TW201406292A - 包含４－胺基－３－氯－５－氟－６－（４－氯－２－氟－３－甲氧基苯基）吡啶－２－羧酸或其衍生物以及三唑并嘧啶磺醯胺之除草組成物 - Google Patents
包含４－胺基－３－氯－５－氟－６－（４－氯－２－氟－３－甲氧基苯基）吡啶－２－羧酸或其衍生物以及三唑并嘧啶磺醯胺之除草組成物 Download PDFInfo
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- TW201406292A TW201406292A TW102126125A TW102126125A TW201406292A TW 201406292 A TW201406292 A TW 201406292A TW 102126125 A TW102126125 A TW 102126125A TW 102126125 A TW102126125 A TW 102126125A TW 201406292 A TW201406292 A TW 201406292A
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- IUQAXCIUEPFPSF-UHFFFAOYSA-N tembotrione Chemical compound ClC1=C(COCC(F)(F)F)C(S(=O)(=O)C)=CC=C1C(=O)C1C(=O)CCCC1=O IUQAXCIUEPFPSF-UHFFFAOYSA-N 0.000 description 1
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- DPOWHSMECVNHAT-YERPJTIDSA-N tetcyclacis Chemical compound C1=CC(Cl)=CC=C1N1[C@H]2[C@H]([C@@H]3[C@H]4N=N3)C[C@H]4[C@H]2N=N1 DPOWHSMECVNHAT-YERPJTIDSA-N 0.000 description 1
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- 150000004867 thiadiazoles Chemical class 0.000 description 1
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- XSKZXGDFSCCXQX-UHFFFAOYSA-N thiencarbazone-methyl Chemical compound COC(=O)C1=CSC(C)=C1S(=O)(=O)NC(=O)N1C(=O)N(C)C(OC)=N1 XSKZXGDFSCCXQX-UHFFFAOYSA-N 0.000 description 1
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- 229940087291 tridecyl alcohol Drugs 0.000 description 1
- 125000002889 tridecyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- ZSDSQXJSNMTJDA-UHFFFAOYSA-N trifluralin Chemical compound CCCN(CCC)C1=C([N+]([O-])=O)C=C(C(F)(F)F)C=C1[N+]([O-])=O ZSDSQXJSNMTJDA-UHFFFAOYSA-N 0.000 description 1
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- AKTQJCBOGPBERP-UHFFFAOYSA-N triflusulfuron Chemical compound FC(F)(F)COC1=NC(N(C)C)=NC(NC(=O)NS(=O)(=O)C=2C(=CC=CC=2C)C(O)=O)=N1 AKTQJCBOGPBERP-UHFFFAOYSA-N 0.000 description 1
- DFFWZNDCNBOKDI-UHFFFAOYSA-N trinexapac Chemical compound O=C1CC(C(=O)O)CC(=O)C1=C(O)C1CC1 DFFWZNDCNBOKDI-UHFFFAOYSA-N 0.000 description 1
- PIHCREFCPDWIPY-UHFFFAOYSA-N tris[2-(2,4-dichlorophenoxy)ethyl] phosphite Chemical compound ClC1=CC(Cl)=CC=C1OCCOP(OCCOC=1C(=CC(Cl)=CC=1)Cl)OCCOC1=CC=C(Cl)C=C1Cl PIHCREFCPDWIPY-UHFFFAOYSA-N 0.000 description 1
- KVEQCVKVIFQSGC-UHFFFAOYSA-N tritosulfuron Chemical compound FC(F)(F)C1=NC(OC)=NC(NC(=O)NS(=O)(=O)C=2C(=CC=CC=2)C(F)(F)F)=N1 KVEQCVKVIFQSGC-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/32—Ingredients for reducing the noxious effect of the active substances to organisms other than pests, e.g. toxicity reducing compositions, self-destructing compositions
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/64—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
- A01N43/647—Triazoles; Hydrogenated triazoles
- A01N43/653—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Dentistry (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
本發明係提供協同性除草組成物，其包含(a)式(I)化合物：□或其農業上可接受之鹽類或酯類，以及(b)三唑并嘧啶磺醯胺類(triazolopyrimidine sulfonamides)，其包括但不侷限於，氯酯磺草胺-甲酯(cloransulam-methyl)、雙氯磺草胺(diclosulam)、雙氟磺草胺(florasulam)、唑嘧磺草胺(flumetsulam)、磺草唑胺(metosulam)、平速爛(penoxsulam)，以及啶磺草胺(pyroxsulam)。本發明組成物提供了，例如，在直播、湛水直播與插秧稻米、穀類、小麥、大麥、燕麥、黑麥、高粱、玉蜀黍/玉米、甘蔗、向日葵、芸苔、油菜、甜菜、大豆、棉花、鳳梨、牧草、草地、牧場、休耕地、草皮、樹與藤園、水生植物、種植作物、蔬菜、工業植被管理(IVM)與路權用地(ROW)中，之不良植被之控制。
Description
本申請案係申請補充美國暫時專利申請號61/675,037，於2012年7月24日提申之內容，以及美國實用新型專利申請號13/832,978，於2013年3月15日提申之內容，每一者於此併入本案以作為參考資料。
本發明係提供一種除草組成物，其包含(a)4-胺基-3-氯-5-氟-6-(4-氯-2-氟-3-甲氧基苯基)吡啶-2-羧酸，或其農業上可接受之酯類或鹽類，以及(b)三唑并嘧啶磺醯胺類。
本發明亦提供控制不良植被之方法，其包含施加(a)4-胺基-3-氯-5-氟-6-(4-氯-2-氟-3-甲氧基苯基)吡啶-2-羧酸，或其農業上可接受之酯類或鹽類，以及(b)三唑并嘧啶磺醯胺類。
預防雜草與其他植被之生長，以保護作物，乃是
農業上不斷出現之問題。為解決此一問題，合成化學領域之研究人員已生產了大量的化合物與化學製劑，以有效控制此種不必要之生長。有多種化學除草劑已被揭示於文獻中，且許多已用於商業用途。然而，仍需要能有效控制不良植被之組成物與方法。
本發明提供之第一個實施例包括除草組成物，其包含一除草有效量之(a)式(I)化合物
或其農業上可接受之鹽類或酯類，以及(b)至少一種三唑并嘧啶磺醯胺。
本發明第二個實施例包括如第一個實施例之混合物，其中式(I)以下列形式之至少一者存在：羧酸、羧酸鹽、芳烷基、烷基酯、未經取代芐基、經取代芐基、C1-4烷基，及/或正丁酯。
本發明第三個實施例包括如第一或第二個實施例之混合物，其中三唑并嘧啶磺醯胺(b)為選自於由氯酯磺草胺-甲酯(cloransulam-methyl)、雙氯磺草胺(diclosulam)、雙氟磺草胺(florasulam)、唑嘧磺草胺(flumetsulam)、磺草
唑胺(metosulam)、平速爛(penoxsulam)，或啶磺草胺(pyroxsulam)，或前述之三唑并嘧啶磺醯胺類之至少一者之其農業上可接受之鹽類、羧酸、羧酸鹽，或酯類組成族群之化合物之至少一者。
本發明第四個實施例包括如第一、第二，或第三個實施例之混合物，其中混合物之三唑并嘧啶磺醯胺為氯酯磺草胺-甲酯，其中式(I)化合物與氯酯磺草胺-甲酯之重量比，以單位gae/ha對比gai/ha或gae/ha對比gae/ha表示，其比例範圍與比例選自於由約1：31至約137：1、約1：1、約2：1、約4：1、約2：1、約2.5：1、約1：1、約0.5：1、約10：1、約20：1、約2.4：1、約4.8：1、約1：1.17、約1：1.2、約2.4：1、約1：17、約1：1.1、約1.0：0.55、約1.0：1.1、約1.8：1、約1.2：1、約0.15：1、約0.3：1、約1：2.2、約1.0：4.4、約1：20至約1：100、約1：10至約1：50、約1：5至約1：25、約1：8至約15：1，以及約2：1至約1：1組成之族群。
本發明第五個實施例包括如第一、第二，或第三個實施例之混合物，其中混合物之三唑并嘧啶磺醯胺為平速爛，其中式(I)化合物與平速爛之重量比，以單位gae/ha對比gai/ha或gae/ha對比gae/ha表示，其比例範圍與比例選自於由約1：23至約65：1、約1：1、約2：1、約1：4、約2：1至約1：4、約1：2至約2：1、約1：2至約4：1、約1：1至約4：1、約1：2.5至約1：0.65、約1：1.5、約1：0.75、約1：0.38、約2.6：1、約1：4至約1：2、約1：4至約1：1、約1.2：1至約10：1、約5：1、約2.4：1、約4.8：1、約17：1、約11：1、約4.3：1、約3：1、約2.2：1、約2.7：1、約0.6：1、約0.4：1、約0.7：1、約1.0：1.25、約1.0：1.7、約3：1、
約4：1、約9.6：1、約1：20至1：60、約1：15至50：1、約1：2至40：1、約1：10至30：1、約1：8至20：1、約1：7至15：1、約1：6至約10：1、約1：5至8：1、約1：4至6：1、約1：3至5：1、約1：2至約4：1、約1：1至約3：1、約1：11至約1：46，以及約1：1至約5：1組成之族群。
本發明第六個實施例包括如第一、第二，或第三個實施例之混合物，其中混合物之三唑并嘧啶磺醯胺為雙氯磺草胺，其中式(I)化合物與雙氯磺草胺之重量比，以單位gae/ha對比gai/ha或gae/ha對比gae/ha表示，其比例範圍與比例選自於由約1：26至約26：1、約1：0.38、約1：0.75、約1：0.38、約1.3：1、約0.7：1、約2.6：1、約0.7：1至約1.3：1、約1.5：1、約1：25至25：1、約1：20至20：1、約1：15至15：1、約1：10至10：1、1：5至約5：1、1：4至約4：1、約1：3至約3：1，以及約1.3：1至約0.6：1組成之族群。
本發明第七個實施例包括如第一、第二，或第三個實施例之混合物，其中混合物之三唑并嘧啶磺醯胺為唑嘧磺草胺，其中式(I)化合物與唑嘧磺草胺之重量比，以單位gae/ha對比gai/ha或gae/ha對比gae/ha表示，其比例範圍與比例選自於由1：40至約272：1、約1.25：1、約2.5：1、約5：1、約1.5：1、約0.32：1、約6.4：1、約1：35至270：1、約1：30至250：1、約1：20至150：1、約1：15至100：1、1：10至75：1、約1：9至約70：1、約1：8至約60：1、約1：7至50：1、約1：6至40：1、約1：5至30：1、約1：4至20：1、約1：3至15：1、約1：2至10：1、約1：3至約5：1，以及約1.28：1至約1.5：1組成之族群。
本發明第八個實施例包括如第一、第二，或第三
個實施例之混合物，其中混合物之三唑并嘧啶磺醯胺為磺草唑胺，其中式(I)化合物與磺草唑胺之重量比，以單位gae/ha對比gai/ha或gae/ha對比gae/ha表示，其比例範圍與比例選自於由約1：5至約300：1、約1：0.8、約1：0.4、約1.5：1、約1：4至約200：1、約1：3至約100：1、約1：2至約50：1，以及約1.28至約5.1：1組成之族群。本發明第九個實施例包括如第一、第二，或第三個實施例之混合物，其中混合物之三唑并嘧啶磺醯胺為雙氟磺草胺，其中式(I)化合物與雙氟磺草胺之重量比，以單位gae/ha對比gai/ha或gae/ha對比gae/ha表示，其比例範圍與比例選自於由約1：5至約300：1、約1.0：0.75、約7.0：1.0、約4：1、約2：3、約2.1、約1：1、約1：2、約1：4、約7：1、約1：4至約200：1、約1：3至約100：1、約1：25至約50：1、約1：2至約30：1、約1：1至約25：1、約1.35：1至約7：1，以及約4：1至約2.3：1組成之族群。
本發明第十個實施例包括如第一、第二，或第三個實施例之混合物，其中混合物之三唑并嘧啶磺醯胺為啶磺草胺，其中式(I)化合物與啶磺草胺之重量比，以單位gae/ha對比gai/ha或gae/ha對比gae/ha表示，其比例範圍與比例選自於由約1：11至約75：1、約1：1、約2：1、約2.3：1、約4：1、約8：1、約11：1、約1.0：0.4、約1：10至約1：70、約1：9至約1：60、約1：8至約1：50、約1：7至約1：40、約1：6至約1：30、約1：5至約1：25、約1：4至約1：20、約1：3至約1：15、約1：2至約1：10、約1：1至約1：8，以及約2.33：1組成之族群。
本發明第十一個實施例包括如第一至第十個實
施例之任何組成物，其中混合物進一步包含農業上可接受之試劑之至少一者，選自於由佐劑、載劑，或安全劑組成之族群。
本發明第十二個實施例包括控制不良植被之方法，其包含以一除草有效量之如第一至第十一個實施例之混合物之至少一者，施加至或以其他方式接觸植被及/或土壤，及/或水之步驟。
本發明第十三個實施例包括如第十二個實施例之方法，其中不良植被係於下列至少一者上加以控制，選自於由直播、湛水直播與插秧稻米、穀類、小麥、大麥、燕麥、黑麥、高粱、玉蜀黍/玉米、甘蔗、向日葵、芸苔、油菜、甜菜、大豆、棉花、鳳梨、牧草、草地、牧場、休耕地、草皮、樹與藤園、水生植物、工業植被管理(IVM)或道路維護(ROW)組成之族群。
本發明第十四個實施例包括如第十二及/或第十三個實施例之方法，其中一除草有效量之混合物，係於出苗前或後施加至下列至少一者：作物、田野、ROW，或稻田。
