UA98628C2 - Process for the sulfinylation of a pyrazole derivative - Google Patents
Process for the sulfinylation of a pyrazole derivativeInfo
- Publication number
- UA98628C2 UA98628C2 UAA200905234A UAA200905234A UA98628C2 UA 98628 C2 UA98628 C2 UA 98628C2 UA A200905234 A UAA200905234 A UA A200905234A UA A200905234 A UAA200905234 A UA A200905234A UA 98628 C2 UA98628 C2 UA 98628C2
- Authority
- UA
- Ukraine
- Prior art keywords
- sulfinylation
- pyrazole derivative
- cfs
- hydroxy group
- amine
- Prior art date
Links
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The present invention relates to a process for the sulfinylation of a pyrazole derivative, characterized in that 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1H-pyrazole-3-carbonitrile (II) is reacted with a sulfinylating agent S in the presence of at least one amine acid complex wherein the amine(s) are selected from cyclic secondary amines and the acid(s) are selected from sulfonic acid derivatives, and with the addition of a halogenating agent, wherein S is [CFS(O)]O; or CFS(O)X wherein X means fluoro, chloro, bromo, iodo, a hydroxy group, or an alkaline or alkaline earth metal salt of the hydroxy group; or mixtures thereof.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US86517806P | 2006-11-10 | 2006-11-10 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| UA98628C2 true UA98628C2 (en) | 2012-06-11 |
Family
ID=41272785
Family Applications (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| UAA200905383A UA98475C2 (en) | 2006-11-10 | 2007-11-05 | Process for the sulfinylation of a pyrazole derivative |
| UAA200905381A UA98474C2 (en) | 2006-11-10 | 2007-11-05 | Process for the sulfinylation of a pyrazole derivative |
| UAA200905234A UA98628C2 (en) | 2006-11-10 | 2007-11-05 | Process for the sulfinylation of a pyrazole derivative |
Family Applications Before (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| UAA200905383A UA98475C2 (en) | 2006-11-10 | 2007-11-05 | Process for the sulfinylation of a pyrazole derivative |
| UAA200905381A UA98474C2 (en) | 2006-11-10 | 2007-11-05 | Process for the sulfinylation of a pyrazole derivative |
Country Status (2)
| Country | Link |
|---|---|
| CN (3) | CN101583602A (en) |
| UA (3) | UA98475C2 (en) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104557713B (en) * | 2013-10-22 | 2018-08-21 | 江苏托球农化股份有限公司 | High-purity ethiprole preparation method |
| CN104926729B (en) * | 2014-03-18 | 2018-01-19 | 上海泰禾国际贸易有限公司 | A kind of method for synthesizing ethiprole |
| CN107963993A (en) * | 2018-01-06 | 2018-04-27 | 江苏托球农化股份有限公司 | A kind of preparation method of high-purity ethiprole |
| WO2020188376A1 (en) * | 2019-03-19 | 2020-09-24 | Gharda Chemicals Limited | A process for synthesis of fipronil |
| CN111004155A (en) * | 2019-09-11 | 2020-04-14 | 浙江埃森化学有限公司 | Preparation method of trifluoromethyl sulfuryl halide |
-
2007
- 2007-11-05 UA UAA200905383A patent/UA98475C2/en unknown
- 2007-11-05 CN CNA2007800496448A patent/CN101583602A/en active Pending
- 2007-11-05 CN CNA2007800496556A patent/CN101578270A/en active Pending
- 2007-11-05 UA UAA200905381A patent/UA98474C2/en unknown
- 2007-11-05 UA UAA200905234A patent/UA98628C2/en unknown
- 2007-11-05 CN CNA2007800496452A patent/CN101589027A/en active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| CN101578270A (en) | 2009-11-11 |
| UA98474C2 (en) | 2012-05-25 |
| CN101589027A (en) | 2009-11-25 |
| UA98475C2 (en) | 2012-05-25 |
| CN101583602A (en) | 2009-11-18 |
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