US3511340A - Method of lubricating a timepiece movement - Google Patents
Method of lubricating a timepiece movement Download PDFInfo
- Publication number
- US3511340A US3511340A US777455A US3511340DA US3511340A US 3511340 A US3511340 A US 3511340A US 777455 A US777455 A US 777455A US 3511340D A US3511340D A US 3511340DA US 3511340 A US3511340 A US 3511340A
- Authority
- US
- United States
- Prior art keywords
- pieces
- lubricating
- rugosity
- lubricant
- solid lubricant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title description 24
- 230000001050 lubricating effect Effects 0.000 title description 7
- 239000000314 lubricant Substances 0.000 description 19
- 239000007787 solid Substances 0.000 description 13
- 239000003921 oil Substances 0.000 description 6
- 230000001133 acceleration Effects 0.000 description 5
- 238000005461 lubrication Methods 0.000 description 5
- 239000000843 powder Substances 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 3
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 3
- 229910052737 gold Inorganic materials 0.000 description 3
- 239000010931 gold Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- ROUIDRHELGULJS-UHFFFAOYSA-N bis(selanylidene)tungsten Chemical compound [Se]=[W]=[Se] ROUIDRHELGULJS-UHFFFAOYSA-N 0.000 description 2
- 238000000151 deposition Methods 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 230000002349 favourable effect Effects 0.000 description 2
- 229910002804 graphite Inorganic materials 0.000 description 2
- 239000010439 graphite Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000010687 lubricating oil Substances 0.000 description 2
- CWQXQMHSOZUFJS-UHFFFAOYSA-N molybdenum disulfide Chemical compound S=[Mo]=S CWQXQMHSOZUFJS-UHFFFAOYSA-N 0.000 description 2
- 229910052982 molybdenum disulfide Inorganic materials 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 1
- 229910001369 Brass Inorganic materials 0.000 description 1
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 229910001128 Sn alloy Inorganic materials 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 239000010953 base metal Substances 0.000 description 1
- 239000010951 brass Substances 0.000 description 1
- 230000002860 competitive effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- LQBJWKCYZGMFEV-UHFFFAOYSA-N lead tin Chemical compound [Sn].[Pb] LQBJWKCYZGMFEV-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000010297 mechanical methods and process Methods 0.000 description 1
- 230000005226 mechanical processes and functions Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- CLDVQCMGOSGNIW-UHFFFAOYSA-N nickel tin Chemical compound [Ni].[Sn] CLDVQCMGOSGNIW-UHFFFAOYSA-N 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 229910052703 rhodium Inorganic materials 0.000 description 1
- 239000010948 rhodium Substances 0.000 description 1
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 description 1
- 239000010979 ruby Substances 0.000 description 1
- 229910001750 ruby Inorganic materials 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G04—HOROLOGY
- G04D—APPARATUS OR TOOLS SPECIALLY DESIGNED FOR MAKING OR MAINTAINING CLOCKS OR WATCHES
- G04D5/00—Oiling devices; Special lubricant containers for watchmakers
Definitions
- the present invention relates to a method of lubricating a timepiece movement, more particularly its escapement.
- the lubrication of the escapement of a timepiece is a problem for which an absolutely satisfactory solution has not yet been found.
- the generally used method consists in depositing by means of an oil-pike a drop of a suitable oil used in watchmaking on the impulse faces of the pallets of the lever. Owing to the successive passages of the teeth of the escape wheel, the drops of oil deposited on the pallets are swept, so that the major portion of the oil is carried outside the functional surfaces, where it can no longer take a part in the lubrication.
- the present invention aims at overcoming the several above-mentioned drawbacks. It has just been mentioned that the application of a solid lubricant gives good results in the watch.
- the lubricating method of the invention aims at increasing the adherence of a solid lubricant on the base material in such a manner that the lubricating layer cannot be destroyed by the conventional cleaning processes used in watchmaking.
- the present invention is based upon the property of certain solid lubricants of strongly adhering to the surface onto which they are applied, inasmuch as the application is made under a 3,511,340 Patented May 12, 1970 strong pressure and the finish of the surface is such that it promotes a catching of the lubricant.
