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US20080202627A1 - Dosing System and Method - Google Patents

Dosing System and Method Download PDF

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Publication number
US20080202627A1
US20080202627A1 US12/020,029 US2002908A US2008202627A1 US 20080202627 A1 US20080202627 A1 US 20080202627A1 US 2002908 A US2002908 A US 2002908A US 2008202627 A1 US2008202627 A1 US 2008202627A1
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Prior art keywords
container
valve
bittering agent
dose
module
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Abandoned
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US12/020,029
Inventor
Gregory V. Mas
Dermot Nolan McLeer
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Falcon Safety Products Inc
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Individual
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Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to US12/020,029 priority Critical patent/US20080202627A1/en
Priority to PCT/US2008/054857 priority patent/WO2008103978A2/en
Assigned to FALCON SAFETY PRODUCTS, INC. reassignment FALCON SAFETY PRODUCTS, INC. ASSIGNMENT OF ASSIGNORS INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: MAS, GREGORY V.
Publication of US20080202627A1 publication Critical patent/US20080202627A1/en
Abandoned legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B65CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65BMACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
    • B65B31/00Packaging articles or materials under special atmospheric or gaseous conditions; Adding propellants to aerosol containers
    • B65B31/003Adding propellants in fluid form to aerosol containers

Definitions

  • Embodiments of the invention relate to systems and methods for introducing chemical agents into aerosol containers.
  • Liquefied-gas aerosol dusters provide a safe, useful, convenient, and economically efficient means of cleaning dust and debris from hard to reach places, where it can be harmful or detrimental. This can be especially true for the multitude of electronic equipment used today, where small foreign particles can render expensive equipment inoperable or shorten its useful life.
  • These aerosol dusters provide an easily available source of pressurized gas that can be used to remove such debris.
  • the liquefied gas and aerosol package components can be chosen so as to deliver a pressurized burst of gas in a preferred cleaning pattern.
  • the aerosol valve and actuator can be configured to deliver the appropriate amount of gas at the right pressure in a range from broad to pinpoint spray patterns. Using liquefied gases provides an ample supply of material for a large number of cleaning tasks in a compact package.
  • duster products provide a safe and valuable function to the consumer, but sometimes are involved in inhalation abuse incidents, like numerous other consumer products.
  • bittering additive agent also referred to herein as a bittering agent, or bitterant
  • a bittering additive agent also referred to herein as a bittering agent, or bitterant
  • a dosing module, valve module and crimping module are all included on a single, automated apparatus. Because of this orientation, the time from when the bittering agent is added to the container, until a valve is placed on the container and subsequently crimped, is relatively short. For this reason, there is relatively little time when the bittering agent is exposed to the ambient environment.
  • the bittering agent by its nature, has a unsavory aroma and/or taste, and minimizing such exposure reduces the unwanted introduction of bittering agent to facility workers and the general facility environment.
  • embodiments of the invention provide for an efficient system and method for adding a bittering agent to aerosol containers.
  • Embodiments can include a method for introducing a bittering agent into an aerosol container.
  • the method can include the steps of: adding a dose of the bittering agent in the container, positioning a valve on the container, crimping the valve to the container, and adding an aerosol propellant to the container.
  • the method can further include the step of adding an actuator to the container.
  • the method can further include the step of testing the container in a bath.
  • the steps of adding a dose of the bittering agent in the container, positioning a valve on the container and crimping the valve onto the container can be performed by an automated device.
  • the time interval between adding a dose of the bittering agent in the container and positioning a valve on the container can be in the range of about 1 to 5 seconds.
  • a distance that the container travels between the steps of adding a dose of the bittering agent in the container and positioning a valve on the container can be in the range of about 2 to 16 inches.
  • Embodiments can include an apparatus for introducing a bittering agent into an aerosol container.
  • the apparatus can include a turntable for positioning the container, a dosing module for adding a dose of the bittering agent in the container when the turntable positions the container proximate the dosing module, a valve module for positioning a valve on the container when the turntable positions the container proximate the valve module, and a crimping module for crimping the valve to the container when the turntable positions the container proximate the valve module.
  • the time interval between when the container is positioned proximate the dosing module and when the container is positioned proximate the valve module can be in the range of about 1 to 5 seconds.
  • a distance between where the container is positioned proximate the dosing module and where the container is positioned proximate the valve module can be in the range of about 2 to 16 inches.
  • FIG. 1 is a flow diagram illustrating certain embodiments of a method of adding a bittering agent to a container
  • FIG. 2 is a schematic diagram illustrating a system for implementing the method shown in FIG. 1 ;
