US1138085A - Method of removing ink from paper-stock. - Google Patents
Method of removing ink from paper-stock. Download PDFInfo
- Publication number
- US1138085A US1138085A US66257911A US1911662579A US1138085A US 1138085 A US1138085 A US 1138085A US 66257911 A US66257911 A US 66257911A US 1911662579 A US1911662579 A US 1911662579A US 1138085 A US1138085 A US 1138085A
- Authority
- US
- United States
- Prior art keywords
- stock
- ink
- paper
- removing ink
- fiber
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title description 5
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 11
- 239000000835 fiber Substances 0.000 description 6
- YKTSYUJCYHOUJP-UHFFFAOYSA-N [O--].[Al+3].[Al+3].[O-][Si]([O-])([O-])[O-] Chemical compound [O--].[Al+3].[Al+3].[O-][Si]([O-])([O-])[O-] YKTSYUJCYHOUJP-UHFFFAOYSA-N 0.000 description 5
- 239000003513 alkali Substances 0.000 description 4
- 239000003518 caustics Substances 0.000 description 4
- 239000004927 clay Substances 0.000 description 4
- 235000011121 sodium hydroxide Nutrition 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 238000004537 pulping Methods 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 2
- -1 fullers earth Chemical compound 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 239000005995 Aluminium silicate Substances 0.000 description 1
- 241000581364 Clinitrachus argentatus Species 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 239000006096 absorbing agent Substances 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 235000012211 aluminium silicate Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229910000286 fullers earth Inorganic materials 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- 230000002879 macerating effect Effects 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000010899 old newspaper Substances 0.000 description 1
- 239000010893 paper waste Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C5/00—Other processes for obtaining cellulose, e.g. cooking cotton linters ; Processes characterised by the choice of cellulose-containing starting materials
- D21C5/02—Working-up waste paper
- D21C5/025—De-inking
- D21C5/027—Chemicals therefor
Definitions
- This invention relates to a certain new and useful improvement in the removal of printers ink from old paper stock, that is to say from stock made up in whole or in part ofwaste printed-paper, as, for instance, from old newspapers, printed books, and the ike;
- the waste paper stock is macerated in the presence of water in a beater engine or any machine for reducing it to a substantially homogeneous pulp.
- a caustic alkali in solution, preferably caustic soda, which has the effect of lifting the ink from the fiber.
- silicate of aluminum such as fullers earth, kaolin and all other clays or silicate of magnesium such as talc, soapstone, etc., which serve to take up, absorb, or carry the ink, thereby segregating it from the fiber.
- the aluminum silicate or clays, carrying with it the ink is separated from the fiber, thereby bringing the stock back quite closely to the original condition and color of raw stock.
- successful results may be obtained by first macerating the waste printed paper stock or book stock with the necessary amount of water to bring it to a pulp. This operation can be carried on in a beater engine or in any other suitable type of pulping machine, and with water at ordinary atmospheric temperatures. To the macerated or pulped stock is then added the caustic alkali and the absorbing agent, in the proportion of,
- caustic soda sodium hydrate
- aluminum silicate or clay per ton of the pulped stock of beater consistency.
- the caustic alkali thereupon exercises its function of lifting the ink from the fiber ofthe stock and the aluminum silicate or clay is found to absorb, take up, and carry the ink, thereby segregat ng it fromthe fiber.
- the operation is facilitated and made uniform by vigorously agitating and mixing the mass for a period varying from say ten minutes to thirty mlnutes according to the character of the stock employed and the desired completeness of the result. In some instances, also, it may be further facilitated by raising the temperature of the stock by the injection of steam or the addition of hot water.
- the aluminum silicate or clay, carrying the ink is washed from the fiber in any suitable manner, as, for instance, in the drum washer in common use in paper mills, in which also the stock may be macerated, treated and washed, or by any other washing method desirable.
Landscapes
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Toxicology (AREA)
- Paper (AREA)
Description
r'r mans near rare MAX CLINE AND CHARLES F. RHODES, OF GLENS FALLS, NEW YORK, ASSIGNORS TO INTERNATIONAL PAPER COMPANY, OF NEW YORK, N. Y., A
CORPORATION OF NEW Patented May 4, i915.
. YORK.
I METHOD OF REMOVING" INK FROM PAPER-STOCK.
1 ,138 Q 85. Specification of Letters Patent.
