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TWI863751B - Device and method for measuring permeability of reinforced fiber mat in resin transfer molding system - Google Patents

Device and method for measuring permeability of reinforced fiber mat in resin transfer molding system Download PDF

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TWI863751B
TWI863751B TW112148756A TW112148756A TWI863751B TW I863751 B TWI863751 B TW I863751B TW 112148756 A TW112148756 A TW 112148756A TW 112148756 A TW112148756 A TW 112148756A TW I863751 B TWI863751 B TW I863751B
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fiber mat
reinforcing fiber
resin
mold cavity
transfer molding
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TW112148756A
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TW202524060A (en
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張智淵
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台鋼學校財團法人台鋼科技大學
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Abstract

一種樹脂轉移成型系統中補強纖維蓆滲透率的測量裝置與方法。該測量方法是將圓環狀的補強纖維蓆同軸置放在圓形模穴中,將補強纖維蓆壓縮成孔隙呈徑向往內或往外逐漸變小狀,並以固定的液體體積流率將樹脂注入模穴。分析取得樹脂之流動前緣移動至補強纖維蓆之各半徑位置時的充填時間與液體壓力。根據模穴、補強纖維蓆之相關參數、該流動前緣移動至每一半徑位置的充填時間與液體壓力值,演算出每一孔隙率對應的科忍尼常數與滲透度。透過該測量方法設計,可在一次樹脂充填過程中,量測取得補強纖維蓆之各種孔隙率對應的滲透度,相當方便實用。A device and method for measuring the permeability of a reinforcing fiber mat in a resin transfer molding system. The measuring method is to coaxially place a ring-shaped reinforcing fiber mat in a circular mold cavity, compress the reinforcing fiber mat into a state where the pores gradually decrease in diameter inward or outward, and inject the resin into the mold cavity at a fixed liquid volume flow rate. The filling time and liquid pressure when the flow front of the resin moves to each radial position of the reinforcing fiber mat are analyzed and obtained. According to the relevant parameters of the mold cavity and the reinforcing fiber mat, the filling time when the flow front moves to each half-diameter position and the liquid pressure value, the König constant and permeability corresponding to each porosity are calculated. Through the design of this measurement method, the permeability corresponding to various porosities of the reinforcing fiber mat can be measured in a single resin filling process, which is very convenient and practical.

Description

樹脂轉移成型系統中補強纖維蓆滲透率的測量裝置與方法Device and method for measuring permeability of reinforced fiber mat in resin transfer molding system

本發明是有關於一種用於樹脂轉移成型之測量裝置與方法,特別是指一種用以測量樹脂轉移成型所使用之補強纖維蓆之滲透度的測量裝置與方法。The present invention relates to a measuring device and method for resin transfer molding, and more particularly to a measuring device and method for measuring the permeability of a reinforcing fiber mat used in resin transfer molding.

補強纖維蓆如玻璃纖維或碳纖維等,經常被用以和樹脂結合以製成纖維複合材料,這類纖維複合材料具有質輕以及高機械強度的特性,因此廣受運輸與運動產業的喜愛。Reinforced fiber mats such as glass fiber or carbon fiber are often combined with resins to make fiber composites. Such fiber composites have the characteristics of light weight and high mechanical strength, and are therefore widely favored by the transportation and sports industries.

樹脂轉移成型技術是目前用以製作纖維複合材料的常見方法。會先將裁切好的補強纖維蓆疊置於模穴內部,然後射入熱固性的樹脂,使其完全滲入補強纖維蓆並硬化後,就可得纖維複合材料。要使用樹脂轉移成型製造高品質纖維複合材料成品,事先了解補強纖維蓆在各種孔隙率下的滲透度是極為重要的。因為這會影響樹脂在纖維孔隙內流動情形、充填所需時間,也會影響成品機械性質。Resin transfer molding technology is a common method used to make fiber composites. The cut fiber mats are stacked and placed inside the mold cavity, and then the thermosetting resin is injected to completely penetrate the fiber mats and harden to obtain the fiber composite. To use resin transfer molding to manufacture high-quality fiber composite products, it is extremely important to understand the permeability of the fiber mats at various porosities in advance. This is because it will affect the flow of resin in the fiber pores, the time required for filling, and the mechanical properties of the finished product.

現有量測補強纖維蓆之滲透度的方法,是將特定孔隙率的補強纖維蓆置入一個轉注成型單元的模穴中,並透過以固定之液體體積流率將樹脂注入該模穴,並透過樹脂於模穴中的流動速度、模穴的壓力變化與該補強纖維蓆的孔隙率,來演算出該補強纖維蓆的滲透度。但目前的方法僅能獲得單一孔隙率之補強纖維蓆的滲透度,如要知道其它孔隙率之補強纖維蓆的滲透度時,得要反覆多次實驗,相當費時。The existing method for measuring the permeability of a reinforcing fiber mat is to place a reinforcing fiber mat of a specific porosity into a mold cavity of a transfer molding unit, and inject resin into the mold cavity at a fixed liquid volume flow rate, and calculate the permeability of the reinforcing fiber mat through the flow rate of the resin in the mold cavity, the pressure change in the mold cavity and the porosity of the reinforcing fiber mat. However, the current method can only obtain the permeability of a reinforcing fiber mat with a single porosity. If you want to know the permeability of reinforcing fiber mats with other porosities, you have to repeat multiple experiments, which is very time-consuming.

因此,本發明的目的,即在提供一種能改善先前技術的至少一個缺點的樹脂轉移成型系統的測量方法。Therefore, an object of the present invention is to provide a measurement method for a resin transfer molding system that can improve at least one disadvantage of the prior art.

於是,本發明樹脂轉移成型系統的測量方法,適用於一次量測取得一補強纖維蓆之各種孔隙率對應的滲透度。該測量方法包含以下步驟:Therefore, the measurement method of the resin transfer molding system of the present invention is applicable to obtaining the permeability corresponding to various porosities of a reinforcing fiber mat in one measurement. The measurement method comprises the following steps:

調變孔隙率步驟。將一圓環狀的補強纖維蓆同軸地水平置放在一個轉注成型單元的一個圓形的模穴中。該轉注成型單元之該模穴的高度是自其中心徑向往內或往外漸低,而會徑向往內或往外逐漸壓縮該補強纖維蓆,使該補強纖維蓆的孔隙呈徑向往內或往外逐漸變小狀。The porosity adjustment step is to coaxially and horizontally place a circular reinforcing fiber mat in a circular mold cavity of a transfer molding unit. The height of the mold cavity of the transfer molding unit is gradually reduced from the center radially inward or outward, and the reinforcing fiber mat is gradually compressed radially inward or outward, so that the pores of the reinforcing fiber mat are gradually reduced radially inward or outward.

分析取得孔隙率步驟。使一分析模組根據該補強纖維蓆之單位面積質量(A w)與密度(D f)、該補強纖維蓆在半徑位置r處的高度(h),演算取得該補強纖維蓆在該模穴之不同半徑位置r的孔隙率(Φ)。 The step of analyzing and obtaining the porosity is to enable an analysis module to calculate and obtain the porosity (Φ) of the reinforcing fiber mat at different radial positions r of the mold cavity according to the unit area mass (A w ) and density (D f ) of the reinforcing fiber mat and the height (h) of the reinforcing fiber mat at the radial position r.

注入樹脂步驟。使一樹脂注射器以固定的液體體積流率將樹脂注入該模穴中心,使樹脂徑向外流動滲入該補強纖維蓆之孔隙中。The resin injection step is to inject the resin into the center of the mold cavity with a resin syringe at a fixed liquid volume flow rate, so that the resin flows radially outward and penetrates into the pores of the reinforcing fiber mat.

影像擷取步驟。使一影像擷取器擷取所述樹脂於該補強纖維蓆中徑向往外流動的影像。使該分析模組分析所述影像,取得所述樹脂之流動前緣移動至該模穴之各個半徑位置時的充填時間(t)。An image capture step is to use an image capturer to capture an image of the resin flowing radially outward in the reinforcing fiber mat. The analysis module is used to analyze the image to obtain the filling time (t) when the flow front edge of the resin moves to each radial position of the mold cavity.