本發明第十五個實施例包括如第十一至第十四個實施例之方法，其中該不良植被係經由對於具下列試劑抗性或耐受性之植物，施行至少一方法而控制，該試劑之作用模式係選自於由草甘膦(glyphosate)、5-烯醇丙酮基莽草酸-3-磷酸鹽(EPSP)合成酶抑制劑、固殺草(glufosinate)、麩胺醯胺酸合成酶抑制劑、麥草畏(dicamba)、苯氧基生長素、吡啶基氧基生長素、合成生長素、生長素運輸抑制劑、
芳基氧基苯氧基丙酸酯、環己烷二酮、苯基吡唑啉、乙醯輔酶A羧化酶(ACCase)抑制劑、咪唑啉酮、磺醯基脲、嘧啶基硫代苯甲酸酯、三唑并嘧啶、磺醯基胺基羰基三唑酮、乙醯乳酸合成酶(ALS)或乙醯羥酸合成酶(AHAS)抑制劑、4-羥基苯基-丙酮酸二氧酶(HPPD)抑制劑、八氫番茄紅素去飽和酶(phytoene desaturase)抑制劑、類胡蘿蔔素生合成抑制劑、原紫質原(protoporphyrinogen)氧化酶(PPO)抑制劑、纖維素生合成抑制劑、有絲分裂抑制劑、微管抑制劑、極長鏈脂肪酸抑制劑、脂肪酸與脂質生合成抑制劑、光合系統I抑制劑、光合系統II抑制劑、三嗪，或溴苯腈(bromoxynil)所組成族群之至少一者。
本發明第十六個實施例包括如第十一至第十五個實施例之至少一方法，其中具有至少一除草劑抗性或耐受性之植物係經處理，且其中抗性或耐受性作物具有多個或複合性狀，對於多重除草劑作用模式之多重除草劑或抑制劑具有耐受性，在一些實施例中，經處理之除草劑抗性植物本身為不良植被。
本發明第十七個實施例包括如第十六個實施例之方法，其中該具抗性或耐受性之雜草為對於多種除草劑、多種化合物類別、多重除草劑作用模式之抑制劑具有抗性或耐受性，或經由多重抗性機制之生物型。
本發明第十八個實施例包括如第十六或第十七個實施例之方法之至少一者，其中具抗性或耐受性之不良植物為對於至少一試劑，及/或一試劑之至少一作用模式具
有抗性或耐受性之生物型，該作用模式選自於由乙醯乳酸合成酶(ALS)或乙醯羥酸合成酶(AHAS)抑制劑、光合系統II抑制劑、乙醯輔酶A羧化酶(ACCase)抑制劑、合成生長素、生長素運輸抑制劑、光合系統I抑制劑、5-烯醇丙酮基莽草酸-3-磷酸鹽(EPSP)合成酶抑制劑、微管組合抑制劑、脂肪酸與脂質生合成抑制劑、原紫質原氧化酶(PPO)抑制劑、類胡蘿蔔素生合成抑制劑、極長鏈脂肪酸(VLCFA)抑制劑、八氫番茄紅素去飽和酶(PDS)抑制劑、麩胺醯胺酸合成酶抑制劑、4-羥基苯基-丙酮酸二氧酶(HPPD)抑制劑、有絲分裂抑制劑、纖維素生合成抑制劑、多重作用模式除草劑、快克草(quinclorac)、芳基胺基丙酸、野燕枯(difenzoquat)、草多索(endothall)，或有機砷類組成族群之一或多者。
本發明第十九個實施例包括控制不良植被之方法，其包含施加一除草有效量之如第五個實施例之至少一混合物之步驟，其中混合物量之施加率，以gai/ha或gae/ha之平速爛表示，其比例與比例範圍選自於由約2、4.28、4.8、8.75、17、35、50與100組成之族群。
本發明第二十個實施例包括如第五與第十九個實施例之方法，其中經控制之植物為選自於由IPOHE、LEFCH、LEFPA、BRAPP、ECHCG、SCPMA、CYPDI、CYPES與ISCRU組成族群之至少一植物，又其他之實施例包括控制選自於由牽牛屬(Ipohe)、千金子屬(Leptochloa)、臂形草屬(Brachiaria)、稗屬(Echinochloa)、莞屬(Scirpus)、莎
草屬(Cyperus)與鴨嘴草屬(Ischaemum)組成族群之植物屬。
本發明第二十一個實施例包括控制不良植被之方法，其包含施加一除草有效量之如第六個實施例之至少一混合物之步驟，其中混合物量之施加率，以gai/ha或gae/ha之雙氯磺草胺表示，其比例與比例範圍選自於由約2、6.62、13.25與26.5組成之族群。
本發明第二十二個實施例包括如第六與第二十一個實施例之方法，其中經控制之植物為選自於由：LEFCH、CYPRO與ECHCG組成族群之至少一植物，又其他之實施例包括控制選自於由千金子屬、莎草屬與稗屬組成族群之植物屬。
本發明第二十三個實施例包括控制不良植被之方法，其包含施加一除草有效量之如第七個實施例之至少一混合物之步驟，其中混合物量之施加率，以gai/ha或gae/ha之唑嘧磺草胺表示，其比例與比例範圍選自於由約2、6.25、12.5、25與50組成之族群。
本發明第二十四個實施例包括如第七與第二十三個實施例之方法，其中經控制之植物為選自於由：BRARP與CYPIR組成族群之至少一植物，又其他之實施例包括控制選自於由臂形草屬與莎草屬組成族群之植物屬。
本發明第二十五個實施例包括控制不良植被之方法，其包含施加一除草有效量之如第八個實施例之至少一混合物之步驟，其中混合物量之施加率，以gai/ha或gae/ha之磺草唑胺表示，其比例與比例範圍選自於由約2、6.25、
12.5與25組成之族群。
本發明第二十六個實施例包括如第八與第二十五個實施例之方法，其中經控制之植物為選自於由LEFCH組成族群之至少一植物，又另一實施例包括控制千金子屬植物。
本發明第二十七個實施例包括控制不良植被之方法，其包含施加一除草有效量之如第九個實施例之至少一混合物之步驟，其中混合物量之施加率，以gai/ha或gae/ha之雙氟磺草胺表示，其比例與比例範圍選自於由約2、1.25、3.75、6.65、12.5、25與50組成之族群。
本發明第二十八個實施例包括如第九與第二十七個實施例之方法，其中經控制之植物為選自於由：SASKR、VEPRE、VIOTR、MATCH、CIRAR與LAMPU組成之族群之至少一植物，又其他實施例包括控制選自於由豬毛菜屬(Salsola)、婆婆納屬(Veronica)、堇菜屬(Viola)、母菊屬(Chamomilla)、薊屬(Cirsium)與野芝麻屬(Lamium)組成族群之植物屬。
本發明第二十九個實施例包括控制不良植被之方法，其包含施加一除草有效量之如第十個實施例之至少一混合物之步驟，其中混合物量之施加率，以gai/ha或gae/ha之啶磺草胺表示，其比例與比例範圍選自於由約2、3.75、7.5與50組成之族群。
本發明第三十個實施例包括如第十與第二十九個實施例之方法，其中經控制之植物為選自於由：CIRAR組成
族群之至少一植物，又其他之實施例包括控制薊屬植物。
本發明第三十一個實施例包括控制不良植被之方法，其包含施加一除草有效量之如第四個實施例之至少一混合物之步驟，其中混合物量之施加率，以gai/ha或gae/ha之氯酯磺草胺-甲酯表示，其比例與比例範圍選自於由約1、2、2.19、4.38、8.75、17.5、35與70組成之族群。
本發明第三十二個實施例包括如第四與第三十一個實施例之方法，其中經控制之植物為選自於由：DIGSA、LEFCH、CYPIR、ECHCG、CYPDI與FIMMI組成族群之至少一植物，又其他之實施例包括控制選自於由馬唐屬(Digitaria)、千金子屬、莎草屬、稗屬與飄拂草屬(Fimbristylis)組成族群之植物屬。
本發明亦提供控制不良植被之方法，其包含施加(a)式(I)化合物或其農業上可接受之酯類或鹽類，以及(b)三唑并嘧啶磺醯胺類。
示範性三唑并嘧啶磺醯胺類包括但不侷限於，氯酯磺草胺-甲酯、雙氯磺草胺、雙氟磺草胺、唑嘧磺草胺、磺草唑胺、平速爛，以及啶磺草胺或其農業上可接受之鹽類、羧酸、羧酸鹽，或酯類。
本發明係提供一種除草組成物，其包含一除草有效量之(a)式(I)化合物
或其農業上可接受之鹽類或酯類，以及(b)三唑并嘧啶磺醯胺類。該組成物亦可包含農業上可接受之佐劑或載劑。
本發明亦提供控制不良植被之方法，包含施加(a)式(I)化合物或其農業上可接受之酯類或鹽類，以及(b)三唑并嘧啶磺醯胺類或其農業上可接受之鹽類或酯類。
使用於此，式(I)化合物具有下列結構：
式(I)化合物之名稱為4-胺基-3-氯-6-(4-氯-2-氟-3-甲氧基苯基)-5-氟吡啶-2-羧酸，並已揭示於美國專利號7,314,849(B2)，在此併入本案以作為參考資料。式(I)化合物之示範
性用途包括，於多種非種植與種植情況下，控制不良植被，其包括禾草科、闊葉與莎草科雜草。
使用於此，三唑并嘧啶磺醯胺類為具有三唑并嘧啶磺醯胺核心結構之除草劑化合物類別。不受任何理論侷限，一般相信其作用模式涉及乙醯乳酸合成酶(ALS)之抑制作用，該酵素為一種植物與微生物常見之酵素，但未於動物中發現。三唑并嘧啶磺醯胺類之示範性除草用途包括但不侷限於，用於滋擾莎草、闊葉與禾本科雜草之控制。
示範性三唑并嘧啶磺醯胺類包括但不侷限於，氯酯磺草胺-甲酯、雙氯磺草胺、雙氟磺草胺、唑嘧磺草胺、磺草唑胺、平速爛，以及啶磺草胺。
使用於此，該氯酯磺草胺-甲酯為甲基3-氯-2-[[(5-乙氧基-7-氟[1,2,4]三唑并[1,5-c]嘧啶-2-基)磺醯基]胺基]苯甲酸酯，並具有下列結構：
其除草活性示範於Tomlin,C.,ed.A World Compendium The Pesticide Manual.15th ed.Alton：BCPC Publications,2009(此後皆指“The Pesticide Manual,Fifteenth Edition,2009.”)。氯酯磺草胺-甲酯之示範性用途包括以其作為除草劑，用於大豆與其他闊葉作物之闊葉雜草之出苗後控制。
使用於此，雙氯磺草胺為N-(2,6-二氯苯基)-5-乙氧基-7-氟[1,2,4]三唑并[1,5-c]嘧啶-2-磺醯胺，並具有下列結構：
其除草活性示範於The Pesticide Manual,Fifteenth Edition,2009。雙氯磺草胺之示範性用途包括以其作為除草劑，用於花生與大豆之闊葉雜草之控制。
使用於此，雙氟磺草胺為N-(2,6-二氟苯基)-8-氟-5-甲氧基[1,2,4]三唑并[1,5-c]嘧啶-2-磺醯胺，並具有下列結構：
其除草活性示範於The Pesticide Manual,Fifteenth Edition,2009。雙氟磺草胺之示範性用途包括以其作為除草劑，用於穀類與玉米之闊葉雜草之出苗後控制。
使用於此，唑嘧磺草胺為N-(2,6-二氟苯基)-5-甲基[1,2,4]三唑并[1,5-a]嘧啶-2-磺醯胺，並具有下列結構：
其除草活性示範於The Pesticide Manual,
Fifteenth Edition,2009。唑嘧磺草胺之示範性用途包括以其作為除草劑，用於大豆、豌豆與玉米之闊葉雜草與禾草之控制。
使用於此，磺草唑胺為N-(2,6-二氯-3-甲基苯基)-5,7-二甲氧基[1,2,4]三唑并[1,5-a]嘧啶-2-磺醯胺，並具有下列結構：
其除草活性示範於The Pesticide Manual,Fifteenth Edition,2009。磺草唑胺之示範性用途包括以其作為除草劑，用於小麥、大麥與黑麥之闊葉雜草之出苗後控制，以及玉米之闊葉雜草之出苗前或後控制。
使用於此，平速爛為2-(2,2-二氟乙氧基)-N-(5,8-二甲氧基[1,2,4]三唑并[1,5-c]嘧啶-2-基)-6-(三氟甲基)苯磺醯胺，並具有下列結構：
其除草活性示範於The Pesticide Manual,Fifteenth Edition,2009。平速爛之示範性用途包括以其作為除草劑，用於稻米之稗屬、闊葉雜草與年生莎草科雜草，
以及高樑、草皮、穀類及樹與藤園之稗屬、闊葉雜草之出苗後控制。在另一範例中，平速爛係用於控制湖泊與池塘之水生雜草。
使用於此，啶磺草胺為N-(5,7-二甲氧基[1,2,4]三唑并[1,5-a]嘧啶-2-基)-2-甲氧基-4-(三氟甲基)-3-吡啶磺醯胺，並具有下列結構：
其除草活性示範於The Pesticide Manual,Fifteenth Edition,2009。啶磺草胺之示範性用途包括以其作為除草劑，用於穀類之年生草與闊葉雜草之大範圍出苗後控制。
使用於此，除草劑意指可撲滅、控制或其他不利地改變植物生長之化合物，例如，活性成分。
使用於此，除草有效或植被控制量為一定量之活性成分，其造成植被不利地改變，例如，引發其偏離自然發展、撲殺、影響其調節、引發其乾燥、引發其發育遲緩，及其類似情形。
使用於此，控制不良植被意指防止、降低、撲殺，或其他不利地改變植物與植被之發育。本文描述了控制不良植被之方法，係透過某些除草劑結合物或組成物之應
用。應用方法包括但不限於，應用於植被或其部位，例如，應用於植被鄰近區域，以及出苗前、出苗後、葉面(散播、定向、帶狀、定點、機械式、躍頂式，或復育)，以及藉由手、背包、機械、牽引機，或空中(飛機和直升機)之應用方法，於水中(in-water)應用(挺水與沉水植被、散播、定點、機械式、水注式、粒狀散播、粒狀定點、振動篩瓶或噴流)。
使用於此，植物與植被包括但不侷限於，發芽種子、新興種苗、自無性繁殖體挺出之植物、未成熟植被，以及成熟植被。
使用於此，農業上可接受之鹽類與酯類，意指具有除草活性，或可於植物、水或土壤中轉換為所述除草劑之鹽類與酯類。示範性農業上可接受酯類為可或可能於如植物、水，或土壤中被水解、氧化、代謝，或以其他方式，轉換為相對應之羧酸者，其取決於pH值，可為解離與未解離形式。
示範性鹽類包括那些衍生自鹼金族或鹼土族金屬者，以及那些衍生自氨與胺者。示範性陽離子包括鈉、鉀、鎂，以及如下式之銨陽離子：R1R2R3R4N+其中R1、R2、R3與R4之每一者皆單獨地代表氫或C1-C12烷基、C3-C12烯基，或C3-C12炔基，其每一者皆任擇地經一或多個羥基、C1-C4烷氧基、C1-C4烷基硫代或苯基取代，其中R1、R2、R3與R4為空間上相容。此外，R1、R2、R3與R4之任兩者結合，可代表脂肪族雙官能基片段，其含有1至12個
碳原子，及至多2個氧或硫原子。其鹽類係藉由經金屬氫氧化物如氫氧化鈉；胺類如氨、三甲基胺、二乙醇胺、2-甲基硫代丙胺、二烯丙基胺、2-丁氧基乙基胺、嗎啉、環十二烷胺，或芐基胺；或氫氧化四烷銨如氫氧化四甲基銨或氫氧化膽鹼處理而製備。
示範性酯類包括衍生自C1-C12烷基、C3-C12烯基、C3-C12炔基或C7-C10經芳基取代之烷基醇類，如甲醇、異丙醇、1-丁醇、2-乙基己醇、丁氧基乙醇、甲氧基丙醇、烯丙基醇、炔丙醇、環己醇，或未經取代或經取代之苯甲醇類者。苯甲醇類可經1-3個取代基取代，該取代基單獨地選自於鹵素、C1-C4烷基或C1-C4烷氧基。酯類之製備，可藉由以乙醇耦合酸類，其中使用任何數量之適用活化試劑，如用於胜肽耦合者，如二環己基碳二亞胺(DCC)或羰基二咪唑(CDI)；於鹼基如三乙基胺或碳酸鋰存在下，以烷化試劑如烷基鹵化物類或烷基磺酸鹽類，與酸類反應；以適當醇類與酸類之相對應醯氯反應；於酸催化劑存在下，以適當醇類與相對應之酸反應；或藉由轉酯作用而達成。
本發明係提供除草組成物，其包含一除草有效量之(a)式(I)化合物
或其農業上可接受之鹽類或酯類，以及(b)三唑并嘧啶磺醯胺類。示範性三唑并嘧啶磺醯胺類包括但不侷限於，氯酯磺草胺-甲酯、雙氯磺草胺、雙氟磺草胺、唑嘧磺草胺、磺草唑胺、平速爛，以及啶磺草胺，或其農業上可接受之鹽類、羧酸、羧酸鹽或酯類。
本發明亦提供控制不良植被之方法，其包含以一除草有效量之(a)式(I)化合物或其農業上可接受鹽類或酯類，以及(b)三唑并嘧啶磺醯胺類接觸植被或其部位，亦即，鄰近植被之區域，或施加至土壤或水，以預防植被出苗或生長。在某些實施例中，該方法採用本文所述之組成物。
此外，在一些實施例中，化合物(I)或其農業上可接受之鹽類或酯類，與三唑并嘧啶磺醯胺類或其農業上可接受之鹽類或酯類之結合物，具有協同性，例如，相較於個別施加，除草活性成分之結合物較具功效。協同性定義為“二或多個因子之交互作用，使得相結合時之功效大於各因子個別施加之預期功效”。Senseman,S.,ed.Herbicide Handbook.9th ed.Lawrence：Weed Science Society of America,2007。在某些實施例中，組成物具有協同性，如科爾比方程式(Colby’s equation)所測定。Colby,S.R.1967.
