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WO2006000020A1 - Improved leaching of base metals - Google Patents

Improved leaching of base metals Download PDF

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Publication number
WO2006000020A1
WO2006000020A1 PCT/AU2005/000901 AU2005000901W WO2006000020A1 WO 2006000020 A1 WO2006000020 A1 WO 2006000020A1 AU 2005000901 W AU2005000901 W AU 2005000901W WO 2006000020 A1 WO2006000020 A1 WO 2006000020A1
Authority
WO
WIPO (PCT)
Prior art keywords
ore
leaching
leach solution
leach
fine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/AU2005/000901
Other languages
French (fr)
Inventor
Colin John Hunter
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EUROPEAN NICKEL PLC
Original Assignee
EUROPEAN NICKEL PLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from AU2004903514A external-priority patent/AU2004903514A0/en
Application filed by EUROPEAN NICKEL PLC filed Critical EUROPEAN NICKEL PLC
Priority to EP05752409A priority Critical patent/EP1769092A4/en
Priority to AU2005256141A priority patent/AU2005256141B2/en
Publication of WO2006000020A1 publication Critical patent/WO2006000020A1/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B1/00—Preliminary treatment of ores or scrap
    • C22B1/14—Agglomerating; Briquetting; Binding; Granulating
    • C22B1/24—Binding; Briquetting ; Granulating
    • C22B1/242—Binding; Briquetting ; Granulating with binders
    • C22B1/243—Binding; Briquetting ; Granulating with binders inorganic
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B1/00—Preliminary treatment of ores or scrap
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B1/00—Preliminary treatment of ores or scrap
    • C22B1/14—Agglomerating; Briquetting; Binding; Granulating
    • C22B1/24—Binding; Briquetting ; Granulating
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0407—Leaching processes
    • C22B23/0415—Leaching processes with acids or salt solutions except ammonium salts solutions
    • C22B23/043—Sulfurated acids or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0453—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B23/0461—Treatment or purification of solutions, e.g. obtained by leaching by chemical methods
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
    • C22B3/06—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
    • C22B3/08—Sulfuric acid, other sulfurated acids or salts thereof
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

Definitions

  • the present invention relates to the leaching of base metals from oxide ores. More particularly, the present invention is intended to have application in the recovery of nickel and cobalt from lateritic ores in the context of heap leaching.
  • the ore after crushing, will contain a significant level of fine particulate material, such as clay or clay-like material. This material, if preventative steps are not taken, can interfere with the permeability of the heap, and consequently reduce the efficiency of the heap leach process.
  • agglomerate the ore with water or process solution, and with cement. The agglomeration is conducted in an agglomeration drum, immediately prior to stacking of the heap.
  • the fine particles stick to the coarser particles and thereby make the subsequently formed heap more permeable to the leach process solution.
  • the fines in the heap are immobilised during agglomeration and cannot then migrate and give rise to blinding of the heap, and/or channelling of leach solution, which may otherwise lead to long leach times and to incompletely leached pockets within the heap.
  • the present invention has as one object thereof to overcome the abovementioned problems associated with the prior art or to at least provide a useful alternative thereto.
  • step b) utilising the fine ore fraction or part thereof to neutralise or partially neutralise the leach agent contained in a pregnant leach solution produced in step b), prior to passing some or all of the pregnant leach solution on for further refinement or other treatment as required.
  • step c) Preferably, some or all of the neutralised or partially neutralised pregnant leach solution of step c) is passed to a base metal recovery circuit.
  • the ore is a laterite ore containing nickel and cobalt.
  • the coarse ore fraction is leached in one or more heaps.
  • the ore may have been agglomerated with sulphuric acid prior to forming the or each heap.
  • sodium metabisulphite or sulphur dioxide is added to a sulphuric acid based leach solution.
  • Figure 1 is a diagrammatic representation of a simple leach circuit in accordance with the method of the present invention
  • Figure 1 there is shown a flow-sheet demonstrating one potential commercial application of a method in accordance with the present invention in use in a heap leach environment.
  • a laterite ore containing nickel and cobalt is mined and crushed to pass through a 12mm screen in a crushing and screening plant 10. During the crushing process, any particles of a size less than about 75 micrometers in diameter ( ⁇ 75 ⁇ m), a fine fraction, are removed from the bulk of the ore and stored in a fines storage facility - A -
  • a coarse ore heap 14 is stacked on an impermeable membrane 16 in known manner, utilising the coarse fraction of ore greater than 75 micrometers.
  • the coarse ore heap 14 has arranged thereon a reticulation system 18 to feed the heap 14 with a sulphuric acid based leach solution from a leach solution pond 20, via a pump 22.
  • the leach solution pond 16 is maintained at a suitable acid strength or pH by the addition of sulphuric acid.
  • Piping 24 is provided to direct pregnant leach solution to a sump 26, from which the pregnant leach solution may flow by gravity through a line 28 to the leach solution pond 20, or may be bled through line 30 from the leaching process to a fines neutralisation circuit 32.
  • the sump 26 contains a pump (not shown).
  • Fine ore from the fines storage facility 12 is utilised in the fines neutralisation circuit 32 to neutralise some or all of the sulphuric acid contained in the solution in the bleed from the heap 14. Some or all of this treated solution may then be passed on to a metals recovery circuit. Solids waste from the fines neutralisation circuit 32 can be discarded, as shown in Figure 1. Alternatively, in the event the solid waste contains high enough metal values, it may be recycled back into the leaching circuit and mixed back into the coarse ore.
  • the method of the present invention can be seen to offer efficiencies when compared with prior art processes, at least in part through the use of fines to neutralise pregnant leach solution prior to metal recover.
  • an agglomeration step may be utilised prior to stacking of the heap 14 and that sodium metabisulphite or sulphur dioxide may be added to the sulphuric acid based leach solution.
  • fine and coarse fraction may differ between applications. That is, the sizing of what constitutes a fine may change depending upon a variety of factors within the method, including the specific mineralogy of the ore. Modifications and variations such as would be apparent to the skilled addressee are considered to fall within the scope of the present invention.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Metallurgy (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