模穴壓力擷取步驟。使壓力感測器量測取得該補強纖維蓆內周緣在各個充填時間的液體壓力(P i)。 The step of acquiring the cavity pressure is to use a pressure sensor to measure the liquid pressure (P i ) at the inner periphery of the reinforcing fiber mat at each filling time.

分析取得科忍尼常數步驟。使該分析模組根據該模穴的尺寸參數、該補強纖維蓆之單位面積質量(A w)、每一半徑位置的該孔隙率、該流動前緣移動至每一半徑位置的該充填時間,及各充填時間點之該液體壓力值,演算出每一孔隙率對應的科忍尼常數(k c)。 The step of analyzing and obtaining the Korenyi constant is to make the analysis module calculate the Korenyi constant (k c ) corresponding to each porosity according to the size parameters of the mold cavity, the unit area mass of the reinforcing fiber mat (A w ), the porosity at each semi-diameter position, the filling time when the flow front moves to each semi-diameter position, and the liquid pressure value at each filling time point.

取得滲透度步驟。使該分析模組根據該補強纖維蓆之每一該孔隙率對應的該科忍尼常數,演算出每一該孔隙率對應的滲透度。The step of obtaining the permeability is to make the analysis module calculate the permeability corresponding to each porosity of the reinforcing fiber mat according to the Korenyi constant corresponding to each porosity of the reinforcing fiber mat.

本發明之功效在於:透過該測量方法的設計,可在一次樹脂充填過程中,量測取得該補強纖維蓆之各種孔隙率對應的滲透度,相當方便實用。The utility of the present invention is that through the design of the measuring method, the permeability corresponding to various porosities of the reinforcing fiber mat can be measured in one resin filling process, which is very convenient and practical.

本發明的另一目的,即在提供一種能改善先前技術的至少一個缺點的樹脂轉移成型系統的測量裝置。Another object of the present invention is to provide a measuring device for a resin transfer molding system that can improve at least one disadvantage of the prior art.

該樹脂轉移成型系統的測量裝置,適用於一次量測取得一補強纖維蓆之各種孔隙率對應的滲透度。該補強纖維蓆呈圓環狀。該測量裝置包含一個轉注成型單元、一個樹脂注射器、一個壓力感測器、一個影像擷取器,及一個分析模組。The measuring device of the resin transfer molding system is suitable for measuring and obtaining the permeability corresponding to various porosities of a reinforcing fiber mat at one time. The reinforcing fiber mat is in a ring shape. The measuring device includes a transfer molding unit, a resin injector, a pressure sensor, an image capturer, and an analysis module.

該轉注成型單元內部界定出一個上下軸向且用以同軸容置該補強纖維蓆之圓形的模穴。該模穴之高度是呈自中心徑向往外漸高或漸低狀。轉注成型單元會往該模穴高度漸低方向逐漸壓縮該補強纖維蓆。The transfer molding unit defines a circular mold cavity in the vertical direction and is used to coaxially accommodate the reinforcing fiber mat. The height of the mold cavity is gradually increased or decreased from the center diameter to the outside. The transfer molding unit will gradually compress the reinforcing fiber mat in the direction of the mold cavity height decreasing.

該樹脂注射器容裝有樹脂,可被驅動而以一預定之液體體積流率將所述樹脂注入該模穴位在該補強纖維蓆內周側的區間,使所述樹脂徑向往外滲流進入該補強纖維蓆中。The resin injector contains resin and can be driven to inject the resin into the area of the mold cavity on the inner circumference of the reinforcing fiber mat at a predetermined liquid volume flow rate, so that the resin radially permeates outward into the reinforcing fiber mat.

該壓力感測器可用以量測該模穴位於該補強纖維蓆內周緣的液體壓力。該影像擷取器可用以朝該轉注成型單元進行影像擷取,以取得該模穴中之所述樹脂在該補強纖維蓆中滲透流動的影像。The pressure sensor can be used to measure the liquid pressure of the mold cavity at the inner periphery of the reinforcing fiber mat. The image capturer can be used to capture images toward the transfer molding unit to obtain images of the resin in the mold cavity penetrating and flowing in the reinforcing fiber mat.

該分析模組訊號連接該壓力感測器與該影像擷取器,包括一個影像分析單元與一個演算單元。該影像分析單元可分析所述影像以取得所述樹脂之流動前緣位於該模穴的半徑位置和對應的該充填時間(t)。該演算單元可根據該補強纖維蓆被壓縮後相對於該模穴中心的每一半徑位置的孔隙率、所述流動前緣移動至每一半徑位置的充填時間、每一充填時間之該液體壓力值,及該模穴的尺寸參數,演算出每一孔隙率對應的滲透度。The analysis module signal connects the pressure sensor and the image capturer, and includes an image analysis unit and a calculation unit. The image analysis unit can analyze the image to obtain the radial position of the flow front edge of the resin in the mold cavity and the corresponding filling time (t). The calculation unit can calculate the permeability corresponding to each porosity according to the porosity of each radial position relative to the center of the mold cavity after the reinforcing fiber mat is compressed, the filling time when the flow front edge moves to each radial position, the liquid pressure value at each filling time, and the size parameters of the mold cavity.

本發明之功效在於:透過該轉注成型單元之該模穴的結構設計,以及該樹脂注射器、該壓力感測器、該影像擷取器與該分析模組的設計,可透過單一次樹脂填充過程,量測取得該補強纖維蓆在各種不同孔隙率情況下的滲透度,相當方便實用。The utility model has the following advantages: through the structural design of the mold cavity of the transfer molding unit, and the design of the resin injector, the pressure sensor, the image capturer and the analysis module, the permeability of the reinforcing fiber mat under various porosity conditions can be measured through a single resin filling process, which is quite convenient and practical.

參閱圖1、2、3,本發明樹脂轉移成型系統中補強纖維蓆滲透率的測量裝置200的一個實施例,適用於一次量測多種孔隙率之補強纖維蓆800的滲透度。該補強纖維蓆800是呈圓環片狀,厚度為h i,內徑為r i,外徑為r o。實施時,該補強纖維蓆800可以是單一片結構物,或者是由多片補強纖維物件層疊構成。該補強纖維蓆800之密度為D f,單位面積質量A wReferring to Figures 1, 2, and 3, an embodiment of a measuring device 200 for the permeability of a reinforcing fiber mat in a resin transfer molding system of the present invention is suitable for measuring the permeability of a reinforcing fiber mat 800 of multiple porosities at one time. The reinforcing fiber mat 800 is in the shape of a circular ring sheet with a thickness of hi , an inner diameter of ri , and an outer diameter of r o . During implementation, the reinforcing fiber mat 800 can be a single sheet structure, or it can be composed of multiple sheets of reinforcing fiber objects stacked in layers. The density of the reinforcing fiber mat 800 is D f , and the mass per unit area is A w .

該測量裝置200包含一個轉注成型單元3、一個連通組接於該轉注成型單元3之樹脂注射器4、一個安裝在該轉注成型單元3之壓力感測器5、一個設置在該轉注成型單元3上方的影像擷取器6,及一個訊號連接該壓力感測器5與該影像擷取器6的分析模組7。The measuring device 200 includes a transfer molding unit 3, a resin syringe 4 connected to the transfer molding unit 3, a pressure sensor 5 installed on the transfer molding unit 3, an image capturer 6 arranged above the transfer molding unit 3, and an analysis module 7 that connects the pressure sensor 5 and the image capturer 6 by signal.

該轉注成型單元3包括一個下模具31、一個疊蓋在該下模具31上方的上模具32,及一個設置在該上模具32的尺規33。該下模具31與該上模具32相配合界定出一個上下軸向之圓形的模穴30。該模穴30之半徑與該補強纖維蓆800之外周緣半徑相同,可用以供該補強纖維蓆800同軸設置。The transfer molding unit 3 includes a lower mold 31, an upper mold 32 overlapping the lower mold 31, and a ruler 33 disposed on the upper mold 32. The lower mold 31 cooperates with the upper mold 32 to define a circular mold cavity 30 in the vertical axial direction. The radius of the mold cavity 30 is the same as the outer peripheral radius of the reinforcing fiber mat 800, so that the reinforcing fiber mat 800 can be coaxially disposed.

