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US20130091913A1 - Method of making an acid-absorbing biosolid composition - Google Patents

Method of making an acid-absorbing biosolid composition Download PDF

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Publication number
US20130091913A1
US20130091913A1 US13/275,153 US201113275153A US2013091913A1 US 20130091913 A1 US20130091913 A1 US 20130091913A1 US 201113275153 A US201113275153 A US 201113275153A US 2013091913 A1 US2013091913 A1 US 2013091913A1
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US
United States
Prior art keywords
acid
absorbing
biosolid
composition
making
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
US13/275,153
Inventor
Abdullah A. Al-Yateem
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Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to US13/275,153 priority Critical patent/US20130091913A1/en
Priority to US13/584,344 priority patent/US8545777B2/en
Publication of US20130091913A1 publication Critical patent/US20130091913A1/en
Abandoned legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/38Removing components of undefined structure
    • B01D53/40Acidic components
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/3078Thermal treatment, e.g. calcining or pyrolizing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/3085Chemical treatments not covered by groups B01J20/3007 - B01J20/3078
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05DINORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D3/00Calcareous fertilisers
    • C05D3/02Calcareous fertilisers from limestone, calcium carbonate, calcium hydrate, slaked lime, calcium oxide, waste calcium products
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F7/00Fertilisers from waste water, sewage sludge, sea slime, ooze or similar masses
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2253/00Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/25Coated, impregnated or composite adsorbents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00Aspects relating to sorbent materials
    • B01J2220/40Aspects relating to the composition of sorbent or filter aid materials
    • B01J2220/48Sorbents characterised by the starting material used for their preparation
    • B01J2220/4875Sorbents characterised by the starting material used for their preparation the starting material being a waste, residue or of undefined composition
    • B01J2220/4887Residues, wastes, e.g. garbage, municipal or industrial sludges, compost, animal manure; fly-ashes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/10Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
    • Y02A40/20Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00Technologies for the production of fuel of non-fossil origin
    • Y02E50/30Fuel from waste, e.g. synthetic alcohol or diesel
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency
    • Y02P20/133Renewable energy sources, e.g. sunlight

Definitions

  • the present invention relates to recycled biosolids, biomasses and the like, and particularly to a method of making an acid-absorbing biosolid composition for removing acidic gasses from gas streams produced by the chemical treatment of sewage sludge.
  • the method of making an acid-absorbing biosolid composition provides a method for the use of recycled materials to produce an acid-absorbing composition that may subsequently be recycled for use as a fertilizer after absorbing the acidic gas.
  • the method includes the steps of: collecting a sewage sludge; drying the sewage sludge to remove water therefrom to form dried sludge; adding hydrochloric acid to the dried sludge to form a liquid intermediary product; heating the liquid intermediary product to produce a dried porous biomass; and mixing inorganic waste material with the dried porous biomass to produce an acid-absorbing biosolid composition.
  • the acid-absorbing biosolid composition may be placed in a gas flow to absorb an acidic component therefrom; and then used as fertilizer following absorption of the acidic component from the gas flow.
  • the method of making an acid-absorbing biosolid composition provides a method for the use of recycled materials to produce an acid-absorbing composition that may subsequently be recycled for use as a fertilizer after absorbing the acidic gas.
  • sewage sludge is collected.
  • the sewage sludge forms the primary component of the recycled acid-absorbing biosolid composition.
  • the sewage sludge should have a pH of about 4.0. If the collected sludge does not naturally have a pH of about 4.0, then the sewage sludge may be treated with an appropriate quantity of acid or base to bring the pH level to about 4.0.
  • the sewage sludge is then dried to completely remove water therefrom. This forms a dried sludge product.
  • the drying is preferably performed through the application of heat in a temperature range of about 600° C. to about 1,000° C.
  • hydrochloric acid is added to the dried sludge to form a liquid intermediary product.
  • the treatment with the hydrochloric acid, or any other suitable type of acid may include stirring or any other suitable type of agitation required to adequately mix the acid with the sludge. This mixing is preferably performed until such time as the pH of the mixture assumes a steady value of between about 1.0 and 4.0.
  • the liquid intermediary product is then, once again, heated to produce a dried porous biomass.
  • the hydrochloric acid is added to increase and activate pores in the dried sludge. These pores are used in the absorption of acidic pollution gases.
  • the dried porous biomass is mixed with an inorganic waste material to produce the acid-absorbing biosolid composition.
  • the inorganic waste material constitutes about 45 wt % of the acid-absorbing biosolid composition.
  • the inorganic material may be magnesium waste, calcium waste, iron waste, iodine waste, rocks, sand, or combinations thereof.
  • organic waste materials such as wood powder, may also be added. It should be understood that any suitable type of waste material may be utilized, such as recyclable wastes produced by distillation plants.
  • the acid-absorbing biosolid composition is placed in a gas flow to absorb an acidic component therefrom.
  • An example of such use is placing the acid-absorbing biosolid composition in a wet gas flow and extracting a sulfur-containing component from the wet gas flow, such as hydrogen sulfide or sulfur dioxide.
  • the acid-absorbing biosolid composition oxidizes the sulfur-containing gases, forming organic and inorganic sulfates of the type used in fertilizers.
  • the acid-absorbing biosolid composition may be used as a fertilizer.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Inorganic Chemistry (AREA)
  • Fertilizers (AREA)

