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WO2008078448A1 - 塩基性アミノ酸塩酸塩結晶の取得方法 - Google Patents

塩基性アミノ酸塩酸塩結晶の取得方法 Download PDF

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Publication number
WO2008078448A1
WO2008078448A1 PCT/JP2007/070555 JP2007070555W WO2008078448A1 WO 2008078448 A1 WO2008078448 A1 WO 2008078448A1 JP 2007070555 W JP2007070555 W JP 2007070555W WO 2008078448 A1 WO2008078448 A1 WO 2008078448A1
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WO
WIPO (PCT)
Prior art keywords
basic
amino acid
crystals
sulfate
basic amino
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/JP2007/070555
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English (en)
French (fr)
Inventor
Mitsuhiro Kishino
Toshimichi Kamei
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ajinomoto Co Inc
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Ajinomoto Co Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ajinomoto Co Inc filed Critical Ajinomoto Co Inc
Priority to EP07830289.0A priority Critical patent/EP2096176B1/en
Priority to MX2009006932A priority patent/MX2009006932A/es
Priority to JP2008550983A priority patent/JPWO2008078448A1/ja
Priority to CN2007800458215A priority patent/CN101558164B/zh
Priority to CA2672714A priority patent/CA2672714C/en
Priority to KR1020097014763A priority patent/KR101046905B1/ko
Publication of WO2008078448A1 publication Critical patent/WO2008078448A1/ja
Priority to US12/491,341 priority patent/US8372606B2/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P13/00—Preparation of nitrogen-containing organic compounds
    • C12P13/04—Alpha- or beta- amino acids
    • C12P13/08—Lysine; Diaminopimelic acid; Threonine; Valine
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P13/00—Preparation of nitrogen-containing organic compounds
    • C12P13/04—Alpha- or beta- amino acids
    • C12P13/10—Citrulline; Arginine; Ornithine
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P13/00—Preparation of nitrogen-containing organic compounds
    • C12P13/04—Alpha- or beta- amino acids
    • C12P13/24—Proline; Hydroxyproline; Histidine

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  • Organic Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Microbiology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Biotechnology (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

　本発明は、硫酸イオンを含有する塩基性アミノ酸発酵液からの、製品収量及び品質が従来技術におけるとほぼ同等であって、しかもより簡便な塩基性アミノ酸塩酸塩の分離取得方法を提供することを目的とする。本発明は、硫酸イオンを含有する塩基性アミノ酸発酵液または塩基性アミノ酸産生微生物の生菌体を触媒とする酵素反応液から塩基性アミノ酸の塩酸塩結晶を取得する方法であって、（１）硫酸イオンを含有する塩基性アミノ酸発酵液または酵素反応液に、カルシウム、カリウム、マグネシウムおよびバリウムからなる群より選択される金属の塩化物を添加して該硫酸イオンを該金属の硫酸塩結晶として析出させ、（２）該塩基性アミノ酸溶液から該金属の硫酸塩結晶を除去し、（３）該金属の硫酸塩結晶を除去した塩基性アミノ酸溶液を、該金属の硫酸塩の飽和溶解度以下に維持しつつ冷却して塩基性アミノ酸をその塩酸塩結晶として析出させ、（４）該塩基性アミノ酸結晶を分離し採取すること、を特徴とする方法を提供する。
PCT/JP2007/070555 2006-12-25 2007-10-22 塩基性アミノ酸塩酸塩結晶の取得方法 Ceased WO2008078448A1 (ja)

Priority Applications (7)

