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TW409144B - Alkyl ether amine conveyor lubricants containing corrosion inhibitors - Google Patents

Alkyl ether amine conveyor lubricants containing corrosion inhibitors Download PDF

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Publication number
TW409144B
TW409144B TW086105628A TW86105628A TW409144B TW 409144 B TW409144 B TW 409144B TW 086105628 A TW086105628 A TW 086105628A TW 86105628 A TW86105628 A TW 86105628A TW 409144 B TW409144 B TW 409144B
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TW
Taiwan
Prior art keywords
composition
surfactant
acid
amine compound
linear
Prior art date
Application number
TW086105628A
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English (en)
Inventor
Kimberly L P Hei
Michael E Besse
Bruce E Schmidt
Christopher S Sykes
Original Assignee
Ecolab Inc
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Publication of TW409144B publication Critical patent/TW409144B/zh

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    • C10M129/02—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen having a carbon chain of less than 30 atoms
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    • C10N2040/44—Super vacuum or supercritical use
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    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/50—Medical uses
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2050/00—Form in which the lubricant is applied to the material being lubricated
    • C10N2050/01—Emulsions, colloids, or micelles
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
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    • C10N2070/02—Concentrating of additives

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Description

409144 經濟部中央標準局員工消費合作社印製 A7 ___B7 _五、發明説明（1 ) 發明頜城 本發明槪括地有關K胺為基質的潤滑劑組成物及使用 方法。更特定言之，本發明係有關含有腐蝕抑制劑的抗微 生物輸送機潤滑劑*其係以包括烷基醚胺及/或二胺化合 物的組成物為基者。 發明昔暑 飲料和其他食品常在機械化輸送機系統上加工和包裝 。這些輸送機系統皆經潤滑以減少在包裝與輸送機荷重承 載面之間的摩擦力。 抗微生物劑可用於可能輸送食物的輸送機系統。飲料 和其他食品在輸送機上濺溢常導致细菌，酵母菌和黴菌的 生長且可能造成黏物或污穢，彼等轉而會妨礙輸送機性能 且也可能損及產品純度和外觀。抗微生物劑特別可用來在 輸送食物的輸送機系統中減少彼等黏污之形成。 在過去，普趫用於這些輸送機系統的荷重承載面上之 潤滑劑典型地含有脂肪酸皂作為活性潤滑劑成份，和抗微 生物劑K控制微生物的生長。不過，脂肪酸皂潤滑劑與水 硬度離子反應的傾尚會損及該潤滑劑的整體性能。 不含脂肪酸的潤滑劑組成物已開發出來Μ期能避免或 消除在用含有硬度雛子的水稀釋潤滑劑時所遇到的沈澱問 題。例如，Jansen *美國專利第4,839,067號揭示一種用 含有潤滑量的中和Cm 8第一脂肪胺之潤滑劑組成物處理 輸送機帶K保養鏈型輸送機帶之方法。不過，如Jansen所 提及者，該第一脂肪酸胺傾向於在水中常發現的雜質陰離 請 閱 意 费 裝 Γ： t im. 訂 本紙張尺度適用中國國家標準（CNS } A4規格（210X297公釐） 409144 A7 ______^7__ 五、發明説明（2 ) 子例如、PCU·3和C〇3·2之存在中形成沈澱物，其會 Μ頗與脂肪酸皂在水硬度存在中的相同方式堵塞噴嘴和污 染輸送機糸統表面。
Schmidt et ai.,美國專利第5，1δ2,035號揭示出使用 脂族醚二胺乙酸鹽與醇糸助溶劑組合用於潤滑劑組成物中 Μ增進物理安定性。
Weber et al.,美國專利第5,062,978號也揭示Κ脂肪 烷胺為基質的水性潤滑劑組成物，其可用於輸送帶操作中 ，尤其是在瓶子的輸送中。 5吐3?卜3，已公開的歐洲專利申請第〇,533,522 41號 揭示含有分枝飽和或不飽和Cs至C21烷基醚胺和二胺之潤 滑劑組成物。該潤滑劑組成物可用於輸送機操作中且也可 以包含界面活性劑，和醇溶劑。 另一種沈澱問題發生於某些食物製造中的黑色沈澱物 形成。這種黑色沈澱物最常發生於碳酸飲料例如啤酒的製 造，處理和裝瓶之中。在過去，這種沈澱物在所述應用中 有不同形成程度。該沈澱物據信是因金屬磨耗上的金屬， 金屬腐蝕，和某些食品污物（在加工環境中另外存在者） 與該應甩中所用潤滑劑交互作用所促成者。 因此仍有需要提出用於所有包裝材料和輸送機表面之 上的抗微生物潤滑劑，其可提供改良的金屬在金屬上的潤 滑性及腐蝕抑制性質。 發明概沭 根據本發明第一部份，提出—種潤滑劑濃縮組成物， 本紙張尺度適用中國國家標準（CNS ) A4規格（2丨0X297公釐） fiuvi--·- ·1 t ·~τΐϊ b—* — [ILIh---^---1裝-- f .. c (請先聞讀背面之注$項再填寫本莧) jI訂 經濟部中央標準局員工消費合作社印製 經濟部中央標準局員工消費合作社印製 409144 A7 B7 五、發明説明（3 ) 其具有潤滑有效量的下式胺化合物 Ri-0-R2-NHa Ri-O-R2-NH-R3-NH2 和彼等的混合物 其中Ri可為線型飽和或不飽和Ce-C1B烷基，R2可為線型或 分枝Ci-C8烷基，且R3可為線型或分枝匕-“烷基。該濃縮 物含有腐蝕抑制劑且也可包含有效量的界面活性劑以在稀 釋和使用時提供清潔力給濃縮物，及有效量的酸以溶解該 胺。視情況，該濃縮物也可包括助溶劑以提供產物安定性 0 本發明也提出一種潤滑劑使用溶液，其係該濃縮物經 稀釋所得者，其中胺化合物的存在濃度為約10 ΡΡΠΙ至10000 ppm 0 根據本發明另一部份提出一種潤滑輸送機糸統的方法 *其係使用本發明潤滑劑濃縮組成物的使用溶液。 本發明為含有線型垸基醚胺和腐蝕抑制劑之潤滑劑。 本發明的線型烷基醚胺潤滑劑可於離子和飲料污物存在中 促進在水性糸統中的潤滑性和溶解性，並於廣pH範圔内保 持溶液形式。本發明潤滑劑可保持穩定且實質地不與系統 中所含自由陰離子和食品污物起反應。再者，本發明線型 烷基醚胺可消除使用醇類溶劑Μ維持濃縮物物理安定性之 需要。本發明組成物也提供減低的金屬腐蝕及改良的金屬 潤潸性。所揭示的本發明也可在低稀釋率下對聚對苯二甲 酸乙二醇酯（PET)，玻璃，和金屬表面提供良好的滑動作 本紙張尺度適用中國國家標牟（CMS ) A4規格（210X297公釐） (請先閲讀背面之注意事項再填寫本頁) 裝. 訂 409144 經濟部中央標準局貝工消費合作社印製 A7 B7 五、發明説明（4 ) 用。再者，本發明潤滑劑也提供在非-食品接觸表面上的 抗微生物效力，可在5分鐘內提供99.9的细菌減少率。 酿住啻倫例夕詳組I說明 本發明係潤滑劑濃縮組成物和使用溶液。該濃縮憮可 為固體或液體。本發明組成物包括線型烷基醚胺化合物* 其可提供潤滑性，抗微生物特性，Μ及常發生於使用環境 中的各種沈澱物形成之減少。本發明組成物也包括腐蝕抑 制劑，清潔劑，酸來源，和選用的助溶劑，及其他組成份 。本發明也包括使用所揭示的本發明組成物之方法。 Α.榼甚醚胺彳h合物 本發明潤滑劑包括一種胺化合物。該胺化合物係用來 增強組成物的潤滑性•進一步的抗微生物特性，及減低或 消除因水稀釋及/或應用表面上的雜質所致各種沈澱物之 形成。 本發明胺化合物可包括任何數目的物種。較佳者，該 胺化合物為具有下列式的烷基醚胺化合物》
