UA82448C2 - СПОСОБ ПОЛУЧЕНИЯ ИНКАПСУЛИРОВАННЫХ НАНОПОРОШКоВ И УСТАНОВКА ДЛЯ ЕГО ОСУЩЕСТВЛЕНИЯ - Google Patents
СПОСОБ ПОЛУЧЕНИЯ ИНКАПСУЛИРОВАННЫХ НАНОПОРОШКоВ И УСТАНОВКА ДЛЯ ЕГО ОСУЩЕСТВЛЕНИЯ Download PDFInfo
- Publication number
- UA82448C2 UA82448C2 UAA200702007A UAA200702007A UA82448C2 UA 82448 C2 UA82448 C2 UA 82448C2 UA A200702007 A UAA200702007 A UA A200702007A UA A200702007 A UAA200702007 A UA A200702007A UA 82448 C2 UA82448 C2 UA 82448C2
- Authority
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- Ukraine
- Prior art keywords
- salt
- substrate
- mentioned
- vapor
- holes
- Prior art date
Links
- 239000011858 nanopowder Substances 0.000 title claims abstract description 30
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 10
- 150000003839 salts Chemical class 0.000 claims abstract description 83
- 239000000463 material Substances 0.000 claims abstract description 63
- 238000000034 method Methods 0.000 claims abstract description 41
- 238000001704 evaporation Methods 0.000 claims abstract description 30
- 230000008020 evaporation Effects 0.000 claims abstract description 29
- 238000009833 condensation Methods 0.000 claims abstract description 15
- 230000005494 condensation Effects 0.000 claims abstract description 14
- 239000000203 mixture Substances 0.000 claims abstract description 7
- 238000010438 heat treatment Methods 0.000 claims abstract description 6
- 239000000758 substrate Substances 0.000 claims description 40
- 239000000843 powder Substances 0.000 claims description 16
- 238000010894 electron beam technology Methods 0.000 claims description 12
- 239000012808 vapor phase Substances 0.000 claims description 12
- 238000009434 installation Methods 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 230000001105 regulatory effect Effects 0.000 claims description 4
- 230000007246 mechanism Effects 0.000 claims description 3
- 239000002245 particle Substances 0.000 abstract description 24
- 239000000126 substance Substances 0.000 abstract description 9
- 229910052751 metal Inorganic materials 0.000 description 31
- 239000002184 metal Substances 0.000 description 31
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 17
- 239000011159 matrix material Substances 0.000 description 17
- 239000002105 nanoparticle Substances 0.000 description 15
- 230000008569 process Effects 0.000 description 15
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 10
- 238000005054 agglomeration Methods 0.000 description 10
- 230000002776 aggregation Effects 0.000 description 10
- 230000015572 biosynthetic process Effects 0.000 description 10
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 9
- 239000012298 atmosphere Substances 0.000 description 9
- 230000001681 protective effect Effects 0.000 description 9
- 229910052802 copper Inorganic materials 0.000 description 8
- 239000010949 copper Substances 0.000 description 8
- 239000007789 gas Substances 0.000 description 8
- 229910052759 nickel Inorganic materials 0.000 description 8
- 230000003993 interaction Effects 0.000 description 7
- 238000009826 distribution Methods 0.000 description 6
- 150000002739 metals Chemical class 0.000 description 6
- PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Chemical compound [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 description 6
- 239000011780 sodium chloride Substances 0.000 description 5
- 230000008859 change Effects 0.000 description 4
- 238000000151 deposition Methods 0.000 description 4
- 230000008021 deposition Effects 0.000 description 4
- 238000010586 diagram Methods 0.000 description 4
- 239000006185 dispersion Substances 0.000 description 4
- 238000005538 encapsulation Methods 0.000 description 4
- 239000007791 liquid phase Substances 0.000 description 4
- 239000002082 metal nanoparticle Substances 0.000 description 4
- 230000003647 oxidation Effects 0.000 description 4
- 238000007254 oxidation reaction Methods 0.000 description 4
- 238000009834 vaporization Methods 0.000 description 4
- 230000008016 vaporization Effects 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- 239000000956 alloy Substances 0.000 description 3