- the lubricating method of the invention comprises the steps of treating the surface of the pieces so as to give them a rugosity lying between .1 and 1,u, and then treating the pieces, brought into this state, into a centrifugal barrel the acceleration of which lies between 1 and 20g and in which are contained, besides the pieces' -to be treated, a solid lubricant in powder form, a carrying mass for the latter and a granulated mass adapted to produce a pressure for fixing the solid lubricant onto the pieces to be treated.
- this surface may be subjected to different types of preparations. It is possible to give to the surface, by a mechanical process, a suitable rugosity, which may be obtained by a grinding, polishing, sanding or any other similar operation. Another process of preparing the surfaces may consist of 'a chemical or galvanic treatment. Among the former, let us cite, for instance, the phosphatation. It is also possible, in order to obtain the desired surface finish, to perform a chemical attack of the surface; in the case of pieces of brass, for instance, the desired rugosity may be obtained by an attack with an acid such as nitric acid or any other bath having the same action.
- a galvanic process is preferably used.
- the piece to be treated being made of steel, a first deposit of gold of normal constitution is effected.
- This deposit serves for promoting the adherence of the next deposit of gold which is effected in such conditiousby reducing the contents of free cyanide of the bath and by adapting the current intensity-that it presents a porous constitution and a rough surface.
- the thus obtained rugosity is easily adjustable by choosing the conditions of the galvanic deposition.
- a gold deposit is preferably effected, since its coefficient of friction with respect to ruby is favourable, but it is also possible to use other metals such as rhodium, silver or alloys such as lead-tin or nickel-tin alloys.
- the rugosity of the surface is adapted in such a manner that the geometry of the piece is not altered and the tolerances of manufacture are respected.
- the rugosity of the piece must lie between .1 and 1 (maximum height of the asperities) and its mean quadratic deviation preferably lies between .06 and .7,u..
- the mean quadratic deviation is, as is wellknown, the square root of the arithmetic average of the squares of the deviations.
- a centrifugal barrel After the pieces have received the desired surface preparation, they are put in a centrifugal barrel.
- the latter is loaded with a mixture of a solid lubricant in powder form (e.g. molybdenum disulfide, graphite or tungsten diselenide), of a carrying mass for the latter (consisting for instance of a plastic material or simply of sawdust) and of a granulated mass, preferably metallic, acting as a charge and serving for producing, when the centrifugal barrel is running, a pressure sufiicient for causing the lubricant to penetrate into the surface of the piece and strongly adhere thereto.
- the said granulated mass may consist for instance of balls of lead or steel, having a diameter of l-2 mm.
- the pieces in the centrifugal barrel After the passage of the pieces in the centrifugal barrel, they may be dipped in a final bath and then dried.
- the final bath comprises, for example, 12% of oil used in watchmaking in dissolution in a solvent such as Freon or benzine.
- a solvent such as Freon or benzine.
- the latter treatment still improves the lubrication.
- Pieces of escapement treated in the described conditions have shown, upon tests made in laboratories, an excellent resistance to the action of the cleaning baths, as well as an excellent behaviour in the watch.
- the invention really brings a solution to the problem, up to now not satisfactorily solved, of the lubrication of the escapement.
- Other friction pieces of the watch, treated by this method have also shown a most favorable behaviour, entirely competitive on the technical point of view with the conventional methods, with the additional advantage of a lubrication of greater duration.
- a method of lubricating a timepiece movement, more particularly its escapement characterized by treating the surface of the pieces so as to give them a rugosity lying between .1 and 1,11, and then treating the pieces, brought into this state, into a centrifugal barrel the acceleration of which lies between 1 and 20g and in which are contained, besides the pieces to be treated, a solid lubricant in powder form, a carrying mass for the latter and a granulated mass adapted to produce a pressure for fixing the solid lubricant onto the pieces to be treated.
- a method according to claim 1 characterized by treating the surface of the pieces so as to give them a rugosity the mean quadratic deviation of which lies between .06 and .7,u.
- a method according to claim 1 characterized in that the desired rugosity of the surface of the pieces is obtained by subjecting said surface to a galvanic treatment,
- the adherence to the base metal being obtained by a first deposit effected in normal conditions, followed by a second deposit effected in modified conditions so that this second deposit has a porous constitution and a rough surface.
- a method according to claim 1 characterized by using sawdust as a carrying mass for the lubricant.
- a method according to claim 1 characterized by using metallic balls as a granulated mass.
