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WO2005101949A3 - A high resolution low temperature solid-state nuclear magnetic resonance probe - Google Patents

A high resolution low temperature solid-state nuclear magnetic resonance probe Download PDF

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Publication number
WO2005101949A3
WO2005101949A3 PCT/EE2005/000005 EE2005000005W WO2005101949A3 WO 2005101949 A3 WO2005101949 A3 WO 2005101949A3 EE 2005000005 W EE2005000005 W EE 2005000005W WO 2005101949 A3 WO2005101949 A3 WO 2005101949A3
Authority
WO
WIPO (PCT)
Prior art keywords
nuclear magnetic
magnetic resonance
high resolution
gas
low temperature
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/EE2005/000005
Other languages
French (fr)
Other versions
WO2005101949A2 (en
Inventor
Ago Samoson
Ivo Heinmaa
Tiit Tuherm
Andres Reinhold
Jaan Past
Raivo Stern
Tiit Anupold
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
KEEMILISE JA BIOLOOGILISE FUEUESIKA INSTITUUT (THE NCS) ATIONAL INSTITUTE OF CHEMICAL PHYSICS AND BIOPHYSI
KEEMILISE JA BIOLOOGILISE FUEU
Original Assignee
KEEMILISE JA BIOLOOGILISE FUEUESIKA INSTITUUT (THE NCS) ATIONAL INSTITUTE OF CHEMICAL PHYSICS AND BIOPHYSI
KEEMILISE JA BIOLOOGILISE FUEU
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by KEEMILISE JA BIOLOOGILISE FUEUESIKA INSTITUUT (THE NCS) ATIONAL INSTITUTE OF CHEMICAL PHYSICS AND BIOPHYSI, KEEMILISE JA BIOLOOGILISE FUEU filed Critical KEEMILISE JA BIOLOOGILISE FUEUESIKA INSTITUUT (THE NCS) ATIONAL INSTITUTE OF CHEMICAL PHYSICS AND BIOPHYSI
Publication of WO2005101949A2 publication Critical patent/WO2005101949A2/en
Publication of WO2005101949A3 publication Critical patent/WO2005101949A3/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00—Arrangements or instruments for measuring magnetic variables
    • G01R33/20—Arrangements or instruments for measuring magnetic variables involving magnetic resonance
    • G01R33/28—Details of apparatus provided for in groups G01R33/44 - G01R33/64
    • G01R33/30—Sample handling arrangements, e.g. sample cells, spinning mechanisms
    • G01R33/307—Sample handling arrangements, e.g. sample cells, spinning mechanisms specially adapted for moving the sample relative to the MR system, e.g. spinning mechanisms, flow cells or means for positioning the sample inside a spectrometer
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00—Arrangements or instruments for measuring magnetic variables
    • G01R33/20—Arrangements or instruments for measuring magnetic variables involving magnetic resonance
    • G01R33/28—Details of apparatus provided for in groups G01R33/44 - G01R33/64
    • G01R33/30—Sample handling arrangements, e.g. sample cells, spinning mechanisms
    • G01R33/31—Temperature control thereof

Landscapes

  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Magnetic Resonance Imaging Apparatus (AREA)
  • Magnetic Bearings And Hydrostatic Bearings (AREA)
  • Rolling Contact Bearings (AREA)

Abstract

This invention relates to an nuclear magnetic resonance (NMR) probe, which enables registering high resolution NMR double resonance spectra in powder samples by high-speed magic angle spinning at low temperatures. The idea of rotating device used in the design is based on using a small-diameter rotor which is placed in a helium gas flowthrough cryostat, ensuring low temperatures. The spinning of the rotor takes place as a result of gas flow directed to the gas bearings supported turbine. New is the use of an effective heat exchanger for cooling down the bearing and turbine gas.
PCT/EE2005/000005 2004-04-20 2005-04-18 A high resolution low temperature solid-state nuclear magnetic resonance probe Ceased WO2005101949A2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EEU200400029 2004-04-20
EEU200400029U EE00582U1 (en) 2004-04-20 2004-04-20 High resolution low temperature solid state nuclear magnetic resonance probe

Publications (2)

Publication Number Publication Date
WO2005101949A2 WO2005101949A2 (en) 2005-11-03
WO2005101949A3 true WO2005101949A3 (en) 2006-08-03

Family

ID=35197406

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EE2005/000005 Ceased WO2005101949A2 (en) 2004-04-20 2005-04-18 A high resolution low temperature solid-state nuclear magnetic resonance probe

Country Status (2)

Country Link
EE (1) EE00582U1 (en)
WO (1) WO2005101949A2 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2981442A1 (en) * 2011-10-17 2013-04-19 Bruker Biospin COLD GAS SUPPLY DEVICE AND NMR INSTALLATION COMPRISING SUCH A DEVICE
CN109187612B (en) * 2018-08-21 2021-04-02 中国科学院广州能源研究所 Method for preparing and loading sample before solid nuclear magnetism representation of gas hydrate

