TWI574913B - The method of granulating insulating fins and boron nitride - Google Patents
The method of granulating insulating fins and boron nitride Download PDFInfo
- Publication number
- TWI574913B TWI574913B TW102109028A TW102109028A TWI574913B TW I574913 B TWI574913 B TW I574913B TW 102109028 A TW102109028 A TW 102109028A TW 102109028 A TW102109028 A TW 102109028A TW I574913 B TWI574913 B TW I574913B
- Authority
- TW
- Taiwan
- Prior art keywords
- boron nitride
- mass
- ray
- sheet
- coupling agent
- Prior art date
Links
- 229910052582 BN Inorganic materials 0.000 title claims description 100
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 title claims description 100
- 238000000034 method Methods 0.000 title claims description 37
- DIOQZVSQGTUSAI-UHFFFAOYSA-N decane Chemical compound CCCCCCCCCC DIOQZVSQGTUSAI-UHFFFAOYSA-N 0.000 claims description 101
- 238000005469 granulation Methods 0.000 claims description 31
- 230000003179 granulation Effects 0.000 claims description 31
- 239000007822 coupling agent Substances 0.000 claims description 29
- 239000000203 mixture Substances 0.000 claims description 21
- 229920001971 elastomer Polymers 0.000 claims description 20
- 239000005060 rubber Substances 0.000 claims description 20
- 125000003277 amino group Chemical group 0.000 claims description 18
- 238000002441 X-ray diffraction Methods 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- 238000004519 manufacturing process Methods 0.000 claims description 12
- 239000000843 powder Substances 0.000 claims description 9
- 229920005989 resin Polymers 0.000 claims description 8
- 239000011347 resin Substances 0.000 claims description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 7
- 239000007921 spray Substances 0.000 claims description 6
- 230000001678 irradiating effect Effects 0.000 claims description 5
- 238000005507 spraying Methods 0.000 claims description 4
- 239000008187 granular material Substances 0.000 claims description 2
- UORVGPXVDQYIDP-UHFFFAOYSA-N borane Chemical compound B UORVGPXVDQYIDP-UHFFFAOYSA-N 0.000 claims 1
- 229910010277 boron hydride Inorganic materials 0.000 claims 1
- -1 polyoxyethylene Polymers 0.000 description 17
- 239000000243 solution Substances 0.000 description 16
- 239000002245 particle Substances 0.000 description 15
- 238000000465 moulding Methods 0.000 description 11
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 7
- 238000002156 mixing Methods 0.000 description 7
- 239000011164 primary particle Substances 0.000 description 7
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 6
- 239000003431 cross linking reagent Substances 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 4
- 229910052796 boron Inorganic materials 0.000 description 4
- 238000003490 calendering Methods 0.000 description 4
- 230000015556 catabolic process Effects 0.000 description 4
- 239000003054 catalyst Substances 0.000 description 4
- 238000004132 cross linking Methods 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- PHQOGHDTIVQXHL-UHFFFAOYSA-N n'-(3-trimethoxysilylpropyl)ethane-1,2-diamine Chemical compound CO[Si](OC)(OC)CCCNCCN PHQOGHDTIVQXHL-UHFFFAOYSA-N 0.000 description 4