Abstract

The method of making an acid-absorbing biosolid composition provides a method for the use of recycled materials to produce an acid-absorbing composition that may then be recycled as a fertilizer after absorbing the acid. The method includes the steps of: collecting sewage sludge; drying the sewage sludge to remove water therefrom to form dried sludge; adding hydrochloric acid to the dried sludge to form a liquid intermediary product; heating the liquid intermediary product to produce a dried porous biomass; and mixing inorganic waste material with the dried porous biomass to produce the acid-absorbing biosolid composition. Thereafter, the acid-absorbing biosolid composition may be placed in a gas flow to absorb an acidic component therefrom; and then recycled for use as fertilizer following absorption of the acidic component from the gas flow.

Description

    BACKGROUND OF THE INVENTION
  • 1. Field of the Invention
  • The present invention relates to recycled biosolids, biomasses and the like, and particularly to a method of making an acid-absorbing biosolid composition for removing acidic gasses from gas streams produced by the chemical treatment of sewage sludge.
  • 2. Description of the Related Art
  • The production of useful biosolids and biomasses from sewage sludge is known. In one such prior method, dewatered sewage sludge is dried to form a granulated organic fertilizer, which is then pyrolized to form a porous end product. Although this and similar fertilizers may also be used for a wide range of applications, they suffer from manufacturing methods that require them to maintain a basic pH throughout their manufacture and usage. This requires that the manufacturing method be relatively complex and inefficient in terms of both cost and manufacturing time. Given that it is desirable to recycle sewage sludge in order to decrease overall energy expenditures, and also to decrease chemical treatments of the sludge, which may have a negative environmental impact, a process that does not require such careful maintenance of a basic pH throughout would be desirable. Furthermore, it is desirable to provide a substance that removes hydrogen sulfide, sulfur dioxide, and other sulfur-containing gases from the gases produced during the chemical treatment of sewage sludge to reduce air pollution that might otherwise contribute to acid rain,
  • Thus, a method of making an acid-absorbing biosolid composition solving the aforementioned problems is desired.
  • SUMMARY OF THE INVENTION
  • The method of making an acid-absorbing biosolid composition provides a method for the use of recycled materials to produce an acid-absorbing composition that may subsequently be recycled for use as a fertilizer after absorbing the acidic gas. The method includes the steps of: collecting a sewage sludge; drying the sewage sludge to remove water therefrom to form dried sludge; adding hydrochloric acid to the dried sludge to form a liquid intermediary product; heating the liquid intermediary product to produce a dried porous biomass; and mixing inorganic waste material with the dried porous biomass to produce an acid-absorbing biosolid composition. Thereafter, the acid-absorbing biosolid composition may be placed in a gas flow to absorb an acidic component therefrom; and then used as fertilizer following absorption of the acidic component from the gas flow.
  • These and other features of the present invention will become readily apparent upon further review of the following specification.
  • DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS
  • The method of making an acid-absorbing biosolid composition provides a method for the use of recycled materials to produce an acid-absorbing composition that may subsequently be recycled for use as a fertilizer after absorbing the acidic gas. Initially, sewage sludge is collected. The sewage sludge forms the primary component of the recycled acid-absorbing biosolid composition. Preferably the sewage sludge should have a pH of about 4.0. If the collected sludge does not naturally have a pH of about 4.0, then the sewage sludge may be treated with an appropriate quantity of acid or base to bring the pH level to about 4.0.
  • The sewage sludge is then dried to completely remove water therefrom. This forms a dried sludge product. The drying is preferably performed through the application of heat in a temperature range of about 600° C. to about 1,000° C. Following the drying of the sewage sludge to completely remove the water therefrom, hydrochloric acid is added to the dried sludge to form a liquid intermediary product. The treatment with the hydrochloric acid, or any other suitable type of acid, may include stirring or any other suitable type of agitation required to adequately mix the acid with the sludge. This mixing is preferably performed until such time as the pH of the mixture assumes a steady value of between about 1.0 and 4.0. The liquid intermediary product is then, once again, heated to produce a dried porous biomass. The hydrochloric acid is added to increase and activate pores in the dried sludge. These pores are used in the absorption of acidic pollution gases.
  • The dried porous biomass is mixed with an inorganic waste material to produce the acid-absorbing biosolid composition. Preferably, the inorganic waste material constitutes about 45 wt % of the acid-absorbing biosolid composition. The inorganic material may be magnesium waste, calcium waste, iron waste, iodine waste, rocks, sand, or combinations thereof. In addition to the inorganic waste material, organic waste materials, such as wood powder, may also be added. It should be understood that any suitable type of waste material may be utilized, such as recyclable wastes produced by distillation plants.
  • In use, the acid-absorbing biosolid composition is placed in a gas flow to absorb an acidic component therefrom. An example of such use is placing the acid-absorbing biosolid composition in a wet gas flow and extracting a sulfur-containing component from the wet gas flow, such as hydrogen sulfide or sulfur dioxide. The acid-absorbing biosolid composition oxidizes the sulfur-containing gases, forming organic and inorganic sulfates of the type used in fertilizers. Following absorption of the acidic component from the gas flow, the acid-absorbing biosolid composition may be used as a fertilizer.
  • It is to be understood that the present invention is not limited to the embodiments described above, but encompasses any and all embodiments within the scope of the following claims.