- 229910045601 alloy Inorganic materials 0.000 description 3
- 239000012071 phase Substances 0.000 description 3
- 230000005855 radiation Effects 0.000 description 3
- 229910052814 silicon oxide Inorganic materials 0.000 description 3
- 235000013024 sodium fluoride Nutrition 0.000 description 3
- 239000011775 sodium fluoride Substances 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 229910001508 alkali metal halide Inorganic materials 0.000 description 2
- 150000008045 alkali metal halides Chemical class 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 238000005566 electron beam evaporation Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- 241000188156 Tamu Species 0.000 description 1
- 239000012190 activator Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- -1 alkali metal salts Chemical class 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000000975 co-precipitation Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000012790 confirmation Methods 0.000 description 1
- 238000007596 consolidation process Methods 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000000313 electron-beam-induced deposition Methods 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 229910000765 intermetallic Inorganic materials 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 239000008204 material by function Substances 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 239000002923 metal particle Substances 0.000 description 1
- 239000002114 nanocomposite Substances 0.000 description 1
- 239000002707 nanocrystalline material Substances 0.000 description 1
- 239000002121 nanofiber Substances 0.000 description 1
- 150000004767 nitrides Chemical class 0.000 description 1
- 229910052755 nonmetal Inorganic materials 0.000 description 1
- 150000002843 nonmetals Chemical class 0.000 description 1
- 230000006911 nucleation Effects 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 229910000679 solder Inorganic materials 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000012916 structural analysis Methods 0.000 description 1
- 239000002887 superconductor Substances 0.000 description 1
- 238000010301 surface-oxidation reaction Methods 0.000 description 1
- 238000007738 vacuum evaporation Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/06—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the coating material
- C23C14/0694—Halides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/24—Vacuum evaporation
- C23C14/28—Vacuum evaporation by wave energy or particle radiation
- C23C14/30—Vacuum evaporation by wave energy or particle radiation by electron bombardment
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Nanotechnology (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Composite Materials (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Crystallography & Structural Chemistry (AREA)
- Toxicology (AREA)
- Physical Vapour Deposition (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
Изобретение относится к способу получения нанопорошков материалов, инкапсулированных в оболочку из соли. В соответствии с изобретением, в замкнутом объеме создают вакуум и проводят одновременно испарение материала и соли со следующей конденсацией смеси их паровых фаз на поверхности подкладки. Испарение компонентов осуществляют путем нагрева заготовок материала и соли, положенной в тигле, посредством лучевой энергии электронных лучей или лучей лазера. Изобретение обеспечивает получение частиц материала наномасштабного размера с высокой степенью химической чистоты. Заявлена также установка для осуществления этого способа.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| UAA200702007A UA82448C2 (ru) | 2007-02-26 | 2007-02-26 | СПОСОБ ПОЛУЧЕНИЯ ИНКАПСУЛИРОВАННЫХ НАНОПОРОШКоВ И УСТАНОВКА ДЛЯ ЕГО ОСУЩЕСТВЛЕНИЯ |
| US12/035,468 US8491972B2 (en) | 2007-02-26 | 2008-02-22 | Method of producing encapsulated nanopowders and installation for its realization |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| UAA200702007A UA82448C2 (ru) | 2007-02-26 | 2007-02-26 | СПОСОБ ПОЛУЧЕНИЯ ИНКАПСУЛИРОВАННЫХ НАНОПОРОШКоВ И УСТАНОВКА ДЛЯ ЕГО ОСУЩЕСТВЛЕНИЯ |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| UA82448C2 true UA82448C2 (ru) | 2008-04-10 |