- a method according to claim 1 characterized in that, after the passage of the pieces in the centrifugal barrel, the pieces are dipped in a final bath and then dried, said bath comprising a little oil used in Watchmaking in dissolution in a solvent.
Landscapes
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Lubricants (AREA)
Description
United States Patent 17,2 7 Int. Cl. F1611 15/02; G40b 43/00 US. Cl. 184-1 12 Claims ABSTRACT OF THE DISCLOSURE A method for lubricating a timepiece movement. The surface of the pieces are given a, rugosity lying between a preferred range. The pieces are then treated in a centrifugal barrel wherein lubricant carried by a mass is deposited onto the pieces. A pressurizing mass fixes the solid lubricant onto the pieces.
The present invention relates to a method of lubricating a timepiece movement, more particularly its escapement.
The lubrication of the escapement of a timepiece is a problem for which an absolutely satisfactory solution has not yet been found. The generally used method consists in depositing by means of an oil-pike a drop of a suitable oil used in watchmaking on the impulse faces of the pallets of the lever. Owing to the successive passages of the teeth of the escape wheel, the drops of oil deposited on the pallets are swept, so that the major portion of the oil is carried outside the functional surfaces, where it can no longer take a part in the lubrication. If this oil excess were discharged into a zone where it would be localized, the harm would not be so great, after all, but it spreads over the whole piece in the form of a film which is more or less thick as the case may be and it reaches functional places on which it is indispensable to avoid the presence of a lubricant, or else the rate of the timepiece is greatly disturbed. It is obvious that numerous solutions have already been proposed to over come this drawback. However, none of them was up to now entirely satisfactory from a technical and economical point of view.
It has been proposed by Swiss Pat. No. 430,589 to apply onto the surface to be lubricated, by means of a micro spraying-pistol, a solid lubricant with a small admixture of a liquid lubricant. This method gives good results and overcomes the above-mentioned drawbacks occurring on applying a liquid lubricant. However, the application by means of a micro spraying-pistol is relatively long and, therefore, little economical. In addition, the thus deposited layer, while presenting a sufficient adherence for the function to be assumed, presents the disadvantage that it is damaged or disappears when it is brought into contact with a liquid such as a cleaning liquid. Due to this fact, the layer disappears on the first repairing of the watch.
The present invention aims at overcoming the several above-mentioned drawbacks. It has just been mentioned that the application of a solid lubricant gives good results in the watch. The lubricating method of the invention aims at increasing the adherence of a solid lubricant on the base material in such a manner that the lubricating layer cannot be destroyed by the conventional cleaning processes used in watchmaking. The present invention is based upon the property of certain solid lubricants of strongly adhering to the surface onto which they are applied, inasmuch as the application is made under a 3,511,340 PatentedMay 12, 1970 strong pressure and the finish of the surface is such that it promotes a catching of the lubricant.
The lubricating method of the invention comprises the steps of treating the surface of the pieces so as to give them a rugosity lying between .1 and 1,u, and then treating the pieces, brought into this state, into a centrifugal barrel the acceleration of which lies between 1 and 20g and in which are contained, besides the pieces' -to be treated, a solid lubricant in powder form, a carrying mass for the latter and a granulated mass adapted to produce a pressure for fixing the solid lubricant onto the pieces to be treated.
In order to obtain the desired rugosity of the surface to be lubricated, this surface may be subjected to different types of preparations. It is possible to give to the surface, by a mechanical process, a suitable rugosity, which may be obtained by a grinding, polishing, sanding or any other similar operation. Another process of preparing the surfaces may consist of 'a chemical or galvanic treatment. Among the former, let us cite, for instance, the phosphatation. It is also possible, in order to obtain the desired surface finish, to perform a chemical attack of the surface; in the case of pieces of brass, for instance, the desired rugosity may be obtained by an attack with an acid such as nitric acid or any other bath having the same action. In order to obviate changes in the dimensions of the pieces during the above-described processes, a galvanic process is preferably used. By Way of example, it is possible to proceed as follows: The piece to be treated being made of steel, a first deposit of gold of normal constitution is effected. This deposit serves for promoting the adherence of the next deposit of gold which is effected in such conditiousby reducing the contents of free cyanide of the bath and by adapting the current intensity-that it presents a porous constitution and a rough surface. The thus obtained rugosity is easily adjustable by choosing the conditions of the galvanic deposition. A gold deposit is preferably effected, since its coefficient of friction with respect to ruby is favourable, but it is also possible to use other metals such as rhodium, silver or alloys such as lead-tin or nickel-tin alloys.