該下模具31具有一個界定出該模穴30之水平底緣的穴底面310,且還具有一個上下貫穿且與該模穴30中心連通的填充孔311,及多個上下貫穿且分佈在其鄰近周緣部位而連通該模穴30與外界的排氣孔312。The lower mold 31 has a cavity bottom surface 310 defining the horizontal bottom edge of the cavity 30, and also has a filling hole 311 that penetrates up and down and is connected to the center of the cavity 30, and a plurality of exhaust holes 312 that penetrate up and down and are distributed in the vicinity of the cavity 30 to connect the cavity 30 with the outside.

該上模具32是呈透明狀,並具有一個與該穴底面310間隔相向,且界定出該模穴30頂緣的穴頂面320。該穴頂面320具有一個於該模穴30中心且半徑為r i之水平狀的中心面部321,及一個自該中心面部321周緣徑向往外並往下傾斜延伸的環面部322。 The upper mold 32 is transparent and has a cavity top surface 320 which is spaced from the cavity bottom surface 310 and defines the top edge of the cavity 30. The cavity top surface 320 has a horizontal central surface 321 with a radius of ri at the center of the cavity 30, and an annular surface 322 extending radially outward and downward from the circumference of the central surface 321.

該模穴30具有一個位於該中心面部321下方的中心區間301,及一個環繞在該中心區間301周圍且高度呈徑向往外漸低的滲流區間302。該中心區間301的高度等於該補強纖維蓆800的厚度(h i),該滲流區間302的高度小於所述厚度(h i)。因此,當該補強纖維蓆800同軸設置在該模穴30時,該中心區間301會對應該補強纖維蓆800之內周緣環繞的區間,該補強纖維蓆800實際上會位在該滲流區間302中,所以該環面部322會往下壓縮位在該滲流區間302內的該補強纖維蓆800,使該補強纖維蓆800的厚度呈徑向往外逐漸變小狀,相對的,使該補強纖維蓆800之孔隙率呈徑向往外逐漸變小狀。 The mold cavity 30 has a central zone 301 located below the central surface 321, and a permeation zone 302 surrounding the central zone 301 and decreasing in height radially outward. The height of the central zone 301 is equal to the thickness ( hi ) of the reinforcing fiber mat 800, and the height of the permeation zone 302 is less than the thickness ( hi ). Therefore, when the reinforcing fiber mat 800 is coaxially disposed in the mold cavity 30, the central zone 301 will correspond to the zone surrounding the inner periphery of the reinforcing fiber mat 800, and the reinforcing fiber mat 800 will actually be located in the permeation zone 302, so the annular portion 322 will compress the reinforcing fiber mat 800 located in the permeation zone 302 downward, so that the thickness of the reinforcing fiber mat 800 gradually decreases radially outward, and correspondingly, the porosity of the reinforcing fiber mat 800 gradually decreases radially outward.

該尺規33是設置在該上模具32頂面,並相對該模穴30中心徑向往外延伸橫跨整個該模穴30。The ruler 33 is disposed on the top surface of the upper mold 32 and extends outward relative to the center diameter of the mold cavity 30 to span the entire mold cavity 30 .

該樹脂注射器4連通組接於該填充孔311,並可被啟動而以一預定的液體體積流率(q i)將所述樹脂801加壓注入該模穴30之該中心區間301,使所述樹脂801從該中心區間301徑向外擴滲入該補強纖維蓆800中。由於該樹脂注射器4為現有構件且類型眾多,也非本發明改良重點,因此不再詳述。 The resin injector 4 is connected to the filling hole 311 and can be activated to inject the resin 801 into the central section 301 of the mold cavity 30 at a predetermined liquid volume flow rate (q i ) under pressure, so that the resin 801 diffuses radially outward from the central section 301 into the reinforcing fiber mat 800. Since the resin injector 4 is an existing component with many types and is not the focus of the present invention, it will not be described in detail.

該壓力感測器5設置在該模穴30之該中心區間301中,且鄰近該補強纖維蓆800之內周緣,可用以感測位於該補強纖維蓆800內周緣(也就是半徑r i處)之所述樹脂801產生的液體壓力。 The pressure sensor 5 is disposed in the central area 301 of the mold cavity 30 and adjacent to the inner periphery of the reinforcing fiber mat 800, and can be used to sense the liquid pressure generated by the resin 801 located at the inner periphery of the reinforcing fiber mat 800 (i.e., at the radius ri ).

該影像擷取器6設置在該轉注成型單元3上方,可用以往下朝該上模具32與該尺規33進行影像擷取,可用以擷取所述樹脂801在該模穴30中流動的影像與該尺規33的影像。The image capturer 6 is disposed above the transfer molding unit 3 and can be used to capture images of the upper mold 32 and the ruler 33 downward, and can be used to capture the image of the resin 801 flowing in the mold cavity 30 and the image of the ruler 33.

參閱圖1、3、4,該分析模組7包括一個影像分析單元71、一個演算單元72,及一個驗證單元73。1 , 3 , and 4 , the analysis module 7 includes an image analysis unit 71 , a calculation unit 72 , and a verification unit 73 .

該影像分析單元71可分析該影像擷取器6取得之影像,可透過目前已知的影像辨識技術分析辨識出所述樹脂801在該補強纖維蓆800中流動時的一流動前緣802,以及該流動前緣802對應該尺規33的刻度,進而得到所述樹脂801之該流動前緣802於該模穴30中的半徑位置(r)。The image analysis unit 71 can analyze the image obtained by the image capture device 6, and can analyze and identify a flow front edge 802 of the resin 801 when it flows in the reinforcing fiber mat 800 through currently known image recognition technology, and the flow front edge 802 corresponds to the scale of the ruler 33, thereby obtaining the radial position (r) of the flow front edge 802 of the resin 801 in the mold cavity 30.

依流體力學理論,當該模穴30之半徑遠大於該補強纖維蓆800的厚度時,該模穴30內之所述樹脂801在該補強纖維蓆800中的流動,可視為液體在多孔性介質的準穩態薄殼流動,樹脂流動速度以達西定律進行描述,容後說明。由於流場的對稱性,所述樹脂801會呈現出一維徑向流動,也就是會從該中心區間301向四周均勻擴散的流動,所以所述樹脂801的在該補強纖維蓆800中流動的流動前緣802的整體形狀應該會概呈圓形。一旦該流動前緣802的形狀偏差圓形超過一定幅度時,表示該轉注成型單元3出現傾斜。該影像分析單元71會進一步分析所述樹脂801的該流動前緣802所構成之形狀,並於判斷所述形狀相對於正圓形偏差大於等於1%以上時,發出一個警示訊息,表示得重新實驗。According to fluid mechanics theory, when the radius of the mold cavity 30 is much larger than the thickness of the reinforcing fiber mat 800, the flow of the resin 801 in the mold cavity 30 in the reinforcing fiber mat 800 can be regarded as a quasi-steady-state thin shell flow of liquid in a porous medium, and the resin flow velocity is described by Darcy's law, which will be explained later. Due to the symmetry of the flow field, the resin 801 will present a one-dimensional radial flow, that is, a flow that diffuses uniformly from the central area 301 to the surroundings, so the overall shape of the flow front 802 of the resin 801 flowing in the reinforcing fiber mat 800 should be roughly circular. Once the shape deviation of the flow front edge 802 exceeds a certain range from the circle, it indicates that the transfer molding unit 3 is tilted. The image analysis unit 71 will further analyze the shape formed by the flow front edge 802 of the resin 801, and when it is determined that the shape deviates from the perfect circle by more than 1%, a warning message is issued, indicating that the experiment must be repeated.