Ri-〇-Rz~NH2, (1)
Ri-O-R2-HH-R3-NH2, (2) 和其混合物 其中h可為線型飽和或不飽和(^-(：18烷基* r2可為線 型或分枝匕-心烷基，且R3可為線型或分枝匕-心烷基。 更佳者，Ri為線型Ci2-CiB烷基，為Ca-Ce線型或分 枝烷基；且R3為線型或分枝C2-CB烷基。 本發明較佳組成物包括式（1)和（2)中， R2為C3且R3為C3之線型烷基醚胺化合物。 本紙張尺度適用中國國家標準（CNS ) A4規格（210X297公釐） I-.-iL-----裝-- C (請先閱讀背面之注意事項再填寫本頁) -fr 4_ A7 ___ B7_ 五、發明説明（5 ) 當所用的胺化合物為式（1)及/或（2)的胺時，Ri為線 型烷基C12-C1S或線型烷基合物。 整體而言，本發明組成物中所用的線型烷基醚胺化合 物可提供於稀釋後的較低使用濃度而有增進的潤潸性。該 胺化合物在濃縮物中的量通常為約0.1重量％至90重量％ ，較佳者約0.25重量％至75重量％，且更佳者約0.5重量 %至50重量％。 該胺物質可在市面上得自Tomah Products Incorpor*-ated * 為PA-19 ， PA-1618 ， PA1816 ， DA1618 ， DA-18 ， DA- 19 ， DA-1816 等。 該濃縮物的使用稀釋率較佳者係經計算M在所欲應用 中得到消毒或衛生效力者。因此之故，本發明組成物中的 活性胺化合物濃度為約10 ppm至10000 ppm，較佳者為約 20 ppm至7500 ppm，且最佳者為約40 ppm至5000 ppm。 B.腐Μ柚制额 本發明濃縮組成物和使用稀釋組成物也包含一腐蝕抑 制劑。可用的腐蝕抑制劑包括多元羧酸例如短鏈二羧酸， 三狻酸，以及磷酸酯，與彼等的組合。可用的磷酸酯包括 磷酸烷酯，一烷基芳基磷酸酯，二烷基芳基磷酸醑，三烷 基芳基磷酸酯，和彼等的混合物例如市面上可得自Witco Chemical Company的Emphos PS 236 〇 更特定言之，該酯化烷基磷酸或磷酸鹽係對應於通式 (3)者：
Ri-〇-[CH2CH2-〇3n-P〇3X2 (3) 本紙張尺度適用中國國家標準（CMS ) A4规格（210X297公釐） 經濟部中央標準局員工消費合作社印製 409144 A7 _____B7_______ 五、發明説明（6 ) 其中Ri為線型或分枝飽和第一烷基，（：8至(：13，X為氫及/ 或鹼金屬，且η為約3至10範圍内的整數。 該酯化烷基芳基磷酸或磷酸鹽係對應於通式（4)者： R2R3-CSH3-O-· [-CH2CH2-O] 11-ΡΟ3Χ2 (4) 其中為線型或分枝飽和第一烷基，CaMC1Q，R3為氫* 或線型或分枝飽和第一烷基，（：8或(：1(]，X為氫及/或鹼金 屬，且η為在約4至約10範園内的整數。 其他可用的腐蝕抑制劑包括三唑類，例如苯并三唑， 甲苯基三唑和氫硫基苯并三唑，及組合著的膦酸酯例如1-羥基亞乙基-1,1-二膦酸，和界面活性劑例如油酸二乙醇 醯胺與椰子兩性基羥基丙基磺酸鹽，及類似者。 根據本發明，較佳的腐蝕抑制劑為多元羧酸例如二羧 酸。較佳的酸包括己二酸，戊二酸，丁二酸力和彼等的混 合物。最佳者為己二酸，戊二酸和丁二酸的混合物，其為 MSFMS0KALAN㊅DCS之名售出之原料。 組成物中的腐蝕抑制劑濃度為濃縮物中的〇·〇5%至25 %，且較佳者為0.1%至20%。於一較佳部份中，該濃縮 物包括約1重量％至約6重量％的腐蝕抑制劑且包含Sokalan® DCS二酸混合物。 Γ：.中筘飆 通常，也可Μ使用中和劑來提供濃縮物和使用溶液兩 者之中的在約5和10之間的有效pH值。 '範例酸包括有機酸和無機酸。可用於本發明組成物中 的無機酸包括例如，鹽酸，磷酸，氫氟酸’硫酸，硝酸， 本紙張尺度適用中國國家標準（CNS ) A4規格（210X297公釐） (請先閲讀背面之注意事項再填寫本頁) •裝. 訂- 經济部中央標準局員工消費合作社印製 Α7 Β7 五、發明説明（7 ) 氫溴酸，和胺磺酸。 可用於本發明中的有機酸包括乙酸，羥乙酸，葡萄糖 酸，乳酸，苯甲酸，C8-C2tI飽和與不飽和脂肪酸，如油酸 ，及彼等的混合物。 酸濃度必須足夠且有效地溶劑化和安定化各種組成份 及本發明濃縮組成物和使用溶液組成物。 D.衷而活性劑 求發明潤猾劑組成物可視情況，不過較佳者，包括界 面活性劑。該等界面活性劑可作為佐劑以增加清潔力和潤 滑性。可在本發明中用為界面活性劑之化合物包括，非離 子界面活性劑，兩性界面活性劑，陰離子界面活性劑，和 '陽離子界面活性劑，及其他化合物。 · 陰離子界面活性劑通常為含有疏水性烴部份體和荷負 電親水性部份體的化合物。