- DMWVYCCGCQPJEA-UHFFFAOYSA-N 2,5-bis(tert-butylperoxy)-2,5-dimethylhexane Chemical compound CC(C)(C)OOC(C)(C)CCC(C)(C)OOC(C)(C)C DMWVYCCGCQPJEA-UHFFFAOYSA-N 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 125000003342 alkenyl group Chemical group 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000001125 extrusion Methods 0.000 description 3
- 239000004744 fabric Substances 0.000 description 3
- 238000010304 firing Methods 0.000 description 3
- 239000003365 glass fiber Substances 0.000 description 3
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- GPBBNPPLBQIADY-UHFFFAOYSA-N 4,4-dimethyloxane Chemical group CC1(C)CCOCC1 GPBBNPPLBQIADY-UHFFFAOYSA-N 0.000 description 2
- SXPGQGNWEWPWQZ-UHFFFAOYSA-N 4-(triethoxymethyl)dodecan-1-amine Chemical compound NCCCC(C(OCC)(OCC)OCC)CCCCCCCC SXPGQGNWEWPWQZ-UHFFFAOYSA-N 0.000 description 2
- MHZGKXUYDGKKIU-UHFFFAOYSA-N Decylamine Chemical compound CCCCCCCCCCN MHZGKXUYDGKKIU-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
- XJDCHDFUMGSEHD-UHFFFAOYSA-N NCCCC(C(OC)(OC)OC)CCCCCCCC Chemical compound NCCCC(C(OC)(OC)OC)CCCCCCCC XJDCHDFUMGSEHD-UHFFFAOYSA-N 0.000 description 2
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical group [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 description 2
- 230000004520 agglutination Effects 0.000 description 2
- 125000003545 alkoxy group Chemical group 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000010292 electrical insulation Methods 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- 230000017525 heat dissipation Effects 0.000 description 2
- 150000002430 hydrocarbons Chemical group 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
- 238000001746 injection moulding Methods 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 238000000691 measurement method Methods 0.000 description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
- 125000000962 organic group Chemical group 0.000 description 2
- 150000001451 organic peroxides Chemical class 0.000 description 2
- 150000002902 organometallic compounds Chemical class 0.000 description 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 229920001296 polysiloxane Polymers 0.000 description 2
- 238000005096 rolling process Methods 0.000 description 2
- 229910052707 ruthenium Inorganic materials 0.000 description 2
- 238000001694 spray drying Methods 0.000 description 2
- 125000003396 thiol group Chemical group [H]S* 0.000 description 2
- 125000000725 trifluoropropyl group Chemical group [H]C([H])(*)C([H])([H])C(F)(F)F 0.000 description 2
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 2
- 238000004073 vulcanization Methods 0.000 description 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 1
- PFMVDWMJBIKZEB-UHFFFAOYSA-N 2,3-ditert-butylbenzenecarboperoxoic acid Chemical compound CC(C)(C)C1=CC=CC(C(=O)OO)=C1C(C)(C)C PFMVDWMJBIKZEB-UHFFFAOYSA-N 0.000 description 1
- XXFUNTSOBHSMBU-UHFFFAOYSA-N 2,4-dichlorobenzamide Chemical compound NC(=O)C1=CC=C(Cl)C=C1Cl XXFUNTSOBHSMBU-UHFFFAOYSA-N 0.000 description 1
- XMNIXWIUMCBBBL-UHFFFAOYSA-N 2-(2-phenylpropan-2-ylperoxy)propan-2-ylbenzene Chemical compound C=1C=CC=CC=1C(C)(C)OOC(C)(C)C1=CC=CC=C1 XMNIXWIUMCBBBL-UHFFFAOYSA-N 0.000 description 1
- 125000001731 2-cyanoethyl group Chemical group [H]C([H])(*)C([H])([H])C#N 0.000 description 1
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 1