所述影像辨識技術大致包括影像二值化處理、雜訊濾除、邊界偵測辨識等。由於所述影像辨識技術為現有影像分析處理技術,且方式眾多,因此不再詳述。The image recognition technology generally includes image binarization processing, noise filtering, boundary detection and recognition, etc. Since the image recognition technology is an existing image analysis and processing technology and there are many ways, it will not be described in detail.

該演算單元72內建有演算程式,可用以演算得到該補強纖維蓆800在每一半徑位置r處的孔隙率(Φ)、每一孔隙率(Φ)對應的科忍尼常數(k c),以及每一孔隙率(Φ)對應的滲透度(K)。關於該演算單元72演算取得該孔隙率、該科忍尼常數與該滲透度的方式,說明如下。 The calculation unit 72 has a built-in calculation program that can be used to calculate the porosity (Φ) of the reinforcing fiber mat 800 at each half-diameter position r, the Korenyi constant (k c ) corresponding to each porosity (Φ), and the permeability (K) corresponding to each porosity (Φ). The method for the calculation unit 72 to calculate the porosity, the Korenyi constant and the permeability is described as follows.

關於取得該補強纖維蓆800之各個半徑位置r處的孔隙率(Φ)。該演算單元72於演算取得該補強纖維蓆800之某一半徑位置r處的孔隙率(Φ)時,會先透過圓柱殼法(Shell method)將該半徑位置r處的模穴體積與纖維總體積求出,再將兩者相除後,就可得纖維體積分率(Φ f ),請參公式(1)。h為在半徑位置r處的模穴高度,如公式(2)所示,其中,m=(ho-hi)/(ro-ri),r i為該補強纖維蓆800之內周緣的半徑, r o為該補強纖維蓆800之外周緣的半徑,h i為該補強纖維蓆800在半徑位置r i處的厚度,h o為該補強纖維蓆800在半徑位置r o處的厚度。2πrdr是微積分表示方法,表示在位置r處向外延伸一微小距離dr,也就是位置r+dr。半徑位置r到半徑位置r+dr的環狀面積是2πrdr。將環狀面積乘上A w,即為半徑位置r處的環狀面積纖維質量,將環狀面積乘上高度,即為半徑位置r處的模穴體積。 Regarding obtaining the porosity (Φ) at each radial position r of the reinforcing fiber mat 800. When the calculation unit 72 calculates the porosity (Φ) at a certain radial position r of the reinforcing fiber mat 800, the cavity volume and the total fiber volume at the radial position r are first calculated by the cylindrical shell method, and then the fiber volume fraction (Φ f ) is obtained by dividing the two, see formula (1). h is the height of the mold cavity at the radius position r, as shown in formula (2), where m=(ho-hi)/(ro-ri), ri is the radius of the inner periphery of the reinforcing fiber mat 800, ro is the radius of the outer periphery of the reinforcing fiber mat 800, hi is the thickness of the reinforcing fiber mat 800 at the radius position ri , and ho is the thickness of the reinforcing fiber mat 800 at the radius position r o . 2πrdr is a calculus representation method, which means that a small distance dr is extended outward from position r, that is, position r+dr. The annular area from radius position r to radius position r+dr is 2πrdr. Multiplying the annular area by A w gives the annular area fiber mass at the radius position r, and multiplying the annular area by the height gives the cavity volume at the radius position r.

因為纖維體積分率(Φ f )與孔隙率(Φ)的關係為Φ f +Φ=1,所以可進一步得到孔隙率(Φ),請參公式(3)。 公式(1) 公式(2) 公式(3) Since the relationship between the fiber volume fraction (Φ f ) and the porosity (Φ) is Φ f +Φ = 1, the porosity (Φ) can be further obtained, see formula (3). Formula (1) Formula (2) Formula (3)

以下說明關於該補強纖維蓆800之各種孔隙率對應之科忍尼常數(k c)的取得。 The following describes how to obtain the Korenyi constant (k c ) corresponding to various porosities of the reinforcing fiber mat 800.

將所述樹脂801的動量方程式(以達西定律取代),如公式(4)。其中, v是所述樹脂的達西速度,μ為所述樹脂的黏度,K是該補強纖維蓆800的滲透度,P為該補強纖維蓆800中之樹脂壓力。 公式(4) The momentum equation of the resin 801 (replaced by Darcy's law) is as shown in Formula (4). Wherein, v is the Darcy velocity of the resin, μ is the viscosity of the resin, K is the permeability of the reinforcing fiber mat 800, and P is the resin pressure in the reinforcing fiber mat 800. Formula (4)

因為是所述樹脂801在該模穴30中是呈對稱的徑向流動,所述樹脂801的流速 ,代入公式(4),可得公式(5)。 公式(5) Because the resin 801 flows symmetrically radially in the mold cavity 30, the flow rate of the resin 801 is , substituting into formula (4), we can get formula (5). Formula (5)

對已充填所述樹脂801的該補強纖維蓆800區域,從半徑位置r i(液體壓力P i),積分至該流動前緣802所在之半徑位置r(液體壓力為0),進而可得半徑位置r i的液體壓力P i,如公式(6)。半徑位置r處的壓力使用的是錶壓力表示法,故液體壓力為0。 公式(6) For the area of the reinforcing fiber mat 800 filled with the resin 801, the liquid pressure Pi at the radial position ri (liquid pressure Pi ) is integrated from the radial position ri (liquid pressure is 0) to the radial position r (liquid pressure is 0) where the flow front 802 is located, and then the liquid pressure Pi at the radial position ri can be obtained, as shown in formula (6). The pressure at the radial position r is expressed in gauge pressure, so the liquid pressure is 0. Formula (6)

使用Kozeny-Carman公式,如公式(7)。 公式(7) Use the Kozeny-Carman formula, as shown in formula (7). Formula (7)

將公式(2)、(3)和(7)代入公式(6),得公式(8)。 公式(8) Substituting formulas (2), (3) and (7) into formula (6), we obtain formula (8). Formula (8)

將公式(8)演算後,可得公式(9)。 公式(9) After calculating formula (8), we can get formula (9). Formula (9)

可透過公式(9)演算取得所述樹脂801之該流動前緣802位移至半徑位置r時之孔隙率條件下的該科忍尼常數(k c)。其中。Φ i為該補強纖維蓆800之半徑位置r i處的孔隙率,也就是該補強纖維蓆800之內周緣處的孔隙率。 The Korenyi constant (k c ) under the porosity condition when the flow front 802 of the resin 801 moves to the radial position r can be calculated by formula (9). Wherein, Φ i is the porosity at the radial position r i of the reinforcing fiber mat 800, that is, the porosity at the inner periphery of the reinforcing fiber mat 800.

接著,該演算單元72會根據該補強纖維蓆800之多個半徑位置的該等孔隙率與對應之該等科忍尼常數,演算得到科忍尼常數與孔隙率的迴歸曲線。該演算單元72取得該迴歸曲線後,就可由該迴歸曲線比對出對應的科忍尼常數。Next, the calculation unit 72 calculates a regression curve of the Korenyi constant and the porosity according to the porosities and the corresponding Korenyi constants at multiple radial positions of the reinforcing fiber mat 800. After the calculation unit 72 obtains the regression curve, the corresponding Korenyi constant can be compared with the regression curve.

最後,該演算模組可根據所得到之科忍尼常數(k c),輸入之任一孔隙率,進一步透過公式(7)演算取得具有該孔隙率之該補強纖維蓆800的滲透度(K)。 Finally, the calculation module can further calculate the permeability (K) of the reinforcing fiber mat 800 having any porosity input according to the obtained Korenyi constant (k c ) through formula (7).

該驗證單元73可在所述樹脂801充填過程中,同步分析該模穴30或該樹脂注入器4是否出現洩漏情況,或該補強纖維蓆800內部孔隙充填不完全。The verification unit 73 can simultaneously analyze whether the mold cavity 30 or the resin injector 4 has leakage, or whether the internal pores of the reinforcing fiber mat 800 are not completely filled during the resin 801 filling process.