典型的市售產品可提供羧酸基 ，磺酸基，硫酸基或磷酸基作為荷負電親水性部份體。特 別適用於本發明潤滑劑組成物中的陰雛子界面活性劑為磷 酸鹽酯。概括地，任何種市售陰離子界面活性劑都可用於 本發明潤滑劑組成物之中。 非離子界面活性劑通常為疏水性化合物，其基本上不 載有電荷且因分子中含有氧而展現出親水性傾向。非離子 界面活性劑涵蓋著廣多種聚合體化合物，其包括，特定言 之但非唯有地，乙氧化烷酚，乙氧化脂族醇，乙氧化胺’ 乙氧化醚胺，羧酸酯，羧醯胺，及聚氧化烯嵌段共聚物。 特別適當的可用於本發明潤滑劑組成物中之非離子界 本紙張尺度適用中國國家標準（CNS > Μ規格（21〇><297公釐） (請先聞讀背面之注意事項$寫本頁) 裝· 409144 A7 B7 五、發明説明（8 ) (請先閱讀背面之注意事項再填寫本頁) 面活性劑為具有通式R1D0((CHa)m〇)n的烷氧化（較佳者， 乙氧化）醇，其中R111為具有約8至約24個碳原子的脂族基 ，]1>為1至約5的整數，且η為1至約40的數，其表分子上的 平均伸乙氧基數目。 陽離子界面活性劑也可用於本發明中且可作為加添的 抗微生物劑。典型例子包括氯化四級銨界面活性劑例如氯 化正烷基二甲基苄基銨，氯化正烷基（Cm8)二 甲基苄基銨，氯化正十四烷基二甲基苄碁銨一水合物*氯 化正烷基（C13-14)二甲基卜萘甲基銨。 兩性界面活性劑，同時含有酸性和鹼性親水基的界面 活性劑也可用於本發明中。兩性界面活性劑可含有常在陰 離子或陽離子界面活性劑中所含的陰雛子基或陽離子基且 可另含可增進界面活性劑性質的羥基或其他親水性基。彼 等兩性界面活性劑包括内銨鹽式界面活性基，磺酸内銨鹽 内界面活性劑，兩性咪唑啉鹽衍生物及其他者。 經濟部中央標準局員工消費合作社印製 於濃縮物/中，界面活性劑的濃度通常為約0.01重量％ 至50重量涔，且較佳者為約0.1重量炻至20重量％。更佳 者，界面活性劑濃度為約1至10重量％且該界面活性劑為 非離子酵乙氧化物例如Neodol 25-7 (得自Shell Chemical )0 E.肋溶蘭 本發明潤滑劑組成物可視情況包括有效量的助溶劑K 供濃縮物的黏度控制和低溫安定性所用。 有多種相容性助溶劑可用於潤滑劑組成物中，包括單 本紙張尺度適用中國國家標準（CNS ) Α4規格（210X297公釐） 409144 A7 _____B7__ 五、發明説明（9 ) 官能性和多官能性醇Μ及乙二醇和乙二醇醚化合物。經發 現最有用者包括垸基醇例如*乙醇，異丙醇等。多官能有 {請先間讀背面之注意事項再填寫本頁) 機醇包括甘油，己二醇，聚乙二醇，丙二醇，山梨糖醇等 〇 較佳的肋溶幽為二官能醇例如烷二醇。經發現在濃縮 物和其使用溶液的安定化中具有突出效力的一種化合物為 己二醇。通常，濃縮物中的助溶劑濃度為約0.1至40重量 %，且較佳者為約1至25重量％。於本發明一更佳部份中 ，該助溶劑的濃度為約3重量％至10重量％且包括己二酵。 操作俐 下面的操作例係用Μ閫逑本發明各種性質，特性和實 施例。不過，這些並不是用來限制本發明範圍者： 實施例1:磨镲和磨耗檢験 用於摩擦和磨耗檢驗中的潤滑劑濃縮物係依表1中所 列製備成的，其係經由將軟水與助溶劑和酸組合，加熱到 120Τ，並混合加入其餘的原料。這些濃縮物的使用溶液 係經由將1000份自來水（5-6粒硬度（grain hardness)) 與2.5份濃縮物組合得到0.25%溶液而製成者。 經濟部中央標準局貝工消費合作社印裝 |適 一度 尺 I張 -紙 本 一準 j標 家 A4 |釐 公 97 409144 A7 B7 五、發明説明（10 ) 盡1 為摩擦和磨耗檢驗製借闬的配方 原料 1A 1B 1C 1D 重量％ C12/C14烷氧丙基-1,3-二胺基丙燒 9.0 8.0 8.0 N，油基-1,3-二胺基丙烷 4.0 N-椰基-1,3-二胺基丙烷 4.0 戊二酸/己二酸/丁二酸1 4.0 乙酸 1.8 1.8 磷酸酯2 18.2 助溶劑 7.0 10.0 10.0 10.0 非離子界面活性 7.0 10.0 10.0 10.0 軟水 73.0 53.8 70.2 70.2 ^11- In HI ^.n— 1^1 ^^^1 ^^^1 — I ( ί.. · (請先閲讀背面之注意事項再％寫本頁) 1 得自BASF Corporation名為Solkalan DCS之二酸混合物0 2 得自liitco Chemical的Eiaphos PS 236鱗酸酯。 使用裝有軟鋼V-型塊（1137)和不銹鋼栓（302)的Falex Friction and Wear Machine (Faville-LeVally Corp., Model: Pin and V-Block)來測定潤滑劑使用溶液的失敗 點（fail point)。將該溶液K100毫升/分速率循環過該 V-塊和栓組合。