TWI455993B - 強化聚酯樹脂組成物 - Google Patents
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- TWI455993B TWI455993B TW099107282A TW99107282A TWI455993B TW I455993 B TWI455993 B TW I455993B TW 099107282 A TW099107282 A TW 099107282A TW 99107282 A TW99107282 A TW 99107282A TW I455993 B TWI455993 B TW I455993B
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- 229920001225 polyester resin Polymers 0.000 title claims 27
- 239000004645 polyester resin Substances 0.000 title claims 27
- 239000000203 mixture Substances 0.000 title claims 18
- 125000004432 carbon atom Chemical group C* 0.000 claims 45
- 125000001424 substituent group Chemical group 0.000 claims 32
- 125000004122 cyclic group Chemical group 0.000 claims 21
- 229910052783 alkali metal Inorganic materials 0.000 claims 20
- 150000001340 alkali metals Chemical group 0.000 claims 20
- -1 sulfonamide compound Chemical class 0.000 claims 16
- 125000000217 alkyl group Chemical group 0.000 claims 14
- 229910052751 metal Inorganic materials 0.000 claims 12
- 239000002184 metal Substances 0.000 claims 12
- 150000003839 salts Chemical class 0.000 claims 11
- 229940124530 sulfonamide Drugs 0.000 claims 11
- 125000003277 amino group Chemical group 0.000 claims 9
- 125000005843 halogen group Chemical group 0.000 claims 9
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims 9
- 239000011256 inorganic filler Substances 0.000 claims 6
- 229910003475 inorganic filler Inorganic materials 0.000 claims 6
- 239000004014 plasticizer Substances 0.000 claims 6
- 125000001820 oxy group Chemical group [*:1]O[*:2] 0.000 claims 5
- 125000003545 alkoxy group Chemical group 0.000 claims 4
- 125000002947 alkylene group Chemical group 0.000 claims 4
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 claims 4
- 150000002148 esters Chemical class 0.000 claims 4
- 239000004721 Polyphenylene oxide Substances 0.000 claims 3
- 229920000570 polyether Polymers 0.000 claims 3
- 229910018626 Al(OH) Inorganic materials 0.000 claims 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 2
- 229910052684 Cerium Inorganic materials 0.000 claims 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims 2
- 125000003342 alkenyl group Chemical group 0.000 claims 2
- 229910052799 carbon Inorganic materials 0.000 claims 2
- ZMIGMASIKSOYAM-UHFFFAOYSA-N cerium Chemical compound [Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce] ZMIGMASIKSOYAM-UHFFFAOYSA-N 0.000 claims 2
- 125000006165 cyclic alkyl group Chemical group 0.000 claims 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 2
- 229920001707 polybutylene terephthalate Polymers 0.000 claims 2
- 229920000139 polyethylene terephthalate Polymers 0.000 claims 2
- 239000005020 polyethylene terephthalate Substances 0.000 claims 2
