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WO2009017102A1 - Epa濃縮油およびdha濃縮油の製造方法 - Google Patents

Epa濃縮油およびdha濃縮油の製造方法 Download PDF

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Publication number
WO2009017102A1
WO2009017102A1 PCT/JP2008/063550 JP2008063550W WO2009017102A1 WO 2009017102 A1 WO2009017102 A1 WO 2009017102A1 JP 2008063550 W JP2008063550 W JP 2008063550W WO 2009017102 A1 WO2009017102 A1 WO 2009017102A1
Authority
WO
WIPO (PCT)
Prior art keywords
enriched oil
dha
epa
oil
production
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/JP2008/063550
Other languages
English (en)
French (fr)
Inventor
Kiyomi Furihata
Hiroyuki Kawahara
Hideaki Yamaguchi
Hideo Ikemoto
Nobushige Doisaki
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nissui Corp
Original Assignee
Nippon Suisan Kaisha Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Suisan Kaisha Ltd filed Critical Nippon Suisan Kaisha Ltd
Priority to US12/669,803 priority Critical patent/US9556401B2/en
Priority to EP08791785.2A priority patent/EP2172558B1/en
Priority to KR1020107004008A priority patent/KR101502191B1/ko
Priority to JP2009525399A priority patent/JP5204776B2/ja
Priority to CA 2693070 priority patent/CA2693070A1/en
Priority to DK08791785.2T priority patent/DK2172558T3/en
Priority to CN200880101265.3A priority patent/CN101765662B/zh
Publication of WO2009017102A1 publication Critical patent/WO2009017102A1/ja
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS OR COOKING OILS
    • A23D9/00—Other edible oils or fats, e.g. shortenings or cooking oils
    • A23D9/02—Other edible oils or fats, e.g. shortenings or cooking oils characterised by the production or working-up
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/02—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils
    • C11C1/04—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils by hydrolysis
    • C11C1/045—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils by hydrolysis using enzymes or microorganisms, living or dead
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/04—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fats or fatty oils
    • C11C3/10—Ester interchange
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/64—Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/64—Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
    • C12P7/6436—Fatty acid esters
    • C12P7/6445—Glycerides
    • C12P7/6458—Glycerides by transesterification, e.g. interesterification, ester interchange, alcoholysis or acidolysis
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/64—Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
    • C12P7/6436—Fatty acid esters
    • C12P7/6445—Glycerides
    • C12P7/6472—Glycerides containing polyunsaturated fatty acid [PUFA] residues, i.e. having two or more double bonds in their backbone

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Biochemistry (AREA)
  • General Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Fats And Perfumes (AREA)

Abstract

　本発明により、酸化マグネシウム等の反応添加剤の存在下でEPAおよびDHAを含有する油脂を炭素数１８以下の脂肪酸に基質特異性を有するリパーゼによりアルコリシス反応させたのちグリセリド画分を分離し、さらにそのグリセリド画分を酸化マグネシウム等の反応添加剤の存在下で、炭素数２０以下の脂肪酸に基質特異性を有するリパーゼによりアルコリシス反応させて、EPA濃縮油およびDHA濃縮油を同時に得る方法が提供される。
PCT/JP2008/063550 2007-07-30 2008-07-29 Epa濃縮油およびdha濃縮油の製造方法 Ceased WO2009017102A1 (ja)

Priority Applications (7)

Application Number Priority Date Filing Date Title
US12/669,803 US9556401B2 (en) 2007-07-30 2008-07-29 Method for producing EPA-enriched oil and DHA-enriched oil
EP08791785.2A EP2172558B1 (en) 2007-07-30 2008-07-29 Method for production of epa-enriched oil and dha-enriched oil
KR1020107004008A KR101502191B1 (ko) 2007-07-30 2008-07-29 Ｅｐａ 농축유 및 ｄｈａ 농축유의 제조 방법
JP2009525399A JP5204776B2 (ja) 2007-07-30 2008-07-29 Ｅｐａ濃縮油およびｄｈａ濃縮油の製造方法
CA 2693070 CA2693070A1 (en) 2007-07-30 2008-07-29 Method for producing epa-enriched oil and dha-enriched oil
DK08791785.2T DK2172558T3 (en) 2007-07-30 2008-07-29 Process for producing an EPA-enriched oil and DHA-enriched oil
CN200880101265.3A CN101765662B (zh) 2007-07-30 2008-07-29 Epa浓缩油和dha浓缩油的制造方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007197253 2007-07-30
JP2007-197253 2007-07-30

Publications (1)

Publication Number Publication Date
WO2009017102A1 true WO2009017102A1 (ja) 2009-02-05

Family

ID=40304332

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/063550 Ceased WO2009017102A1 (ja) 2007-07-30 2008-07-29 Epa濃縮油およびdha濃縮油の製造方法