Calculation of the synergistic and antagonistic response of herbicide combinations.Weeds 15：20-22。
在一些實施例中，式(I)化合物或其鹽類或酯類，及氯酯磺草胺-甲酯、雙氯磺草胺、雙氟磺草胺、唑嘧磺草胺、磺草唑胺、平速爛與啶磺草胺，或其農業上可接受之鹽類、羧酸、羧酸鹽或酯類，係配製於一組成物中，其於槽內混合，並同時施加，或依序施加。
將化合物直接施加至任何生長階段之植物或植物部位，以展現其除草活性。所產生之功效取決於欲控制之植物物種、植物之生長階段、稀釋之應用參數與噴霧液滴大小、固體成分之顆粒大小、使用時之環境條件、使用之特定化合物、使用之特定佐劑與載劑、土壤型態及其類似情況，以及化學物質施加量。這些與其他因子可被調整，以增進非選擇性與選擇性之除草作用。在一些實施例中，本文所述之組成物係以出苗後、出苗前，或水中方式施加至水灌稻田或水體(如池塘、湖泊與溪流)中相對未成熟之不良植被，以達到雜草之最大控制。
在一些實施例中，本文提供之組成物與方法係用於控制作物，其包括但不侷限於，經直播、湛水直播與插秧之稻米、穀類、小麥、大麥、燕麥、黑麥、高粱、玉蜀黍/玉米、甘蔗、向日葵、芸苔、油菜、甜菜、大豆、棉花、鳳梨、牧草、草地、牧場、休耕地、草皮、樹與藤園、種植作物、蔬菜、水生植物、工業植被管理(IVM)與道路維護(ROW)，之雜草。
在某些實施例中，本文提供之組成物與方法係用於控制稻米中之雜草。在某些實施例中，稻米為經直播、湛水直播，或插秧之稻米。
本文所述之組成物與方法可用於控制在具草甘膦-耐受性-、5-烯醇丙酮基莽草酸-3-磷酸鹽(EPSP)合成酶抑制劑-耐受性-、固殺草-耐受性-、麩胺醯胺酸合成酶抑制劑-耐受性-、麥草畏-耐受性-、苯氧基生長素-耐受性-、吡啶基氧基生長素-耐受性-、生長素-耐受性-、生長素運輸抑制劑-耐受性-、芳基氧基苯氧基丙酸酯-耐受性-、環己烷二酮-耐受性-、苯基吡唑啉-耐受性-、乙醯輔酶A羧化酶(ACCase)抑制劑-耐受性-、咪唑啉酮-耐受性-、磺醯基脲-耐受性-、嘧啶基硫代苯甲酸酯-耐受性-、二甲氧基嘧啶-耐受性-、三唑并嘧啶-耐受性-、磺醯基胺基羰基三唑酮-耐受性-、乙醯乳酸合成酶(ALS)或乙醯羥酸合成酶(AHAS)抑制劑-耐受性-、4-羥基苯基-丙酮酸二氧酶(HPPD)抑制劑-耐受性-、八氫番茄紅素去飽和酶抑制劑-耐受性-、類胡蘿蔔素生合成抑制劑-耐受性-、原紫質原氧化酶(PPO)抑制劑-耐受性-、纖維素生合成抑制劑-耐受性-、有絲分裂抑制劑-耐受性-、微管抑制劑-耐受性-、極長鏈脂肪酸抑制劑-耐受性-、脂肪酸與脂質生合成抑制劑-耐受性-、光合系統I抑制劑-耐受性-、光合系統II抑制劑-耐受性-、三嗪-耐受性-，以及溴苯腈-耐受性-作物(例如，但不侷限於，大豆、棉花、油菜/芸苔、稻米、穀類、玉蜀黍、高粱、向日葵、甜菜、甘蔗、草皮等)中之不良植被，舉例而言，結合於草甘膦、EPSP合成酶抑
制劑、固殺草、麩胺醯胺酸合成酶抑制劑、麥草畏、苯氧基生長素、吡啶基氧基生長素、合成生長素、生長素運輸抑制劑、芳基氧基苯氧基丙酸酯、環己烷二酮、苯基吡唑啉、ACCase抑制劑、咪唑啉酮、磺醯基脲、嘧啶基硫代苯甲酸酯、二甲氧基嘧啶類、三唑并嘧啶類、磺醯基胺基羰基三唑酮、ALS或AHAS抑制劑、HPPD抑制劑、八氫番茄紅素去飽和酶抑制劑、類胡蘿蔔素生合成抑制劑、PPO抑制劑、纖維素生合成抑制劑、有絲分裂抑制劑、微管抑制劑、極長鏈脂肪酸抑制劑、脂肪酸與脂質生合成抑制劑、光合系統I抑制劑、光合系統II抑制劑、三嗪，以及溴苯腈。組成物與方法可用於控制具有多個或複合性狀之作物之不良植被，其對於多重作用模式之多種化學物質及/或抑制劑具有耐受性。在一些實施例中，式(I)化合物或其鹽類或酯類，以及補充用除草劑或其鹽類或酯類，係結合除草劑使用，該除草劑對於欲處理之作物具有選擇性，且其輔助了這些化合物以特定之施加率對於雜草之控制。在一些實施例中，本文所述之組成物與其他補充用除草劑係同時施加，無論是結合物配方、槽混合物或依序進行。
組成物與方法可用於控制在具有農藝壓力耐受性(包括但不侷限於，乾旱、嚴寒、燥熱、鹽、水、養分、肥沃度、pH值)、病蟲害耐受性(包括但不侷限於，昆蟲、真菌與病原體)，與作物改良性狀(包括但不侷限於，產量；蛋白質、醣類，或油含量；蛋白質、醣類，或油組成物；植物高度及植物架構)之作物中之不良植被。
本發明提供之組成物與方法可用於控制不良植被。不良植被包括但不侷限於，在稻米、穀類、小麥、大麥、燕麥、黑麥、高粱、玉蜀黍/玉米、甘蔗、向日葵、芸苔、油菜、甜菜、大豆、棉花、鳳梨、牧草、草地、牧場、休耕地、草皮、樹與藤園、水生植物、種植作物、蔬菜、工業植被管理(IVM)與道路維護(ROW)中所出現之不良植被。
在一些實施例中，本發明提供之方法係用於控制稻米中之不良植被。在某些實施例中，該不良植被為寬葉臂形草(Brachiaria platyphylla(Groseb.)Nash)或扁葉尾稃草(Urochloa platyphylla(Nash)R.D.Webster)(闊葉信號草，BRAPP)、馬唐(Digitaria sanguinalis(L.)Scop.)(大馬唐草，DIGSA)、稗屬物種(Echinochloa species)(ECHSS)、稗(Echinochloa crus-galli(L.)P.Beauv.)(稗草，ECHCG)、無芒稗(Echinochloa crus-pavonis(Kunth)Schult.)(海灣稗，ECHCV)、光頭稗(Echinochloa colonum(L.)LINK)(芒稷ECHCO)、水田稗(Echinochloa oryzoides(Ard.)Fritsch)(早水草，ECHOR)、水稗(Echinochloa oryzicola(Vasinger)Vasinger)(晚水草，ECHPH)、稻稗(Echinochloa phyllopogon(Stapf)Koso-Pol.)(稻米稗草，ECHPH)、多穗稗(Echinochloa polystachya(Kunth)Hitchc.)(匍匐河邊草，ECHPO)、田間鴨嘴草(Ischaemum rugosum Salisb.)(鴨嘴草，ISCRU)、千金子(Leptochloa chinensis(L.)Nees)(油麻，LEFCH)、團穗千金子(Leptochloa fascicularis(Lam.)Gray)(叢生千金子，
LEFFA)、類黍千金子(Leptochloa panicoides(Presl.)Hitchc.)(亞馬遜千金子，LEFPA)、稻屬(Oryza)物種(雜草稻，ORYSS)、洋野黍(Panicum dichotomiflorum(L.)Michx.)(秋黍子PANDI)、毛花雀稗(Paspalum dilatatum Poir.)(雀稗草，PASDI)、羅氏草(Rottboellia cochinchinensis(Lour.)W.D.Clayton)(羅氏草，ROOEX)、莎草屬(Cyperus)物種(CYPSS)、異花莎草(Cyperus difformis L.)(莎草，CYPDI)、假刺莎草(Cyperus dubius Rottb.)(MAPDU)、油莎草(Cyperus esculentus L.)(黃莎草，CYPES)、碎米莎草(Cyperus iria L.)(米莎草，CYPIR)、香附子(Cyperus rotundus L.)(紫莎草，CYPRO)、水莎草(Cyperus serotinus Rottb./C.B.Clarke)(汐澤莎草，CYPSE)、荸薺屬(Eleocharis)物種(ELOSS)、水虱草(Fimbristylis miliacea(L.)Vahl)(水虱草，FIMMI)、擬莞屬(Schoenoplectus)物種(SCPSS)、大井氏水莞(Schoenoplectus juncoides Roxb.)(日本蘆葦，SCPJU)、宜蘭莞草(Bolboschoenus maritimus(L.)Palla或海荊三稜(Schoenoplectus maritimus L.Lye))(田蒜仔，SCPMA)、水毛花(Schoenoplectus mucronatus L.)(稻田蘆葦，SCPMU)、合萌屬(Aeschynomene)物種(合萌，AESSS)、空心蓮子草(Alternanthera philoxeroides(Mart.)Griseb.)(空心蓮子草，ALRPH)、澤瀉(Alisma plantago-aquatica L.)(澤瀉，ALSPA)、莧屬(Amaranthus)物種(藜與莧，AMASS)、長葉水莧菜(Ammannia coccinea Rottb.)(紅莖，AMMCO)、圓葉鴨跖草(Commelina benghalensis L.)(飯包草，
COMBE)、旱蓮草(Eclipta alba(L.)Hassk.)(美國假菊，ECLAL)、沼生異蕊花(Heteranthera limosa(SW.)Willd./Vahl)(鴨沙拉，HETLI)、腎形異蕊花(Heteranthera reniformis R.& P.)(圓葉異芯花屬，HETRE)、牽牛花屬(Ipomoea)物種(牽牛花，IPOSS)、碗仔花(Ipomoea hederacea(L.)Jacq.)(牽牛花，IPOHE)、美洲母草(Lindernia dubia(L.)Pennell)(低等泥花草，LIDDU)、水丁香屬(Luawigia)物種(LUDSS)、細葉水丁香(Ludwigia linifolia Poir.)(東南毛草龍，LUDLI)、水丁香(Ludwigia octovalvis(Jacq.)Raven)(長果實毛草龍，LUDOC)、雨久花(Monochoria korsakowii Regel & Maack)(鴨舌草屬，MOOKA)、鴨舌草(Monchoria vaginalis(Burm.F.)C.Presl ex Kuhth)(鴨舌草屬，MOOVA)、裸花水竹葉(Murdannia nudiflora(L.)Brenan)(細竹草，MUDNU)、賓州蓼(Polygonum pensylvanicum L.)(賓州蓼，POLPY)、春蓼(Polygonum persicaria L.)(春蓼，POLPE)、水蓼(Polygonum hydropiperoides Michx.)(軟蓼，POLHP)、印度小圓葉(Rotala indica(Willd.)Koehne)(印度水豬母乳，ROTIN)、慈姑屬(Sagittaria)物種(慈姑，SAGSS)、田菁(Sesbania exaltata(Raf.)Cory/Rydb.Ex Hill)(麻田菁，SEBEX)，或尖瓣花(Sphenoclea zeylanica Gaertn.)(鵝草，SPDZE)。
在一些實施例中，本發明提供之方法係用於控制穀類中之不良植被。在某些實施例中，該不良植被為大穗看麥娘(Alopecurus myosuroides Huds.)(黑草，ALOMY)、阿
披拉草(Apera spica-venti(L.)Beauv.)(知風草，APESV)、野燕麥(Avena fatua L.)(野燕麥，AVEFA)、旱雀麥(Bromus tectorum L.)(旱雀麥，BROTE)、義大利黑麥草(Lolium multiflorum Lam.)(義大利黑麥草，LOLMU)、小加拿麗鷸草(Phalaris minor Retz.)(小種子金絲雀草，PHAMI)、早熟禾(Poa annua L.)(年生蘭草，POANN)、金色狗尾草(Setaria pumila(Poir.)Roemer & J.A.Schultes)(金狗尾草，SETLU)、狗尾草(Setaria viridis(L.)Beauv.)(狗尾草，SETVI)、反枝莧(Amaranthus retroflexus L.)(反枝莧，AMARE)、芸苔屬(Brassica)物種(BRSSS)、紅心藜(Chenopodium album L.)(藜草，CHEAL)、絲路薊(Cirsium arvense(L.)Scop.)(加拿大薊，CIRAR)、拉拉藤(Galium aparine L.)(八仙草，GALAP)、毛地膚(Kochia scoparia(L.)Schrad.)(地膚屬，KCHSC)、圓齒野芝麻(Lamium purpureum L.)(紫色野蕁麻，LAMPU)、德國洋甘菊(Matricaria recutita L.)(野生甘菊，MATCH)、同花母菊(Matricaria matricarioides(Less.)Porter)(鳳梨草，MATMT)、罌粟花(Papaver rhoeas L.)(罌粟，PAPRH)、卷莖蓼(Polygonum convolvulus L.)(野蕎麥，POLCO)、刺沙蓬(Salsola tragus L.)(俄羅斯薊，SASKR)、歐白芥屬(Sinapis)物種(SINSS)、野芥(Sinapis arvensis L.)(野生芥菜，SINAR)、賽繁縷(Stellaria media(L.)Vill.)(繁縷，STEME)、阿拉伯婆婆納(Veronica persica Poir.)(波斯婆婆納，VERPE)、野生堇菜(Viola arvensis Murr.)(野生堇，VIOAR)，或三色堇(Viola tricolor L.)(野生堇，VIOTR)。