同時，將該falex設定到50 psi 5分鐘， 然後Μ 5分鐘間隔依次增加到200，250，300等直到大幅 不確定的轉矩讀值或突然的壓力損失顯示栓及/或V-形塊 磨耗因而敗壞之時為止。在發生微小壓力損失的事件中將 壓力重新設定到Μ—分鐘間隔的所欲位準。於每一分鐘記 錄經由齒調整所測量的轉矩，壓力和磨耗。 本纸張尺度適用中國國家標準（CNS > A4規格（210X297公釐） 訂 經濟部中央榇準局員工消費合作社印製 409144 A7 B7 五、發明説明（11 ) 表2 _擦和磨耗生时點宙 配方 胺類別 酸源 pH 失敗點 (psi) 經過的時間 (分：秒） 1A1 線型醚二胺 二酸混合物 6.8 330 20 ： 00 1B1 線型醚二胺 磷酸酯 7.3 200 6 ： 45 1C 線型醚二胺 乙酸 7.6 190 5 ： 00 1D 烷二胺 乙酸 7.6 200 5 ： 30 1代表本發明揭示之配方 用二酸組合中和線型醚胺可導致軟鋼與不銹鋼之間的 摩擦和磨耗之減低。利用乙酸中和的市售潤滑劑和實驗潤 滑劑兩者都在50 psi下平衡5分鐘後不久即失敗。 窨施例2:腐鋪池制 依表3所列經由將軟水與指定的酸和助溶劑組合，熱 至12(TF，再混合加入其餘原料而製備成潤滑劑濃縮物。 (請先閲讀背面之注意事項再填寫本頁) -裝- 訂- 經濟部中央標準局員工消費合作社印製 本紙張尺度適用中國國家標準（CNS )从規格（210><297公釐） 409144 A7 B7 五、發明説明（12 ) 表3 世酖鋼腐飩檢酴用的配方 原料 2A 2B 2C 2D 2E 重量％ 十四烷氧丙基-1，3-二胺基丙烷 6.0 6.0 6.0 h ϋ/Ci 5烷氧丙基-1,3-二胺基丙烷 6.0 6.0 戊三酸/己二酸/丁二酸1 4.0 乙酸 2.2 1.1 乙醇酸 4.0 4.0 磷酸酯2 9.1 助溶劑 3.0 3.0 3.0 5.0 5.0 非離子界面活性 10.0 10.0 10.0 10.0 10.0 腐蝕添加劑3 5.0 軟水 77.0 78.8 70.8 70.0 75.0 (請先閲讀背面之注$項再填寫本頁) 經济部中央標隼局員工消費合作社印製 1可得自BASF Corporation名為Solkalan DCS之二酸混合物。 2可得自Witco的磷酸酯Emphos PS 236。 3下文所述腐蝕添加劑。 要對含有各種中和劑的潤滑劑濃縮物檢驗軟鋼腐蝕抑 制劑時》用1000份含有5-6粒硬度的自來水製備0.25%使 用溶液並用稀Κ0Η將該使用溶液的pH調整到9。將預清潔過 的IX 3吋冷軋鋼（#1018)板浸於該使用溶液中使該使用溶 液覆蓋一半的該鋼板試料。於24小時後目視評估該鋼板的 腐蝕和使用溶液的澄清性，並根據下面所列的描逑予Μ評 等。所有檢驗都Κ二重複完成。根據下面的標度評估諸樣 品。 本紙張尺度適用中國國家標準（CNS > Α4規格（21〇X297公釐） 409144 A7 B7 五、發明説明（13 ) 等鈒密液宪觀_ 鋼板腐触 1 溶液不變 沒有可看出的腐蝕跡象 2 溶液稍微變色非常輕微的腐蝕’ 1-5%的鋼板表面積顯示出腐蝕。 3 溶液變色中度腐蝕， 6-10%的鋼板表面積顯示出腐蝕。 4 溶液圼深琥珀嚴重腐蝕’ 11-90%的鋼板表面積 色 顯示出腐独。 恙4 ，邓，和咒酖缅腐鋪檢驗銪果 (0.25炻溶液調到pH 9, 24小時後評等） 配方 組成份 2個讀值的腐蝕評等 溶液澄清度 鋼板外觀 2A 戊二酸/己二酸/丁二酸 2,2 2,1 2B 乙酸 3,3 3,2 2C 磷酸酯/乙酸 2,3 (請先閲讀背面之注意事項再填寫本頁) .秀· 經濟部中央標準局員工消費合作社印製 要對含有各種腐蝕抑制劑的潤滑劑濃縮物檢驗軟鋼腐 蝕抑制時，係用配方2D和2E製備0.5%使用溶液。對於此 評估，係用含有5-6粒硬度的1000份自來水組合5份濃縮物 並用稀Κ0Η將溶液pH值調到8而製備成溶液。將預-清潔過 的1x3冷軋鋼（#1018)盤浸漬在該使用溶液中使得該使用溶 液覆蓋該鋼板試料的一半。於24小時後目視評估鋼板的腐
本紙張尺度適用中國國家襟準（CNS ) A4規格（210X297公釐） 409144 Α7 Β7 五、發明説明（14 ) 蝕情形和使用溶液的澄清性，並予Μ評等。所有檢驗都以 二重複完成。 表5 ffi方21)和2Ε的躭鋼腐鈾掄酴法里 (0.50%溶液調到pH 8，48小時後評等) 配方 腐蝕添加劑 2個讀值的腐蝕評等 溶液澄清性 鋼板外觀 2D 己二酸 1,1 2,2 2D D-異抗壞血酸 2,2 1,2 2D 乳酸 3,3 1,1 2D 蘋果酸 2,2 1,2 2D 油酸二乙醇醸胺1 3,3 1,1 2D 椰子兩性羥丙基磺酸鈉3 3,3 1,1 2Ε 撕 3,3 2,2 1 Rhone Poulenc所售的Alkamide WRS-166。 3 Rhone Poulenc所售的Miranol CS° (請先閲讀背面之注意事項再爽寫本頁) -裝· -訂' 經濟部中央標準局員工消费合作社印製 各種腐蝕抑制劑且特別是二酸可在線型烷基醚胺調配 物中提供軟鋼的抗腐蝕作用。再者*酸物種顯然地可以摻 加而有腐蝕抑制劑與胺中和劑之雙重角色，有益於生產成 本和效率。 上面的說明，實施例和數據可提供本發明組成物的製 造和使用之完整說明。由於可Μ做成本發明許多實胞例而 不違離本發明旨意和範圍，因此本發明係存在於後文所附 申請專利範圍中。 本紙張尺度適用中國國家標準（CNS > Α4規格（210Χ2ς>7公釐）