  • FIG. 3 is a schematic diagram illustrating a portion of system for implementing the method shown in FIG. 1 ;
  • FIG. 4 is a more detailed view of the portion of the system shown in FIG. 3 ;
  • FIG. 5 is a schematic diagram illustrating a portion of system for implementing the method shown in FIG. 1 .
  • Embodiments of the invention relate to a system and method for introducing a chemical agent into a container.
  • a method for adding a bittering agent to an aerosol container can include depositing a dose of bittering agent into a container (step S 10 ), adding a valve to the container (step S 12 ), and crimping the valve to the container (step S 14 ).
  • a dose module 220 can be used to add a dose of a bittering agent into a container 210 .
  • a valve module 230 can position a valve on the container 210 .
  • a crimp module 240 can crimp the valve to the container 210 .
  • a propellant module 250 can be used to add propellant to the container 210 .
  • the container 210 can be tested in a bath module 260 .
  • an actuator can be placed on the container 210 by the actuator module 270 .
  • Dose module 220 can include a dispenser and a syringe 222 , coupled by an air line.
  • the dispenser 224 causes a bitterent placed in the syringe 222 to be added to the container 210 in a relatively precisely determined amount.
  • dispenser 224 can be triggered, via, for example, switches, to initiate the addition of the dose of bitterent when container 210 is in a predetermined position.
  • position sensor mechanism 226 can include a combination of one or more limit switches, spring return cylinder switches, and track switches.
  • portions of the position sensor mechanism 226 , as well as the dispenser 224 can operate with the use of air system.
  • dose module 224 can include two dispensers 224 , two syringes 222 and two position sensor mechanisms 226 such that two containers can be dosed with bitterent simultaneously, or substantially simultaneously.
  • FIG. 5 there is shown a top partial schematic view of an embodiment of a system as described above.
  • Containers 221 are positioned on turntable module 300 .
  • Dispensers 224 initiate the dosing of bitterent from syringes 222 .
  • the turntable then indexes the containers 221 to the valve placer module 230 , where a valve is positioned on each of containers 221 .
  • the turntable module 300 indexes the containers to a position proximate the crimper module 240 .
  • the valves can be crimped to the containers 221 .
  • the syringe 222 of dosing module 220 , valve placer module 230 and crimper module 240 are all included on a single, automated apparatus. Because of this orientation, the time from when the bittering agent is added to the container 221 , until a valve is placed on the container and subsequently crimped, is relatively short. For this reason, there is relatively little time when the bittering agent is exposed to the ambient environment.
  • the bittering agent by its nature, has an unsavory aroma and/or taste, and minimizing such exposure reduces the unwanted introduction of bittering agent to facility workers and the general facility environment.
  • time T 1 (the time from when the container 221 is at the dosing module 220 to when the container is at the valve placer module 230 ) can preferably be in the range of 1 to 5 seconds, more preferably in the range of 1 to 3 seconds, and most preferably, about 2.5 seconds.
  • Time T 2 (the time from when the container 221 is at the dosing module 220 to when the container is at the crimper module 240 ) can preferably be in the range of 4 to 10 seconds, more preferably in the range of 6 to 8 seconds, and most preferably, about 7 seconds. In other embodiments, other times can be used.
  • Distance D 1 (the distance between when the container 221 is at the dosing module 220 to when the container is at the valve placer module 230 ) can preferably be in the range of 2 to 16 inches, more preferably in the range of 4 to 8 inches, and most preferably, about 6.25 inches.
  • Distance D 2 (the distance between when the container 221 is at the dosing module 220 to when the container is at the crimper module 240 ) can preferably be in the range of 5 to 11 inches, more preferably in the range of 7 to 9 inches, and most preferably, about 8.75 inches. In other embodiments, other distances can be used. These distances are measured along the generally arcuate path traveled by the containers while moving about the turntable.
  • Container 221 can be made of tinplate, aluminum, glass, or other materials as is known to those of skill in the art.
  • the bittering agent can be denatonium benzoate, or other bittering agents, as are known to those of skill in the art.
  • the propellant can be a liquefied gas, for use with aerosol spray containers, as is known to those of skill in the art.
  • a liquefied aerosol dusting composition can be used, as described in U.S. patent application Ser. No. 11/895,070, filed on Aug. 22, 2007, and titled “A liquefied-gas Aerosol Dusting Composition Containing Denatonium Benzoate,” the contents of which are hereby incorporated by reference herein.
  • the dispenser 224 of dose module 220 can be an Ultra 2400 workstation dispenser, as produced by EFD Inc., of East Buffalo, R.I.
  • the Ultra 2400 workstation includes a digital display, an air management system, and precision time increment adjustment capabilities for precise dose deposit controls.
  • turntable 300 can use a rotary index mechanism and aerosol filling system as provided by Terco Inc., of Bloomington, Ill.
  • dispenser 224 and turntable 300 have been coupled such that dispenser 224 works cooperatively and automatically with turntable 300 .
  • actuation of the EFD fluid dispenser 221 is coupled to the position of container 221 , thus minimizing the possibility of accidental discharge of bitterant from syringe 222 .
  • a propellant can be added to the container (step S 16 ).
  • the container can be tested in a bath (step S 18 ), and, an actuator can be added to the container (step S 20 ).