- SJECZPVISLOESU-UHFFFAOYSA-N 3-trimethoxysilylpropan-1-amine Chemical compound CO[Si](OC)(OC)CCCN SJECZPVISLOESU-UHFFFAOYSA-N 0.000 description 1
- BLNVISNJTIRAHF-UHFFFAOYSA-N 4-chlorobenzamide Chemical class NC(=O)C1=CC=C(Cl)C=C1 BLNVISNJTIRAHF-UHFFFAOYSA-N 0.000 description 1
- 239000004925 Acrylic resin Substances 0.000 description 1
- 229920000178 Acrylic resin Polymers 0.000 description 1
- XXWPFQMOOMIFKK-UHFFFAOYSA-N CC1=CC=C(C=C1)C(C1=CC=CC=C1)OOC(C1=CC=CC=C1)C1=CC=C(C=C1)C Chemical compound CC1=CC=C(C=C1)C(C1=CC=CC=C1)OOC(C1=CC=CC=C1)C1=CC=C(C=C1)C XXWPFQMOOMIFKK-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 229930040373 Paraformaldehyde Natural products 0.000 description 1
- 238000005411 Van der Waals force Methods 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000007259 addition reaction Methods 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 239000012298 atmosphere Substances 0.000 description 1
- IUTYMBRQELGIRS-UHFFFAOYSA-N boric acid;1,3,5-triazine-2,4,6-triamine Chemical compound OB(O)O.NC1=NC(N)=NC(N)=N1 IUTYMBRQELGIRS-UHFFFAOYSA-N 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 125000002603 chloroethyl group Chemical group [H]C([*])([H])C([H])([H])Cl 0.000 description 1
- 125000004218 chloromethyl group Chemical group [H]C([H])(Cl)* 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000006482 condensation reaction Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 125000004093 cyano group Chemical group *C#N 0.000 description 1
- 125000000753 cycloalkyl group Chemical group 0.000 description 1
- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 description 1
- 125000001511 cyclopentyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C1([H])[H] 0.000 description 1
- DIOQZVSQGTUSAI-NJFSPNSNSA-N decane Chemical group CCCCCCCCC[14CH3] DIOQZVSQGTUSAI-NJFSPNSNSA-N 0.000 description 1
- 229910052805 deuterium Inorganic materials 0.000 description 1
- 125000004431 deuterium atom Chemical group 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 125000001301 ethoxy group Chemical group [H]C([H])([H])C([H])([H])O* 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 125000003983 fluorenyl group Chemical group C1(=CC=CC=2C3=CC=CC=C3CC12)* 0.000 description 1
- 125000002485 formyl group Chemical group [H]C(*)=O 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 125000005843 halogen group Chemical group 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 229910017053 inorganic salt Inorganic materials 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 229920002098 polyfluorene Polymers 0.000 description 1
- 229920006324 polyoxymethylene Polymers 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 238000007348 radical reaction Methods 0.000 description 1
- 239000012744 reinforcing agent Substances 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- 239000011135 tin Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 125000003944 tolyl group Chemical group 0.000 description 1
Landscapes
- Cooling Or The Like Of Semiconductors Or Solid State Devices (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Manufacture Of Macromolecular Shaped Articles (AREA)
- Inorganic Insulating Materials (AREA)