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  1. 煩請委爾吩：一{.，本袞帒广&是否變更原實質内容 經濟部智慧財產局員工消費合作社印製 第86105628號專利再審查案申請專利範圍修正本 修正曰期：89年05月 1. 一種濶滑劑濃縮組成物，其包含： a. —潤滑有效量之至少一種胺化合物，該胺化合物 具有下列化學式： R!-0-R2-NH2, 和彼等的混合物 其中I為線型飽和或不飽和C6-C18烷基，尺2為線型或 分枝CrC8亞烷基，且Rs為線型或分枝0「(：8亞烷基； b_ —防蝕有效量之一種腐蝕抑制劑.，該腐银抑制劑 包含二羧酸、三羧酸或其等之混合物；及 c_ 一界面活性劑，其去污量有效地提供清潔力給該 組成物，其中該界面活性劑包含陰離子界面活性 劑、非離子界面活性劑、陽離子界面活性劑、兩 性界面活性劑或其等之混合物，其中該濃縮組成 物具有約5至10的pH值且可被稀釋以產生一具有 pH值大於7之潤滑劑。 2. —種含水潤滑劑，其包含一主要部份的含水稀釋劑， 約10 ppm至10000 ppm的至少一種胺化合物，該胺化 合物具有下列化學式： Rr〇-R2-NH2, Rr0-R2-NH-R3-NH2J 和彼等的混合物 本紙張尺度適用中國國家標準（CNS)A4規格（210 X 297公釐） c請先閲讀背面之注意i項再填寫本頁) 幻·!--------線丨
    煩請委爾吩：一{.，本袞帒广&是否變更原實質内容 經濟部智慧財產局員工消費合作社印製 第86105628號專利再審查案申請專利範圍修正本 修正曰期：89年05月 1. 一種濶滑劑濃縮組成物，其包含： a. —潤滑有效量之至少一種胺化合物，該胺化合物 具有下列化學式： R!-0-R2-NH2, 和彼等的混合物 其中I為線型飽和或不飽和C6-C18烷基，尺2為線型或 分枝CrC8亞烷基，且Rs為線型或分枝0「(：8亞烷基； b_ —防蝕有效量之一種腐蝕抑制劑.，該腐银抑制劑 包含二羧酸、三羧酸或其等之混合物；及 c_ 一界面活性劑，其去污量有效地提供清潔力給該 組成物，其中該界面活性劑包含陰離子界面活性 劑、非離子界面活性劑、陽離子界面活性劑、兩 性界面活性劑或其等之混合物，其中該濃縮組成 物具有約5至10的pH值且可被稀釋以產生一具有 pH值大於7之潤滑劑。 2. —種含水潤滑劑，其包含一主要部份的含水稀釋劑， 約10 ppm至10000 ppm的至少一種胺化合物，該胺化 合物具有下列化學式： Rr〇-R2-NH2, Rr0-R2-NH-R3-NH2J 和彼等的混合物 本紙張尺度適用中國國家標準（CNS)A4規格（210 X 297公釐） c請先閲讀背面之注意i項再填寫本頁) 幻·!--------線丨
    A8 Βδ C8 DS -Ju. 經濟部智慧財產局員工消費合作社印製 409^144 、申請專利範圍 其中1為線型飽和或不飽和Ce-C18烷基，112為線型或 分枝CrC8亞烷基’且r3為線型或分枝(^-(：8亞烷基； 一防蝕有效量之一種腐蝕抑制劑，該腐蝕抑制劑包含 二羧酸、三羧酸或其等之混合物；一去污量之界面活 性劑’其在使用時有效地提供清潔力，其中該界面活 性劑包含陰離子界面活性劑、非離子界面活性劑、陽 離子界面活性劑、兩性界面活性劑或其等之混合物， 其中該濃縮組成物具有約7至10的pH值。 . 3·如申請專利範圍第1項之組成物，其中該胺化合物的 濃度為約0.1重量％至9〇重量％。 4. 如申請專利範圍第2項之組成物，其中該胺化合物的 濃度為約0.1重量％至90重量％。 5. 如申請專利範圍第1、2、3或4項之組成物，其中該胺 化合物為單胺化合物，且Ri為線型ci2_Ci6烷基，以及 Κ·2為 烧基。 6. 如申請專利範圍第1、2、3或4項之組成物，其中該胺 化合物為單胺化合物，Ri為選自於由ci〇_Ci2烷基、 Cw-Cw院基和彼等的混合物所構成之群中，且]^為（：2_ c6亞烷基。 7，如申請專利範圍第1、2、3或4項之組成物，其中該胺 化合物為二胺化合物，RigCi2_Ci6烷基，1為(：2_(：6亞 院基’且尺3為(：2-(：6亞烷基。 8.如申請專利範圍第1、2、3或4項之組成物，其中該胺 化合物為二胺化合物，Ri為選自於由Ci〇_Ci2烷基、 (請先閱讀背面之注意事項再填寫本頁)