在一些實施例中，本發明提供之方法係用於控制牧野、休耕地、IVM與ROW中之不良植被。在某些實施例中，該不良植被為猪草(Ambrosia artemisiifolia L.)(豚草，AMBEL)、決明(Cassia obtusifolia)(決明，CASOB)、斑點矢車菊(Centaurea maculosa auct.non Lam.)(斑點矢車菊，CENMA)、絲路薊(加拿大薊，CIRAR)、田旋花(Convolvulus arvensis L.)(野生旋花，CONAR)、胡蘿蔔(Daucus carota L.)(野生蘿蔔，DAUCA)、乳漿大戟(Euphorbia esula L.)(乳漿大戟，EPHES)、刺萵苣(Lactuca serriola L./Torn.)(萵苣，LACSE)、長葉車前草(Plantago lanceolata L.)(長葉車前草，PLALA)、大羊蹄(Rumex obtusifolius L.)(闊葉羊蹄，RUMOB)、刺金午時花(Sida spinosa L.)(刺黃花稔，SIDSP)、野芥(Sinapis arvensis L.)(野生芥菜，SINAR)、苦苣菜(Sonchus arvensis L.)(多年生苦菜，SONAR)、一枝黃花屬(Solidago)物種(一枝黃花，SOOSS)、西洋蒲公英(Taraxacum officinale G.H.Weber ex Wiggers)(蒲公英，TAROF)、白三葉草(Trifolium repens L.)(白三葉，TRFRE)，或大蕁麻(Urtica dioica L.)(蕁麻，URTDI)。
在一些實施例中，本發明提供之方法係用於控制行栽作物、樹與藤作物與多年生作物中所出現之不良植被。在某些實施例中，該不良植被為大穗看麥娘(黑草，ALOMY)、野燕麥(野燕麥，AVEFA)、俯仰臂形草(Brachiaria decumbens Stapf.)，或伏莖尾稃草(Urochloa decumbens
(Stapf)R.D.Webster)(蘇里南草，BRADC)、珊狀臂形草(Brachiaria brizantha(Hochst.ex A.Rich.)Stapf.)，或珊狀尾稃草(Urochloa brizantha(Hochst.ex A.Rich.)R.D.)(鬍子草，BRABR)、寬葉臂形草或扁葉尾稃草(闊葉信號草，BRAPP)、車前臂形草(Brachiaria plantaginea(Link)Hitchc.)，或車前尾稃草(Urochloa plantaginea(Link)R.D.Webster)(車前臂形草，BRAPL)、蒺藜草(Cenchrus echinatus L.)(蒺藜草，CENEC)、平枝馬唐(Digitaria horizontalis Willd.)(牙買加馬唐，DIGHO)、台灣馬唐(Digitaria insularis(L.)Mez ex Ekman)(酢漿草，TRCIN)、馬唐(大馬唐草，DIGSA)、稗(稗草，ECHCG)、光頭稗(芒稷ECHCO)、牛筋草(Eleusine indica(L.)Gaertn.)(牛筋草，ELEIN)、義大利黑麥草(義大利黑麥草，LOLMU)、洋野黍(秋黍子PANDI)、稷(Panicum miliaceum L.)(野生小米黍子，PANMI)、法氏狗尾草(Setaria faberi Herrm.)(大狗尾草，SETFA)、狗尾草(狗尾草，SETVI)、詹森草(Sorghum halepense(L.)Pers.)(詹森草，SORHA)、蜀黍(Sorghum bicolor(L.)Moench ssp.Arundinaceum)(野生甘蔗，SORVU)、油莎草(黃莎草，CYPES)、香附子(紫莎草，CYPRO)、苘麻(Abutilon theophrasti Medik.)(絨毛葉，ABUTH)、莧屬物種(藜與莧，AMASS)、猪草(豚草，AMBEL)、裸穗猪草(Ambrosia psilostachya DC.)(西部豚草，AMBPS)、三裂葉猪草(Ambrosia trifida L.)(大豚草，AMBTR)、冠萼蔓錦葵(Anoda cristata(L.)Schlecht.)(馬刺蔓錦葵，ANVCR)、敘利亞馬利
筋(Asclepias syriaca L.)(乳草，ASCSY)、大花咸豐草(Bidens pilosa L.)(咸豐草，BIDPI)、豐花草屬(Borreria)物種(BOISS)、翼豐花草(Borreria alata(Aubl.)DC.)或翼鴨舌黃舅(Spermacoce alata Aubl.)(闊葉鈕釦草，BOILF)、闊葉鴨舌黃舅(Spermacose latifolia)(闊葉鈕釦草，BOILF)、紅心藜(藜草，CHEAL)、絲路薊(加拿大薊，CIRAR)、圓葉鴨跖草(飯包草，COMBE)、曼陀羅(Datura stramonium L.)(曼陀羅，DATST)、胡蘿蔔(Daucus carota L.)(野生蘿蔔，DAUCA)、白苞猩猩草(Euphorbia heterophylla L.)(野生一品紅，EPHHL)、大飛揚草(Euphorbia hirta L.)或飛揚草(Chamaesyce hirta(L.)Millsp.)(花園大戟，EPHHI)、齒裂大戟(Euphorbia dentata Michx.)(鋸齒大戟，EPHDE)、美洲假蓬(Erigeron bonariensis L.)或美洲假蓬(Conyza bonariensis(L.)Cronq.)(美洲假蓬，ERIBO)、加拿大蓬(Erigeron canadensis L.)或加拿大蓬(Conyza canadensis(L.)Cronq.)(加拿大蓬，ERICA)、野茼蒿(Conyza sumatrensis(Retz.)E.H.Walker)(長蓬，ERIFL)、向日葵(Helianthus annuus L.)(向日葵，HELAN)、長梗毛娥房藤(Jacquemontia tamnifolia(L.)Griseb.)(牽牛花，IAQTA)、碗仔花(牽牛花，IPOHE)、白星薯(Ipomoea lacunosa L.)(白牽牛，IPOLA)、刺萵苣(萵苣，LACSE)、馬齒莧(Portulaca oleracea L.)(馬齒莧，POROL)、擬鴨舌黃屬(Richardia)物種(馬齒莧，RCHSS)、金午時花屬(Sida)物種(金午時花，SIDSS)、刺金午時花(刺黃花稔，SIDSP)、野芥(野生芥菜，SINAR)、美
東龍葵(Solanum ptychanthum Dunal)(美東龍葵，SOLPT)、長柄菊(Tridax procumbens L.)(衣扣菊，TRQPR)，或羊帶來(Xanthium strumarium L.)(羊帶來，XANST)。
在一些實施例中，本發明提供之方法係用於控制草皮中之不良植被。在某些實施例中，該不良植被為雛菊(Bellis perennis L.)(英國菊，BELPE)、油莎草(黃莎草，CYPES)、莎草屬物種(CYPSS)、馬唐(大馬唐草，DIGSA)、維州鈕釦草(Diodia virginiana L.)(維州鈕釦草，DIQVI)、大戟屬(Euphorbia)物種(大戟，EPHSS)、金錢薄荷(Glechoma hederacea L.)(地藤，GLEHE)、銅錢草(Hydrocotyle umbellata L.)(錢草，HYDUM)、水蜈蚣屬(Kyllinga)物種(水蜈蚣，KYLSS)、寶蓋草(Lamium amplexicaule L.)(寶蓋草，LAMAM)、裸花水竹葉(細竹草，MUDNU)、酢漿草屬(Oxalis)物種(酢漿草，OXASS)、大車前(Plantago major L.)(闊葉車前，PLAMA)、長葉車前草(Plantago lanceolata L.)(鹿角/窄葉車前，PLALA)、真珠草(Phyllanthus urinaria L.)(葉下珠，PYLTE)、大羊蹄(闊葉羊蹄，RUMOB)、佛州水蘇(Stachys floridana Shuttlew.)(佛州水蘇，STAFL)、賽繁縷(繁縷，STEME)、西洋蒲公英(蒲公英，TAROF)、白三葉草(白三葉，TRFRE)，或堇菜屬(野生堇，VIOSS)。
在一些實施例中，本發明提供之組成物與方法係用於控制由禾草科、闊葉與莎草科雜草組成之不良植被。在某些實施例中，本發明提供之組成物與方法係用於控制包括臂形草屬、母菊屬、薊屬、莎草屬、馬唐屬、稗屬、
飄拂草屬、鴨嘴草屬、牽牛花屬、野芝麻屬、千金子屬、母菊屬(Matricaria)、豬毛菜屬、擬莞屬(Schoenoplectus)、婆婆納屬與堇菜屬之不良植被。
在一些實施例中，化合物(I)或其農業上可接受之酯類或鹽類，及氯酯磺草胺-甲酯、雙氯磺草胺、雙氟磺草胺、磺草唑胺、平速爛與啶磺草胺，或其農業上可接受之鹽類或酯類之結合物，係用於控制寬葉臂形草或扁葉尾稃草(闊葉信號草，BRAPP)、臭甘菊(Chamomilla chamomilla(L.)Rydb.)(臭甘菊，MATCH)、異花莎草(莎草，CYPDI)、油莎草(黃莎草，CYPES)、絲路薊(加拿大薊，CIRAR)、碎米莎草(米莎草，CYPIR)、馬唐(大馬唐草，DIGSA)、稗(稗草，ECHCG)、稗屬(ECHSS)、水虱草(水虱草，FIMMI)、碗仔花(牽牛花，IPOHE)、田間鴨嘴草(鴨嘴草，ISCRU)、圓齒野芝麻(紫色野蕁麻，LAMPU)、千金子(油麻，LEFCH)、類黍千金子(亞馬遜千金子，LEFPA)、俄羅斯薊(Salsola iberica(L.))(俄羅斯薊，SASKR)、大井氏水莞(日本蘆葦，SCPJU)、阿拉伯婆婆納(Veronica persica Poir.)(波斯婆婆納，VERPE)與三色堇(Viola tricolor L.)(野生堇，VIOTR)。
式(I)化合物或其農業上可接受鹽類或酯類，可用於控制具除草劑抗性或耐受性之雜草。使用式(I)化合物或其農業上可接受鹽類或酯類之結合物，及本文所述之組成物之方法，亦可用於控制具除草劑抗性或耐受性之雜草。示範性之具抗性或耐受性雜草包括但不侷限於，乙醯乳酸
合成酶(ALS)或乙醯羥酸合成酶(AHAS)抑制劑(例如，咪唑啉酮類、磺醯基脲類、嘧啶基硫代苯甲酸酯類、三唑并嘧啶類、磺醯基胺基羰基三唑酮類)、光合系統II抑制劑(例如，苯基胺甲酸酯類、噠嗪酮類(pyridazinones)、三嗪類、三嗪酮類、尿嘧啶類、醯胺類、尿素類、苯并噻二嗪酮類、腈類、苯基噠嗪類)、乙醯輔酶A羧化酶(ACCase)抑制劑(例如，芳基氧基苯氧基丙酸酯類、環己烷二酮類、苯基吡唑啉類)、合成生長素(例如，苯甲酸類、苯氧基羧酸類、吡啶羧酸類、喹啉羧酸類)、生長素運輸抑制劑(例如，鄰苯二甲酸酯類(phthalamates)、縮胺脲)、光合系統I抑制劑(例如，聯吡啶類)、5-烯醇丙酮基莽草酸-3-磷酸鹽(EPSP)合成酶抑制劑(例如，草甘膦)、麩胺醯胺酸合成酶抑制劑(例如，固殺草、雙丙胺膦(bialafos))、微管組合抑制劑(例如，苯甲醯胺類、苯甲酸、二硝基苯胺類、磷醯胺酯類、吡啶類)、有絲分裂抑制劑(例如，胺基甲酸酯類)、極長鏈脂肪酸(VLCFA)抑制劑(例如，乙醯胺類、氯乙醯胺類、氧基乙醯胺類、四唑啉酮類)、脂肪酸與脂質合成抑制劑(例如，二硫代磷酸酯類、硫代胺基甲酸酯類、苯并呋喃類、氯碳酸類)、原紫質原氧化酶(PPO)抑制劑(例如，二苯基醚類、N-苯酞醯亞胺類、噁二唑類、噁唑啶二酮、苯基吡唑類、嘧啶二酮類、噻二唑類、三唑酮類)、類胡蘿蔔素生合成抑制劑(例如，可滅蹤(clomazone)、殺草強(amitrole)、苯草醚(aclonifen))、八氫番茄紅素去飽和酶(PDS)抑制劑(例如，醯胺類、甲醯苯胺(anilidex)、呋喃酮類、苯基丁醯胺類、噠嗪酮類、吡
啶類)、4-羥基苯基-丙酮酸二氧酶(HPPD)抑制劑(例如，紅千層酮類(callistemones)、異噁唑類、吡唑類、三酮類)、纖維素生合成抑制劑(例如，腈類、苯甲醯胺類、快克草、三唑并甲醯胺類)、具多重作用模式之除草劑如快克草，以及未經分類之除草劑如芳基胺基丙酸類、野燕枯、草多索與具有機砷類抗性或耐受性之生物型。示範性之具抗性或耐受性雜草包括但不侷限於，具多種除草劑抗性或耐受性之生物型、具多種化合物類別抗性或耐受性之生物型、具多重除草劑作用模式抗性或耐受性之生物型，以及具多重抗性或耐受性機制之生物型(例如，標的位置抗性或代謝抗性)。
在本文所述組成物與方法之某些實施例中，式(I)化合物或其鹽類或酯類係結合氯酯磺草胺-甲酯或其鹽類、羧酸、羧酸鹽，或酯類使用。關於組成物，在一些實施例中，式(I)化合物或其鹽類或酯類與氯酯磺草胺-甲酯或其鹽類、羧酸、羧酸鹽或酯類之重量比，係介於約1：31至約137：1之範圍內。在某些實施例中，式(I)化合物或其鹽類或酯類與氯酯磺草胺-甲酯或其鹽類、羧酸、羧酸鹽或酯類之重量比，係介於約1：2至約10：1之範圍內。在特殊實施例中，式(I)化合物或其鹽類或酯類與氯酯磺草胺-甲酯或其鹽類、羧酸、羧酸鹽或酯類之重量比，係介於約1：8至約15：1之範圍內。在某些實施例中，式(I)化合物或其鹽類或酯類與氯酯磺草胺-甲酯或其鹽類、羧酸、羧酸鹽或酯類之重量比，係介於約1：4至約22：1之範圍內。在某些實施例中，式(I)化合物或其鹽類或酯類與氯酯磺草胺-甲酯或其鹽類、羧