當所述樹脂801流入該補強纖維蓆800後,在充填時間t,所述樹脂801流到該補強纖維蓆800之半徑位置r處時,流入該補強纖維蓆800的樹脂體積量Q,可以使用微積分方式求得,如公式(10) 公式(10) After the resin 801 flows into the reinforcing fiber mat 800, at the filling time t, when the resin 801 flows to the radial position r of the reinforcing fiber mat 800, the volume Q of the resin flowing into the reinforcing fiber mat 800 can be obtained using the calculus method, as shown in formula (10) Formula (10)

因該樹脂注射器4是以固定的液體體積流率(q i)將所述樹脂801注入該模穴30中,所以將該液體體積流率乘以充填時間t k,就可得到注入該模穴30中的樹脂體積Q。因質量不滅,所以可得公式(11)。 Q=q i*t k 公式(11) Since the resin injector 4 injects the resin 801 into the mold cavity 30 at a fixed liquid volume flow rate (q i ), the volume Q of the resin injected into the mold cavity 30 can be obtained by multiplying the liquid volume flow rate by the filling time t k . Since the mass is not destroyed, the formula (11) can be obtained. Q=q i *t k Formula (11)

該驗證單元73可根據該液體體積流率(q i)與該流動前緣802位移至一半徑位置r時的充填時間(t),計算出該模穴30在該充填時間(t)時所容置的樹脂體積量(Q)。然後,該驗證單元73會透過公式(11)演算出所述樹脂801之該流動前緣802位移至該半徑位置r時的理論時間(t k),並分析判斷該理論時間(t k)與該充填時間(t)的差值,若該理論時間與該充填時間的差值過大,表示樹脂注入器4或該轉注成型單元3可能出現洩漏情況,或該補強纖維蓆800內部孔隙充填不完全情況。在本實施例中,該驗證單元73會於判斷該理論時間和該實際時間的差值超過1秒時,發出一個警示訊息,表示得重新試驗。 The verification unit 73 can calculate the resin volume (Q) contained in the mold cavity 30 at the filling time (t) according to the liquid volume flow rate (q i ) and the filling time (t) when the flow front edge 802 moves to the half-diameter position r. Then, the verification unit 73 calculates the theoretical time (t k ) when the flow front 802 of the resin 801 moves to the radius position r through formula (11), and analyzes and determines the difference between the theoretical time (t k ) and the filling time (t). If the difference between the theoretical time and the filling time is too large, it indicates that the resin injector 4 or the transfer molding unit 3 may leak, or the internal pores of the reinforcing fiber mat 800 are not completely filled. In this embodiment, the verification unit 73 will issue a warning message when it is determined that the difference between the theoretical time and the actual time exceeds 1 second, indicating that the test must be repeated.

參閱圖1、3、4、5,本發明樹脂轉移成型系統的測量裝置200用於分析取得該補強纖維蓆800在不同孔隙率情況下的滲透度時,所執行之測量方法的一個實施例包含以下步驟:Referring to FIGS. 1, 3, 4, and 5, the measuring device 200 of the resin transfer molding system of the present invention is used to analyze and obtain the permeability of the reinforcing fiber mat 800 under different porosities. An embodiment of the measuring method includes the following steps:

調變孔隙率步驟901。將該補強纖維蓆800同軸地水平置放在該轉注成型單元3的該模穴30中,而將該補強纖維蓆800壓縮成厚度呈徑向往外逐漸變小狀,使該補強纖維蓆800的孔隙呈徑向往外逐漸變小狀。Porosity adjustment step 901: The reinforcing fiber mat 800 is coaxially and horizontally placed in the mold cavity 30 of the transfer molding unit 3, and the reinforcing fiber mat 800 is compressed to a thickness that gradually decreases in diameter outward, so that the pores of the reinforcing fiber mat 800 gradually decrease in diameter outward.

分析取得孔隙率步驟902。使該分析模組7的該演算單元72根據該模穴30的尺寸參數、該補強纖維蓆800被壓縮後之半徑位置r處的纖維總體積,以公式(2)與公式(3)演算取得該補強纖維蓆800位於半徑位置r處的孔隙率(Φ)。Analyze and obtain porosity step 902. The calculation unit 72 of the analysis module 7 calculates the porosity (Φ) of the reinforcing fiber mat 800 at the radial position r according to the size parameters of the mold cavity 30 and the total volume of the fiber at the radial position r after the reinforcing fiber mat 800 is compressed using formula (2) and formula (3).

注入樹脂步驟903。使該樹脂注射器4以固定的該液體體積流率(qi)將樹脂801注入該模穴30的該中心區間301,使樹脂801徑向往外流動滲入該補強纖維蓆800之孔隙中。Resin injection step 903 : The resin injector 4 injects the resin 801 into the central area 301 of the mold cavity 30 at a fixed liquid volume flow rate (qi), so that the resin 801 flows radially outward and penetrates into the pores of the reinforcing fiber mat 800 .

影像擷取步驟904。使該影像擷取器6擷取所述樹脂801於該補強纖維蓆800中徑向往外流動的影像與該尺規33的影像。於此同時,該分析模組7之該影像分析單元71會分析所述影像,以取得所述樹脂801之該流動前緣802移動至該模穴30之各個半徑位置時的該充填時間(t)。Image capture step 904. The image capture device 6 captures the image of the resin 801 flowing radially outward in the reinforcing fiber mat 800 and the image of the ruler 33. At the same time, the image analysis unit 71 of the analysis module 7 analyzes the image to obtain the filling time (t) when the flow front edge 802 of the resin 801 moves to each radial position of the mold cavity 30.

模穴壓力擷取步驟905。使該壓力感測器5量測取得該補強纖維蓆800內周緣在各個充填時間的液體壓力(P i)。 The cavity pressure acquisition step 905 is to make the pressure sensor 5 measure the liquid pressure (P i ) of the inner periphery of the reinforcing fiber mat 800 at each filling time.

分析科忍尼常數步驟906。使該演算單元72透過公式(9)演算取得所述樹脂801之該流動前緣802位移至半徑位置r時之孔隙率條件下的所述科忍尼常數(k c)。 The Korenyi constant analysis step 906 is to cause the calculation unit 72 to calculate the Korenyi constant (k c ) under the porosity condition when the flow front 802 of the resin 801 moves to the radius position r through formula (9).

分析取得迴歸曲線步驟907。使該演算單元72根據該補強纖維蓆800在多個半徑位置處之該等孔隙率與對應之該等科忍尼常數,演算得到科忍尼常數與孔隙率的該迴歸曲線。Analyze and obtain the regression curve step 907. The calculation unit 72 calculates the regression curve of the Korenyi constant and the porosity according to the porosities and the corresponding Korenyi constants of the reinforcing fiber mat 800 at multiple radial positions.

取得滲透度步驟908,使該演算單元72根據該補強纖維蓆800之每一該孔隙率,以該迴歸曲線分析出該科忍尼常數。然後,使該演算單元72根據該孔隙率與該科忍尼常數,以公式(7)演算出每一該孔隙率對應的滲透度。In the step 908 of obtaining the permeability, the calculation unit 72 uses the regression curve to analyze the Korenyi constant according to each porosity of the reinforcing fiber mat 800. Then, the calculation unit 72 uses the porosity and the Korenyi constant to calculate the permeability corresponding to each porosity according to formula (7).

實施時,在本發明之另一實施態樣中,該演算單元72不以建立該迴歸曲線為必要,於該取得滲透度步驟908,可使該演算單元72根據特定半徑位置處的該孔隙率求取對應的該科忍尼常數,然後以公式(7)直接演算取得具有該孔隙率之該補強纖維蓆800的該滲透度。In practice, in another embodiment of the present invention, the calculation unit 72 is not required to establish the regression curve. In the step 908 of obtaining the permeability, the calculation unit 72 can obtain the corresponding Korenyi constant according to the porosity at a specific radius position, and then directly calculate the permeability of the reinforcing fiber mat 800 with the porosity using formula (7).