    A8 Βδ C8 DS -Ju. 經濟部智慧財產局員工消費合作社印製 409^144 、申請專利範圍 其中1為線型飽和或不飽和Ce-C18烷基，112為線型或 分枝CrC8亞烷基’且r3為線型或分枝(^-(：8亞烷基； 一防蝕有效量之一種腐蝕抑制劑，該腐蝕抑制劑包含 二羧酸、三羧酸或其等之混合物；一去污量之界面活 性劑’其在使用時有效地提供清潔力，其中該界面活 性劑包含陰離子界面活性劑、非離子界面活性劑、陽 離子界面活性劑、兩性界面活性劑或其等之混合物， 其中該濃縮組成物具有約7至10的pH值。 . 3·如申請專利範圍第1項之組成物，其中該胺化合物的 濃度為約0.1重量％至9〇重量％。 4. 如申請專利範圍第2項之組成物，其中該胺化合物的 濃度為約0.1重量％至90重量％。 5. 如申請專利範圍第1、2、3或4項之組成物，其中該胺 化合物為單胺化合物，且Ri為線型ci2_Ci6烷基，以及 Κ·2為 烧基。 6. 如申請專利範圍第1、2、3或4項之組成物，其中該胺 化合物為單胺化合物，Ri為選自於由ci〇_Ci2烷基、 Cw-Cw院基和彼等的混合物所構成之群中，且]^為（：2_ c6亞烷基。 7，如申請專利範圍第1、2、3或4項之組成物，其中該胺 化合物為二胺化合物，RigCi2_Ci6烷基，1為(：2_(：6亞 院基’且尺3為(：2-(：6亞烷基。 8.如申請專利範圍第1、2、3或4項之組成物，其中該胺 化合物為二胺化合物，Ri為選自於由Ci〇_Ci2烷基、 (請先閱讀背面之注意事項再填寫本頁)
    六、 ^Bcs 經濟部智慧財產局員工消費合作社印製 409144 申請專利範圍 Ci4-C1G烧基和彼等的混合物所構成之群申，1為匚2-〇0 亞炫·基’且R3為02-(1；6亞烧基。 9·如申請專利範圍第1、2、3或4項之组成物，其更包含 一助溶劑。 10.如申請專利範圍第9項之組成物，其中該助溶劑係選 自於由乙二醇、醇、乙二醇醚和彼等的混合物所構成 之群中。 11·如申請專利範圍第10項之組成物，其中該助溶劑包含 存在濃度為約0.1重量％至40重量％之己二醇。 12.如申請專利範園第1、2、3或4項之組成物，其中該腐 蝕抑制劑包含存在濃度為約0.05重量％至25重量％之 二叛酸。 丄3.如申請專利範圍第12項之組成物，其中該二羧酸係選 自戊二酸、己二酸、丁二酸和彼等的混合物之中者。 14. 如申請專利範園第1項之組成物，其中該界面活性劑 包含存在濃度為約0.01重量％至50重量％之非離子界 面活性劑〇 15. 如申請專利範圍第14項之組成物，其中該非離子界面 活性劑具有約1至40莫耳的伸乙氧基。 16. 如申請專利範圍第1、2、3或4項之組成物，其中該組 成物為固體。 17. 如申請專利範圍第1'2、3或4項之組成物，其中該組 成物為液體。 18. 如申請專利範圍第1、2、3或4項之組成物，其更包含 一 -3- (請先閲讀背面之注意事項再填寫本頁)
    本紙張尺度適財關家標準（cns)A4規i (210x 297 公釐） 六、 ^Bcs 經濟部智慧財產局員工消費合作社印製 409144 申請專利範圍 Ci4-C1G烧基和彼等的混合物所構成之群申，1為匚2-〇0 亞炫·基’且R3為02-(1；6亞烧基。 9·如申請專利範圍第1、2、3或4項之组成物，其更包含 一助溶劑。 10.如申請專利範圍第9項之組成物，其中該助溶劑係選 自於由乙二醇、醇、乙二醇醚和彼等的混合物所構成 之群中。 11·如申請專利範圍第10項之組成物，其中該助溶劑包含 存在濃度為約0.1重量％至40重量％之己二醇。 12.如申請專利範園第1、2、3或4項之組成物，其中該腐 蝕抑制劑包含存在濃度為約0.05重量％至25重量％之 二叛酸。 丄3.如申請專利範圍第12項之組成物，其中該二羧酸係選 自戊二酸、己二酸、丁二酸和彼等的混合物之中者。 14. 如申請專利範園第1項之組成物，其中該界面活性劑 包含存在濃度為約0.01重量％至50重量％之非離子界 面活性劑〇 15. 如申請專利範圍第14項之組成物，其中該非離子界面 活性劑具有約1至40莫耳的伸乙氧基。 16. 如申請專利範圍第1、2、3或4項之組成物，其中該組 成物為固體。 17. 如申請專利範圍第1'2、3或4項之組成物，其中該組 成物為液體。 18. 如申請專利範圍第1、2、3或4項之組成物，其更包含 一 -3- (請先閲讀背面之注意事項再填寫本頁)
