US1318793A - Evaporating apparatus and method of operating the same - Google Patents
Evaporating apparatus and method of operating the same Download PDFInfo
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- US1318793A US1318793A US1318793DA US1318793A US 1318793 A US1318793 A US 1318793A US 1318793D A US1318793D A US 1318793DA US 1318793 A US1318793 A US 1318793A
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- 238000000034 method Methods 0.000 title description 9
- 238000001704 evaporation Methods 0.000 title description 8
- 230000000694 effects Effects 0.000 description 58
- 239000007788 liquid Substances 0.000 description 49
- 238000010438 heat treatment Methods 0.000 description 10
- 238000009835 boiling Methods 0.000 description 9
- 230000008020 evaporation Effects 0.000 description 3
- 239000012141 concentrate Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 241001527902 Aratus Species 0.000 description 1
- 102100035683 Axin-2 Human genes 0.000 description 1
- 101700047552 Axin-2 Proteins 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 230000002277 temperature effect Effects 0.000 description 1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/26—Multiple-effect evaporating
Definitions
- One object of myv invention is to reduce the amount of heat required for the evaporation or concentration of a given 'body of liquid and more particularly to elficiently utilize the heat present in a multiple efiect evaporator, for raising the temperature of the liquid to be later evaporated with a view to lessening the amount of steam relosses of the liquid operated on due to its being carried by the vapors in the form of finely divided particles from one effect to the heating compartment of the next eflect.
- Figure 1 is a side elevation partly in section andto some extent dia ammatic, illustrating my invention as app ied to a multiple efl'ect evaporator;
- Fig. 2 is a plan partly in section further illlstrating the apparatus shown in Fig. 1;
- Figs. 3 to 6 inclusive are diagrammatic views illustrating various modifications of my invention.
- 1 4 represent the pans or individual eflects of a multiple efit'ect evaporator having heating drums'58 and including auxiliary casings or catch-alls 9--12.
- the heating drum 5 of the first effect has an inlet 13 for steam and itscatchall 9 is connected to deliver vapor throu h a pipe 14 to the heating drum 6 of t e second effect 2.
- other pipes 15 and 16' connect the catch-alls 10 and 11 of drums a pipe the effects 2 and 3with the heatin 7 and 8 of the effects 3 and 4, an
- each of the four catch-alls 9.12 is mounted an economizer 19 consisting of a horizontally extended and preferably cylin drical shell 20 extending at one end outside of the evaporator and having tube sheets in which are mounted the ends of a series of tubes 21. These latter at one end all connect with a chamber'22 and at the opposite end part of them connect with a chamber 23 and the other part with a chamber 24:.
- a partition 25 extends across the lower part ofeach of the catch-alls so as to serve as a baflie and deflect around the economizer casing 20, the vapors arising from the lower part of the efiect and flowing toward the vapor outlet pipe 14.
- valved branch pipe 27 from each of the vapor pipes 14, 15 and 16 to the interior of each of the shells or casings 20 for the reception of a portion of the vapors so as to permit these to. circulate around the tubes 21 of the several economizers.
- the pipes 27 may be omitted and the vapor admitted to the casings 20 through a suitable opening in a part of its body within the catch-all as indicated at 26 in the efiect 1.
- Each of the economizer shells or casings- 20 has a pipe 28 connected to. deliver liquid condensing therein to the steam space-of the heating drum of the next efl'ect, although the economizer of the last efl'ect has its casing connected through a pipe 29 to the vaporreceiving space of the condenser 18.
- the condenser is connected through a' pipe 30 with an air pump 31 and in that form of my invention shown in Figs. 1 and 2, the liquor to be evaporated or concentrated is delivered by a pump 32 through a pipe 33 to the chamber 23 of the economizer of the fourth effect and the second or outlet chamber 24 is connected by a pipe 34 to the receiving chamber of the economizer of the efi'ect 3.