Since the pieces to be treated are very small, it is important that the rugosity of the surface is adapted in such a manner that the geometry of the piece is not altered and the tolerances of manufacture are respected. For this purpose, the rugosity of the piece must lie between .1 and 1 (maximum height of the asperities) and its mean quadratic deviation preferably lies between .06 and .7,u.. The mean quadratic deviation is, as is wellknown, the square root of the arithmetic average of the squares of the deviations.
After the pieces have received the desired surface preparation, they are put in a centrifugal barrel. The latter is loaded with a mixture of a solid lubricant in powder form (e.g. molybdenum disulfide, graphite or tungsten diselenide), of a carrying mass for the latter (consisting for instance of a plastic material or simply of sawdust) and of a granulated mass, preferably metallic, acting as a charge and serving for producing, when the centrifugal barrel is running, a pressure sufiicient for causing the lubricant to penetrate into the surface of the piece and strongly adhere thereto. The said granulated mass may consist for instance of balls of lead or steel, having a diameter of l-2 mm.
The centrifugal barrel provokes accelerations lying between 1 and 20g (g=acceleration of gravity), the value of these accelerations and the diameter of the balls of the granulated mass being adapted to the mechanical resistance of the pieces to be treated.
After the passage of the pieces in the centrifugal barrel, they may be dipped in a final bath and then dried.
The final bath comprises, for example, 12% of oil used in watchmaking in dissolution in a solvent such as Freon or benzine. The latter treatment still improves the lubrication.
Pieces of escapement treated in the described conditions, have shown, upon tests made in laboratories, an excellent resistance to the action of the cleaning baths, as well as an excellent behaviour in the watch. The invention really brings a solution to the problem, up to now not satisfactorily solved, of the lubrication of the escapement. Other friction pieces of the watch, treated by this method, have also shown a most favorable behaviour, entirely competitive on the technical point of view with the conventional methods, with the additional advantage of a lubrication of greater duration.
What is claimed is:
1. A method of lubricating a timepiece movement, more particularly its escapement, characterized by treating the surface of the pieces so as to give them a rugosity lying between .1 and 1,11, and then treating the pieces, brought into this state, into a centrifugal barrel the acceleration of which lies between 1 and 20g and in which are contained, besides the pieces to be treated, a solid lubricant in powder form, a carrying mass for the latter and a granulated mass adapted to produce a pressure for fixing the solid lubricant onto the pieces to be treated.
2. A method according to claim 1, characterized by treating the surface of the pieces so as to give them a rugosity the mean quadratic deviation of which lies between .06 and .7,u.
3. A method according to claim 1, characterized in that the desired rugosity of the surface of the pieces is obtained by subjecting said surface to a mechanical treatment.
4. A method according to claim 1, characterized in that the desired rugosity of the surface of the pieces is obtained by subjecting said surface to a chemical treatment.
5. A method according to claim 1, characterized in that the desired rugosity of the surface of the pieces is obtained by subjecting said surface to a galvanic treatment,
the adherence to the base metal being obtained by a first deposit effected in normal conditions, followed by a second deposit effected in modified conditions so that this second deposit has a porous constitution and a rough surface.
5 6. A method according to claim 1, characterized by using molybdenum disulfide as a solid lubricant.
7. A method according to claim 1, characterized by using graphite as a solid lubricant.
1O 8. A method according to claim 1, characterized by using tungsten diselenide as a solid lubricant.
9. A method according to claim 1, characterized by using a plastic material in powder form as a carrying mass for the lubricant.
10. A method according to claim 1, characterized by using sawdust as a carrying mass for the lubricant.
11. A method according to claim 1, characterized by using metallic balls as a granulated mass.
12. A method according to claim 1, characterized in that, after the passage of the pieces in the centrifugal barrel, the pieces are dipped in a final bath and then dried, said bath comprising a little oil used in Watchmaking in dissolution in a solvent.
References Cited UNITED STATES PATENTS 1,129,304 2/1915 Loudenbeck 184l 2,993,567 7/1961 Schachner 1841 3,225,866 12/1965 Bernett et a1 l841 FOREIGN PATENTS 847,541 9/1960 Great Britain.