樹脂流動前緣分析步驟909。使該分析模組7分析所述影像中之所述樹脂801的該流動前緣802所構成之形狀,並於判斷所述形狀相對於正圓形偏差大於等於1%以上時,發出一個警示訊息。Resin flow front analysis step 909: The analysis module 7 analyzes the shape formed by the flow front 802 of the resin 801 in the image, and issues a warning message when it is determined that the deviation of the shape from a perfect circle is greater than or equal to 1%.

驗證步驟910。使該分析模組7根據該液體體積流率(q i)與該流動前緣802位移至特定半徑位置(r)時的充填時間(t),計算出該模穴30在該充填時間(t)時所容置的樹脂體積量(Q),並使該分析模組7根據公式(11)演算出所述樹脂801之該流動前緣802位移至該特定半徑位置(r)時的該理論時間(t k)。再使該分析模組7於該理論時間(t k)與該充填時間(t)之差值大於1秒時,發出一個警示訊息。 Verification step 910. The analysis module 7 calculates the resin volume (Q) contained in the mold cavity 30 at the filling time (t) according to the liquid volume flow rate (q i ) and the filling time (t) when the flow front edge 802 moves to the specific radius position (r), and the analysis module 7 calculates the theoretical time (t k ) when the flow front edge 802 of the resin 801 moves to the specific radius position (r) according to formula ( 11 ). The analysis module 7 then issues a warning message when the difference between the theoretical time (t k ) and the filling time (t) is greater than 1 second.

在本實施例中,是將該模穴30之高度設計成徑向往外逐漸降低狀,藉以將該補強纖維蓆800處理成孔隙率呈徑向往外逐漸變小狀,而方便在一次的樹脂801填充過程中,量測取得該補強纖維蓆800之不同孔隙率的該滲透度。但實施時,在本發明之另一實施態樣中,也可將該模穴30之高度設計成徑向往外逐漸變大狀,使該模穴30可將該補強纖維蓆800處理成孔隙呈徑向往外逐漸變大狀,同樣可用以在一次樹脂801填充過程中,量測取得該補強纖維蓆800在各種孔隙率條件下之滲透度。In this embodiment, the height of the mold cavity 30 is designed to gradually decrease radially outward, so that the porosity of the reinforcing fiber mat 800 gradually decreases radially outward, and it is convenient to measure the permeability of the reinforcing fiber mat 800 with different porosities during one resin 801 filling process. However, in practice, in another embodiment of the present invention, the height of the mold cavity 30 can also be designed to gradually increase in diameter outward, so that the mold cavity 30 can process the reinforcing fiber mat 800 into a shape in which the pores gradually increase in diameter outward. Similarly, it can be used to measure the permeability of the reinforcing fiber mat 800 under various porosity conditions during a single resin 801 filling process.

另外,在本實施例中,是將該上模具32設計成透明狀,並使該影像擷取器6朝下對該上模具32進行影像擷取,藉以取得在該模穴30中流動之所述樹脂801的影像。但實施時,在本發明之另一實施態樣中,也可改為將該下模具31設計成透明狀,並使該影像擷取器6往上朝該下模具31進行影像擷取,藉以取得所述樹脂801在該模穴30中流動的影像。In addition, in this embodiment, the upper mold 32 is designed to be transparent, and the image capturer 6 is directed downward to capture the image of the upper mold 32, so as to obtain the image of the resin 801 flowing in the mold cavity 30. However, in practice, in another embodiment of the present invention, the lower mold 31 may be designed to be transparent, and the image capturer 6 is directed upward to capture the image of the lower mold 31, so as to obtain the image of the resin 801 flowing in the mold cavity 30.

綜上所述,透過該轉注成型單元3之該模穴30的結構設計,以及該樹脂注射器4、該壓力感測器5、該影像擷取器6與該分析模組7的設計,以及該測量方法的設計,可透過單一次樹脂801填充過程,量測取得該補強纖維蓆800在各種不同孔隙率情況下的滲透度,相當方便實用。因此,本發明樹脂轉移成型系統的測量裝置200與測量方法,確實是一種相當創新且方便實用的創作,確實能達成本發明的目的。In summary, through the structural design of the mold cavity 30 of the transfer molding unit 3, the design of the resin injector 4, the pressure sensor 5, the image capture device 6 and the analysis module 7, and the design of the measurement method, the permeability of the reinforcing fiber mat 800 under various porosity conditions can be measured through a single resin 801 filling process, which is quite convenient and practical. Therefore, the measurement device 200 and the measurement method of the resin transfer molding system of the present invention are indeed a very innovative and convenient creation, and can indeed achieve the purpose of the present invention.

惟以上所述者,僅為本發明的實施例而已,當不能以此限定本發明實施的範圍,凡是依本發明申請專利範圍及專利說明書內容所作的簡單的等效變化與修飾,皆仍屬本發明專利涵蓋的範圍內。However, the above is only an embodiment of the present invention and should not be used to limit the scope of implementation of the present invention. All simple equivalent changes and modifications made according to the scope of the patent application of the present invention and the content of the patent specification are still within the scope of the present patent.

200:測量裝置 3:轉注成型單元 30:模穴 301:中心區間 302:滲流區間 31:下模具 310:穴底面 311:填充孔 312:排氣孔 32:上模具 320:穴頂面 321:中心面部 322:環面部 33:尺規 4:樹脂注射器 5:壓力感測器 6:影像擷取器 7:分析模組 71:影像分析單元 72:演算單元 73:驗證單元 800:補強纖維蓆 801:樹脂 802:流動前緣 901:調變孔隙率步驟 902:分析取得孔隙率步驟 903:注入樹脂步驟 904:影像擷取步驟 905:模穴壓力擷取步驟 906:分析科忍尼常數步驟 907:分析取得迴歸曲線步驟 908:取得滲透度步驟 909:樹脂流動前緣分析步驟 910:驗證步驟200: Measuring device 3: Transfer molding unit 30: Mold cavity 301: Center section 302: Permeation section 31: Lower mold 310: Cavity bottom surface 311: Filling hole 312: Exhaust hole 32: Upper mold 320: Cavity top surface 321: Center surface 322: Ring surface 33: Ruler 4: Resin syringe 5: Pressure sensor 6: Image capturer 7: Analysis module 71: Image analysis unit 72: Calculation unit 73: Verification unit 800: Reinforced fiber mat 801: Resin 802: Flow front edge 901: Porosity adjustment step 902: Step of analyzing and obtaining porosity 903: Step of injecting resin 904: Step of capturing images 905: Step of capturing cavity pressure 906: Step of analyzing Korenyi constant 907: Step of analyzing and obtaining regression curve 908: Step of obtaining permeability 909: Step of analyzing resin flow front 910: Step of verification

本發明的其他的特徵及功效,將於參照圖式的實施方式中清楚地呈現,其中: 圖1是一個側剖視圖,示意說明本發明樹脂轉移成型系統的測量裝置的一個實施例的結構; 圖2是一個不完整的側剖視分解圖,示意說明該實施例的一個轉注成型單元與一個補強纖維蓆的結構; 圖3是一個俯視圖,示意說明該實施例的一個模穴中的樹脂徑向往外滲透入該補強纖維蓆時的情況; 圖4是一個功能方塊圖,說明該實施例之功能架構;及 圖5是一個步驟流程圖,說明本發明樹脂轉移成型系統的測量方法的一個實施例。 Other features and effects of the present invention will be clearly presented in the embodiments with reference to the drawings, wherein: FIG. 1 is a side sectional view schematically illustrating the structure of an embodiment of the measuring device of the resin transfer molding system of the present invention; FIG. 2 is an incomplete side sectional exploded view schematically illustrating the structure of a transfer molding unit and a reinforcing fiber mat of the embodiment; FIG. 3 is a top view schematically illustrating the situation when the resin in a mold cavity of the embodiment radially permeates into the reinforcing fiber mat; FIG. 4 is a functional block diagram illustrating the functional architecture of the embodiment; and FIG. 5 is a step flow chart illustrating an embodiment of the measuring method of the resin transfer molding system of the present invention.