Application Number Priority Date Filing Date Title
EP07830289.0A EP2096176B1 (en) 2006-12-25 2007-10-22 Method of obtaining crystal of hydrochloride of basic amino acid
MX2009006932A MX2009006932A (es) 2006-12-25 2007-10-22 Metodo para obtener cristales de un clorhidrato de aminoacido basico.
JP2008550983A JPWO2008078448A1 (ja) 2006-12-25 2007-10-22 塩基性アミノ酸塩酸塩結晶の取得方法
CN2007800458215A CN101558164B (zh) 2006-12-25 2007-10-22 碱性氨基酸盐酸盐结晶的取得方法
CA2672714A CA2672714C (en) 2006-12-25 2007-10-22 Method for obtaining crystals of a basic amino acid hydrochloride
KR1020097014763A KR101046905B1 (ko) 2006-12-25 2007-10-22 염기성 아미노산 염산염 결정의 수득 방법
US12/491,341 US8372606B2 (en) 2006-12-25 2009-06-25 Methods for obtaining crystals of a basic amino acid hydrochloride

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2006347650 2006-12-25
JP2006-347650 2006-12-25

Related Child Applications (1)

Application Number Title Priority Date Filing Date
US12/491,341 Continuation US8372606B2 (en) 2006-12-25 2009-06-25 Methods for obtaining crystals of a basic amino acid hydrochloride

Publications (1)

Publication Number Publication Date
WO2008078448A1 true WO2008078448A1 (ja) 2008-07-03

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Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2007/070555 Ceased WO2008078448A1 (ja) 2006-12-25 2007-10-22 塩基性アミノ酸塩酸塩結晶の取得方法

Country Status (10)

Country Link
US (1) US8372606B2 (ja)
EP (1) EP2096176B1 (ja)
JP (1) JPWO2008078448A1 (ja)
KR (1) KR101046905B1 (ja)
CN (1) CN101558164B (ja)
BR (1) BRPI0703692B1 (ja)
CA (1) CA2672714C (ja)
MX (1) MX2009006932A (ja)
RU (1) RU2460799C2 (ja)
WO (1) WO2008078448A1 (ja)

Cited By (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2009088049A1 (ja) 2008-01-10 2009-07-16 Ajinomoto Co., Inc. 発酵法による目的物質の製造法
WO2010084995A2 (en) 2009-01-23 2010-07-29 Ajinomoto Co.,Inc. A method for producing an l-amino acid
WO2011016301A1 (ja) 2009-08-03 2011-02-10 味の素株式会社 ビブリオ属細菌を用いたｌ－リジンの製造法
WO2011024555A1 (ja) 2009-08-28 2011-03-03 味の素株式会社 Ｌ－アミノ酸の製造法
WO2011055710A1 (ja) 2009-11-06 2011-05-12 味の素株式会社 Ｌ－アミノ酸の製造法
EP2345667A2 (en) 2010-01-15 2011-07-20 Ajinomoto Co., Inc. A method for producing an L-amino acid using a bacterium of the enterobacteriaceae family
WO2011096554A1 (ja) 2010-02-08 2011-08-11 味の素株式会社 変異型ｒｐｓＡ遺伝子及びＬ－アミノ酸の製造法
WO2012077739A1 (ja) 2010-12-10 2012-06-14 味の素株式会社 Ｌ－アミノ酸の製造法
WO2012137689A1 (ja) 2011-04-01 2012-10-11 味の素株式会社 Ｌ－システインの製造法
WO2012144472A1 (ja) 2011-04-18 2012-10-26 味の素株式会社 Ｌ－システインの製造法
WO2013069634A1 (ja) 2011-11-11 2013-05-16 味の素株式会社 発酵法による目的物質の製造法
WO2014185430A1 (ja) 2013-05-13 2014-11-20 味の素株式会社 Ｌ－アミノ酸の製造法
EP3165608A1 (en) 2015-10-30 2017-05-10 Ajinomoto Co., Inc. Method for producing l-amino acid of glutamate family
EP3385389A1 (en) 2017-04-03 2018-10-10 Ajinomoto Co., Inc. Method for producing l-amino acid from fructose
JP2021515551A (ja) * 2018-03-05 2021-06-24 アレボ・アクチボラゲットＡｒｅｖｏ Ａｂ 塩基性アミノ酸の分離
WO2022092018A1 (ja) 2020-10-28 2022-05-05 味の素株式会社 Ｌ－アミノ酸の製造法
WO2023013655A1 (ja) 2021-08-02 2023-02-09 味の素株式会社 食品の風味を改善する方法
WO2023195475A1 (ja) 2022-04-04 2023-10-12 味の素株式会社 寄生植物を防除する方法
EP4345166A2 (en) 2022-09-30 2024-04-03 Ajinomoto Co., Inc. Method for producing l-amino acid
WO2025141837A1 (ja) 2023-12-28 2025-07-03 味の素株式会社 Ｌ－グルタミン酸生産菌およびｌ－グルタミン酸の製造方法
WO2025141838A1 (ja) 2023-12-28 2025-07-03 味の素株式会社 Ｌ－グルタミン酸生産菌およびｌ－グルタミン酸の製造方法