Claims (11)

I claim:
1. A method of making an acid-absorbing biosolid composition, comprising the steps of:
collecting sewage sludge;
drying the sewage sludge to remove water therefrom to form dried sludge;
adding an acid to the dried sludge to form a liquid intermediary product;
heating the liquid intermediary product to produce a dried, porous biomass; and
mixing inorganic waste material with the dried porous biomass to produce an acid-absorbing biosolid composition.
2. The method of making an acid-absorbing biosolid composition as recited in claim 1, further comprising the step of adjusting the sewage sludge to a pH of about 4.0 prior to said drying step.
3. The method of making an acid-absorbing biosolid composition as recited in claim 2, wherein said step of adding the acid to the dried sludge comprises adding hydrochloric acid to the dried sludge to form the liquid intermediary product.
4. The method of making an acid-absorbing biosolid composition as recited in claim 3, wherein the hydrochloric acid is dilute hydrochloric acid.
5. The method of making an acid-absorbing biosolid composition as recited in claim 1, wherein said step of drying the sewage sludge comprises heating the sewage sludge to a temperature between about 600° C. and about 1,000° C.
6. The method of making an acid-absorbing biosolid composition as recited in claim 1, wherein said step of mixing the inorganic waste material with the dried porous biomass comprises adding the inorganic waste material to the dried porous biomass so that the inorganic waste material constitutes about 45 wt % of the acid-absorbing biosolid composition.
7. The method of making an acid-absorbing biosolid composition as recited in claim 1, wherein the inorganic waste material comprises at least one material selected from the group consisting of magnesium waste, calcium waste, iron waste, iodine waste, rocks, and sand.
8. The method of making an acid-absorbing biosolid composition as recited in claim 1, further comprising the step of adding organic waste material to the dried porous biomass.
9. The method of making an acid absorbing biosolid composition as recited in claim 8, wherein said step of adding the organic waste material to the dried porous biomass comprises adding wood powder to the dried porous biomass.
10. A method using an acid-absorbing biosolid composition prepared according to claim 1, comprising the step of placing the acid-absorbing biosolid composition in a gas flow to absorb an acidic component therefrom.
11. A method of recycling the used acid-absorbing biosolid composition according to claim 10, comprising the step of recycling the acid-absorbing biosolid composition as fertilizer following absorption of the acidic component from the gas flow.
US13/275,153 2011-10-17 2011-10-17 Method of making an acid-absorbing biosolid composition Abandoned US20130091913A1 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
US13/275,153 US20130091913A1 (en) 2011-10-17 2011-10-17 Method of making an acid-absorbing biosolid composition
US13/584,344 US8545777B2 (en) 2011-10-17 2012-08-13 Method of making an acid-absorbing biosolid composition

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US13/584,344 Expired - Fee Related US8545777B2 (en) 2011-10-17 2012-08-13 Method of making an acid-absorbing biosolid composition

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8968440B1 (en) * 2014-02-05 2015-03-03 Phosfix Fertilizer & Soil Amendment LLC Fertilizer production

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104888696B (en) * 2015-04-29 2017-05-03 北京绿洁美科技有限公司 Preparation method of defluorination material based on biomass solid wastes

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20050039508A1 (en) * 2003-05-27 2005-02-24 Burnham Jeffrey C. Organic recycling with metal addition
WO2006091645A2 (en) * 2005-02-23 2006-08-31 Blue Water Investments Manufacturing of bioorganic-augmented high nitrogen-containing inorganic fertilizer
US8192519B2 (en) * 2005-03-09 2012-06-05 Vitag Corporation Beneficiated, heat-dried biosolid pellets
US7476372B2 (en) * 2006-06-28 2009-01-13 Holloman Corporation Flue gas scrubbing process utilizing biosolids
MX2009001945A (en) * 2006-08-23 2009-04-14 Carbon Solutions Inc Acid-impregnated activated carbon and methods of forming and using the same.
WO2008101250A1 (en) * 2007-02-16 2008-08-21 Vitag Corporation Process for treating sludge and manufacturing bioorganically-augmented high nitrogen-containing inorganic fertilizer

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8968440B1 (en) * 2014-02-05 2015-03-03 Phosfix Fertilizer & Soil Amendment LLC Fertilizer production

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Publication number Publication date
US20130091914A1 (en) 2013-04-18
US8545777B2 (en) 2013-10-01

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