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  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Nozzles (AREA)
  • Containers And Packaging Bodies Having A Special Means To Remove Contents (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

A method for introducing a bittering agent into an aerosol container. The method can include the steps of: adding a dose of the bittering agent in the container, positioning a valve on the container, crimping the valve to the container, and adding an aerosol propellant to the container. The method can further include the step of adding an actuator to the container. The method can further include the step of testing the container in a bath. The steps of adding a dose of the bittering agent in the container and positioning a valve on the container can be performed by an automated device.

Description

    CROSS-REFERENCE TO RELATED APPLICATION
  • This application claims the benefit of U.S. Provisional Patent Application No. 60/891,426, filed on Feb. 23, 2007, the contents of which are hereby incorporated by reference herein.
  • FIELD OF THE INVENTION
  • Embodiments of the invention relate to systems and methods for introducing chemical agents into aerosol containers.
  • BACKGROUND OF THE INVENTION
  • Liquefied-gas aerosol dusters provide a safe, useful, convenient, and economically efficient means of cleaning dust and debris from hard to reach places, where it can be harmful or detrimental. This can be especially true for the multitude of electronic equipment used today, where small foreign particles can render expensive equipment inoperable or shorten its useful life. These aerosol dusters provide an easily available source of pressurized gas that can be used to remove such debris. Packaged in appropriately designed aerosol cans, the liquefied gas and aerosol package components can be chosen so as to deliver a pressurized burst of gas in a preferred cleaning pattern. The aerosol valve and actuator can be configured to deliver the appropriate amount of gas at the right pressure in a range from broad to pinpoint spray patterns. Using liquefied gases provides an ample supply of material for a large number of cleaning tasks in a compact package.
  • Manufacturers and suppliers of these products expend significant resources and energy toward good product stewardship with goals of providing products that are safe when used as intended. Thus, these duster products provide a safe and valuable function to the consumer, but sometimes are involved in inhalation abuse incidents, like numerous other consumer products.
  • Accordingly, there is a need for a liquefied-gas aerosol dusting composition with a bittering additive agent (also referred to herein as a bittering agent, or bitterant) that does not interfere with normal product use but is detectable in an inhalation abusive scenario so as to potentially discourage the practice. Consequently, there is a need in the art for a system and method for successfully adding bittering agents to an aerosol container.
  • SUMMARY OF THE INVENTION
  • The above-described problems are addressed and a technical solution is achieved in the art by systems and methods for introducing a chemical agent into a container.
  • Beneficially, a dosing module, valve module and crimping module are all included on a single, automated apparatus. Because of this orientation, the time from when the bittering agent is added to the container, until a valve is placed on the container and subsequently crimped, is relatively short. For this reason, there is relatively little time when the bittering agent is exposed to the ambient environment. The bittering agent, by its nature, has a unsavory aroma and/or taste, and minimizing such exposure reduces the unwanted introduction of bittering agent to facility workers and the general facility environment. In addition, embodiments of the invention provide for an efficient system and method for adding a bittering agent to aerosol containers.
  • Embodiments can include a method for introducing a bittering agent into an aerosol container. The method can include the steps of: adding a dose of the bittering agent in the container, positioning a valve on the container, crimping the valve to the container, and adding an aerosol propellant to the container. The method can further include the step of adding an actuator to the container. The method can further include the step of testing the container in a bath. The steps of adding a dose of the bittering agent in the container, positioning a valve on the container and crimping the valve onto the container can be performed by an automated device.