- Organic Insulating Materials (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2012093555A JP5761111B2 (ja) | 2012-04-17 | 2012-04-17 | 絶縁放熱シート及び窒化ホウ素の造粒方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| TW201402452A TW201402452A (zh) | 2014-01-16 |
| TWI574913B true TWI574913B (zh) | 2017-03-21 |
Family
ID=49460093
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW102109028A TWI574913B (zh) | 2012-04-17 | 2013-03-14 | The method of granulating insulating fins and boron nitride |
Country Status (3)
| Country | Link |
|---|---|
| JP (1) | JP5761111B2 (ja) |
| CN (1) | CN103374226B (ja) |
| TW (1) | TWI574913B (ja) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103994347A (zh) * | 2014-04-23 | 2014-08-20 | 王定锋 | 导热绝缘粉末和树脂混合成型的led散热结构和led线性灯 |
| KR102318231B1 (ko) * | 2015-01-29 | 2021-10-27 | 엘지이노텍 주식회사 | 무기충전재, 이를 포함하는 수지 조성물, 그리고 이를 이용한 방열 기판 |
| JP6497291B2 (ja) * | 2015-10-14 | 2019-04-10 | 信越化学工業株式会社 | 絶縁放熱シート |
| CN107022196A (zh) * | 2016-02-02 | 2017-08-08 | 中兴通讯股份有限公司 | 导热材料、其制备方法及导热件 |
| JP6786047B2 (ja) * | 2016-08-24 | 2020-11-18 | 三菱瓦斯化学株式会社 | 熱伝導シートの製造方法 |
| JP7175586B2 (ja) * | 2016-08-24 | 2022-11-21 | 三菱瓦斯化学株式会社 | 窒化ホウ素粒子凝集体、その製造方法、組成物及び樹脂シート |
| JP6683091B2 (ja) * | 2016-09-26 | 2020-04-15 | トヨタ自動車株式会社 | 窒化ホウ素粒子集合体を含む有機無機コンポジット材料の製造方法 |
| JP2020055961A (ja) * | 2018-10-03 | 2020-04-09 | 信越化学工業株式会社 | 制御された熱伝導率分布を有する樹脂シート及びその製造方法 |
| GB2583351B (en) * | 2019-04-24 | 2024-12-25 | Talga Tech Limited | Functionalised Graphene and Coatings Comprising the Same |
| KR102465161B1 (ko) * | 2019-11-06 | 2022-11-09 | 주식회사 아모그린텍 | 방열 시트, 이의 제조방법 및 이를 포함하는 전자기기 |
| CN114213986A (zh) * | 2021-11-17 | 2022-03-22 | 深圳市鸿富诚新材料股份有限公司 | 一种导热绝缘石墨烯垫片及其制备方法 |
| CN117384526B (zh) * | 2023-11-29 | 2024-04-02 | 佛山市耐高建材有限公司 | 一种防水涂料及其制备方法 |
| CN119286261B (zh) * | 2024-11-08 | 2025-06-13 | 深圳市佰盈新材料科技有限公司 | 一种低密度减重导热硅胶及其制备方法 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0959425A (ja) * | 1995-08-28 | 1997-03-04 | Tatsumori:Kk | 高熱伝導性複合粒子 |
| JP3461651B2 (ja) * | 1996-01-24 | 2003-10-27 | 電気化学工業株式会社 | 六方晶窒化ほう素粉末及びその用途 |
| CN101809734A (zh) * | 2007-09-26 | 2010-08-18 | 三菱电机株式会社 | 导热性片材和功率模块 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6438451A (en) * | 1987-08-05 | 1989-02-08 | Denki Kagaku Kogyo Kk | Filler |
| JPH06157010A (ja) * | 1992-11-20 | 1994-06-03 | Central Glass Co Ltd | 安定化した過炭酸ソーダ組成物及びその製造方法 |
| JPH1160216A (ja) * | 1997-08-04 | 1999-03-02 | Shin Etsu Chem Co Ltd | 熱伝導性窒化ホウ素フィラー及び絶縁放熱シート |
| JP3782033B2 (ja) * | 2001-09-07 | 2006-06-07 | 株式会社カネボウ化粧品 | 化粧料 |
| JP5063710B2 (ja) * | 2010-01-05 | 2012-10-31 | 三菱電機株式会社 | パワーモジュール |
-
2012
- 2012-04-17 JP JP2012093555A patent/JP5761111B2/ja not_active Expired - Fee Related
-
2013
- 2013-03-14 TW TW102109028A patent/TWI574913B/zh not_active IP Right Cessation
- 2013-04-16 CN CN201310130748.9A patent/CN103374226B/zh not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0959425A (ja) * | 1995-08-28 | 1997-03-04 | Tatsumori:Kk | 高熱伝導性複合粒子 |
| JP3461651B2 (ja) * | 1996-01-24 | 2003-10-27 | 電気化学工業株式会社 | 六方晶窒化ほう素粉末及びその用途 |
| CN101809734A (zh) * | 2007-09-26 | 2010-08-18 | 三菱电机株式会社 | 导热性片材和功率模块 |
Also Published As
| Publication number | Publication date |
|---|---|
| JP5761111B2 (ja) | 2015-08-12 |
| TW201402452A (zh) | 2014-01-16 |
| CN103374226B (zh) | 2017-04-12 |
| JP2013220971A (ja) | 2013-10-28 |
| CN103374226A (zh) | 2013-10-30 |
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