- liquid space of the economizer of the efiect 3 is connected by a pi e 35 with the economizer of the efiect 2, t e latter in turn bein connected by a pipe 36 with the economlzer of the eflect 1 and having its second chamber 24 connected through a pipe 37 to deliver liquid into the liquid-receivmg space of the first effect 1.
- t e in turn bein connected by a pipe 36 with the economlzer of the eflect 1 and having its second chamber 24 connected through a pipe 37 to deliver liquid into the liquid-receivmg space of the first effect 1.
- the lowest portion of the first eflect is connected through a pipe 38 with the liquid receiving space of the second effect 2 and the lowest part of the latter is connected through a pipe 39 with the liquid-receiving space of the efi'ect 3, Whose lowest portion is connected by a pipe 40 to the liquid receiving space of the' effect 4.
- the lowest part of the latter has connected to it a pipe 41 whereby the concentrated liquor may be ,delivered to any desired apparatus or storage receptacle.
- each economizer connects to each economizer an air pipe 60 and through a main 61, connect these pipes to the suction pipe 30 of the air pump; thereby keeping the economizers free of air and non-condensible gases as well as improving the circulation and action of the steam or water vapor.
- the relatively cold liquor is first acted on by the heat of the relatively low temperature vapors delivered from the last effect, and as it passes successively through the economizers of the third and second efiects, its temperature is successively increased until it finally flows into the liquid boiling' s ace of the first efi'ect at a temperature but little below that required to cause it to boil,
- liquid after being concentrated or evaporated in each of the efiects, to a predetermined extent is passed through the pipe 38, 39 or 410 as the case may be, to the next effect and is finally delivered in a highly concentrated condition through the pipe 41.
- the cold raw liquor is delivered through apipe 33 to the economizer in the fourth efi'ect and from the latter through the pipe 34: t0 the economizer in the third 120 effect, after which it flows through 'a pipe 50 to the boilingor liquid receiving space of the fourth efi'ect. From the lowest point of this fourth effect it will be delivered or forced through a pi e 51 to the li uid boil- 125 ing space of the e ect 3, thence t rough a pipe 52 from the lowest point of this effect to the liquid receiving space of the edect 2 and from-the lowest point of this latter to the liquid receiving space of the efiect- 1, 13c
- Fig. 4 I have shown an arran ement of apparatus identical with that of igs. 1 and 2, except that the i e 55 is connected between the pipe 37 and t e pipe 38 so that a portion of the liquid flowing from the economizer 19 of the first effect may be de livered to the liquid receivin space of said effect and the remainder to t e corresponding compartment of the second effect.
- liquor under treatment divides after flowing through and being heated in the economizer through the pipe 57 to the liquid boiling space of the effect 3 while'the remainder passes through the economizer 19 and thereafter divides between the pipe 56 in the economizer 19.
- highly heated liquid from this latter economizer is delivered to the liquid boiling space" of the effect 1 and the partially concentrated liquid from this effect with the hot raw liquor from the pipe 56 is supplied to the effect .2.
- the liquor delivered from this to the pip'e39, mixed with thepartially heated liquor delivered from the pipe 57, is then successivelv delivered to and acted on by the twolast effects 3 and 4. 4
- the heated liquid delivered to the first effect is at a temperature but slightlv below its temperature of boiling within that effect so that only sufficient steam is consumed to bring its temperature to the particular boiling point due to the pressure existing in that effect, in addition to the steam necessary. to vaporize said liquid.
- an evaporator including a catch-all and a vapor delivery pipe; an economizer mounted in said catchall; a conduit connecting the vapor delivery pipe and the vapor receiving space of said economizer; a conduit for conductin liquor to the economizer; and a second con uit for conducting liquid from the economi'zer to the liquid receiving compartment of the evaporator.
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Description
E. A. NEWHALL.
EVAPORATING APPARATUS AND METHOD OF OPERATING THE SAME.
APPLICATION FILED MAY 9. 1917.
1,318,793. Patented Oct. 14,1919.
3 SHEETSSHEET I.
Irw E mv Z 7&6 fleaor .7 y 316 x.