  • The time interval between adding a dose of the bittering agent in the container and positioning a valve on the container can be in the range of about 1 to 5 seconds.
  • A distance that the container travels between the steps of adding a dose of the bittering agent in the container and positioning a valve on the container can be in the range of about 2 to 16 inches.
  • Embodiments can include an apparatus for introducing a bittering agent into an aerosol container. The apparatus can include a turntable for positioning the container, a dosing module for adding a dose of the bittering agent in the container when the turntable positions the container proximate the dosing module, a valve module for positioning a valve on the container when the turntable positions the container proximate the valve module, and a crimping module for crimping the valve to the container when the turntable positions the container proximate the valve module.
  • The time interval between when the container is positioned proximate the dosing module and when the container is positioned proximate the valve module can be in the range of about 1 to 5 seconds.
  • A distance between where the container is positioned proximate the dosing module and where the container is positioned proximate the valve module can be in the range of about 2 to 16 inches.
  • BRIEF DESCRIPTION OF THE DRAWINGS
  • Embodiments of the invention will be more readily understood from the detailed description of exemplary embodiments presented below considered in conjunction with the attached drawings, of which:
  • FIG. 1 is a flow diagram illustrating certain embodiments of a method of adding a bittering agent to a container;
  • FIG. 2 is a schematic diagram illustrating a system for implementing the method shown in FIG. 1;
  • FIG. 3 is a schematic diagram illustrating a portion of system for implementing the method shown in FIG. 1;
  • FIG. 4 is a more detailed view of the portion of the system shown in FIG. 3; and
  • FIG. 5 is a schematic diagram illustrating a portion of system for implementing the method shown in FIG. 1.
  • It is to be understood that the attached drawings are for purposes of illustrating the concepts of the invention and may not be to scale.
  • DETAILED DESCRIPTION OF THE INVENTION
  • Embodiments of the invention relate to a system and method for introducing a chemical agent into a container.
  • With reference to FIG. 1, in some embodiments, a method for adding a bittering agent to an aerosol container can include depositing a dose of bittering agent into a container (step S10), adding a valve to the container (step S12), and crimping the valve to the container (step S14).
  • With reference to FIG. 2, a system, shown in schematic form, in accordance with some embodiments can be used to perform the above-described method. A dose module 220 can be used to add a dose of a bittering agent into a container 210. Next, a valve module 230 can position a valve on the container 210. A crimp module 240 can crimp the valve to the container 210. A propellant module 250 can be used to add propellant to the container 210. The container 210 can be tested in a bath module 260. Finally, an actuator can be placed on the container 210 by the actuator module 270.
  • With reference to FIGS. 3 and 4, an embodiment is shown in more detailed schematic form. Dose module 220 can include a dispenser and a syringe 222, coupled by an air line. The dispenser 224 causes a bitterent placed in the syringe 222 to be added to the container 210 in a relatively precisely determined amount. In some embodiments, dispenser 224 can be triggered, via, for example, switches, to initiate the addition of the dose of bitterent when container 210 is in a predetermined position. Whether container 210 is in a predetermined position for dosing can be signaled by position sensor mechanism 226, which can include a combination of one or more limit switches, spring return cylinder switches, and track switches. In some embodiments, portions of the position sensor mechanism 226, as well as the dispenser 224, can operate with the use of air system.
  • In some embodiments, dose module 224 can include two dispensers 224, two syringes 222 and two position sensor mechanisms 226 such that two containers can be dosed with bitterent simultaneously, or substantially simultaneously.