Family
ID=39818981
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| UAA200702007A UA82448C2 (ru) | 2007-02-26 | 2007-02-26 | СПОСОБ ПОЛУЧЕНИЯ ИНКАПСУЛИРОВАННЫХ НАНОПОРОШКоВ И УСТАНОВКА ДЛЯ ЕГО ОСУЩЕСТВЛЕНИЯ |
Country Status (2)
| Country | Link |
|---|---|
| US (1) | US8491972B2 (ru) |
| UA (1) | UA82448C2 (ru) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2010144070A2 (en) | 2009-06-10 | 2010-12-16 | Boris Paton | Method to produce nanoparticles of metal-oxygen system of the specified composition by electron beam evaporation and condensation in vacuum |
| RU2407102C2 (ru) * | 2009-03-10 | 2010-12-20 | Государственное образовательное учреждение высшего профессионального образования "Владимирский Государственный Университет" (ВлГУ) | Способ формирования наноструктур |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102010041003A1 (de) | 2010-09-20 | 2012-03-22 | Sb Limotive Company Ltd. | Verfahren zum Überwachen von mindestens zwei Mikrocontrollern |
| DE102014110802B3 (de) * | 2014-07-30 | 2015-12-31 | Ald Vacuum Technologies Gmbh | Herstellung von Nanopulvern |
| CN105986227A (zh) * | 2015-02-16 | 2016-10-05 | 中国科学院金属研究所 | 一种镧钙锰氧-氧化镍纳米复合薄膜材料及其制备方法 |
| CN106932318B (zh) * | 2015-12-30 | 2021-01-15 | 中国科学院电子学研究所 | 半导体泵浦碱金属蒸气激光器的诊断装置及方法 |
| RU2643287C2 (ru) * | 2016-04-19 | 2018-01-31 | Федеральное государственное бюджетное учреждение науки Институт электрофизики Уральского отделения Российской академии наук (ИЭФ УрО РАН) | Способ получения нанопорошка соединений и смесевых составов и устройство для его реализации |
| RU2643288C2 (ru) * | 2016-04-20 | 2018-01-31 | Федеральное государственное бюджетное учреждение науки Институт электрофизики Уральского отделения Российской академии наук (ИЭФ УрО РАН) | Способ получения нанопорошка неметалла |
| CN108044122B (zh) * | 2017-11-14 | 2020-03-27 | 中国航发北京航空材料研究院 | 一种Nb-Si基合金空心涡轮叶片的制备方法 |
| CN108044123B (zh) * | 2017-11-14 | 2020-03-31 | 中国航发北京航空材料研究院 | 一种具有定向凝固组织的Nb-Si-Ti合金制备方法 |
| CN108456853B (zh) * | 2018-03-12 | 2021-01-29 | Oppo广东移动通信有限公司 | 制备电子设备壳体的方法、电子设备壳体和电子设备 |
| CN110004411B (zh) * | 2019-03-29 | 2021-05-11 | 北京钢研新冶工程设计有限公司 | 一种合金镀膜方法 |
| CN110385442A (zh) * | 2019-09-05 | 2019-10-29 | 宁波广新纳米材料有限公司 | 一种太阳能电池银浆用超细银铋合金粉的生产方法 |
| CN111360257A (zh) * | 2020-03-27 | 2020-07-03 | 中国商用飞机有限责任公司 | 一种提升3d打印高强铝合金粉末成形性的方法 |
| CN118595449B (zh) * | 2024-08-08 | 2024-12-06 | 江苏镭纳新材料科技有限公司 | 一种基于等离子体的超细纳米粉体制造装置及其制造方法 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5498446A (en) * | 1994-05-25 | 1996-03-12 | Washington University | Method and apparatus for producing high purity and unagglomerated submicron particles |
| US20030145681A1 (en) * | 2002-02-05 | 2003-08-07 | El-Shall M. Samy | Copper and/or zinc alloy nanopowders made by laser vaporization and condensation |
| WO2006083326A2 (en) * | 2004-08-07 | 2006-08-10 | Cabot Corporation | Gas dispersion manufacture of nanoparticulates and nanoparticulate-containing products and processing thereof |
-
2007
- 2007-02-26 UA UAA200702007A patent/UA82448C2/ru unknown
-
2008
- 2008-02-22 US US12/035,468 patent/US8491972B2/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2407102C2 (ru) * | 2009-03-10 | 2010-12-20 | Государственное образовательное учреждение высшего профессионального образования "Владимирский Государственный Университет" (ВлГУ) | Способ формирования наноструктур |
| WO2010144070A2 (en) | 2009-06-10 | 2010-12-16 | Boris Paton | Method to produce nanoparticles of metal-oxygen system of the specified composition by electron beam evaporation and condensation in vacuum |
| WO2010144070A3 (en) * | 2009-06-10 | 2011-05-26 | Boris Paton | Method to produce nanoparticles of metal-oxygen system of the specified composition by electron beam evaporation and condensation in vacuum |
Also Published As
| Publication number | Publication date |
|---|---|
| US8491972B2 (en) | 2013-07-23 |
| US20080268178A1 (en) | 2008-10-30 |
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