877,122 9/1961 Great Britain.
ROBERT A. OLEARY, Primary Examiner M. A. ANTONAKAS, Assistant Examiner US. Cl. X.R. 58121
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH1724367A CH493880A (en) | 1967-12-09 | 1967-12-09 | Lubrication process for timepieces, in particular for the escapement |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US3511340A true US3511340A (en) | 1970-05-12 |
Family
ID=4423875
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US777455A Expired - Lifetime US3511340A (en) | 1967-12-09 | 1968-11-20 | Method of lubricating a timepiece movement |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US3511340A (en) |
| CH (2) | CH1724367A4 (en) |
| DE (1) | DE1808687A1 (en) |
| GB (1) | GB1213836A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3694885A (en) * | 1969-07-11 | 1972-10-03 | Far Fab Assortiments Reunies | Method of manufacturing an escapement lever for a timepiece |
| US3738101A (en) * | 1969-07-11 | 1973-06-12 | Far Fab Assortiments Reunies | Timepiece escapement lever |
| US3826076A (en) * | 1972-07-19 | 1974-07-30 | Fab D Assortiments Reunies | Anchor escapement for time-measuring instruments |
| US4123897A (en) * | 1975-06-04 | 1978-11-07 | Kabushiki Kaisha Daini Seikosha | Second jumper spring |
| EP0438775A3 (en) * | 1990-01-22 | 1991-11-13 | General Electric Company | Lubricated bearing retainer for x-ray tube |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2009210552A (en) * | 2008-02-07 | 2009-09-17 | Seiko Epson Corp | Contact component and timepiece |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1129304A (en) * | 1910-08-01 | 1915-02-23 | Westinghouse Air Brake Co | Method of lubrication. |
| GB847541A (en) * | 1957-12-05 | 1960-09-07 | English Electric Co Ltd | Improvements in and relating to dry lubrication |
| US2993567A (en) * | 1957-06-07 | 1961-07-25 | Straumann Inst Ag | Dry lubrication |
| US3225866A (en) * | 1963-11-19 | 1965-12-28 | Marianne K Bernett | Lubrication system for fine mechanisms |
-
1967
- 1967-12-09 CH CH1724367D patent/CH1724367A4/xx unknown
- 1967-12-09 CH CH1724367A patent/CH493880A/en not_active IP Right Cessation
-
1968
- 1968-11-13 DE DE19681808687 patent/DE1808687A1/en active Pending
- 1968-11-20 US US777455A patent/US3511340A/en not_active Expired - Lifetime
- 1968-11-22 GB GB55431/68A patent/GB1213836A/en not_active Expired
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1129304A (en) * | 1910-08-01 | 1915-02-23 | Westinghouse Air Brake Co | Method of lubrication. |
| US2993567A (en) * | 1957-06-07 | 1961-07-25 | Straumann Inst Ag | Dry lubrication |
| GB877122A (en) * | 1957-06-07 | 1961-09-13 | Straumann Inst Ag | Improvements in dry-lubricated components |
| GB847541A (en) * | 1957-12-05 | 1960-09-07 | English Electric Co Ltd | Improvements in and relating to dry lubrication |
| US3225866A (en) * | 1963-11-19 | 1965-12-28 | Marianne K Bernett | Lubrication system for fine mechanisms |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3694885A (en) * | 1969-07-11 | 1972-10-03 | Far Fab Assortiments Reunies | Method of manufacturing an escapement lever for a timepiece |
| US3738101A (en) * | 1969-07-11 | 1973-06-12 | Far Fab Assortiments Reunies | Timepiece escapement lever |
| US3826076A (en) * | 1972-07-19 | 1974-07-30 | Fab D Assortiments Reunies | Anchor escapement for time-measuring instruments |
| US4123897A (en) * | 1975-06-04 | 1978-11-07 | Kabushiki Kaisha Daini Seikosha | Second jumper spring |
| EP0438775A3 (en) * | 1990-01-22 | 1991-11-13 | General Electric Company | Lubricated bearing retainer for x-ray tube |
Also Published As
| Publication number | Publication date |
|---|---|
| GB1213836A (en) | 1970-11-25 |
| DE1808687A1 (en) | 1969-08-21 |
| CH493880A (en) | 1970-01-30 |
| CH1724367A4 (en) | 1970-01-30 |
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