A method for the leaching of base metals from oxide ores, the method characterised by the method steps of: a) Separating the ore to be leached into fine and coarse fractions or streams; b) Leaching the coarse fraction of the ore in a leach solution with a suitable leach agent for the leaching of the contained metals; and Utilising the fine ore fraction or part thereof to neutralise or partially neutralise the leach agent contained in a pregnant leach solution produced in step b), prior to passing some or all of the pregnant leach solution on for further refinement or other treatment as required.

Description

"Improved Leaching of Base Metals"
Field of the Invention
The present invention relates to the leaching of base metals from oxide ores. More particularly, the present invention is intended to have application in the recovery of nickel and cobalt from lateritic ores in the context of heap leaching.
Background Art
The application of heap leaching techniques in the recovery of base metals, for example copper, from oxide ore deposits is well established. For example, if copper is the base metal of interest and the host rock is sufficiently oxidised, the oxide ore can be crushed to a suitable size, stacked in heaps and leached with a sulphuric acid solution (SME Minerals Processing Handbook, Ed. NL Weiss, Society of Mineral Engineers ISBN 0-89520-433-6).
It is often the case that the ore, after crushing, will contain a significant level of fine particulate material, such as clay or clay-like material. This material, if preventative steps are not taken, can interfere with the permeability of the heap, and consequently reduce the efficiency of the heap leach process. In dealing with such ores, it is common practice to agglomerate the ore with water or process solution, and with cement. The agglomeration is conducted in an agglomeration drum, immediately prior to stacking of the heap.
In the agglomeration process the fine particles stick to the coarser particles and thereby make the subsequently formed heap more permeable to the leach process solution. The fines in the heap are immobilised during agglomeration and cannot then migrate and give rise to blinding of the heap, and/or channelling of leach solution, which may otherwise lead to long leach times and to incompletely leached pockets within the heap.
Where sulphuric acid is used to heap leach nickel from laterite ores, the leach kinetics can be very slow. High acid strength leach solutions may be utilised to partially overcome this. In such a situation the rate of acid consumption as the solution passes through the heap will also be slow and the acid strength in the solution emanating from the base of the heap will not vary greatly from that in the solution being supplied to the top of the heap. This will result in a high acid concentration in the solution that is being bled from the leaching circuit into the metals recovery circuit. If it is not possible to recover this acid then this can become a major operating cost, which will be compounded by the need to add more chemicals, such as limestone, in order to neutralise the acid so that the base metals can be effectively recovered.
The present invention has as one object thereof to overcome the abovementioned problems associated with the prior art or to at least provide a useful alternative thereto.
The preceding discussion of the background art is intended to facilitate an understanding of the present invention only. It should be appreciated that the discussion is not an acknowledgement or admission that any of the material referred to was part of the common general knowledge in Australia or any other country or region as at the priority date of the application.
Disclosure of the Invention
In accordance with the present invention there is provided a method for the leaching of base metals from oxide ores, the method characterised by the method steps of:
a) Separating the ore to be leached into fine and coarse fractions or streams;
b) Leaching the coarse fraction of the ore in a leach solution with a suitable leach agent for the leaching of the contained metals; and
c) Utilising the fine ore fraction or part thereof to neutralise or partially neutralise the leach agent contained in a pregnant leach solution produced in step b), prior to passing some or all of the pregnant leach solution on for further refinement or other treatment as required.
Preferably, some or all of the neutralised or partially neutralised pregnant leach solution of step c) is passed to a base metal recovery circuit.
Still preferably, the ore is a laterite ore containing nickel and cobalt.
Still further preferably, the coarse ore fraction is leached in one or more heaps.
In one form of the invention, the ore may have been agglomerated with sulphuric acid prior to forming the or each heap.
In a further form of the invention sodium metabisulphite or sulphur dioxide is added to a sulphuric acid based leach solution.
Brief Description of the Drawings
The present invention will now be described, by way of example only, with reference to one embodiment of the present invention and the accompanying drawings, in which:-
Figure 1 is a diagrammatic representation of a simple leach circuit in accordance with the method of the present invention;
Best Mode(s) for Carrying Out the Invention
In Figure 1 there is shown a flow-sheet demonstrating one potential commercial application of a method in accordance with the present invention in use in a heap leach environment.
A laterite ore containing nickel and cobalt is mined and crushed to pass through a 12mm screen in a crushing and screening plant 10. During the crushing process, any particles of a size less than about 75 micrometers in diameter (<75μm), a fine fraction, are removed from the bulk of the ore and stored in a fines storage facility - A -
12. A coarse ore heap 14 is stacked on an impermeable membrane 16 in known manner, utilising the coarse fraction of ore greater than 75 micrometers.
The coarse ore heap 14 has arranged thereon a reticulation system 18 to feed the heap 14 with a sulphuric acid based leach solution from a leach solution pond 20, via a pump 22. The leach solution pond 16 is maintained at a suitable acid strength or pH by the addition of sulphuric acid.
Piping 24 is provided to direct pregnant leach solution to a sump 26, from which the pregnant leach solution may flow by gravity through a line 28 to the leach solution pond 20, or may be bled through line 30 from the leaching process to a fines neutralisation circuit 32. The sump 26 contains a pump (not shown).
Fine ore from the fines storage facility 12 is utilised in the fines neutralisation circuit 32 to neutralise some or all of the sulphuric acid contained in the solution in the bleed from the heap 14. Some or all of this treated solution may then be passed on to a metals recovery circuit. Solids waste from the fines neutralisation circuit 32 can be discarded, as shown in Figure 1. Alternatively, in the event the solid waste contains high enough metal values, it may be recycled back into the leaching circuit and mixed back into the coarse ore.
The method of the present invention can be seen to offer efficiencies when compared with prior art processes, at least in part through the use of fines to neutralise pregnant leach solution prior to metal recover.
It is envisaged that an agglomeration step may be utilised prior to stacking of the heap 14 and that sodium metabisulphite or sulphur dioxide may be added to the sulphuric acid based leach solution.
It is further envisaged that the distinction between fine and coarse fraction may differ between applications. That is, the sizing of what constitutes a fine may change depending upon a variety of factors within the method, including the specific mineralogy of the ore. Modifications and variations such as would be apparent to the skilled addressee are considered to fall within the scope of the present invention.