- 239000005711 Benzoic acid Substances 0.000 claims 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 125000003118 aryl group Chemical group 0.000 claims 1
- 125000004429 atom Chemical group 0.000 claims 1
- 229910052788 barium Inorganic materials 0.000 claims 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 claims 1
- 235000010233 benzoic acid Nutrition 0.000 claims 1
- 229910052791 calcium Inorganic materials 0.000 claims 1
- 239000011575 calcium Substances 0.000 claims 1
- 150000001721 carbon Chemical group 0.000 claims 1
- 150000001924 cycloalkanes Chemical class 0.000 claims 1
- 125000000753 cycloalkyl group Chemical group 0.000 claims 1
- 239000003365 glass fiber Substances 0.000 claims 1
- 229910052742 iron Inorganic materials 0.000 claims 1
- 229910052746 lanthanum Inorganic materials 0.000 claims 1
- FZLIPJUXYLNCLC-UHFFFAOYSA-N lanthanum atom Chemical compound [La] FZLIPJUXYLNCLC-UHFFFAOYSA-N 0.000 claims 1
- 229910052749 magnesium Inorganic materials 0.000 claims 1
- 239000011777 magnesium Substances 0.000 claims 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 claims 1
- 239000002245 particle Substances 0.000 claims 1
- 229920003207 poly(ethylene-2,6-naphthalate) Polymers 0.000 claims 1
- 229920000747 poly(lactic acid) Polymers 0.000 claims 1
- 239000011112 polyethylene naphthalate Substances 0.000 claims 1
- 239000004626 polylactic acid Substances 0.000 claims 1
- 229910052712 strontium Inorganic materials 0.000 claims 1
- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 claims 1
- 125000000547 substituted alkyl group Chemical group 0.000 claims 1
- 239000010936 titanium Substances 0.000 claims 1
- 229910052719 titanium Inorganic materials 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
- 229910052725 zinc Inorganic materials 0.000 claims 1
- 239000011701 zinc Substances 0.000 claims 1
- 229910052726 zirconium Inorganic materials 0.000 claims 1
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/36—Sulfur-, selenium-, or tellurium-containing compounds
- C08K5/45—Heterocyclic compounds having sulfur in the ring
- C08K5/46—Heterocyclic compounds having sulfur in the ring with oxygen or nitrogen in the ring
- C08K5/47—Thiazoles
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L67/00—Compositions of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Compositions of derivatives of such polymers
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/04—Reinforcing macromolecular compounds with loose or coherent fibrous material
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- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/04—Reinforcing macromolecular compounds with loose or coherent fibrous material
- C08J5/0405—Reinforcing macromolecular compounds with loose or coherent fibrous material with inorganic fibres