  • With reference to FIG. 5, there is shown a top partial schematic view of an embodiment of a system as described above. Containers 221 are positioned on turntable module 300. Dispensers 224 initiate the dosing of bitterent from syringes 222. The turntable then indexes the containers 221 to the valve placer module 230, where a valve is positioned on each of containers 221. Next, the turntable module 300 indexes the containers to a position proximate the crimper module 240. At the crimper module 240, the valves can be crimped to the containers 221.
  • Thus, the syringe 222 of dosing module 220, valve placer module 230 and crimper module 240 are all included on a single, automated apparatus. Because of this orientation, the time from when the bittering agent is added to the container 221, until a valve is placed on the container and subsequently crimped, is relatively short. For this reason, there is relatively little time when the bittering agent is exposed to the ambient environment. The bittering agent, by its nature, has an unsavory aroma and/or taste, and minimizing such exposure reduces the unwanted introduction of bittering agent to facility workers and the general facility environment.
  • Specifically, with reference to FIGS. 1, 2 and 5, time T1 (the time from when the container 221 is at the dosing module 220 to when the container is at the valve placer module 230) can preferably be in the range of 1 to 5 seconds, more preferably in the range of 1 to 3 seconds, and most preferably, about 2.5 seconds. Time T2 (the time from when the container 221 is at the dosing module 220 to when the container is at the crimper module 240) can preferably be in the range of 4 to 10 seconds, more preferably in the range of 6 to 8 seconds, and most preferably, about 7 seconds. In other embodiments, other times can be used.
  • Distance D1 (the distance between when the container 221 is at the dosing module 220 to when the container is at the valve placer module 230) can preferably be in the range of 2 to 16 inches, more preferably in the range of 4 to 8 inches, and most preferably, about 6.25 inches. Distance D2 (the distance between when the container 221 is at the dosing module 220 to when the container is at the crimper module 240) can preferably be in the range of 5 to 11 inches, more preferably in the range of 7 to 9 inches, and most preferably, about 8.75 inches. In other embodiments, other distances can be used. These distances are measured along the generally arcuate path traveled by the containers while moving about the turntable.
  • Container 221 can be made of tinplate, aluminum, glass, or other materials as is known to those of skill in the art. The bittering agent can be denatonium benzoate, or other bittering agents, as are known to those of skill in the art. The propellant can be a liquefied gas, for use with aerosol spray containers, as is known to those of skill in the art. In some embodiments, a liquefied aerosol dusting composition can be used, as described in U.S. patent application Ser. No. 11/895,070, filed on Aug. 22, 2007, and titled “A liquefied-gas Aerosol Dusting Composition Containing Denatonium Benzoate,” the contents of which are hereby incorporated by reference herein.
  • In some embodiments, the dispenser 224 of dose module 220 can be an Ultra 2400 workstation dispenser, as produced by EFD Inc., of East Providence, R.I. As is known to those of skill in the art, the Ultra 2400 workstation includes a digital display, an air management system, and precision time increment adjustment capabilities for precise dose deposit controls.
  • In some embodiments, turntable 300 can use a rotary index mechanism and aerosol filling system as provided by Terco Inc., of Bloomington, Ill.
  • By way of sensor mechanism 226 (see FIG. 4), the dispenser 224 and turntable 300 have been coupled such that dispenser 224 works cooperatively and automatically with turntable 300. By way of embodiments of the invention, actuation of the EFD fluid dispenser 221 is coupled to the position of container 221, thus minimizing the possibility of accidental discharge of bitterant from syringe 222.
  • With reference to FIGS. 1 and 2, optionally, as is known in the art, a propellant can be added to the container (step S16). Next, the container can be tested in a bath (step S18), and, an actuator can be added to the container (step S20).
  • It is to be understood that the exemplary embodiments are merely illustrative of the invention and that many variations of the above-described embodiments may be devised by one skilled in the art without departing from the scope of the invention. It is therefore intended that all such variations be included within the scope of the following claims and their equivalents.