No Drawing.
To all whom it may concern: Be it known that we, MAX GLINE and CHARLES F. Rnonns, citizens of the United skilled in the art to which it appertains to make and use the same.
This invention relates to a certain new and useful improvement in the removal of printers ink from old paper stock, that is to say from stock made up in whole or in part ofwaste printed-paper, as, for instance, from old newspapers, printed books, and the ike; I
In the practice of the invention, the waste paper stock is macerated in the presence of water in a beater engine or any machine for reducing it to a substantially homogeneous pulp. To the original or macerated stock, containing the ink to be removed, is added a caustic alkali, in solution, preferably caustic soda, which has the effect of lifting the ink from the fiber. There is also added to the original or macerated stock a quantity of silicate of aluminum such as fullers earth, kaolin and all other clays or silicate of magnesium such as talc, soapstone, etc., which serve to take up, absorb, or carry the ink, thereby segregating it from the fiber. Finally, by a washing operation, the aluminum silicate or clays, carrying with it the ink, is separated from the fiber, thereby bringing the stock back quite closely to the original condition and color of raw stock.
As an illustration of the successful practice of the invention, it may be stated that successful results may be obtained by first macerating the waste printed paper stock or book stock with the necessary amount of water to bring it to a pulp. This operation can be carried on in a beater engine or in any other suitable type of pulping machine, and with water at ordinary atmospheric temperatures. To the macerated or pulped stock is then added the caustic alkali and the absorbing agent, in the proportion of,
Application filed November 27, 1911. Serial No. 662,579.
say, forty pounds of caustic soda (sodium hydrate), and forty pounds of aluminum silicate or clay, per ton of the pulped stock of beater consistency. The caustic alkali thereupon exercises its function of lifting the ink from the fiber ofthe stock and the aluminum silicate or clay is found to absorb, take up, and carry the ink, thereby segregat ng it fromthe fiber. The operation is facilitated and made uniform by vigorously agitating and mixing the mass for a period varying from say ten minutes to thirty mlnutes according to the character of the stock employed and the desired completeness of the result. In some instances, also, it may be further facilitated by raising the temperature of the stock by the injection of steam or the addition of hot water. Thereupon the aluminum silicate or clay, carrying the ink, is washed from the fiber in any suitable manner, as, for instance, in the drum washer in common use in paper mills, in which also the stock may be macerated, treated and washed, or by any other washing method desirable.
What we claim is:
1. The process of removing ink from waste newspaper stock, book stock, and the like, which consists in pulping the stock, adding a caustic alkali thereto for lifting the ink, adding aluminum silicate or clay, to absorb the lifted ink, and washing out the ink-carrying absorbent; substantially as described.
2. The process of removing ink from wastev newspaper stock, book stock, and the like, which consists in pulping the stock, lifting the ink by adding about 2% of caustic soda, absorbing the lifted ink by add;
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US66257911A US1138085A (en) | 1911-11-27 | 1911-11-27 | Method of removing ink from paper-stock. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US66257911A US1138085A (en) | 1911-11-27 | 1911-11-27 | Method of removing ink from paper-stock. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US1138085A true US1138085A (en) | 1915-05-04 |
Family
ID=3206183
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US66257911A Expired - Lifetime US1138085A (en) | 1911-11-27 | 1911-11-27 | Method of removing ink from paper-stock. |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US1138085A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5755926A (en) * | 1992-02-24 | 1998-05-26 | Kimberly-Clark Worldwide, Inc. | Integrated pulping process of waste paper yielding tissue-grade paper fibers |
| US20100006242A1 (en) * | 2008-07-09 | 2010-01-14 | Duggirala Prasad Y | Deinking a cellulosic substrate using magnesium silicate |
-
1911
- 1911-11-27 US US66257911A patent/US1138085A/en not_active Expired - Lifetime
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5755926A (en) * | 1992-02-24 | 1998-05-26 | Kimberly-Clark Worldwide, Inc. | Integrated pulping process of waste paper yielding tissue-grade paper fibers |
| US20100006242A1 (en) * | 2008-07-09 | 2010-01-14 | Duggirala Prasad Y | Deinking a cellulosic substrate using magnesium silicate |
| US8133350B2 (en) | 2008-07-09 | 2012-03-13 | Nalco Company | Deinking a cellulosic substrate using magnesium silicate |
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