 | 2023-09-22 | 镇江欧卯新材料有限公司 | Panel steam explosion control method and system |
| CN117238400A (en) * | 2023-10-08 | 2023-12-15 | 云南中烟工业有限责任公司 | A prediction method for the chemical composition of tobacco stem steam explosion based on BP neural network |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101912149B (en) * | 2010-08-13 | 2012-11-07 | 川渝中烟工业有限责任公司 | Method for improving tobacco stalk quality by combining steam explosion and enzyme treatment technology |
| EP2649888B1 (en) | 2012-04-10 | 2020-02-19 | Swedish Match North Europe AB | A smokeless tobacco composition comprising non-tobacco fibers and a method for its manufacture |
| CN102697167B (en) * | 2012-06-25 | 2014-04-16 | 湖北中烟工业有限责任公司 | Preparation method for tobacco stem extract with assistance of steam explosion |
| EP3054794B1 (en) | 2013-10-09 | 2017-05-31 | Swedish Match North Europe AB | An oral smokeless tobacco composition comprising liberated, delignified tobacco fibres and a method for its manufacture |
| CN110742304A (en) * | 2019-10-22 | 2020-02-04 | 红塔辽宁烟草有限责任公司 | Complex enzyme preparation for improving quality grade of expanded tobacco shreds and application thereof |
| CN113418823A (en) * | 2021-08-10 | 2021-09-21 | 湖北中烟工业有限责任公司 | Device for detecting tobacco sheet pulp in papermaking method |
| CN113519883B (en) * | 2021-08-25 | 2022-03-01 | 杨伟祖 | Novel flexible tobacco stem pulping process |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0568526A (en) * | 1991-09-12 | 1993-03-23 | T Hasegawa Co Ltd | Manufacturing method of extract for tobacco aroma |
| US5873372A (en) * | 1995-08-02 | 1999-02-23 | Brown & Williamson Tobacco Corporation | Process for steam explosion of tobacco stem |
| CN1257670A (en) * | 1998-12-20 | 2000-06-28 | 朱大恒 | Method and equipment for expanding tobacco |
| US6298859B1 (en) * | 1998-07-08 | 2001-10-09 | Novozymes A/S | Use of a phenol oxidizing enzyme in the treatment of tobacco |
| CN101228967A (en) * | 2007-12-26 | 2008-07-30 | 广东中烟工业公司 | A method for improving the quality of tobacco stems |
| CN101912149A (en) * | 2010-08-13 | 2010-12-15 | 川渝中烟工业公司 | The Method of Combining Steam Explosion and Enzyme Treatment to Improve the Quality of Tobacco Stems |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4307733A (en) * | 1978-09-20 | 1981-12-29 | Philip Morris, Inc. | Process for the treatment of tobacco materials |
| GB2069814A (en) * | 1980-02-27 | 1981-09-03 | Inst Przemyslu Fermentacyjnego | Microbiological treatment of tobacco and forming reconstituted tobacco or substitute |
| CN1169465C (en) * | 2001-07-27 | 2004-10-06 | 中国科学院化工冶金研究所 | Steam puffing treatment method of tobacco material |
| CN101288505A (en) * | 2007-12-06 | 2008-10-22 | 云南万芳生物技术有限公司 | Method for improving quality of the tobacco leaf expanded cut stem by microorganism enzyme |
| CN101711600B (en) * | 2008-10-08 | 2012-04-25 | 武汉达汇创新科技有限公司 | Process for biochemically treating cut stems |
-
2010
- 2010-08-13 CN CN2010102523941A patent/CN101912149B/en not_active Expired - Fee Related
-
2011
- 2011-05-03 GB GB1302998.8A patent/GB2495893B/en not_active Expired - Fee Related
- 2011-05-03 KR KR1020127017884A patent/KR101256081B1/en not_active Expired - Fee Related
- 2011-05-03 WO PCT/CN2011/000778 patent/WO2012019420A1/en not_active Ceased
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0568526A (en) * | 1991-09-12 | 1993-03-23 | T Hasegawa Co Ltd | Manufacturing method of extract for tobacco aroma |
| US5873372A (en) * | 1995-08-02 | 1999-02-23 | Brown & Williamson Tobacco Corporation | Process for steam explosion of tobacco stem |
| US6298859B1 (en) * | 1998-07-08 | 2001-10-09 | Novozymes A/S | Use of a phenol oxidizing enzyme in the treatment of tobacco |
| CN1257670A (en) * | 1998-12-20 | 2000-06-28 | 朱大恒 | Method and equipment for expanding tobacco |
| CN101228967A (en) * | 2007-12-26 | 2008-07-30 | 广东中烟工业公司 | A method for improving the quality of tobacco stems |
| CN101912149A (en) * | 2010-08-13 | 2010-12-15 | 川渝中烟工业公司 | The Method of Combining Steam Explosion and Enzyme Treatment to Improve the Quality of Tobacco Stems |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2015108378A1 (en) | 2014-01-17 | 2015-07-23 | Samsung Electronics Co., Ltd. | Device to device communication method and apparatus |
| CN115067530A (en) * | 2022-06-23 | 2022-09-20 | 红云红河烟草(集团)有限责任公司 | A flexible silk-making process processing method for improving cigarette comfort |
| CN115067530B (en) * | 2022-06-23 | 2023-11-17 | 红云红河烟草(集团)有限责任公司 | Flexible cut tobacco making process processing method for improving cigarette comfort |
| CN116509044A (en) * | 2023-02-15 | 2023-08-01 | 河南中烟工业有限责任公司 | Method for degrading lignin content of tobacco stems |
| CN116791389A (en) * | 2023-08-08 | 2023-09-22 | 镇江欧卯新材料有限公司 | Panel steam explosion control method and system |
| CN117238400A (en) * | 2023-10-08 | 2023-12-15 | 云南中烟工业有限责任公司 | A prediction method for the chemical composition of tobacco stem steam explosion based on BP neural network |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101912149A (en) | 2010-12-15 |
| KR101256081B1 (en) | 2013-04-19 |
| KR20120084340A (en) | 2012-07-27 |
| GB201302998D0 (en) | 2013-04-03 |
| GB2495893B (en) | 2013-11-06 |
| CN101912149B (en) | 2012-11-07 |
| GB2495893A (en) | 2013-04-24 |
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