Country Status (8)

Country Link
US (1) US9556401B2 (ja)
EP (1) EP2172558B1 (ja)
JP (1) JP5204776B2 (ja)
KR (1) KR101502191B1 (ja)
CN (1) CN101765662B (ja)
CA (1) CA2693070A1 (ja)
DK (1) DK2172558T3 (ja)
WO (1) WO2009017102A1 (ja)

Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010183881A (ja) * 2009-02-13 2010-08-26 Kao Corp ドコサヘキサエン酸高含有油脂の製造方法
JP2010265417A (ja) * 2009-05-15 2010-11-25 Mizusawa Ind Chem Ltd バイオ燃料の製造方法
WO2011149040A1 (ja) * 2010-05-28 2011-12-01 日本水産株式会社 リパーゼによる高度不飽和脂肪酸含有油脂の製造方法
JP2013055893A (ja) * 2011-09-07 2013-03-28 Nippon Suisan Kaisha Ltd 高度不飽和脂肪酸濃縮油の製造方法
JP2013533346A (ja) * 2010-06-30 2013-08-22 ロダース・クロックラーン・ビー・ブイ 植物油の処理
WO2013172346A1 (ja) 2012-05-14 2013-11-21 日本水産株式会社 環境汚染物質を低減させた高度不飽和脂肪酸又は高度不飽和脂肪酸エチルエステル及びその製造方法
JP2014510165A (ja) * 2011-02-11 2014-04-24 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー 微生物バイオマスから脂質含有組成物を得る方法
WO2015029364A1 (ja) * 2013-08-30 2015-03-05 備前化成株式会社 高純度オメガ３系脂肪酸エチルエステルの生産方法
WO2015046436A1 (ja) * 2013-09-26 2015-04-02 キユーピー株式会社 低級アルコール脂肪酸エステル化物含有組成物の製造方法および低級アルコール脂肪酸エステル化物含有組成物
US9050308B2 (en) 2012-01-06 2015-06-09 Omthera Pharmaceuticals, Inc. DPA-enriched compositions of omega-3 polyunsaturated fatty acids in free acid form
WO2016153065A1 (ja) * 2015-03-25 2016-09-29 キユーピー株式会社 Ｄｈａ含有グリセリド含有組成物の製造方法
WO2016158605A1 (ja) * 2015-04-01 2016-10-06 キユーピー株式会社 低級アルコール脂肪酸エステル化物含有組成物の製造方法および低級アルコール脂肪酸エステル化物含有組成物
US9492545B2 (en) 2012-05-07 2016-11-15 Omthera Pharmaceuticals Inc. Compositions of statins and omega-3 fatty acids
WO2017094804A1 (ja) * 2015-12-01 2017-06-08 日本水産株式会社 ドコサヘキサエン酸含有油及びその製造方法
WO2020050303A1 (ja) * 2018-09-04 2020-03-12 日本水産株式会社 リパーゼ加水分解反応を用いる高度不飽和脂肪酸含有グリセリドの製造方法

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RU2014146265A (ru) 2009-12-30 2015-07-10 Басф Фарма (Калланиш) Лимитед Способ хроматографического разделения с псевдодвижущимся слоем
JP5416861B2 (ja) * 2011-03-03 2014-02-12 日本水産株式会社 リパーゼによる高度不飽和脂肪酸含有油脂の製造方法
GB201111595D0 (en) 2011-07-06 2011-08-24 Equateq Ltd Improved process
GB201111601D0 (en) 2011-07-06 2011-08-24 Equateq Ltd New process
GB201111594D0 (en) 2011-07-06 2011-08-24 Equateq Ltd New improved process
GB201111591D0 (en) 2011-07-06 2011-08-24 Equateq Ltd Further new process
GB201111589D0 (en) 2011-07-06 2011-08-24 Equateq Ltd New modified process
GB201300354D0 (en) 2013-01-09 2013-02-20 Basf Pharma Callanish Ltd Multi-step separation process
CN104130860B (zh) * 2013-05-03 2020-03-31 丰益(上海)生物技术研发中心有限公司 利用固定化疏棉状嗜热丝孢菌脂肪酶富集长链多不饱和脂肪酸的方法
US9428711B2 (en) 2013-05-07 2016-08-30 Groupe Novasep Chromatographic process for the production of highly purified polyunsaturated fatty acids
US8802880B1 (en) 2013-05-07 2014-08-12 Group Novasep Chromatographic process for the production of highly purified polyunsaturated fatty acids
EP3118186B1 (fr) * 2013-12-11 2022-02-09 Novasep Process Installation chromatographique de production d acides gras polyinsatures
JP6303017B2 (ja) 2014-01-07 2018-03-28 ノヴァセプ プロセスＮｏｖａｓｅｐ Ｐｒｏｃｅｓｓ 芳香族アミノ酸を精製する方法
CN106687113B (zh) * 2014-06-06 2021-09-03 海洋原料公司 ω-3组合物、剂型及使用方法
JP2016182046A (ja) * 2015-03-25 2016-10-20 キユーピー株式会社 低級アルコール脂肪酸エステル化物含有組成物の製造方法
TWI646195B (zh) * 2017-08-25 2019-01-01 國立高雄科技大學 一種脂肪酶填充床生物反應器用於連續式合成二十二碳六烯酸酯類與二十碳五烯酸酯類
EP3586642A1 (en) 2018-06-21 2020-01-01 Nuseed Pty Ltd Ala enriched polyunsaturated fatty acid compositions
EP3586640A1 (en) 2018-06-21 2020-01-01 Nuseed Pty Ltd Dha enriched polyunsaturated fatty acid compositions
CN112048380B (zh) * 2020-09-03 2022-06-14 广州白云山汉方现代药业有限公司 一种采用混合填料精准控制大豆油中硬脂酸含量的方法
CN112266939B (zh) * 2020-10-30 2022-12-13 江南大学 一种酶法富集油脂中多不饱和脂肪酸甘油酯的方法
KR20230090652A (ko) 2021-12-15 2023-06-22 박민경 농축우유 가공방법 및 이에 의해 가공된 농축우유를 이용한 커피음료