酸、羧酸鹽或酯類之重量比，係介於約1：2至約11：1之範圍內。在某些實施例中，本發明提供之組成物包含式(I)化合物或其芐基酯與氯酯磺草胺-甲酯。在一實施例中，組成物包含式(I)化合物與氯酯磺草胺-甲酯，其中式(I)化合物與氯酯磺草胺-甲酯之重量比為約1：1.7至約11：1。在一實施例中，組成物包含式(I)化合物之芐基酯與氯酯磺草胺-甲酯，其中式(I)化合物之芐基酯與氯酯磺草胺-甲酯之重量比，為約1：2至約4：1。在一實施例中，組成物包含式(I)化合物之芐基酯與氯酯磺草胺-甲酯，其中式(I)化合物之芐基酯與氯酯磺草胺-甲酯之重量比，為約1：2至約4：1。在一特殊實施例中，組成物包含式(I)化合物之芐基酯與氯酯磺草胺-甲酯，其中式(I)化合物之芐基酯與氯酯磺草胺-甲酯之重量比，為約1：8至約15：1。關於方法，在某些實施例中，該方法包含以本文所述之組成物接觸不良植被或其部位，或施加至土壤或水，以預防植被出苗或生長。在一些實施例中，依據活性成分於組成物中之總量，組成物以約每公頃4克活性成分(gai/ha)至約362 gai/ha之施加率施加。在某些實施例中，依據活性成分於組成物中之總量，組成物以約6 gai/ha至約40 gai/ha之施加率施加。在特殊實施例中，依據活性成分於組成物中之總量，組成物以約6 gai/ha至約67 gai/ha之施加率施加。在一些實施例中，該方法包含以式(I)化合物或其鹽類或酯類，與氯酯磺草胺-甲酯或其鹽類、羧酸、羧酸鹽或酯類，例如，依序地或同時地，接觸不良植被或其部位，或施加至土壤或水，以預防植被出苗或生長。在一些
實施例中，氯酯磺草胺-甲酯或其鹽類、羧酸、羧酸鹽或酯類之施加率為約2.2 gai/ha至約62 gai/ha，且式(I)化合物或其鹽類或酯類之施加率為約每公頃2克酸當量(gae/ha)至約300 gae/ha。在一些實施例中，氯酯磺草胺-甲酯或其鹽類、羧酸、羧酸鹽或酯類之施加率為約1 gai/ha至約16 gai/ha，且式(I)化合物或其鹽類或酯類之施加率為約每公頃2 g酸當量(gae/ha)至約45 gae/ha。在一些實施例中，氯酯磺草胺-甲酯或其鹽類、羧酸、羧酸鹽或酯類之施加率為約2.19 gai/ha至約8.75 gai/ha，且式(I)化合物或其鹽類或酯類之施加率為約每公頃4.38 g酸當量(gae/ha)至約21.2 gae/ha。在一些實施例中，氯酯磺草胺-甲酯或其鹽類、羧酸、羧酸鹽或酯類之施加率為約2.19 gai/ha至約35 gai/ha，且式(I)化合物或其鹽類或酯類之施加率為約每公頃4.38 g酸當量(gae/ha)至約32 gae/ha。在某些實施例中，該方法使用式(I)化合物或其芐基酯與氯酯磺草胺-甲酯。在一實施例中，該方法使用式(I)化合物與氯酯磺草胺-甲酯，其中式(I)化合物之施加率為約每公頃5.3 g酸當量(gae/ha)至約21.2 gae/ha，且氯酯磺草胺-甲酯之施加率為約2.19 gai/ha至約8.75 gai/ha。在一實施例中，該方法使用式(I)化合物與氯酯磺草胺-甲酯，其中式(I)化合物之施加率為約每公頃4.38 g酸當量(gae/ha)至約32 gae/ha，且氯酯磺草胺-甲酯之施加率為約2.19 gai/ha至約35 gai/ha。在一實施例中，該方法使用式(I)化合物之芐基酯與氯酯磺草胺-甲酯，其中式(I)化合物之芐基酯之施加率為約每公頃4.38 g酸當量(gae/ha)至約17.5 gae/ha，且氯
酯磺草胺-甲酯之施加率為約2.19 gai/ha至約8.75 gai/ha。在一實施例中，該方法使用式(I)化合物之芐基酯與氯酯磺草胺-甲酯，其中式(I)化合物之芐基酯之施加率為約每公頃4.38 g酸當量(gae/ha)至約32 gae/ha，且氯酯磺草胺-甲酯之施加率為約2.19 gai/ha至約35 gai/ha。在某些實施例中，該方法與組成物以式(I)化合物或其鹽類或酯類，結合氯酯磺草胺-甲酯或其鹽類、羧酸、羧酸鹽，或酯類，用於控制CYPDI、CYPIR、DIGSA、ECHCG、FIMMI或LEFCH。
在本文所述組成物與方法之某些實施例中，式(I)化合物或其鹽類或酯類係結合雙氯磺草胺或其鹽類使用。關於組成物，在一些實施例中，式(I)化合物或其鹽類或酯類與雙氯磺草胺或其鹽類之重量比，係介於約1：26至約26：1之範圍內。在某些實施例中，式(I)化合物或其鹽類或酯類與雙氯磺草胺或其鹽類之重量比，係介於約1：3至約2.6：1之範圍內。在某些實施例中，式(I)化合物或其鹽類或酯類與雙氯磺草胺或其鹽類之重量比，係介於約1：3至約6：1之範圍內。在某些實施例中，式(I)化合物或其鹽類或酯類與雙氯磺草胺或其鹽類之重量比，係介於約1：1.5至約3：1之範圍內。在某些實施例中，本發明提供之組成物包含式(I)化合物或其芐基酯與雙氯磺草胺。在一實施例中，組成物包含式(I)化合物與雙氯磺草胺，其中式(I)化合物與雙氯磺草胺之重量比為約1：1.5至約3：1。在一實施例中，組成物包含式(I)化合物之芐基酯與雙氯磺草胺，其中式(I)化合物之芐基酯與雙氯磺草胺之重量比，為約1.3：1至約3：1。關於
方法，在某些實施例中，該方法包含以本文所述之組成物接觸不良植被或其部位，或施加至土壤或水，以預防植被出苗或生長。在一些實施例中，依據活性成分於組成物中之總量，組成物以約每公頃9克活性成分(gai/ha)至約353 gai/ha之施加率施加。在某些實施例中，依據活性成分於組成物中之總量，組成物以約10 gai/ha至約40 gai/ha之施加率施加。在一些實施例中，該方法包含以式(I)化合物或其鹽類或酯類與雙氯磺草胺或其鹽類，例如，依序地或同時地，接觸不良植被或其部位，或施加至土壤或水，以預防植被出苗或生長。在一些實施例中，雙氯磺草胺或其鹽類之施加率為約6.6 gai/ha至約53 gai/ha，且式(I)化合物或其鹽類或酯類之施加率為約每公頃2克酸當量(gae/ha)至約300 gae/ha。在一些實施例中，雙氯磺草胺或其鹽類之施加率為約3 gai/ha至約26 gai/ha，且式(I)化合物或其鹽類或酯類之施加率為約每公頃2 g酸當量(gae/ha)至約35 gae/ha。在一些實施例中，雙氯磺草胺或其鹽類之施加率為約6.62 gai/ha至約13.25 gai/ha，且式(I)化合物或其鹽類或酯類之施加率為約每公頃4.38 g酸當量(gae/ha)至約17.5 gae/ha。在某些實施例中，該方法使用式(I)化合物或其芐基酯與雙氯磺草胺。在一實施例中，該方法使用式(I)化合物與雙氯磺草胺，其中式(I)化合物之施加率為約每公頃4.38 g酸當量(gae/ha)至約17.5 gae/ha，且雙氯磺草胺之施加率為約6.6 gai/ha至約13.2 gai/ha。在一實施例中，該方法使用式(I)化合物之芐基酯與雙氯磺草胺，其中式(I)化合物之芐基酯之施加率為約
每公頃17.5 g酸當量(gae/ha)，且雙氯磺草胺之施加率為約6.6 gai/ha至約13.2 gai/ha。在某些實施例中，該方法與組成物以式(I)化合物或其鹽類或酯類結合雙氯磺草胺或其鹽類，用於控制CYPRO、ECHCG或LEFCH。
在本文所述組成物與方法之某些實施例中，式(I)化合物或其鹽類或酯類係結合雙氟磺草胺或其鹽類使用。關於組成物，在一些實施例中，式(I)化合物或其鹽類或酯類與雙氟磺草胺或其鹽類之重量比，係介於約1：5至約300：1之範圍內。在某些實施例中，式(I)化合物或其鹽類或酯類與雙氟磺草胺或其鹽類之重量比，係介於約1.5：1至約4：1之範圍內。在某些實施例中，式(I)化合物或其鹽類或酯類與雙氟磺草胺或其鹽類之重量比，係介於約1：1.5至約14：1之範圍內。在某些實施例中，式(I)化合物或其鹽類或酯類與雙氟磺草胺或其鹽類之重量比，係介於約1：0.75至約7：1之範圍內。在某些實施例中，本發明提供之組成物包含式(I)化合物或其芐基酯與雙氟磺草胺。在一實施例中，組成物包含式(I)化合物之芐基酯與雙氟磺草胺，其中式(I)化合物之芐基酯與雙氟磺草胺之重量比為約1：0.75至約7：1。關於方法，在某些實施例中，該方法包含以本文所述之組成物接觸不良植被或其部位，或施加至土壤或水，以預防植被出苗或生長。在一些實施例中，依據活性成分於組成物中之總量，組成物以約每公頃3克活性成分(gai/ha)至約310 gai/ha之施加率施加。在某些實施例中，依據活性成分於組成物中之總量，組成物以約6 gai/ha至約15 gai/ha之施加率
施加。在一些實施例中，該方法包含以式(I)化合物或其鹽類或酯類與雙氟磺草胺或其鹽類，例如，依序地或同時地，接觸不良植被或其部位，或施加至土壤或水，以預防植被出苗或生長。在一些實施例中，雙氟磺草胺或其鹽類之施加率為約1.0 gai/ha至約10 gai/ha，且式(I)化合物或其鹽類或酯類之施加率為約每公頃2克酸當量(gae/ha)至約300 gae/ha。在一些實施例中，雙氟磺草胺或其鹽類之施加率為約0.62 gai/ha至約8 gai/ha，且式(I)化合物或其鹽類或酯類之施加率為約每公頃2.5 g酸當量(gae/ha)至約18 gae/ha。在一些實施例中，雙氟磺草胺或其鹽類之施加率為約1.25 gai/ha至約3.75 gai/ha，且式(I)化合物或其鹽類或酯類之施加率為約每公頃5 g酸當量(gae/ha)至約8.75 gae/ha。在某些實施例中，該方法使用式(I)化合物或其芐基酯與雙氟磺草胺。在一實施例中，該方法使用式(I)化合物之芐基酯與雙氟磺草胺，其中式(I)化合物之芐基酯之施加率為約5 g酸當量每公頃(gae/ha)至約8.75 gae/ha，且雙氟磺草胺之施加率為約1.25 gai/ha至約3.75 gai/ha。在某些實施例中，該方法與組成物以式(I)化合物或其鹽類或酯類結合雙氟磺草胺或其鹽類，用於控制CIRAR、LAMPU、MATCH、SASKR、VERPE或VIOTR。
在本文所述組成物與方法之某些實施例中，式(I)化合物或其鹽類或酯類係結合唑嘧磺草胺或其鹽類使用。關於組成物，在一些實施例中，式(I)化合物或其鹽類或酯類與唑嘧磺草胺或其鹽類之重量比，係介於約1：40至約
272：1之範圍內。在某些實施例中，式(I)化合物或其鹽類或酯類與唑嘧磺草胺或其鹽類之重量比，係介於約1：32至約45：1之範圍內。在特殊實施例中，式(I)化合物或其鹽類或酯類與唑嘧磺草胺或其鹽類之重量比，係介於約1：3至約5：1之範圍內。在某些實施例中，該組成物包含式(I)化合物或其芐基或正丁基酯類與唑嘧磺草胺或其鹽類。關於方法，在某些實施例中，該方法包含以本文所述之組成物接觸不良植被或其部位，或施加至土壤或水，以預防植被出苗或生長。在一些實施例中，依據活性成分於組成物中之總量，組成物以約每公頃3克活性成分(gai/ha)至約380 gai/ha之施加率施加。在某些實施例中，依據活性成分於組成物中之總量，組成物以約4 gai/ha至約120 gai/ha之施加率施加。在特殊實施例中，依據活性成分於組成物中之總量，組成物以約14 gai/ha至約57 gai/ha之施加率施加。在一些實施例中，該方法包含以式(I)化合物或其鹽類或酯類與唑嘧磺草胺或其鹽類，例如，依序地或同時地，接觸不良植被或其部位，或施加至土壤或水，以預防植被出苗或生長。在一些實施例中，唑嘧磺草胺或其鹽類之施加率為約1.1 gai/ha至約80 gai/ha，且式(I)化合物或其鹽類或酯類之施加率為約每公頃2克酸當量(gae/ha)至約300 gae/ha。在特殊實施例中，唑嘧磺草胺或其鹽類之施加率為約6 gai/ha至約25 gai/ha，且式(I)化合物或其鹽類或酯類之施加率為約每公頃8克酸當量(gae/ha)至約32 gae/ha。在某些實施例中，該方法與組成物以式(I)化合物或其鹽類或酯類結合唑嘧磺草胺
或其鹽類，用於控制BRAPP或CYPIR。
在本文所述組成物與方法之某些實施例中，式(I)化合物或其鹽類或酯類係結合磺草唑胺或其鹽類使用。關於組成物，在一些實施例中，式(I)化合物或其鹽類或酯類，與磺草唑胺或其鹽類之重量比，係介於約1：5至約300：1之範圍內。在某些實施例中，式(I)化合物或其鹽類或酯類與磺草唑胺或其鹽類之重量比，係介於約1：2至約70：1之範圍內。在某些實施例中，式(I)化合物或其鹽類或酯類與磺草唑胺或其鹽類之重量比，係介於約1：0.75至約5：1之範圍內。在某些實施例中，該組成物包含式(I)化合物或其芐基或正丁基酯類與磺草唑胺。關於方法，在某些實施例中，該方法包含以本文所述之組成物接觸不良植被或其部位，或施加至土壤或水，以預防植被出苗或生長。在一些實施例中，依據活性成分於組成物中之總量，組成物以約每公頃4克活性成分(gai/ha)至約310 gai/ha之施加率施加。在某些實施例中，依據活性成分於組成物中之總量，組成物以6 gai/ha至約70 gai/ha之施加率施加。在一些實施例中，該方法包含以式(I)化合物或其鹽類或酯類，與磺草唑胺或其鹽類，例如，依序地或同時地，接觸不良植被或其部位，或施加至土壤或水，以預防植被出苗或生長。在一些實施例中，磺草唑胺或其鹽類之施加率為約2 gai/ha至約10 gai/ha，且式(I)化合物或其鹽類或酯類之施加率為約每公頃2克酸當量(gae/ha)至約300 gae/ha。在一些實施例中，磺草唑胺或其鹽類之施加率為約2 gai/ha至約10 gai/ha，且式(I)