Citations (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4254373A (en) * 1977-06-03 1981-03-03 Lippmaa Endel T Sensor for generating nuclear magnetic resonance signals
US4511841A (en) * 1982-06-17 1985-04-16 Chemagnetics, Inc. Method and apparatus for high speed magic angle spinning
US4899111A (en) * 1988-08-03 1990-02-06 The Regents Of The University Of California Probe for high resolution NMR with sample reorientation
US5122745A (en) * 1989-07-28 1992-06-16 The Dow Chemical Company Method and apparatus for determining molecular dynamics of materials
US5202633A (en) * 1990-11-01 1993-04-13 Doty Scientific, Inc. High temperature nmr sample spinner
US5298864A (en) * 1990-03-15 1994-03-29 Bruker Analytische Messtechnik Gmbh Nuclear magnetic resonance spectrometer and method for measuring the nuclear magnetic resonance
US5325059A (en) * 1992-03-26 1994-06-28 Doty Scientific Inc. DOR NMR sample spinner
US5754048A (en) * 1996-07-17 1998-05-19 Bruker Instruments, Inc. Method and apparatus for precisely controlling the periodic motion of an object
US6130537A (en) * 1997-03-20 2000-10-10 Doty Scientific Inc. HR MAS NMR coils with magic angle capacitors
US6320384B1 (en) * 1996-12-23 2001-11-20 David F. Doty Thermal buffering of cross-coils in high-power NMR decoupling
US20030052678A1 (en) * 2001-07-27 2003-03-20 The University Of Chicago Rotational exchange gradient imager for in situ magnetic resonance analyses in ultracentrifuge sedimentation of biological materials and rheology investigations
US20030102867A1 (en) * 2001-10-03 2003-06-05 Jeol Ltd. High-speed sample spinner for solid NMR spectroscopy
US20030199751A1 (en) * 2000-10-13 2003-10-23 Benjamin Gonzalez Method and device for analysing the intracellular chemical state of living cells by nuclear magnetic resonance
US20040070398A1 (en) * 2002-10-15 2004-04-15 Wong Wai Ha RF coil for magic angle spinning probe
US20040222796A1 (en) * 2003-02-04 2004-11-11 Munson Eric Jon Solid-state nuclear magnetic resonance probe

Patent Citations (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4254373A (en) * 1977-06-03 1981-03-03 Lippmaa Endel T Sensor for generating nuclear magnetic resonance signals
US4511841A (en) * 1982-06-17 1985-04-16 Chemagnetics, Inc. Method and apparatus for high speed magic angle spinning
US4899111A (en) * 1988-08-03 1990-02-06 The Regents Of The University Of California Probe for high resolution NMR with sample reorientation
US5122745A (en) * 1989-07-28 1992-06-16 The Dow Chemical Company Method and apparatus for determining molecular dynamics of materials
US5298864A (en) * 1990-03-15 1994-03-29 Bruker Analytische Messtechnik Gmbh Nuclear magnetic resonance spectrometer and method for measuring the nuclear magnetic resonance
US5202633A (en) * 1990-11-01 1993-04-13 Doty Scientific, Inc. High temperature nmr sample spinner
US5325059A (en) * 1992-03-26 1994-06-28 Doty Scientific Inc. DOR NMR sample spinner
US5754048A (en) * 1996-07-17 1998-05-19 Bruker Instruments, Inc. Method and apparatus for precisely controlling the periodic motion of an object
US6320384B1 (en) * 1996-12-23 2001-11-20 David F. Doty Thermal buffering of cross-coils in high-power NMR decoupling
US6130537A (en) * 1997-03-20 2000-10-10 Doty Scientific Inc. HR MAS NMR coils with magic angle capacitors
US20030199751A1 (en) * 2000-10-13 2003-10-23 Benjamin Gonzalez Method and device for analysing the intracellular chemical state of living cells by nuclear magnetic resonance
US20030052678A1 (en) * 2001-07-27 2003-03-20 The University Of Chicago Rotational exchange gradient imager for in situ magnetic resonance analyses in ultracentrifuge sedimentation of biological materials and rheology investigations
US20030102867A1 (en) * 2001-10-03 2003-06-05 Jeol Ltd. High-speed sample spinner for solid NMR spectroscopy
US20040070398A1 (en) * 2002-10-15 2004-04-15 Wong Wai Ha RF coil for magic angle spinning probe
US20040222796A1 (en) * 2003-02-04 2004-11-11 Munson Eric Jon Solid-state nuclear magnetic resonance probe

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
HACKMANN A ET AL: "Magic-Angle Spinning NMR at Near-Liquid-Helium Temperatures", JOURNAL OF MAGNETIC RESONANCE, ACADEMIC PRESS, ORLANDO, FL, USA, vol. 79, no. 1, August 1988 (1988-08-01), pages 148 - 153, XP002377650 *
MARTIN R W ET AL: "Variable temperature system using vortex tube cooling and fiber optic temperature measurement for low temperature magic angle spinning NMR", JOURNAL OF MAGNETIC RESONANCE, ACADEMIC PRESS, ORLANDO, FL, US, vol. 168, no. 2, 27 March 2004 (2004-03-27), pages 202 - 209, XP004508572, ISSN: 1090-7807 *
MARTIN RACHEL W ET AL: "Design of a triple resonance magic angle sample spinning probe for high field solid state nuclear magnetic resonance", REVIEW OF SCIENTIFIC INSTRUMENTS, AMERICAN INSTITUTE OF PHYSICS, US, vol. 74, no. 6, June 2003 (2003-06-01), pages 3045 - 3061, XP012040877, ISSN: 0034-6748 *
MIZUNO T ET AL: "Switching-angle sample spinning NMR probe with a commercially available 20kHz spinning system", JOURNAL OF MAGNETIC RESONANCE, ACADEMIC PRESS, ORLANDO, FL, US, vol. 171, no. 1, 23 August 2004 (2004-08-23), pages 15 - 19, XP004609229, ISSN: 1090-7807 *

Also Published As

Publication number Publication date
WO2005101949A2 (en) 2005-11-03
EE00582U1 (en) 2006-01-16

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