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US528513A - Method of improving surfaces of aluminium - Google Patents

Method of improving surfaces of aluminium Download PDF

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Publication number
US528513A
US528513A US528513DA US528513A US 528513 A US528513 A US 528513A US 528513D A US528513D A US 528513DA US 528513 A US528513 A US 528513A
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Prior art keywords
aluminium
acid
mixture
aluminum
improving
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    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23GCLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
    • C23G1/00Cleaning or pickling metallic material with solutions or molten salts
    • C23G1/02Cleaning or pickling metallic material with solutions or molten salts with acid solutions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D2111/00Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
    • C11D2111/10Objects to be cleaned
    • C11D2111/14Hard surfaces
    • C11D2111/22Electronic devices, e.g. PCBs or semiconductors

Definitions

  • nitric acid is to place in the dilute nitric acid a piece of aluminum, and to add hydrofluoric acid until gas is evolved freely from the surface of the aluminum. Such evolution of gas will indicate that theacids have been combined properly. Having ascertained the proper proportions (which are, of course, variable because of the uncertain strength of the hydrofluoric acid of commerce, and variable also according'to the temperature of the mixture for a hot solution of the acid may be used when more 1 u e than a cold solution),
  • the aluminum to be treated is immersed therein and is allgweimomainuntititssur face heco n es bright. It is then removed and washed, prefefably'with hot water, and havoperation is complete.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
  • ing And Chemical Polishing (AREA)

Description

To aZZ whom it may concern:
Be itknown that I, ARTHUR V. DAvIs, of Pittsburg, in the county of Allegheny and State of Pennsylvania, have invented a new i i 5 and useful Improvement in Methods of Im- 11 proving Surfaces of Aluminium,of which the tion. A
I I have discovered that by treating the aluminum with a combination of hydrofl lm'ic acid alg d nitrig acid, its surface appearance da'fibe greatly improved, and the dullness of the metal removed so as to enhance its value in the arts. Neither hydrofluoric acid alone nor nitric acid alone will afiord the desired I I result satisfactorily, but by a mixture of them, or by their conjoint and successive use,
excellent results are obtained.
7 To determine the proper proportions of 20 hydrofluoric acid of any given commercial strength to be added to the concentrated nitric acidof commerce in order to prepare a desirable mixture for my purpose, I may proceed as followsz-Nitric acid of commerce 2 5 having specific gravity of about 31.4: Baum i'spreferably diluted with, say, about one to twenty parts of water. The proportion of wa- Q ter used is variable according to the temperature of the mixture of acids ultimately employed for treating the aluminum, for when I the mixture is to be used hot a less proportion of acid will answer, than when the mixture is cold. A good working test of the pro- ME'THQD or IMPROVING SURFACES OF ALummlumi SPECIFICATION forming part of Letters Patent No. 528,513, dated October 30, 1 894.
Application filed January 24, 1894- Berlal Ila 497,912. (No specimens-) following is a full, clear, and exact descripportion of hydrofluoric acid to be added to the PATENT OFFICE.
ARTHUR. v. DAVIS,- or PITTSBURG, PENNSYLVANIA.
nitric acid is to place in the dilute nitric acid a piece of aluminum, and to add hydrofluoric acid until gas is evolved freely from the surface of the aluminum. Such evolution of gas will indicate that theacids have been combined properly. Having ascertained the proper proportions (which are, of course, variable because of the uncertain strength of the hydrofluoric acid of commerce, and variable also according'to the temperature of the mixture for a hot solution of the acid may be used when more 1 u e than a cold solution),
the aluminum to be treated is immersed therein and is allgweimomainuntititssur face heco n es bright. It is then removed and washed, prefefably'with hot water, and havoperation is complete.
I do not limit myself to the use of the acids in any given proportion, nor do I disclaim the addition of other materials or steps in the practice of my process; but I What I claim is--- a The method of improving the surface appearance of aluminum, which consists in treating the surface with a mixture of h 6gpfluoric and and nitric acid, substantla y as M; uh-W m "a I s I ing been dried by sawdust or otherwise, the 1 In testimony whereof I have hereunto set W, B. Coawm.
US528513D Method of improving surfaces of aluminium Expired - Lifetime US528513A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2916458A (en) * 1954-11-12 1959-12-08 Aerojet General Co Pickling solution
US2933421A (en) * 1949-03-21 1960-04-19 Herbert H Hyman Dissolution method of removing bonding agents
US2963805A (en) * 1957-09-03 1960-12-13 Boeing Co Porcelain enameled foil labels
US3039910A (en) * 1958-11-10 1962-06-19 Aluminum Co Of America Treating aluminum surfaces
US5063651A (en) * 1978-02-21 1991-11-12 Varian Associates, Inc. Method of manufacturing a low emissivity liquid nitrogen dewar

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2933421A (en) * 1949-03-21 1960-04-19 Herbert H Hyman Dissolution method of removing bonding agents
US2916458A (en) * 1954-11-12 1959-12-08 Aerojet General Co Pickling solution
US2963805A (en) * 1957-09-03 1960-12-13 Boeing Co Porcelain enameled foil labels
US3039910A (en) * 1958-11-10 1962-06-19 Aluminum Co Of America Treating aluminum surfaces
US5063651A (en) * 1978-02-21 1991-11-12 Varian Associates, Inc. Method of manufacturing a low emissivity liquid nitrogen dewar

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