化合物或其鹽類或酯類之施加率為約每公頃8克酸當量(gae/ha)至約32 gae/ha。在某些實施例中，該方法與組成物以式(I)化合物或其鹽類或酯類，結合磺草唑胺或其鹽類，用於控制LEFCH。
在本文所述組成物與方法之某些實施例中，式(I)化合物或其鹽類或酯類係結合平速爛或其鹽類使用。關於組成物，在一些實施例中，式(I)化合物或其鹽類或酯類與平速爛或其鹽類之重量比，係介於約1：25至約69：1之範圍內。在某些實施例中，式(I)化合物或其鹽類或酯類，與平速爛或其鹽類之重量比，係介於約1：11至約46：1之範圍內。在某些實施例中，式(I)化合物或其鹽類或酯類與平速爛或其鹽類之重量比，係介於約1：8至約8：1之範圍內。在某些實施例中，式(I)化合物或其鹽類或酯類與平速爛或其鹽類之重量比，係介於約1：4至約4：1之範圍內。在某些實施例中，本發明提供之組成物包含式(I)化合物或其芐基或正丁基酯類與平速爛。在一實施例中，組成物包含式(I)化合物之芐基酯與平速爛，其中式(I)化合物與平速爛之重量比為約1：4至約2：1。在一實施例中，組成物包含式(I)化合物之芐基酯與平速爛，其中式(I)化合物之芐基酯與平速爛之重量比為約1：4至約4：1。在一實施例中，組成物包含式(I)化合物之芐基酯與平速爛，其中式(I)化合物與平速爛之重量比為約1：11至約46：1。在一實施例中，組成物包含式(I)化合物之正丁基酯與平速爛，其中式(I)化合物之正丁基酯與平速爛之重量比為約1：4至約4：1。關於方法，在某些實施例中，該方
法包含以本文所述之組成物接觸不良植被或其部位，或施加至土壤或水，以預防植被出苗或生長。在一些實施例中，依據活性成分於組成物中之總量，組成物以約每公頃7克活性成分(gai/ha)至約350 gai/ha之施加率施加。在某些實施例中，依據活性成分於組成物中之總量，組成物以約9 gai/ha至約250 gai/ha之施加率施加。在一些實施例中，該方法包含以式(I)化合物或其鹽類或酯類，與平速爛或其鹽類，例如，依序地或同時地，接觸不良植被或其部位，或施加至土壤或水，以預防植被出苗或生長。在一些實施例中，平速爛或其鹽類之施加率為約7.5 gai/ha至約50 gai/ha，且式(I)化合物或其鹽類或酯類之施加率為約每公頃2克酸當量(gae/ha)至約300 gae/ha。在一些實施例中，平速爛或其鹽類之施加率為約2 gai/ha至約100 gai/ha，且式(I)化合物或其鹽類或酯類之施加率為約每公頃2 g酸當量(gae/ha)至約400 gae/ha。在一些實施例中，平速爛或其鹽類之施加率為約4.38 gai/ha至約50 gai/ha，且式(I)化合物或其鹽類或酯類之施加率為約每公頃4.38 g酸當量(gae/ha)至約200 gae/ha。在某些實施例中，該方法使用式(I)化合物或其芐基或正丁基酯類，以及平速爛。在一實施例中，該方法使用式(I)化合物與平速爛，其中式(I)化合物之施加率為約每公頃4.38 g酸當量(gae/ha)至約35 gae/ha，且平速爛之施加率為約8.75 gai/ha至約40 gai/ha。在一實施例中，該方法使用式(I)化合物之芐基酯與平速爛，其中式(I)化合物之芐基酯之施加率為約每公頃4.38 g酸當量(gae/ha)至約200 gae/ha，且平速爛
之施加率為約4.38gai/ha至約50 gai/ha。在一實施例中，該方法使用式(I)化合物之正丁基酯與平速爛，其中式(I)化合物之正丁基酯之施加率為約每公頃4.38 g酸當量(gae/ha)至約17.5 gae/ha，且平速爛之施加率為約4.38 gai/ha至約17.5 gai/ha。在某些實施例中，該方法與組成物以式(I)化合物或其鹽類或酯類，結合平速爛或其鹽類，用於控制BRAPP、CYPDI、CYPES、ECHCG、ECHSS、IPOHE、ISCRU、LEFCH、LEFPA或SCPJU。
在本文所述組成物與方法之某些實施例中，式(I)化合物或其鹽類或酯類係結合啶磺草胺或其鹽類使用。關於組成物，在一些實施例中，式(I)化合物或其鹽類或酯類，與啶磺草胺或其鹽類之重量比，係介於約1：11至約75：1之範圍內。在某些實施例中，式(I)化合物或其鹽類或酯類與啶磺草胺或其鹽類之重量比，係介於約1：10至約3：1之範圍內。在某些實施例中，式(I)化合物或其鹽類或酯類，與啶磺草胺或其鹽類之重量比，係介於約1：1至約2：0.4之範圍內。在某些實施例中，式(I)化合物或其鹽類或酯類與啶磺草胺或其鹽類之重量比，係介於約1：.4至約1：0.4之範圍內。在某些實施例中，本發明提供之組成物包含式(I)化合物或其芐基酯與啶磺草胺。在一實施例中，組成物包含式(I)化合物之芐基酯與啶磺草胺，其中式(I)化合物之芐基酯與啶磺草胺之重量比為約1：0.4。關於方法，在某些實施例中，該方法包含以本文所述之組成物接觸不良植被或其部位，或施加至土壤或水，以預防植被出苗或生長。在一些
實施例中，依據活性成分於組成物中之總量，組成物以約每公頃4克活性成分(gai/ha)至約362 gai/ha之施加率施加。在某些實施例中，依據活性成分於組成物中之總量，組成物以約5 gai/ha至約22 gai/ha之施加率施加。在一些實施例中，該方法包含以式(I)化合物或其鹽類或酯類與啶磺草胺或其鹽類，例如，依序地或同時地，接觸不良植被或其部位，或施加至土壤或水，以預防植被出苗或生長。在一些實施例中，啶磺草胺或其鹽類之施加率為約3 gai/ha至約23 gai/ha，且式(I)化合物或其鹽類或酯類之施加率為約每公頃2克酸當量(gae/ha)至約300 gae/ha。在一些實施例中，啶磺草胺或其鹽類之施加率為約1 gai/ha至約12 gai/ha，且式(I)化合物或其鹽類或酯類之施加率為約每公頃4 g酸當量(gae/ha)至約20 gae/ha。在一些實施例中，啶磺草胺或其鹽類之施加率為約2 gai/ha至約6 gai/ha，且式(I)化合物或其鹽類或酯類之施加率為約每公頃8 g酸當量(gae/ha)至約10 gae/ha。在某些實施例中，該方法使用式(I)化合物或其芐基酯與啶磺草胺。在一實施例中，該方法使用式(I)化合物之芐基酯與啶磺草胺，其中式(I)化合物之芐基酯之施加率為約每公頃8.75 g酸當量(gae/ha)，且啶磺草胺或其鹽類之施加率為約3.75 gai/ha。在某些實施例中，該方法與組成物以式(I)化合物或其鹽類或酯類結合啶磺草胺或其鹽類，用於控制CIRAR。
本文所述混合物之成分可個別地或作為多重除草系統之一部分施加。
本文所述混合物可結合一或多個其他除草劑施加，以控制更廣泛之不良植被。當結合其他除草劑使用時，組成物可與其他單一除草劑或多種除草劑一起配製、可與其他單一除草劑或多種除草劑一起槽混合，或可與其他單一除草劑或多種除草劑依序施加。一些可用於與本文所述組成物與方法結合之除草劑，包括但不限於：4-CPA；4-CPB；4-CPP；2,4-D；2,4-D膽鹼鹽、2,4-D酯類與胺類、2,4-DB；3,4-DA；3,4-DB；2,4-DEB；2,4-DEP；3,4-DP；2,3,6-TBA；2,4,5-T；2,4,5-TB；乙草胺(acetochlor)、亞喜芬(acifluorfen)、苯草醚、丙烯醛、拉草(alachlor)、草毒死(allidochlor)、亞汰草(alloxydim)、烯丙基醇、艾羅克(alorac)、胺嗪酮(ametridione)、草殺淨(ametryn)、胺嗪草酮(amibuzin)、胺唑草酮(amicarbazne)、醯嘧磺隆(amidosulfuron)、胺環吡克(aminocyclopyrachlor)、氯胺吡啶酸(aminopyralid)、甲基胺草磷(amiprofos-methyl)、殺草強、胺磺酸銨、莎稗磷(anilofos)、甲氧平草隆(anisuron)、亞速爛(asulam)、阿特拉通(atraton)、草脫淨(atrazine)、草芬定(azafenidin)、四唑嘧磺隆(azimsulfuron)、滅蘇民(aziprotryne)、燕麥靈(barban)、BCPC、氟丁醯草胺(beflubutamid)、草除靈(benazolin)、醯苯草酮(bencarbazone)、倍尼芬(benfluralin)、苯福塞(benfuresate)、芐嘧磺隆(bensulfuron-methyl)、地散磷(bensulide)、禾草丹(benthiocarb)、本達隆鈉(bentazon-sodium)、胺酸殺(benzadox)、雙苯嘧草酮(benzfendizone)、芐草胺
(benzipram)、苯并雙環酮(benzobicyclon)、吡草酮(benzofenap)、氟草黃(benzofluor)、新燕靈(benzoylprop)、苯噻隆(benzthiazuron)、畢拉草(bialaphos)、環吡草酮(bicyclopyrone)、必芬諾(bifenox)、雙丙胺醯膦(bilanafos)、雙草醚(bispyribac-sodium)、硼砂、克草(bromacil)、除草溴(bromobonil)、溴丁草胺(bromobutide)、殺草全(bromofenoxim)、溴苯腈、溴莠敏(brompyrazon)、丁基拉草(butachlor)、布芬草(butafenacil)、抑草磷(butamifos)、丁烯草胺(butenachlor)、丁硫咪唑酮(buthidazole)、匍隆(buthiuron)、比達寧(butralin)、莎稗磷(butroxydim)、炔草隆(buturon)、拔敵草(butylate)、二甲胂酸(cacodylic acid)、苯酮唑(cafenstrole)、氯酸鈣、氰胺化鈣、卡苯二氯(cambendichlor)、卡巴速爛(carbasulam)、卡草胺(carbetamide)、異噁甲草威(carboxazole)、氯草丹(chlorprocarb)、乙基克繁草(carfentrazone-ethyl)、CDEA、CEPC、甲氧基護谷(chlomethoxyfen)、克攔本(chloramben)、丁醯草胺(chloranocryl)、克寄普(chlorazifop)、氯阿淨(chlorazine)、滅落寧(chlorbromuron)、氯炔靈(chlorbufam)、乙氧隆(chloreturon)、伐草克(chlorfenac)、燕麥酯(chlorfenprop)、氟咪殺(chlorflurazole)、整形醇(chlorflurenol)、氯草敏(chloridazon)、氯嘧磺隆(chlorimuron)、草枯醚(chlornitrofen)、三氯丙酸(chloropon)、綠麥隆(chlorotoluron)、枯草隆(chloroxuron)、氯塞尼爾(chloroxynil)、克普芬(chlorpropham)、氯磺隆
(chlorsulfuron)、大克草(chlorthal)、草克樂(chlorthiamid)、吲哚酮草酯(cinidon-ethyl)、環庚草醚(cinmethylin)、醚磺隆(cinosulfuron)、咯草隆(cisanilide)、克草同(clethodim)、氯碘吡啶酯(cliodinate)、炔草酯(clodinafop-propargyl)、力平之(clofop)、可滅蹤、克普草(clomeprop)、果美生長素(cloprop)、克氧定(cloproxydim)、畢克草(clopyralid)、CMA、硫酸銅、CPMF、CPPC、醚草敏(credazine)、甲酚(cresol)、苄草隆(cumyluron)、氰草淨(cyanatryn)、氰乃淨(cyanazine)、草滅特(cycloate)、環吡莫(cyclopyrimorate)、環磺隆(cyclosulfamuron)、環殺草(cycloxydim)、環莠隆(cycluron)、丁基賽伏草(cyhalofop-butyl)、賽伯刈(cyperquat)、環丙津(cyprazine)、三環噻草胺(cyprazole)、環醯草胺(cypromid)、汰草龍(daimuron)、得拉本(dalapon)、邁隆(dazomet)、異丁草胺(delachlor)、雙苯胺靈(desmedipham)、敵草淨(desmetryn)、二醛酯(di-allate)、麥草畏、二氯苯腈(dichlobenil)、雙氯醛脲(dichloralurea)、芐胺靈(dichlormate)、滴丙酸(dichlorprop)、滴丙酸-P、禾草靈(diclofop-methyl)、二乙除草快(diethamquat)、乙甲草胺(diethatyl)、戊味禾草靈(difenopenten)、枯莠隆(difenoxuron)、野燕枯、吡氟草胺(diflufenican)、二氟吡隆(diflufenzopyr)、惡唑隆(dimefuron)、草丹(dimepiperate)、二甲草胺(dimethachlor)、愛落殺(dimethametryn)、汰草滅(dimethenamid)、汰草滅-P、草滅散(dimexano)、草噠酮(dimidazon)、撻乃安(dinitramine)、地樂特(dinofenate)、丙