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CN104892437A (zh) * 2015-05-15 2015-09-09 南通荣泰生物科技有限公司 一种l-盐酸赖氨酸的生产工艺
CN105175275B (zh) * 2015-07-01 2017-03-01 山东民强生物科技股份有限公司 一种l‑鸟氨酸的分离纯化方法
CN107963650A (zh) * 2017-12-15 2018-04-27 湖南师范大学 一种氨基酸络合物合成工艺中的母液处理方法
CN118026894A (zh) * 2022-11-14 2024-05-14 安徽华恒生物科技股份有限公司 一种瓜氨酸的分离纯化方法
KR20250035158A (ko) * 2023-09-05 2025-03-12 씨제이제일제당 (주) 고순도 아르기닌의 제조방법

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Cited By (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2009088049A1 (ja) 2008-01-10 2009-07-16 Ajinomoto Co., Inc. 発酵法による目的物質の製造法
EP2749652A2 (en) 2008-01-10 2014-07-02 Ajinomoto Co., Inc. A method for producing a target substance by fermentation
WO2010084995A2 (en) 2009-01-23 2010-07-29 Ajinomoto Co.,Inc. A method for producing an l-amino acid
WO2011016301A1 (ja) 2009-08-03 2011-02-10 味の素株式会社 ビブリオ属細菌を用いたｌ－リジンの製造法
WO2011024555A1 (ja) 2009-08-28 2011-03-03 味の素株式会社 Ｌ－アミノ酸の製造法
WO2011055710A1 (ja) 2009-11-06 2011-05-12 味の素株式会社 Ｌ－アミノ酸の製造法
EP2345667A2 (en) 2010-01-15 2011-07-20 Ajinomoto Co., Inc. A method for producing an L-amino acid using a bacterium of the enterobacteriaceae family
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WO2014185430A1 (ja) 2013-05-13 2014-11-20 味の素株式会社 Ｌ－アミノ酸の製造法
EP3165608A1 (en) 2015-10-30 2017-05-10 Ajinomoto Co., Inc. Method for producing l-amino acid of glutamate family
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JP2021515551A (ja) * 2018-03-05 2021-06-24 アレボ・アクチボラゲットＡｒｅｖｏ Ａｂ 塩基性アミノ酸の分離
JP7503496B2 (ja) 2018-03-05 2024-06-20 アレボ・アクチボラゲット 塩基性アミノ酸の分離
WO2022092018A1 (ja) 2020-10-28 2022-05-05 味の素株式会社 Ｌ－アミノ酸の製造法
WO2023013655A1 (ja) 2021-08-02 2023-02-09 味の素株式会社 食品の風味を改善する方法
WO2023195475A1 (ja) 2022-04-04 2023-10-12 味の素株式会社 寄生植物を防除する方法
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WO2025141837A1 (ja) 2023-12-28 2025-07-03 味の素株式会社 Ｌ－グルタミン酸生産菌およびｌ－グルタミン酸の製造方法
WO2025141838A1 (ja) 2023-12-28 2025-07-03 味の素株式会社 Ｌ－グルタミン酸生産菌およびｌ－グルタミン酸の製造方法

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MX2009006932A (es) 2009-07-06
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US20090291477A1 (en) 2009-11-26
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