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- C08K5/00—Use of organic ingredients
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- C08K5/0016—Plasticisers
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- C08K5/435—Sulfonamides
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- C08L67/00—Compositions of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Compositions of derivatives of such polymers
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Claims (17)
- 一種強化聚酯樹脂組成物，其特徵為，相對於聚酯樹脂100質量份含有(A)成份之無機填充劑10至100質量份，及(B)成份之具有下述一般式(1) (式中，R1 及R2 各自獨立為氫原子、鹵原子、鹼金屬原子、胺基、可具有支鏈或取代基之碳原子數1至10的烷基、可具有支鏈或取代基之碳原子數1至10的烷氧基、或可具有取代基之碳原子數3至30的環狀基，R1 及R2 可鍵結形成環狀基，n為1或2之數，n為1時M為鹼金屬原子或Al(OH)3-n ，n為2時複數的R1 及R2 可各自相異，M為鎂、鈣、鍶、鋇、鈦、錳、鐵、鋅、矽、鋯、釔及鉿中所選出的2價金屬原子、Al(OH)3-n ，或可具有取代基之碳原子數1至12的伸烷基、可具有取代基之碳原子數2至12的伸鏈烯基、可具有取代基之碳原子數3至8的環伸烷基、具有醚鍵之碳原子數4至20的伸烷基、被環伸烷基中斷的碳原子數5至20的伸烷基、可具有取代基之碳原子數6至12的伸芳基、及此等之組合所成群中選出的鍵結基，M為鍵結基時R1 、R2 中任何一方為鹼金屬)所 表示的構造之磺胺化合物的金屬鹽0.1至0.3質量份。
- 如申請專利範圍第1項之強化聚酯樹脂組成物，其中相對於前述聚酯樹脂100質量份，另含有0.1至20質量份之(C)成份的聚醚酯系可塑劑及/或苯甲酸酯系可塑劑中至少一種。
- 如申請專利範圍第1項之強化聚酯樹脂組成物，其中表示前述(B)成份的一般式(1)中之M為鹼金屬原子。
- 如申請專利範圍第1項之強化聚酯樹脂組成物，其中前述(B)成份之磺胺化合物的金屬鹽為，具有下述一般式(2) (式中，R1 及R2 各自獨立為氫原子、鹵原子、鹼金屬原子、胺基、可具有支鏈或取代基之碳原子數1至10的烷基、可具有支鏈或取代基之碳原子數1至10的烷氧基、或可具有取代基之碳原子數3至30的環狀基，R1 及R2 可鍵結形成環狀基，X為鹼金屬原子)所表示的構造。
- 如申請專利範圍第1項之強化聚酯樹脂組成物，其中前述(B)成份之磺胺化合物的金屬鹽為，具有下述一般式(3) (式中，環A為碳原子數3至30之環狀基，R2 及R3 各自獨立為氫原子、鹵原子、鹼金屬原子、胺基、可具有支鏈或取代基之碳原子數1至10的烷基、碳原子數1至10之可具有支鏈或取代基的烷氧基、或可具有取代基之碳原子數3至27的環狀基，R2 及R3 可鍵結形成環狀基，X為鹼金屬原子，p為0至3之整數，p為2以上之整數時複數的R3 可各自相異，環A及全部R3 之合計碳原子數為3至30)所表示的構造。
- 如申請專利範圍第1項之強化聚酯樹脂組成物，其中前述(B)成份之磺胺化合物的金屬鹽為，具有下述一般式(4) (式中，環A及環B各自獨立為碳原子數3至30之環狀基，R3 及R4 各自獨立為氫原子、鹵原子、鹼金屬原子、胺基、可具有支鏈或取代基之碳原子數1至10的烷基、可具有支鏈或取代基之碳原子數1至10之的烷氧基、或可具有取代基之碳原子數3至27的環狀基，R3 及R4 可鍵 結形成環狀基，X為鹼金屬原子，p為0至3之整數，p為2以上時複數的R3 可各自相異，q為0至3之整數，q為2以上時複數的R4 可各自相異，環A及全部R3 之合計碳原子數、環B及全部R4 之合計碳原子數各自為3至30)所表示的構造。
- 如申請專利範圍第1項之強化聚酯樹脂組成物，其中前述(B)成份之磺胺化合物的金屬鹽為，具有下述一般式(5) (式中，R5 為氫原子、鹵原子、鹼金屬原子、胺基、可具有支鏈或取代基之碳原子數1至10的烷基、可具有支鏈或取代基之碳原子數1至10的烷氧基、或可具有取代基之碳原子數3至24的環狀基，X為鹼金屬原子，p為0至3之整數，p為2以上時複數的R5 可各自相異)所表示的構造。
- 如申請專利範圍第1項之強化聚酯樹脂組成物，其中前述(B)成份之磺胺化合物的金屬鹽為，具有下述一般式(6) (式中，R2 及R6 各自獨立為氫原子、鹵原子、鹼金屬原子、胺基、可具有支鏈或取代基之碳原子數1至10的烷基、可具有支鏈或取代基之碳原子數1至10的烷氧基、或可具有取代基之環狀基，R2 為環狀基時碳原子數為3至30，R6 為環狀基時碳原子數為3至23，R2 及R6 可鍵結形成環狀基，X為鹼金屬原子，p為0至3之整數，p為2以上時複數的R6 可各自相異)所表示的構造。
- 如申請專利範圍第1項之強化聚酯樹脂組成物，其中前述(B)成份之磺胺化合物的金屬鹽為，具有下述一般式(7) (式中，R7 、R8 各自獨立為為氫原子、鹵原子、鹼金屬原子、胺基、可具有支鏈或取代基之碳原子數1至10的烷基、可具有支鏈或取代基之碳原子數1至10之的烷氧基、或可具有取代基之碳原子數3至30的環狀基，R7 及R8 可鍵結形成環狀基，X1 及X2 各自獨立為鹼金屬原子， L為鍵結基的，可具有支鏈或取代基之碳原子數1至12的伸烷基、可具有支鏈或取代基之碳原子數2至12的伸鏈烯基、可具有取代基之碳原子數3至8的環伸烷基、具有醚鍵之碳原子數4至20的伸烷基、被環伸烷基中斷的全碳原子數5至20之伸烷基，或可具有支鏈或取代基之碳原子數6至12之伸芳基)所表示的構造。
- 如申請專利範圍第1項之強化聚酯樹脂組成物，其中前述(B)成份之磺胺化合物的金屬鹽之平均粒徑為10μm以下。
- 如申請專利範圍第1項之強化聚酯樹脂組成物，其中前述(B)成份之磺胺化合物的金屬鹽之含水率為3質量%以下。
- 如申請專利範圍第1項之強化聚酯樹脂組成物，其中前述(A)成份之無機填充劑為纖維狀無機填充劑。
- 如申請專利範圍第1項之強化聚酯樹脂組成物，其中前述(A)成份之無機填充劑為玻璃纖維。