硝酚(dinoprop)、戊硝酚(dinosam)、地樂酚(dinoseb)、特樂酚(dinoterb)、草乃敵(diphenamid)、異丙凈(dipropetryn)、敵草快(diquat)、賽鬆(disul)、汰硫草(dithiopyr)、達有龍(diuron)、DMPA、DNOC、DSMA、EBEP、克菊特(eglinazine)、草多索、易普乃(epronaz)、EPTC、抑草蓬(erbon)、戊草丹(esprocarb)、乙丁烯氟靈(ethalfluralin)、乙柳醯胺(ethbenzamide)、胺苯磺隆(ethametsulfuron)、磺噻隆(ethidimuron)、抑草威(ethiolate)、益苯胺(ethobenzamid)、益多苯胺(etobenzamid)、益覆滅(ethofumesate)、氯氟草醚(ethoxyfen)、亞速隆(ethoxysulfuron)、硝草酚(etinofen)、益靈滅(etnipromid)、乙氧苯草胺(etobenzanid)、EXD、芬速爛(fenasulam)、涕丙酸(fenoprop)、精噁唑禾草靈(fenoxaprop)、芬殺草(fenoxaprop-P-ethyl)、芬殺草+雙苯噁唑酸(isoxadifen-ethyl)、芬諾殺磺隆(fenoxasulfone)、芬得克(fenteracol)、噻唑禾草靈(fenthiaprop)、四唑醯草胺(fentrazamide)、非草隆(fenuron)、硫酸亞鐵、麥草氟(flamprop)、麥草氟-M、伏速隆(flazasulfuron)、伏寄普(fluazifop)、伏寄普-P-丁基、異丙草酯(fluazolate)、氟酮磺隆(flucarbazone)、氟吡磺隆(flucetosulfuron)、貝殺靈(fluchloralin)、氟噻草胺(flufenacet)、三吡氟草胺(flufenican)、氟噠嗪草酯(flufenpyr-ethyl)、氟滅凈(flumezin)、氟烯草酸(flumiclorac-pentyl)、丙炔氟草胺(flumioxazin)、炔草胺(flumipropyn)、伏草隆(fluometuron)、三氟硝草醚(fluorodifen)、乙羧氟草醚(fluoroglycofen)、唑
啶草(fluoromidine)、氟除草醚(fluoronitrofen)、氟硫隆(fluothiuron)、氟胺草唑(flupoxam)、氟丙草酯(flupropacil)、四氟丙酸(flupropanate)、氟啶嘧磺隆(flupyrsulfuron)、氟啶草酮(fluridone)、氟咯草酮(flurochloridone)、氟氯比(fluroxypyr)、氟氯比異辛酯(fluroxypyr-meptyl)、呋草酮(flurtamone)、嗪草酸(fluthiacet)、氟磺胺草醚(fomesafen)、甲胺磺隆(foramsulfuron)、殺木膦(fosamine)、氟烯草酸(fumiclorac)、呋氧草醚(furyloxyfen)、固殺草、固殺草銨、固殺草-P-銨、草甘膦鹽類與酯類、呼拉噻芬(halauxifen)、甲基呼拉噻芬、拉塞芬(halosafen)、氯吡嘧磺隆(halosulfuron-methyl)、氟啶草(haloxydine)、甲基合氯氟(haloxyfop-methyl)、合氯氟-P-甲基、六氯丙酮(hexachloroacetone)、六氟鹽(hexaflurate)、菲殺淨(hexazinone)、咪草酸(imazamethabenz)、甲氧咪草煙(imazamox)、甲咪唑煙酸(imazapic)、咪唑煙酸(imazapyr)、咪唑喹啉酸(imazaquin)、唑嘧磺隆(imazosulfuron)、氯酯磺草胺-甲酯、茚草酮(indanofan)、茚嗪氟草胺(indaziflam)、除草碘(iodobonil)、碘甲烷、碘磺隆(iodosulfuron)、乙基碘磺隆鈉鹽(iodosulfuron-ethyl-sodium)、碘吩磺隆(iofensulfuron)、碘塞尼爾(ioxynil)、抑草津(ipazine)、艾分卡巴腙(ipfencarbazone)、異草啶(iprymidam)、草特靈(isocarbamid)、異草定(isocil)、丁嗪草酮(isomethiozin)、異草完隆(isonoruron)、異普林(isopolinate)、異樂靈(isopropalin)、異丙隆(isoproturon)、異惡隆(isouron)、異噁
草胺(isoxaben)、異噁氯草酮(isoxachlortole)、異噁唑草酮(isoxaflutole)、異惡草醚(isoxapyrifop)、卡靈草(karbutilate)、環己二酮(ketospiradox)、乳氟禾草靈(lactofen)、環草定(lenacil)、理有龍(linuron)、MAA、MAMA、MCPA酯類與胺類、硫乙基MCPA、MCPB、甲氯丙酸(mecoprop)、甲氯丙酸-P、地樂施(medinoterb)、滅芬草(mefenacet)、氟草磺(mefluidide)、滅莠津(mesoprazine)、二磺隆(mesosulfuron)、硝磺酮(mesotrione)、斯美地(metam)、噁唑醯草胺(metamifop)、苯嗪草酮(metamitron)、滅草胺(metazachlor)、雙醚氯吡嘧磺隆(metazosulfuron)、二甲噠草伏(metflurazon)、噻唑隆(methabenzthiazuron)、馬普林(methalpropalin)、滅草唑(methazole)、甲硫苯威(methiobencarb)、異噁唑啉(methiozolin)、滅草恆(methiuron)、醚草通(methometon)、格草淨(methoprotryne)、溴甲烷、異硫氰酸甲酯、甲基殺草隆(methyldymron)、吡喃隆(metobenzuron)、撲奪草(metobromuron)、莫多草淨(metolachlor)、甲氧隆(metoxuron)、嗪草酮(metribuzin)、磺隆(metsulfuron)、甲基磺隆(metsulfuron-methyl)、稻得壯(molinate)、庚醯草胺(monalide)、單甲異噁隆(monisouron)、氯乙酸、綠谷隆(monolinuron)、滅草隆(monuron)、伐草快(morfamquat)、MSMA、萘丙胺(naproanilide)、敵草胺(napropamide)、鈉得爛(naptalam)、草不隆(neburon)、煙嘧磺隆(nicosulfuron)、吡氯草胺(nipyraclofen)、甲磺樂靈(nitralin)、護谷(nitrofen)、三氟甲草醚(nitrofluorfen)、氟草
敏(norflurazon)、草完隆(noruron)、OCH、坪草丹(orbencarb)、鄰二氯苯、嘧苯胺磺隆(orthosulfamuron)、黃草消(oryzalin)、丙炔噁草酮(oxadiargyl)、樂滅草(oxadiazon)、草噠松(oxapyrazon)、環氧嘧磺隆(oxasulfuron)、噁嗪草酮(oxaziclomefone)、復祿芬(oxyfluorfen)、乙基派芬草(paraflufen-ethyl)、對氟隆(parafluron)、巴拉刈、克草蜢(pebulate)、壬酸、施得圃(pendimethalin)、五氯酚、蔬草滅(pentanochlor)、環戊噁草酮(pentoxazone)、佈福松(perfluidone)、烯草胺(pethoxamid)、棉胺寧(phenisopham)、苯敵草(phenmedipham)、乙基苯敵草、醯草隆(phenobenzuron)、醋酸苯汞酯、毒莠定(picloram)、氟吡醯草胺(picolinafen)、唑啉草酯(pinoxaden)、哌草磷(piperophos)、亞砷酸鉀、疊氮化鉀、氰酸鉀、普拉草(pretilachlor)、甲基氟嘧磺隆(primisulfuron-methyl)、環丙腈津(procyazine)、胺氟樂靈(prodiamine)、氟唑草胺(profluazol)、環丙氟靈(profluralin)、環苯草酮(profoxydim)、甘撲津(proglinazine)、調環酸鈣(prohexadione-calcium)、撲減通(prometon)、撲草淨(prometryn)、拿草特(pronamide)、毒草胺(propachlor)、除草靈(propanil)、普拔草(propaquizafop)、撲滅津(propazine)、苯胺靈(propham)、異丙草胺(propisochlor)、丙苯磺隆(propoxycarbazone)、咪唑嘧磺隆(propyrisulfuron)、戊炔草胺(propyzamide)、甲硫磺樂靈(prosulfalin)、芐草丹(prosulfocarb)、氟磺隆(prosulfuron)、
撲滅生(proxan)、拔地草(prynachlor)、噠嗪酮乙酸(pydanon)、雙唑草腈(pyraclonil)、乙基派芬草(pyraflufen-ethyl)、磺酰草吡唑(pyrasulfotole)、雙唑草腈(pyrazogyl)、芐草唑(pyrazolynate)、乙基吡嘧磺隆(pyrazosulfuron-ethyl)、普芬草(pyrazoxyfen)、嘧啶肟草醚(pyribenzoxim)、稗草畏(pyributicarb)、氯草定(pyriclor)、噠嗪醇(pyridafol)、必汰草(pyridate)、環酯草醚(pyriftalid)、嘧草醚(pyriminobac)、吡嘧沙泛(pyrimisulfan)、嘧硫草醚(pyrithiobac-sodium)、派羅克殺草碸(pyroxasulfone)、快克草、氯甲喹啉酸(quinmerac)、莫克草(quinoclamine)、克藻胺(quinonamid)、快伏草(quizalofop)、快伏草-P-乙基、硫氰苯胺(rhodethanil)、碸嘧磺隆(rimsulfuron)、殺芬草(saflufenacil)、S-莫多草淨、另丁津(sebuthylazine)、密草通(secbumeton)、西殺草(sethoxydim)、環草隆(siduron)、西瑪津(simazine)、西瑪通(simeton)、西草淨(simetryn)、SMA、亞砷酸鈉、疊氮化鈉、氯酸鈉、磺草酮(sulcotrione)、菜草畏(sulfallate)、甲磺草胺(sulfentrazone)、甲嘧磺隆(sulfometuron)、硫復松(sulfosate)、磺醯磺隆(sulfosulfuron)、硫酸、sulglycapin、滅草靈(swep)、SYN-523、TCA、牧草胺(tebutam)、得匍隆(tebuthiuron)、特糠酯酮(tefuryltrione)、環磺酮(tembotrione)、得殺草(tepraloxydim)、特草定(terbacil)、特草靈(terbucarb)、特丁草胺(terbuchlor)、特丁通(terbumeton)、特丁津(terbuthylazine)、去草淨(terbutryn)、四氟隆(tetrafluron)、
欣克草(thenylchlor)、噻氟隆(thiazafluron)、噻草啶(thiazopyr)、噻二唑草胺(thidiazimin)、噻苯隆(thidiazuron)、甲基噻克松(thiencarbazone-methyl)、噻吩磺隆(thifensulfuron)、甲基噻吩磺隆(thifensulfurn-methyl)、殺丹(thiobencarb)、仲草丹(tiocarbazil)、地氯靈(tioclorim)、苯吡唑草酮(topramezone)、三甲苯草酮(tralkoxydim)、氟酮磺草胺(triafamone)、野麥畏(tri-allate)、醚苯磺隆(triasulfuron)、三嗪氟草胺(triaziflam)、苯磺隆(tribenuron)、甲基苯磺隆、殺草畏(tricamba)、綠草定膽鹼鹽(triclopyr choline salt)、綠草定酯類與鹽類、三地芬(tridiphane)、草達津(trietazine)、三氟啶磺隆(trifloxysulfuron)、三福林(trifluralin)、氟胺磺隆(triflusulfuron)、草普(trifop)、三氟禾草肟(trifopsime)、三羥嗪(trihydroxytriazine)、三甲隆(trimeturon)、三丙酸甘油酯(tripropindan)、草達克(tritac)、三氟甲磺隆(tritosulfuron)、萬隆(vernolate)、二甲苯草胺(xylachlor)，及其鹽類、酯類、光學活性異構物與混合物。