901:調變孔隙率步驟 901: Porosity adjustment step

902:分析取得孔隙率步驟 902: Step of analyzing and obtaining porosity

903:注入樹脂步驟 903: Resin injection step

904:影像擷取步驟 904: Image capture step

905:模穴壓力擷取步驟 905: Cavity pressure capture step

906:分析科忍尼常數步驟 906: Steps to analyze Korreny's constant

907:分析取得迴歸曲線步驟 907: Analyze and obtain the regression curve step

908:取得滲透度步驟 908: Steps to obtain permeability

909:樹脂流動前緣分析步驟 909: Resin flow front analysis step

910:驗證步驟 910: Verification steps

Claims (10)

一種樹脂轉移成型系統的測量方法,適用於一次量測取得一補強纖維蓆之各種孔隙率對應的滲透度,包含以下步驟: 調變孔隙率步驟,將一圓環狀的補強纖維蓆同軸地水平置放在一個轉注成型單元的一個圓形的模穴中,該轉注成型單元之該模穴的高度是自其中心徑向往內或往外漸低,而會徑向往內或往外逐漸壓縮該補強纖維蓆,使該補強纖維蓆的孔隙呈徑向往內或往外逐漸變小狀; 分析取得孔隙率步驟,使一分析模組根據該補強纖維蓆之單位面積質量(A w)與密度(D f)、該補強纖維蓆在半徑位置r處的高度(h),演算取得該補強纖維蓆在該模穴之不同半徑位置r的孔隙率(Φ); 注入樹脂步驟,以固定的液體體積流率將樹脂注入該模穴中心,使樹脂徑向外流動滲入該補強纖維蓆之孔隙中; 影像擷取步驟,使一影像擷取器擷取所述樹脂於該補強纖維蓆中徑向往外流動的影像,使該分析模組分析所述影像,取得所述樹脂之流動前緣移動至該模穴之各個半徑位置時的充填時間(t); 模穴壓力擷取步驟,使一壓力感測器量測取得該補強纖維蓆內周緣在各個充填時間的液體壓力(P i); 分析科忍尼常數步驟,使該分析模組根據該模穴的尺寸參數、該補強纖維蓆之單位面積質量(A w)與每一半徑位置的該孔隙率、所述樹脂的流動前緣移動至每一半徑位置的該充填時間,及各充填時間點之該液體壓力值,演算出每一孔隙率對應的科忍尼常數(k c);及 取得滲透度步驟,使該分析模組根據該補強纖維蓆之每一該孔隙率對應的該科忍尼常數,演算出每一該孔隙率對應的滲透度。 A measurement method for a resin transfer molding system is applicable to obtaining the permeability corresponding to various porosities of a reinforcing fiber mat in one measurement, comprising the following steps: a porosity adjustment step, wherein a ring-shaped reinforcing fiber mat is coaxially and horizontally placed in a circular mold cavity of a transfer molding unit, wherein the height of the mold cavity of the transfer molding unit is gradually reduced from the center radially inward or outward, and the reinforcing fiber mat is gradually compressed radially inward or outward, so that the pores of the reinforcing fiber mat are gradually reduced radially inward or outward; A porosity analysis step, wherein an analysis module calculates the porosity (Φ) of the reinforcing fiber mat at different radial positions r of the mold cavity according to the unit area mass (A w ) and density (D f ) of the reinforcing fiber mat and the height (h) of the reinforcing fiber mat at the radial position r; A resin injection step, wherein the resin is injected into the center of the mold cavity at a fixed liquid volume flow rate so that the resin flows radially outward and penetrates into the pores of the reinforcing fiber mat; An image capture step, in which an image capturer captures an image of the resin flowing radially outward from the reinforcing fiber mat, and the analysis module analyzes the image to obtain the filling time (t) when the flow front edge of the resin moves to each radial position of the mold cavity; a mold cavity pressure capture step, in which a pressure sensor measures and obtains the liquid pressure (P i ) of the inner periphery of the reinforcing fiber mat at each filling time; a Korenyi constant analysis step, in which the analysis module analyzes the image based on the size parameters of the mold cavity, the unit area mass (A w ) and the porosity at each hemidiameter position, the filling time for the flow front of the resin to move to each hemidiameter position, and the liquid pressure value at each filling time point, to calculate the Korenyi constant (k c ) corresponding to each porosity; and a permeability acquisition step, so that the analysis module calculates the permeability corresponding to each porosity according to the Korenyi constant corresponding to each porosity of the reinforced fiber mat. 如請求項1所述的樹脂轉移成型系統的測量方法,還包含分析取得迴歸曲線步驟,使該分析模組根據多個半徑位置之該等孔隙率與對應之該等科忍尼常數演算得到科忍尼常數與孔隙率的迴歸曲線,於該取得滲透度步驟,該分析模組會根據該迴歸曲線計算出該科忍尼常數,並根據該科忍尼常數與該孔隙率演算出對應的滲透度。The measurement method of the resin transfer molding system as described in claim 1 also includes a step of analyzing and obtaining a regression curve, so that the analysis module calculates the regression curve of the König constant and the porosity based on the porosities at multiple radius positions and the corresponding König constants. In the step of obtaining the permeability, the analysis module calculates the König constant based on the regression curve, and calculates the corresponding permeability based on the König constant and the porosity. 如請求項2所述的樹脂轉移成型系統的測量方法,其中,於該調變孔隙率步驟,是使該補強纖維蓆的孔隙呈徑向往外逐漸變小狀,該測量方法還包含一個驗證步驟,使該分析模組根據該液體體積流率(q i)與該流動前緣位移至一特定半徑位置(r)時的充填時間(t),計算出該模穴在該充填時間(t)時所容置的樹脂體積量(Q),並使該分析模組根據以下公式演算出所述樹脂之該流動前緣位移至該特定半徑位置時的理論時間(t k),使該分析模組於該理論時間(t k)與該充填時間(t)之差值大於1秒時,發出一個警示訊息, Q=q i*t k ,m=(h o-h i)/(r o-r i) 其中,r i為該補強纖維蓆內周緣相對於該模穴中心的半徑距離,r o為該補強纖維蓆之外周緣相對於該模穴中心的半徑距離,Φ i為該補強纖維蓆內周緣處的孔隙率,h i為該模穴在r i半徑位置時的高度,h o是該模穴位在r o半徑位置時的高度。 The measurement method of the resin transfer molding system as described in claim 2, wherein, in the porosity adjustment step, the pores of the reinforcing fiber mat are made to gradually decrease in diameter outward, and the measurement method further comprises a verification step, wherein the analysis module calculates the resin volume (Q) contained in the mold cavity at the filling time (t) according to the liquid volume flow rate (q i ) and the filling time (t) when the flow front edge is displaced to a specific radial position (r), and the analysis module calculates the theoretical time (t k ) when the flow front edge of the resin is displaced to the specific radial position according to the following formula, and the analysis module verifies the theoretical time (t k ) at the theoretical time (t k ) and the filling time (t) is greater than 1 second, a warning message is issued, Q = q i * t k , m=( ho - hi )/( ro - ri ) wherein ri is the radius of the inner periphery of the reinforcing fiber mat relative to the center of the mold cavity, ro is the radius of the outer periphery of the reinforcing fiber mat relative to the center of the mold cavity, Φi is the porosity at the inner periphery of the reinforcing fiber mat, hi is the height of the mold cavity at the ri radius, and ho is the height of the mold cavity at the ro radius. 如請求項1所述的樹脂轉移成型系統的測量方法,還包含一個樹脂流動前緣分析步驟,使該分析模組分析所述影像中之所述樹脂的該流動前緣所構成之形狀,並於判斷所述形狀相對於正圓形偏差大於等於1%以上時,發出一個警示訊息。The measurement method of the resin transfer molding system as described in claim 1 also includes a resin flow front analysis step, so that the analysis module analyzes the shape formed by the flow front of the resin in the image, and issues a warning message when it is determined that the deviation of the shape from the perfect circle is greater than or equal to 1%. 一種樹脂轉移成型系統的測量裝置,適用於一次量測取得一補強纖維蓆之各種孔隙率對應的滲透度,該補強纖維蓆呈圓環狀,該測量裝置包含: 一個轉注成型單元,內部界定出一個上下軸向且用以同軸容置該補強纖維蓆之圓形的模穴,該模穴之高度是呈自中心徑向往外漸高或漸低狀,該轉注成型單元會往該模穴高度漸低方向逐漸壓縮該補強纖維蓆; 一個樹脂注射器,容裝有樹脂,可被驅動而以一預定之液體體積流率將所述樹脂注入該模穴位在該補強纖維蓆內周側的區間,使所述樹脂徑向往外滲流進入該補強纖維蓆中; 一個壓力感測器,可用以量測該模穴位於該補強纖維蓆內周緣的液體壓力; 一個影像擷取器,可用以朝該轉注成型單元進行影像擷取,以取得該模穴中之所述樹脂在該補強纖維蓆中滲透流動的影像;及 一個分析模組,訊號連接該壓力感測器與該影像擷取器,包括一個影像分析單元與一個演算單元,該影像分析單元可分析所述影像以取得所述樹脂之流動前緣位於該模穴的半徑位置與對應之充填時間(t),該演算單元可根據該補強纖維蓆被壓縮後相對於該模穴中心的每一半徑位置的孔隙率、所述流動前緣移動至每一半徑位置的充填時間、每一充填時間之該液體壓力值,及該模穴的尺寸參數,演算出每一孔隙率對應的滲透度。 