E. A. NEWHALL.
EVAPORATING APPARATUS AND METHOD OF OPERATING THE SAME.
APPLICATION FILED MAY 0. 19!].
Patented Oct. '14, MM.
3 SHEETS-SHEET 2.
Ezfw
E. A, NEWHALL.
EVAPORATING APPARATUS AND METHOD OF OPERATING THE SAME.
APPLICATION FILED MAY 9. 1917. 1,318,798. Patented (m.14,1919.
3 SHEETS-SHEET 3.
UNITED STATES PATENT OFFICE.
EZRA A. N EWHALL, OF PHILADELPHIA, PENNSYLVANIA.
EVAPORATING APPARATUS AND METHOD OF OPERATING THE SAME.
Specification of Letters Patent.
Patented Oct. 14, 1919.
Application filed May 9, 1917. Seria1No. 167,466.
To all whom it may concern:
Be 'itknown that I, EZRA A. NEWHALL, a citizen of the United States, residing in Philadelphia, Pennsylvania, have invented Evaporating, Apparatus and Methods ofOpcrating the Same,'ot which the following is a specification.
One object of myv invention is to reduce the amount of heat required for the evaporation or concentration of a given 'body of liquid and more particularly to elficiently utilize the heat present in a multiple efiect evaporator, for raising the temperature of the liquid to be later evaporated with a view to lessening the amount of steam relosses of the liquid operated on due to its being carried by the vapors in the form of finely divided particles from one effect to the heating compartment of the next eflect. a
These objects andother advantageous ends I secure as hereinafter set forth, reference bein had to the accompanying drawings, in w ich,
Figure 1 is a side elevation partly in section andto some extent dia ammatic, illustrating my invention as app ied to a multiple efl'ect evaporator;
Fig. 2 is a plan partly in section further illlstrating the apparatus shown in Fig. 1; an
Figs. 3 to 6 inclusive are diagrammatic views illustrating various modifications of my invention.
In the above drawings, 1 4 represent the pans or individual eflects of a multiple efit'ect evaporator having heating drums'58 and including auxiliary casings or catch-alls 9--12. The heating drum 5 of the first effect has an inlet 13 for steam and itscatchall 9 is connected to deliver vapor throu h a pipe 14 to the heating drum 6 of t e second effect 2. Similarly other pipes 15 and 16' connect the catch-alls 10 and 11 of drums a pipe the effects 2 and 3with the heatin 7 and 8 of the effects 3 and 4, an
17 connects the catch-all 12 of the fourth efi'ect to a condenser 18.
In each of the four catch-alls 9.12, is mounted an economizer 19 consisting of a horizontally extended and preferably cylin drical shell 20 extending at one end outside of the evaporator and having tube sheets in which are mounted the ends of a series of tubes 21. These latter at one end all connect with a chamber'22 and at the opposite end part of them connect with a chamber 23 and the other part with a chamber 24:. A partition 25 extends across the lower part ofeach of the catch-alls so as to serve as a baflie and deflect around the economizer casing 20, the vapors arising from the lower part of the efiect and flowing toward the vapor outlet pipe 14.
In addition there is preferably a valved branch pipe 27 from each of the vapor pipes 14, 15 and 16 to the interior of each of the shells or casings 20 for the reception of a portion of the vapors so as to permit these to. circulate around the tubes 21 of the several economizers. Obviously the pipes 27 may be omitted and the vapor admitted to the casings 20 through a suitable opening in a part of its body within the catch-all as indicated at 26 in the efiect 1.
Each of the economizer shells or casings- 20 has a pipe 28 connected to. deliver liquid condensing therein to the steam space-of the heating drum of the next efl'ect, although the economizer of the last efl'ect has its casing connected through a pipe 29 to the vaporreceiving space of the condenser 18.