- 如申請專利範圍第1項之強化聚酯樹脂組成物，其中前述聚酯樹脂為含有聚對苯二甲酸乙二醇酯、聚萘二甲酸乙二醇酯、聚對苯二甲酸丁二醇酯、聚對苯二甲酸丁二酯及聚乳酸所成群中選出的至少一種以上者。
- 如申請專利範圍第1項之強化聚酯樹脂組成物，其中前述聚酯樹脂為，含有聚對苯二甲酸乙二醇酯者。
- 一種強化聚酯樹脂組成物，其特徵為，相對於前述聚酯樹脂100質量份含有 (A)成份之無機填充劑10至100質量份，及(B)成份之具有下述一般式(3) (式中，環A為碳原子數3至30之環狀基，R2 及R3 各自獨立為氫原子、鹵原子、鹼金屬原子、胺基、可具有支鏈或取代基之碳原子數1至10的烷基、碳原子數1至10之可具有支鏈或取代基的烷氧基、或可具有取代基之碳原子數3至27的環狀基，R2 及R3 可鍵結形成環狀基，X為鹼金屬原子，p為0至3之整數，p為2以上之整數時複數的R3 可各自相異，環A及全部R3 之合計碳原子數為3至30)所表示的構造之磺胺化合物的金屬鹽0.1至0.3質量份，另外相對於前述聚酯樹脂100質量份含有0.1至20質量份之(C)成份的聚醚酯系可塑劑及/或苯甲酸酯系可塑劑中至少一種。
- 一種強化聚酯樹脂組成物，其特徵為，相對於前述聚酯樹脂100質量份含有(A)成份之無機填充劑10至100質量份，及(B)成份之具有下述一般式(5) (式中，R5 為氫原子、鹵原子、鹼金屬原子、胺基、可具有支鏈或取代基之碳原子數1至10的烷基、可具有支鏈或取代基之碳原子數1至10的烷氧基、或可具有取代基之碳原子數3至24的環狀基，X為鹼金屬原子，p為0至3之整數，p為2以上時複數的R5 可各自相異)所表示的構造之磺胺化合物的金屬鹽0.1至0.3質量份，另外相對於前述聚酯樹脂100質量份含有0.1至20質量份之(C)成份的聚醚酯系可塑劑及/或苯甲酸酯系可塑劑中至少一種。
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| WO2013012002A1 (ja) * | 2011-07-20 | 2013-01-24 | ウィンテックポリマー株式会社 | 樹脂成形体及び自動車内装部品 |
| JP5876721B2 (ja) | 2011-12-20 | 2016-03-02 | 株式会社Adeka | マスターバッチの製造方法 |
| JP5974574B2 (ja) * | 2012-03-23 | 2016-08-23 | 富士ゼロックス株式会社 | 樹脂組成物、および樹脂成形体 |
| JP6177672B2 (ja) * | 2013-11-26 | 2017-08-09 | 株式会社Adeka | マスターバッチの製造方法 |
| CN104974479B (zh) * | 2015-06-10 | 2017-01-11 | 浙江格美机电科技有限公司 | 化学泵泵壳和材料配方及其制造方法 |
| KR102252550B1 (ko) | 2018-09-28 | 2021-05-14 | 롯데첨단소재(주) | 열가소성 수지 조성물 및 이로부터 제조된 성형품 |
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| US4753975A (en) * | 1983-05-11 | 1988-06-28 | Allied-Signal Inc. | Polyester molding composition containing low viscosity polyester reaction product |
| US5115016A (en) * | 1986-12-30 | 1992-05-19 | General Electric Company | Reinforced polyester molding compositions having high gloss and improved resistance to warping |
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| KR100211533B1 (ko) * | 1997-03-26 | 1999-08-02 | 김윤 | 결정화 속도가 빠른 지방족 폴리에스테르수지의 제조방법 |
| DE19907831A1 (de) * | 1999-02-24 | 2000-08-31 | Bayer Ag | Flammwidrige thermoplastische Formmasse |
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| CN101977987B (zh) * | 2008-03-21 | 2013-03-27 | 株式会社Adeka | 聚酯树脂组合物 |
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| KR101715715B1 (ko) | 2017-03-13 |
| WO2010104103A1 (ja) | 2010-09-16 |
| CN102348760B (zh) | 2013-09-11 |
| CN102348760A (zh) | 2012-02-08 |
| EP2407514A1 (en) | 2012-01-18 |
| TW201100490A (en) | 2011-01-01 |
| IL215032A0 (en) | 2011-11-30 |
| BRPI1009354B1 (pt) | 2020-01-14 |
| KR20110131281A (ko) | 2011-12-06 |
| IL215032A (en) | 2016-04-21 |
| JP5467631B2 (ja) | 2014-04-09 |
| BRPI1009354A2 (pt) | 2016-03-08 |
| US20120004363A1 (en) | 2012-01-05 |
| EP2407514B1 (en) | 2017-03-01 |
| JP2010209302A (ja) | 2010-09-24 |
| US8829084B2 (en) | 2014-09-09 |
| EP2407514A4 (en) | 2014-04-23 |
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