Claims

Claims
1. A method for the leaching of base metals from oxide ores, the method characterised by the method steps of:
a) Separating the ore to be leached into fine and coarse fractions or streams;
b) Leaching the. coarse fraction of the ore in a leach solution with a suitable leach agent for the leaching of the contained metals; and
c) Utilising the fine ore fraction or part thereof to neutralise or partially neutralise the leach agent contained in a pregnant leach solution produced in step b), prior to passing some or all of the pregnant leach solution on for further refinement or other treatment as required.
2. A method according to claim 1 , wherein some or all of the neutralised or partially neutralised pregnant leach solution of step c) is passed to a base metal recovery circuit.
3. A method according to claim 1 or 2, wherein the ore is a laterite ore containing nickel and cobalt.
4. A method according to any of claims 1 to 3, wherein the coarse ore faction is leached in one or more heaps.
5. A method according to claim 4, wherein the ore is agglomerated with sulphuric acid prior to forming the or each heap.
6. A method according to any one of claims 1 to 4, wherein the leach agent is or contains sulphuric acid.
7. A method according to claim 5, wherein sodium metabisulphite or sulphur dioxide is added to the sulphuric acid based leach solution.
8. A method according to any one of the preceding claims, wherein ore particles less than about 75μm constitute the fine fraction.
9. A method according to any one of the preceding claims, wherein ore particles greater than about 75μm constitute the coarse fraction.
10. A method for the heap leaching of nickel and/or cobalt from oxide ores, the method characterised by the method steps of:
(a) Separating the ore to be leached into fine and coarse ore fractions or steams;
(b) Leaching the coarse fraction of the ore in one or more heaps with a leach solution containing a sulfuric acid based leach agent; and
(c) Utilising the fine ore fraction or part thereof to neutralise or partially neutralise the leach agent contained in a pregnant leach solution produced in step b), prior to passing at least a portion of the pregnant leach solution to a base metal recovery circuit.
11. A method for the leaching of base metals from oxide ores, the method substantially as hereinbefore described with reference to the accompanying figure.
PCT/AU2005/000901 2004-06-29 2005-06-22 Improved leaching of base metals Ceased WO2006000020A1 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
EP05752409A EP1769092A4 (en) 2004-06-29 2005-06-22 Improved leaching of base metals
AU2005256141A AU2005256141B2 (en) 2004-06-29 2005-06-22 Improved leaching of base metals

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
AU2004903514 2004-06-29
AU2004903514A AU2004903514A0 (en) 2004-06-29 Improved Heap Leaching of Base Metals from their Ores

Publications (1)

Publication Number Publication Date
WO2006000020A1 true WO2006000020A1 (en) 2006-01-05

Family

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PCT/AU2005/000901 Ceased WO2006000020A1 (en) 2004-06-29 2005-06-22 Improved leaching of base metals

Country Status (3)

Country Link
EP (1) EP1769092A4 (en)
RU (1) RU2346996C2 (en)
WO (1) WO2006000020A1 (en)

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