The condenser is connected through a' pipe 30 with an air pump 31 and in that form of my invention shown in Figs. 1 and 2, the liquor to be evaporated or concentrated is delivered by a pump 32 through a pipe 33 to the chamber 23 of the economizer of the fourth effect and the second or outlet chamber 24 is connected by a pipe 34 to the receiving chamber of the economizer of the efi'ect 3. Likewise the liquid space of the economizer of the efiect 3 is connected by a pi e 35 with the economizer of the efiect 2, t e latter in turn bein connected by a pipe 36 with the economlzer of the eflect 1 and having its second chamber 24 connected through a pipe 37 to deliver liquid into the liquid-receivmg space of the first effect 1. Obviously the detail construction of the economizers is immateral since the liquid may be made to flow through each of them in any number of passes or in any desired manner without departing from my invention.
The lowest portion of the first eflect is connected through a pipe 38 with the liquid receiving space of the second effect 2 and the lowest part of the latter is connected through a pipe 39 with the liquid-receiving space of the efi'ect 3, Whose lowest portion is connected by a pipe 40 to the liquid receiving space of the' effect 4. The lowest part of the latter has connected to it a pipe 41 whereby the concentrated liquor may be ,delivered to any desired apparatus or storage receptacle.
In addition to the above I connect to each economizer an air pipe 60 and through a main 61, connect these pipes to the suction pipe 30 of the air pump; thereby keeping the economizers free of air and non-condensible gases as well as improving the circulation and action of the steam or water vapor.
Under conditions of operation, steam at a suitable pressure is delivered to the steam inlet 13 of the first'efi'ect, the condenser 18 is put in operation and raw liquor, usually in a cold condition, is delivered by the pump 32 through the pipe 33 to the economizer 19 of the fourth efi'ect. After flowing through the tubes of the latter, said liquor passes through the pipe 3 1 to the economizer of the third eflect, thence through the pi e 35 to the economizer of the second e ect and thereafter through the ipe 36 to the economizer of the first effect, om which it is delivered through the pipe 37 to the liquid boiling space of said eifect.
Obviously whenthe apparatus is in operation, vapor from the boiling liquid of each effect passes through the pipe 27 or other suitable opening or connection and heats the tubes in the casing 20 of the economizer in its particular-catch-all, ultimately condensing and being conducted through the pipe 28 into the heating drum of the next effect.
As a result of this method of procedure, the relatively cold liquor is first acted on by the heat of the relatively low temperature vapors delivered from the last effect, and as it passes successively through the economizers of the third and second efiects, its temperature is successively increased until it finally flows into the liquid boiling' s ace of the first efi'ect at a temperature but little below that required to cause it to boil,
a portion of the latent heat of the vapor flowing from the effect in which any particular economizer is mounted being converted into sensible heat which increases the temperature of the liquor.
It is obvious that the capacity of the apparatus is also increased since the economizers provide additional heating surface and vapors condensed in them must be replaced by additional evaporation in their respective effects in order to evaporate the required volume in the next succeeding effect.
As is understood by those skilled in the art, liquid after being concentrated or evaporated in each of the efiects, to a predetermined extent is passed through the pipe 38, 39 or 410 as the case may be, to the next effect and is finally delivered in a highly concentrated condition through the pipe 41. By means of the above method and apparatus I find that there is a material reduction in the amount of heat required for the evaporation or concentration of a given body of liquid, this being due partly to the prevention of heat radlation due to the mounting of the economizers within the easings of the effects and partly to the efficient 90 utilization of the heat of the vapors to suecessively raise the temperature of the liquid to be evaporated or concentrated. Moreover, owing to the peculiar arrangement of the economizer casings and their associated parts within the catch-alls of the several efi'ects, there is a reduction in the amount of liquor mechanically carried by the vapors from the liquor space of one effect to the heating drum of the nextefiect.