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Cited By (31)

* Cited by examiner, † Cited by third party
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JP2010183881A (ja) * 2009-02-13 2010-08-26 Kao Corp ドコサヘキサエン酸高含有油脂の製造方法
JP2010265417A (ja) * 2009-05-15 2010-11-25 Mizusawa Ind Chem Ltd バイオ燃料の製造方法
WO2011149040A1 (ja) * 2010-05-28 2011-12-01 日本水産株式会社 リパーゼによる高度不飽和脂肪酸含有油脂の製造方法
US10138502B2 (en) 2010-05-28 2018-11-27 Nippon Suisan Kaisha, Ltd. Method for producing oil containing polyunsaturated fatty acid using lipase
US9161553B2 (en) 2010-06-30 2015-10-20 Loders Croklaan B.V. Processing of vegetable oils
JP2013533346A (ja) * 2010-06-30 2013-08-22 ロダース・クロックラーン・ビー・ブイ 植物油の処理
JP2014510165A (ja) * 2011-02-11 2014-04-24 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー 微生物バイオマスから脂質含有組成物を得る方法
JP2013055893A (ja) * 2011-09-07 2013-03-28 Nippon Suisan Kaisha Ltd 高度不飽和脂肪酸濃縮油の製造方法
US9050308B2 (en) 2012-01-06 2015-06-09 Omthera Pharmaceuticals, Inc. DPA-enriched compositions of omega-3 polyunsaturated fatty acids in free acid form
US9050309B2 (en) 2012-01-06 2015-06-09 Omthera Pharmaceuticals, Inc. DPA-enriched compositions of omega-3 polyunsaturated fatty acids in free acid form
US10117844B2 (en) 2012-01-06 2018-11-06 Omthera Pharmaceuticals, Inc. DPA-enriched compositions of omega-3 polyunsaturated fatty acids in free acid form
US9492545B2 (en) 2012-05-07 2016-11-15 Omthera Pharmaceuticals Inc. Compositions of statins and omega-3 fatty acids
EP4414356A2 (en) 2012-05-14 2024-08-14 Nissui Corporation Highly unsaturated fatty acid or highly unsaturated fatty acid ethyl ester with reduced environmental pollutants, and method for producing same
EP3971165A1 (en) 2012-05-14 2022-03-23 Nippon Suisan Kaisha, Ltd. Highly unsaturated fatty acid or highly unsaturated fatty acid ethyl ester with reduced environmental pollutants, and method for producing same
WO2013172346A1 (ja) 2012-05-14 2013-11-21 日本水産株式会社 環境汚染物質を低減させた高度不飽和脂肪酸又は高度不飽和脂肪酸エチルエステル及びその製造方法
WO2015029364A1 (ja) * 2013-08-30 2015-03-05 備前化成株式会社 高純度オメガ３系脂肪酸エチルエステルの生産方法
JP2015063653A (ja) * 2013-08-30 2015-04-09 備前化成株式会社 高純度オメガ３系脂肪酸エチルエステルの生産方法
WO2015046436A1 (ja) * 2013-09-26 2015-04-02 キユーピー株式会社 低級アルコール脂肪酸エステル化物含有組成物の製造方法および低級アルコール脂肪酸エステル化物含有組成物
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