A measuring device for a resin transfer molding system is suitable for measuring the permeability corresponding to various porosities of a reinforcing fiber mat at one time. The reinforcing fiber mat is in the shape of a ring. The measuring device comprises: A transfer molding unit, which defines a circular mold cavity in the upper and lower axial directions and is used to coaxially accommodate the reinforcing fiber mat. The height of the mold cavity is gradually increased or decreased from the center diameter to the outside. The transfer molding unit will gradually compress the reinforcing fiber mat in the direction of the decreasing height of the mold cavity; A resin injector containing resin can be driven to inject the resin into the cavity at the inner periphery of the reinforcing fiber mat at a predetermined liquid volume flow rate, so that the resin radially permeates outward into the reinforcing fiber mat; A pressure sensor can be used to measure the liquid pressure of the cavity at the inner periphery of the reinforcing fiber mat; An image capturer can be used to capture images toward the transfer molding unit to obtain images of the resin in the cavity penetrating and flowing in the reinforcing fiber mat; and An analysis module, signal-connected to the pressure sensor and the image capturer, includes an image analysis unit and a calculation unit. The image analysis unit can analyze the image to obtain the radial position of the flow front edge of the resin in the mold cavity and the corresponding filling time (t). The calculation unit can calculate the permeability corresponding to each porosity according to the porosity of each radial position relative to the center of the mold cavity after the reinforcing fiber mat is compressed, the filling time when the flow front edge moves to each radial position, the liquid pressure value at each filling time, and the size parameters of the mold cavity. 如請求項5所述的樹脂轉移成型系統的測量裝置,其中,該轉注成型單元包括一個下模具,及一個疊蓋在該下模具上而與該下模具相配合界定出該模穴的上模具,該下模具與該上模具其中一者呈透明狀,該影像擷取器可朝透明狀之該上模具或該下模具進行影像擷取。A measuring device for a resin transfer molding system as described in claim 5, wherein the transfer molding unit includes a lower mold and an upper mold superimposed on the lower mold and cooperating with the lower mold to define the mold cavity, and one of the lower mold and the upper mold is transparent, and the image capturer can capture images of the transparent upper mold or the lower mold. 如請求項6所述的樹脂轉移成型系統的測量裝置,其中,該轉注成型單元還包括一個設置在透明之該下模具或該上模具,且相對該模穴中心徑向往外延伸的尺規,該影像擷取器可擷取所述流動前緣相對該尺規的影像。A measuring device for a resin transfer molding system as described in claim 6, wherein the transfer molding unit further includes a ruler disposed on the transparent lower mold or the upper mold and extending outward relative to the center diameter of the mold cavity, and the image capturer can capture the image of the flow front edge relative to the ruler. 如請求項5或7所述的樹脂轉移成型系統的測量裝置,其中,該影像分析單元可分析所述樹脂的該流動前緣所構成之形狀,並於判斷所述形狀相對於正圓形偏差大於等於1%以上時,發出一個警示訊息。A measuring device for a resin transfer molding system as described in claim 5 or 7, wherein the image analysis unit can analyze the shape formed by the flow front edge of the resin and issue a warning message when it is determined that the deviation of the shape from a perfect circle is greater than or equal to 1%. 如請求項5所述的樹脂轉移成型系統的測量裝置,其中,該模穴之高度是呈徑向往外漸低狀,該分析模組還包括一個驗證單元,該驗證單元可根據該液體體積流率(q i)與該流動前緣位移至一特定半徑位置(r)時的充填時間,計算出該模穴在該該充填時間(t)時所容置的樹脂體積量(Q),該驗證單元會根據以下公式演算出所述樹脂之該流動前緣位移至該特定半徑位置時的理論時間(t k),且該驗證單元會於判斷該理論時間(t k)與該充填時間(t)之差值大於1秒時,發出一個警示訊息, Q=q i*t k ,m=(h o-h i)/(r o-r i) 其中,r i為該補強纖維蓆內周緣相對於該模穴中心的半徑距離,r o為該補強纖維蓆之外周緣相對於該模穴中心的半徑距離,Φ i為該補強纖維蓆內周緣處的孔隙率,h i為該模穴在半徑位置r i時的高度,h o是該模穴位在半徑位置r o時的高度。 A measuring device for a resin transfer molding system as described in claim 5, wherein the height of the mold cavity is gradually decreasing radially outward, and the analysis module further includes a verification unit. The verification unit can calculate the volume of resin (Q) contained in the mold cavity at the filling time (t) based on the liquid volume flow rate (q i ) and the filling time when the flow front edge moves to a specific radial position (r). The verification unit will calculate the theoretical time (t k ) when the flow front edge of the resin moves to the specific radial position according to the following formula, and the verification unit will issue a warning message when it is determined that the difference between the theoretical time (t k ) and the filling time (t) is greater than 1 second, Q=q i *t k , m=( ho - hi )/( ro - ri ) wherein ri is the radius of the inner periphery of the reinforcing fiber mat relative to the center of the mold cavity, r0 is the radius of the outer periphery of the reinforcing fiber mat relative to the center of the mold cavity, Φi is the porosity at the inner periphery of the reinforcing fiber mat, hi is the height of the mold cavity at the radial position ri , and ho is the height of the mold cavity at the radial position r0 . 如請求項6所述的樹脂轉移成型系統的測量裝置,其中,該下模具或該上模具具有多個連通該模穴周緣與外界的排氣孔。A measuring device for a resin transfer molding system as described in claim 6, wherein the lower mold or the upper mold has a plurality of exhaust holes connecting the periphery of the mold cavity with the outside world.
TW112148756A 2023-12-14 2023-12-14 Device and method for measuring permeability of reinforced fiber mat in resin transfer molding system TWI863751B (en)

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Citations (3)

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Publication number Priority date Publication date Assignee Title
CN202599794U (en) * 2012-05-14 2012-12-12 西北工业大学 Measuring device for axial steady-state infiltration rate of continuous fiber beams
CN104297121A (en) * 2013-07-17 2015-01-21 中国科学院宁波材料技术与工程研究所 Measurement method for in-plane unsaturated permeability rates of natural fiber fabric
US20200061941A1 (en) * 2017-05-05 2020-02-27 Coretech System Co., Ltd. Method for measuring a flowing property in a resin transfer molding system

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202599794U (en) * 2012-05-14 2012-12-12 西北工业大学 Measuring device for axial steady-state infiltration rate of continuous fiber beams
CN104297121A (en) * 2013-07-17 2015-01-21 中国科学院宁波材料技术与工程研究所 Measurement method for in-plane unsaturated permeability rates of natural fiber fabric
US20200061941A1 (en) * 2017-05-05 2020-02-27 Coretech System Co., Ltd. Method for measuring a flowing property in a resin transfer molding system

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