While the arrangement of piping and apparatus shown in Figs. 1 and 2 will give good results for certain purposes, I may under certain conditions provide economizers in certain only of the effects. Thus 105 in Fig. 3, for example, I have shown a system of apparatus in which there are but two economizers 19, mounted in the third and fourth effects of the evaporator respex tively, and in such case the condensed vapor 110 from the economizer of the effect 3 would be delivered through the pipe 28 to the heating drum 8 of the efi'ect 4 and the water from the economizer of this latter efl'ect would be delivered through the pipe 29 to the con- 115 denser,
As before, the cold raw liquor is delivered through apipe 33 to the economizer in the fourth efi'ect and from the latter through the pipe 34: t0 the economizer in the third 120 effect, after which it flows through 'a pipe 50 to the boilingor liquid receiving space of the fourth efi'ect. From the lowest point of this fourth effect it will be delivered or forced through a pi e 51 to the li uid boil- 125 ing space of the e ect 3, thence t rough a pipe 52 from the lowest point of this effect to the liquid receiving space of the edect 2 and from-the lowest point of this latter to the liquid receiving space of the efiect- 1, 13c
from Whose lowest ortion concentrated liquor is delivered or ischarged through a pipe 54. I
In Fig. 4, I have shown an arran ement of apparatus identical with that of igs. 1 and 2, except that the i e 55 is connected between the pipe 37 and t e pipe 38 so that a portion of the liquid flowing from the economizer 19 of the first effect may be de livered to the liquid receivin space of said effect and the remainder to t e corresponding compartment of the second effect.
n that form of my invention shown in F ig. 5, the apparatus and connections are similar to that of Fig. 1, except that the economizer 19 of the first effect is of smaller dimensions than the economizers in the other 1.
and thereafter being delivered through the pipe 37 to the liquidboiling space of the effect 1, and the remainder passing through the pipe'56 to the pipe 38 and into the liquid boiling compartment of the effect 2, Where it is concentrated with the partially concentrated liquid delivered through the pipe 38 from the effect 1.
11 the case of the arrangement shown in Fig. 6, the connections and apparatus are the same as in Fig. 5, except that a by-pass 57 is provided between the pipe and the pipe 39, in addition to which the economizer 19" of the. effect 2 is of smaller capacity than the economizer of the effect 3, but larger.
than the economizer 19 of the first effect.
liquor under treatment divides after flowing through and being heated in the economizer through the pipe 57 to the liquid boiling space of the effect 3 while'the remainder passes through the economizer 19 and thereafter divides between the pipe 56 in the economizer 19. As a result, highly heated liquid from this latter economizer is delivered to the liquid boiling space" of the effect 1 and the partially concentrated liquid from this effect with the hot raw liquor from the pipe 56 is supplied to the effect .2. The liquor delivered from this to the pip'e39, mixed with thepartially heated liquor delivered from the pipe 57, is then successivelv delivered to and acted on by the twolast effects 3 and 4. 4
It is to be understood that the various figures of drawing are designed to illustrate merely the general arrangement of apparatus and piping and for this reason are largely diagrammatic, it being understood that in every case .there are provided the attachments and auxiliary apparatus neces- Under operating conditions therefore, the.
sary to cause the circulation of the liquid described as well as to. control the flow of said liquid and of the vapor, permit observation of the progress of the operation and of the performance of the ap aratus, etc.
It is also to be noted. that t e liquid condensing in each economizer is led to the next lower effect where it gives up heat to assist in the operation of the same.
It will be understood that the heated liquid delivered to the first effect is at a temperature but slightlv below its temperature of boiling within that effect so that only sufficient steam is consumed to bring its temperature to the particular boiling point due to the pressure existing in that effect, in addition to the steam necessary. to vaporize said liquid.
Owing to the mode of operation described, a there is a material saving of the steam 85 required to concentrate a given quantity of liquid. It is also to be noted that while in some cases it is preferable to feed the liquid as shown in Fig. 1, from'the economizer in the .last effect successively through a number of economizers to that in the first effect and thereafter concentrate said liquor by delivering-it successively from the first or highest temperature effect to the last effect, I may, as shown in Fig. 3, after heating said liquor in one or more economizers, beginning with that of the last effect, cause the liquid to flow in a direction counter to thatof the vapor by feeding it successively from the fourth to the first effects as indicated.