Claims (29)

1. A method for introducing a bittering agent into an aerosol container, the method comprising the steps of:
adding a dose of the bittering agent in the container;
positioning a valve on the container;
crimping the valve to the container; and
adding an aerosol propellant to the container.
2. The method of claim 1, further comprising the step of adding an actuator to the container.
3. The method of claim 2, further comprising testing the container in a bath.
4. The method of claim 1, wherein the time interval between adding a dose of the bittering agent in the container and positioning a valve on the container is about 1 to 5 seconds.
5. The method of claim 1, wherein the time interval between adding a dose of the bittering agent in the container and positioning a valve on the container is about 1 to 3 seconds.
6. The method of claim 1, wherein the time interval between adding a dose of the bittering agent in the container and positioning a valve on the container is about 2.5 seconds.
7. The method of claim 1, wherein a distance that the container travels between the steps of adding a dose of the bittering agent in the container and positioning a valve on the container is about 2 to 16 inches.
8. The method of claim 1, wherein a distance that the container travels between the steps of adding a dose of the bittering agent in the container and positioning a valve on the container is about 4 to 8 inches.
9. The method of claim 1, wherein a distance that the container travels between the steps of adding a dose of the bittering agent in the container and positioning a valve on the container is about 6.25 inches.
10. The method of claim 1 wherein the time interval between adding a dose of the bittering agent in the container and crimping the valve to the container is about 4 to 10 seconds.
11. The method of claim 1, wherein the time interval between adding a dose of the bittering agent in the container and crimping the valve to the container is about 6 to 8 seconds.
12. The method of claim 1, wherein the time interval between adding a dose of the bittering agent in the container and crimping the valve to the container is about 7 seconds.
13. The method of claim 1, wherein a distance that the container travels between the steps of adding a dose of the bittering agent in the container and crimping the valve to the container is about 5 to 11 inches.
14. The method of claim 1, wherein a distance that the container travels between the steps of adding a dose of the bittering agent in the container and crimping the valve to the container is about 7 to 9 inches.
15. The method of claim 1, wherein a distance that the container travels between the steps of adding a dose of the bittering agent in the container and crimping the valve to the container is about 8.75 inches.
16. The method of claim 1, wherein the bittering agent comprises denatonium benzoate.
17. The method of claim 1, wherein the aerosol propellant comprises a liquefied gas.
18. The method of claim 1, wherein the aerosol propellant and the bittering agent form a liquefied-gas aerosol dusting composition.
19. The method of claim 1, wherein the steps of adding a dose of the bittering agent in the container and positioning a valve on the container are performed by an automated device.
20. The method of claim 1, wherein the steps of adding a dose of the bittering agent in the container and positioning a valve on the container are performed by an automated device.
21. The method of claim 20, wherein the automated device comprises an indexing turntable.
22. An apparatus for introducing a bittering agent into an aerosol container comprising:
a turntable for positioning the container;
a dosing module for adding a dose of the bittering agent in the container when the turntable positions the container proximate the dosing module; and
a valve module for positioning a valve on the container when the turntable positions the container proximate the valve module.
23. The apparatus of claim 22, wherein the time interval between when the container is positioned proximate the dosing module and when the container is positioned proximate the valve module is about 1 to 5 seconds.
24. The apparatus of claim 22, wherein the time interval between when the container is positioned proximate the dosing module and when the container is positioned proximate the valve module is about 1 to 3 seconds.
25. The apparatus of claim 22, wherein the time interval between when the container is positioned proximate the dosing module and when the container is positioned proximate the valve module is about 2.5 seconds.
26. The apparatus of claim 22, wherein a distance between where the container is positioned proximate the dosing module and where the container is positioned proximate the valve module is about 2 to 16 inches.
27. The apparatus of claim 22, wherein a distance between where the container is positioned proximate the dosing module and where the container is positioned proximate the valve module is about 4 to 8 inches.
28. The apparatus of claim 22, wherein a distance between where the container is positioned proximate the dosing module and where the container is positioned proximate the valve module is about 6.25 inches.
29. The apparatus of claim 22, wherein the bittering agent comprises denatonium benzoate.
US12/020,029 2007-02-23 2008-01-25 Dosing System and Method Abandoned US20080202627A1 (en)

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US20090209877A1 (en) * 2008-02-15 2009-08-20 Hai Zhang automated qualitative mask fit tester

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WO2008103978A2 (en) 2008-08-28

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