    本紙張尺度適財關家標準（cns)A4規i (210x 297 公釐） 409144 A8B8C8D8 六、申請專利範圍 經濟部智慧財產局員工消費合作社印製 一中和劑。 19·如申請專利範圍第18項之組成物其中該中和劑包含 選自於下列群中之酸：乙酸、羥乙酸、葡萄糖酸乳 酸、苯Ψ酸和彼等的混合物。 2〇.如申請專利範圍第1、2、3或4項之組成物其中該組 成物具有一消毒位準的抗微生物效力。 21. —種潤滑輸送機系統的方法，其使用包含一潤滑有效 $之至少一種胺化合物的被稀釋之潤滑劑濃縮組成 物’該胺化合物具有下列化學式； Ri-〇-R2-NH2, ⑴ RrO-R2-NH-R3-NH2, (2) 和彼等的混合物 其中I為線型飽和或不飽和C(rCi8烷基，1為線型或 分枝Ci 〇8亞燒基，且尺3為線型或分枝亞貌基； 一防蝕有效量之一種腐蝕抑制劑，該腐蝕抑制劑包含 一羧酸、二羧酸或其等之混合物；一去污量之界面活 性劑，其在稀釋和使用時有效地提供清潔力，其中該 界面活性劑包含陰離子界面活性劑、陽離子界面活性 劑、非離子界面活性劑、兩性界面活性劑或其等之混 合物，以及其中該組成物具有約7至10的pH值，該方 法包含下列諸步驟： a. 調配該潤滑劑濃縮組成物以使之具有約〇. 1重量％ 至约90重量％的該胺化合物；及 b. 以一主要部份的含水稀釋劑稀釋該潤滑劑濃 <請先閱讀啃面之注^^項再填寫本頁) ----I---- --------- -I n I ____ -4· i紙張尺度適用中國國家標準（CNS)A4規格⑽x 297公髮） 409144 A8B8C8D8 六、申請專利範圍 經濟部智慧財產局員工消費合作社印製 一中和劑。 19·如申請專利範圍第18項之組成物其中該中和劑包含 選自於下列群中之酸：乙酸、羥乙酸、葡萄糖酸乳 酸、苯Ψ酸和彼等的混合物。 2〇.如申請專利範圍第1、2、3或4項之組成物其中該組 成物具有一消毒位準的抗微生物效力。 21. —種潤滑輸送機系統的方法，其使用包含一潤滑有效 $之至少一種胺化合物的被稀釋之潤滑劑濃縮組成 物’該胺化合物具有下列化學式； Ri-〇-R2-NH2, ⑴ RrO-R2-NH-R3-NH2, (2) 和彼等的混合物 其中I為線型飽和或不飽和C(rCi8烷基，1為線型或 分枝Ci 〇8亞燒基，且尺3為線型或分枝亞貌基； 一防蝕有效量之一種腐蝕抑制劑，該腐蝕抑制劑包含 一羧酸、二羧酸或其等之混合物；一去污量之界面活 性劑，其在稀釋和使用時有效地提供清潔力，其中該 界面活性劑包含陰離子界面活性劑、陽離子界面活性 劑、非離子界面活性劑、兩性界面活性劑或其等之混 合物，以及其中該組成物具有約7至10的pH值，該方 法包含下列諸步驟： a. 調配該潤滑劑濃縮組成物以使之具有約〇. 1重量％ 至约90重量％的該胺化合物；及 b. 以一主要部份的含水稀釋劑稀釋該潤滑劑濃 <請先閱讀啃面之注^^項再填寫本頁) ----I---- --------- -I n I ____ -4· i紙張尺度適用中國國家標準（CNS)A4規格⑽x 297公髮） 409144 六、申請專利範圍 成物以使之形成一被稀釋的潤滑劑濃縮組成物； 以及 C·將該被稀釋的潤滑劑濃縮組成物施加到所欲之使 用表面上。 22.如申請專利範圍第21項之方法，其中被稀釋的潤滑劑 濃縮組成物係與聚對苯二甲酸乙二醇酯相容。 經濟部智慧財產局員工消費合作社印製 本紙張尺度適用中國國家標準（CNS)A4規格（210 X 297公g ) 409144 六、申請專利範圍 成物以使之形成一被稀釋的潤滑劑濃縮組成物； 以及 C·將該被稀釋的潤滑劑濃縮組成物施加到所欲之使 用表面上。 22.如申請專利範圍第21項之方法，其中被稀釋的潤滑劑 濃縮組成物係與聚對苯二甲酸乙二醇酯相容。 經濟部智慧財產局員工消費合作社印製 本紙張尺度適用中國國家標準（CNS)A4規格（210 X 297公g )
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PL185138B1 (pl) 2003-02-28
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DE69704757T2 (de) 2001-09-20
EP0847436A1 (en) 1998-06-17
US5723418A (en) 1998-03-03
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CN1070529C (zh) 2001-09-05
BR9702268A (pt) 1999-07-20
DE69704757D1 (de) 2001-06-13
EP0847436B1 (en) 2001-05-09
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WO1997045509A1 (en) 1997-12-04
CA2224966C (en) 2001-09-18

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