' I claim 1. The method of operating a multiple effect which consists in causing liquid to ditional raw liquor to one of the effects other than the first.
3. The method of operating a multiple effect which consists in feeding to the first effect a body of raw liquor to be evaporated; thereafter evaporating said liquor in the first, and succeeding effects; mixing raw liquor with the partiall evaporated liquor from the first effect; an delivering the mixture to the second effect.
4. The combination of an evaporator including a catch-all and a vapor delivery pipe; an economizer mounted in said catchall; a conduit connecting the vapor delivery pipe and the vapor receiving space of said economizer; a conduit for conductin liquor to the economizer; and a second con uit for conducting liquid from the economi'zer to the liquid receiving compartment of the evaporator.
5. The combination of a series of evaporators; economizers mounted in vapor receiving portions of said evaporators respectively; means .for causing liquid to successively flow through said economizers to the liquid receiving space of one of the evaporators; and means for" by-passing liquid around one of the economizers and its evaporator.
6. The combination of a series of evaporators 5 economizers mounted in the vapor receiving portion of said evaporators respectively; means for causing liquid to suc- 'cessively flow through said economizers to the liquid receiving space of one of the evaporators; and means for by-passing liquid around one of the economizers and its evaporator, at least one of said economizers being of smaller capacity than the others.
7. The combination of an evaporator; an economizer mounted in said evaporator so as to be heated by vapor therefrom and extending outside of the same; a conduit connecting the outside part of the economizer with the vapor outlet pipe of the evaporator; and means for causing liquid to pass successively through the economizer and the evaporator.
8. The combination with a multiple efiect of economizers respectively mounted in a plurality of'the effects and each having a portion extending outside of its efiect; means for delivering liquid to the economizers and from said economizers to the liquid boiling compartment of at least one of the efi'ects; va or pipes connecting the eilects; and a con uit rom each vapor pipe to the outside part of the adjacent economizer.
9. The combination with a multiple effect of a series of economizers including casings res ectively mounted Within the individual e ects and tubes in said casings; conduits for causin liquid to flow successively through the tu es of said economizers conduits for delivering condensed liquid from the casings to the steam spaces of the next lowest e'fiects respectively; and means for causing the liquid from the last economizer to be successively evaporated in the eifects.
In witness whereof Iaflix my signature.
EZRA. A. NEWHALL.
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US1318793A true US1318793A (en) | 1919-10-14 |
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ID=3386268
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US1318793D Expired - Lifetime US1318793A (en) | Evaporating apparatus and method of operating the same |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US1318793A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2934477A (en) * | 1956-08-09 | 1960-04-26 | Badger Mfg Company | Flash-type distillation system |
| US2941590A (en) * | 1955-03-14 | 1960-06-21 | Rosenblad Curt Fredrik | Multiple evaporation methods |
| US2942657A (en) * | 1957-05-28 | 1960-06-28 | Bowen Corp | Vapor compression evaporation |
| US3150028A (en) * | 1960-07-18 | 1964-09-22 | Separator Ab | Plate heat exchanger for evaporation or distillation of liquids |
| US3354932A (en) * | 1965-05-28 | 1967-11-28 | Blaw Knox Co | Multiple-effect evaporator structure |
-
0
- US US1318793D patent/US1318793A/en not_active Expired - Lifetime
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2941590A (en) * | 1955-03-14 | 1960-06-21 | Rosenblad Curt Fredrik | Multiple evaporation methods |
| US2934477A (en) * | 1956-08-09 | 1960-04-26 | Badger Mfg Company | Flash-type distillation system |
| US2942657A (en) * | 1957-05-28 | 1960-06-28 | Bowen Corp | Vapor compression evaporation |
| US3150028A (en) * | 1960-07-18 | 1964-09-22 | Separator Ab | Plate heat exchanger for evaporation or distillation of liquids |
| US3354932A (en) * | 1965-05-28 | 1967-11-28 | Blaw Knox Co | Multiple-effect evaporator structure |
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