本文所述之組成物與方法，可進一步結合草甘膦、5-烯醇丙酮基莽草酸-3-磷酸鹽(EPSP)合成酶抑制劑、固殺草、麩胺醯胺酸合成酶抑制劑、麥草畏、苯氧基生長素、吡啶基氧基生長素、合成生長素、生長素運輸抑制劑、芳基氧基苯氧基丙酸酯、環己烷二酮、苯基吡唑啉、乙醯輔酶A羧化酶(ACCase)抑制劑、咪唑啉酮、磺醯基脲、嘧啶基硫代苯甲酸酯、二甲氧基嘧啶、三唑并嘧啶、磺醯基胺基羰基三唑酮、乙醯乳酸合成酶(ALS)或乙醯羥酸合成酶
(AHAS)抑制劑、4-羥基苯基-丙酮酸二氧酶(HPPD)抑制劑、八氫番茄紅素去飽和酶抑制劑、類胡蘿蔔素生合成抑制劑、原紫質原氧化酶(PPO)抑制劑、纖維素生合成抑制劑、有絲分裂抑制劑、微管抑制劑、極長鏈脂肪酸抑制劑、脂肪酸與脂質生合成抑制劑、光合系統I抑制劑、光合系統II抑制劑、三嗪，與溴苯腈，用於具草甘膦-耐受性、EPSP合成酶抑制劑-耐受性、固殺草-耐受性、麩胺醯胺酸合成酶抑制劑-耐受性、麥草畏-耐受性、苯氧基生長素-耐受性、吡啶基氧基生長素-耐受性、生長素-耐受性、生長素運輸抑制劑-耐受性、芳基氧基苯氧基丙酸酯-耐受性、環己烷二酮-耐受性、苯基吡唑啉-耐受性、ACCase-耐受性、咪唑啉酮-耐受性、磺醯基脲-耐受性、嘧啶基硫代苯甲酸酯-耐受性、三唑并嘧啶-耐受性、磺醯基胺基羰基三唑酮-耐受性、ALS-或AHAS-耐受性、HPPD-耐受性、八氫番茄紅素去飽和酶抑制劑-耐受性、類胡蘿蔔素生合成抑制劑-耐受性、PPO-耐受性、纖維素生合成抑制劑-耐受性、有絲分裂抑制劑-耐受性、微管抑制劑-耐受性、極長鏈脂肪酸抑制劑-耐受性、脂肪酸與脂質生合成抑制劑-耐受性、光合系統I抑制劑-耐受性、光合系統II抑制劑-耐受性、三嗪-耐受性、溴苯腈-耐受性之作物，以及具有多個或複合性狀而對於多種化學物質具耐受性，及/或具有經由單一及/或多重抗性機制之多重作用模式之作物。在一些實施例中，式(I)化合物或其鹽類或酯類，與補充用除草劑或其鹽類或酯類，係與該除草劑結合使用，該除草劑對於欲處理作物具有選擇性，且其
輔助了這些化合物以特定之施加率對於雜草之控制。在一些實施例中，本文所述之組成物與其他補充用除草劑係同時施加，無論是結合物配方、槽混合物或依序施加。
在一些實施例中，本文所述之組成物係結合一或多個除草劑安全劑使用，如AD-67(MON 4660)、解草嗪(benoxacor)、禾草丹(benthiocarb)、油菜素內酯(brassinolide)、解毒喹(cloquintocet(mexyl))、解草胺腈(cyometrinil)、汰草龍(daimuron)、二氯丙烯胺(dichlormid)、二環酮(dicyclonon)、草丹(dimepiperate)、二硫松(disulfoton)、解草唑(fenchlorazole-ethyl)、解草啶(fenclorim)、解草胺(flurazole)、氟草肟(fluxofenim)、解草噁唑(furilazole)、誘敏蛋白質(harpin proteins)、雙苯噁唑酸、急草殺(jiecaowan)、急草希(jiecaoxi)、吡唑解草酯(mefenpyr-diethyl)、滅草寧(mephenate)、萘二甲酸酐(naphthalic anhydride(NA))、解草腈(oxabetrinil)、R29148與N-苯基-磺醯基苯甲酸醯胺類，以增進其選擇性。在一些實施例中，安全劑係用於稻米、穀類、玉蜀黍或玉米等設置。在一些實施例中，安全劑為解毒喹或其酯類或鹽類。在某些實施例中，解毒喹係用於對抗組成物對於稻米與穀類之有害影響。在一些實施例中，安全劑為解毒喹。
在一些實施例中，本文所述之組成物係結合一或多個植物生長調節劑使用，如2,3,5-三碘苯甲酸、IAA、IBA、萘乙醯胺、α-萘醋酸、芐基腺嘌呤、4-羥基苯乙醇、裂殖素(kinetin)、玉米素(zeatin)、草多索、乙烯利
(ethephon)、五氯酚、噻苯隆(thidiazuron)、脫葉磷(tribufos)、艾維激素(aviglycine)、乙烯利、順丁烯二醯肼、赤黴素(gibberellins)、赤黴酸(gibberellic acid)、脫落酸(abscisic acid)、嘧啶醇(ancymidol)、殺木膦(fosamine)、草甘雙膦(glyphosine)、異嘧醇(isopyrimol)、茉莉酸(jasmonic acid)、順丁烯二醯肼、甲哌啶(mepiquat)、2,3,5-三碘苯甲酸、變形素(morphactins)、雙整形醇(dichlorflurenol)、呋嘧醇(flurprimidol)、氟草磺(mefluidide)、巴克素(paclobutrazol)、得拉生長素(tetcyclacis)、烯效唑(uniconazole)、油菜素內酯、乙基油菜素內酯、環己醯亞胺、乙烯、滅速克(methasulfocarb)、調環酸(prohexadione)、抑芽唑(triapenthenol)與抗倒酯(trinexapac)。
在一些實施例中，植物生長調節劑係用於一或多個作物或設置，如稻米、穀類作物、玉蜀黍、玉米、闊葉作物、芸苔/油菜、草皮、鳳梨、甘蔗、向日葵、牧草、草地、牧場、休耕地、樹與藤園、種植作物、蔬菜，以及非作物(觀賞)設置。在一些實施例中，植物生長調節劑係混合於式(I)化合物，或混合於式(I)化合物與三唑并嘧啶磺醯胺，以對植物產生優先之有利效果。
在一些實施例中，本文提供之組成物進一步包含至少一農業上可接受佐劑或載劑。適用之佐劑或載劑對於價值作物不應產生植物毒性，特別是在作物存在下，用於選擇性雜草控制之組成物之施加濃度，且不應與除草成分或其他組成物成分進行化學反應。此類混合物可設計成直
接施加至雜草或其部位，或可為濃縮物或配方，其正常情況下係於施加前以額外之載劑與佐劑稀釋。其可為固體，例如，粉劑、顆粒劑、水分散性顆粒劑或可濕性粉末，或液體，例如，可乳化濃縮物、溶液、乳液或懸液。其亦可以預混合物或混合罐提供。
適用之農業上佐劑與載劑包括但不侷限於，作物油濃縮物；壬基酚乙氧基化物；芐基椰子烷基二甲基四級銨鹽；石油烴摻合物、烷基酯類、有機酸，與陰離子界面活性劑；C9-C11烷基多醣苷；磷酸化醇乙氧基化物；天然一級醇(C12-C16)乙氧基化物；二-二級丁基酚EO-PO嵌段共聚合物；甲基聚矽氧烷末端(cap)；壬基酚乙氧基化物+尿素硝酸銨；乳化甲基種籽油；十三烷醇(合成)乙氧基化物(8EO)；牛脂胺乙氧基化物(15 EO)；PEG(400)二油酸酯-99。
可使用之液體載劑包括水與有機溶劑。有機溶劑包括但不侷限於，石油分餾物或烴類如礦物油、芳族溶劑、石蠟油，及其類似物；蔬菜油如大豆油、油菜籽油、橄欖油、蓖麻油、葵花籽油、椰子油、玉米油、棉籽油、亞麻籽油、棕櫚油、花生油、紅花油、芝麻油、桐油及其類似物；上述蔬菜油之酯類；單元醇類或二羥基、三羥基，或較低級多元醇(含4-6個羥基)之酯類，如2-乙基己基硬脂酸酯、正丁基油酸酯、肉荳蔻酸異丙基酯、丙二醇二油酸酯、琥珀酸二辛酯、己二酸二丁酯、鄰苯二甲酸二辛酯及其類似物；單、二與多羧酸類之酯類及其類似物。特定之有機溶劑包括但不限於，甲苯、二甲苯、石油腦、作物油、丙
酮、甲基乙基酮、環己酮、三氯乙烯、過氯乙烯、乙酸乙酯、乙酸戊酯、乙酸丁酯、丙二醇單甲基醚、二乙二醇單甲基醚、甲醇、乙醇、異丙醇、戊醇、乙二醇、丙二醇、甘油、N-甲基-2-吡咯烷酮、N,N-二甲基烷基醯胺、二甲亞碸、液體肥料及其類似物。在某些實施例中，水為用於濃縮物稀釋之載劑。
適用之固體載劑包括但不侷限於，滑石、葉臘石黏土、矽土、凹土、高嶺土、矽藻土(kieselguhr)、白堊、矽藻土(diatomaceous earth)、石灰、碳酸鈣、膨潤土(bentonite clay)、漂白土(Fuller's earth)、棉籽殼、麵粉、大豆粉、浮石、木粉、核桃殼粉、木質素、纖維素，及其類似物。
在一些實施例中，本文所述之組成物進一步包含一或多個界面活性劑。在一些實施例中，此類界面活性劑係用於固體與液體組成物，以及在某些實施例中，其經設計可於施加前以載劑稀釋。界面活性劑可為陰離子、陽離子或非離子性質，並可作為乳化劑、潤濕劑、懸浮劑，或用於其他用途。本發明配方亦可使用描述於，包括“McCutcheon’s Detergents and Emulsifiers Annual,”MC Publishing Corp.,Ridgewood,New Jersey,1998與“Encyclopedia of Surfactants,”Vol.I-III,Chemical Publishing Co.,New York,1980-81，之界面活性劑。界面活性劑包括但不限於，烷基硫酸鹽類，如二乙醇銨月桂基硫酸鹽；烷基芳基磺酸鹽類，如十二烷基苯磺酸鈣；烷基酚-亞烷基氧化物加成產物，如壬基酚-C18乙氧基化物；乙醇-
亞烷基氧化物加成產物，如十三烷醇-C16乙氧基化物；肥皂，如硬脂酸鈉；烷基萘磺酸鹽類，如二丁基萘磺酸鈉；磺琥珀酸鹽類之二烷基酯類，如二(2-乙基己基)磺琥珀酸鈉；山梨醇酯類，如山梨糖醇油酸酯；四級胺類，如月桂基三甲基氯化銨；脂肪酸之聚乙二醇酯類，如聚乙二醇硬脂酸酯；氧化乙烯與氧化丙烯之嵌段共聚合物；單與二烷基磷酸酯類之鹽類；蔬菜或種籽油，如大豆油、油菜籽油/芥花籽油、橄欖油、蓖麻油、葵花籽油、椰子油、玉米油、棉籽油、亞麻籽油、棕櫚油、花生油、紅花油、芝麻油、桐油及其類似物；以及上述植物油之酯類，以及在某些實施例中，甲基酯類。
在一些實施例中，這些材料，如植物油或種子油及其酯類，可互換使用，以作為農業上佐劑、作為液體載劑，或作為界面活性劑。
可用於本發明組成物之其他示範性添加劑包括但不侷限於，相容性試劑、消泡劑、螯合劑、中和劑與緩衝劑、腐蝕抑制劑、染劑、增味劑、擴展劑、滲透助劑、黏著劑、分散劑、增稠劑、凝固點下降劑、抗微生物試劑，及其類似物。組成物亦可包含其他相容之成分，舉例而言，其他除草劑、植物生長調節劑、殺菌劑、殺蟲劑及其類似物，並可與液體肥料或固體、顆粒肥料載劑如硝酸銨、尿素及其類似物，一起配製。
在一些實施例中，本文所述之組成物活性成分濃度為約0.0005至98重量百分比。在一些實施例中，濃度為
約0.0006至90重量百分比。在經設計以作為濃縮物之組成物中，其活性成分，在某些實施例中，以濃度約0.1至98重量百分比存在，且在某些實施例中，約0.5至90重量百分比。此類組成物，在某些實施例中，於施加前以惰性載劑如水稀釋。通常，施加至雜草或雜草部位之經稀釋組成物，在某些實施例中，含有約0.0003至1.5重量百分比之活性成分，以及在某些實施例中，含有約0.0008至1.0重量百分比。
本發明之組成物可藉由使用常規之地面或空中撒粉機、噴霧器與撒粒機、藉由加入灌溉或稻田水，以及藉由其他本技術領域習知之常規方法，施加至雜草或其部位。
本文所述之實施例與下列範例係用於說明本發明之用途，而非旨在侷限本發明主張之範疇。此述組成物之其他修飾、用途或組合，為熟習此技術領域者所顯而易見，而不脫離後附申請專利範圍之精神與範疇。
將欲檢測植物品種之種子或小堅果種植於土壤基質中，其製備係以80與20之比例混合壤土或砂質壤土(例如，28.6百分比之粉砂、18.8百分比之黏土與52.6百分比之砂粒，伴隨pH值約5.8及約1.8百分比之有機質含量)與鈣質砂礫。將土壤基質置於塑膠盆中，其體積為1夸脫且表面積為83.6平方公分(cm2)。當需要確保良好發芽率與健康之植物時，進行殺菌劑處理，及/或其他化學性或物理性處理。
植物於溫室內生長8-22天，其中每日光照期約14小時，並於日間維持約29℃，且夜間維持約26℃。視需要於灌溉液中加入營養物(Peters Excel® 15-5-15 5-Ca 2-Mg與鐵螯合物)並定期加水。視需要以懸吊式金屬鹵素1000瓦燈管提供輔助照明。當植物到達第一至第四真葉期時進行檢測。
所進行之處理係由4-胺基-3-氯-5-氟-6-(4-氯-2-氟-3-甲氧基-苯基)吡啶-2-羧酸(化合物A)之酸類或酯類，其每一者皆配製成SC(懸浮濃縮物)、各種除草成分之單獨形式，與其結合物，組成。化合物A之形式係以酸當量為基礎施加。
經檢測之化合物A(式I化合物)之形式包括：
依據欲檢測之施加率、配方中活性成分濃度或酸當量，計算處理需求量，故以施加率187 L/ha與施加體積12 mL施加。
在含配方化合物之處理方面，將測得之化合物量個別置於25 mL玻璃瓶中，並以一定體積之1.25%(v/v)Agri-Dex®作物油濃縮物稀釋，以取得12X儲液。若受測化合物不易溶解，可加熱及/或超音波震盪該混合物。施加溶液之製備，係以10 mL之1.25%(v/v)作物油濃縮物之水性混合物，稀釋各適量儲液(例如，1 mL)，取得適當之最終濃度，因而最終之噴霧溶液含有1.25+/-0.05%(v/v)作物油濃縮物。
在含技術級化合物之處理方面，將秤重之化合物量個別置於25 mL玻璃瓶中，並以一定體積之97：3 v/v丙酮/DMSO溶解，以取得12X儲液。若受測化合物不易溶解，
可加熱及/或超音波震盪該混合物。施加溶液之製備，可以10 mL之1.5%(v/v)作物油濃縮物之水性混合物，稀釋各適量儲液(例如，1 mL)，取得適當之最終濃度，因而最終之噴霧溶液含有1.25%(v/v)作物油濃縮物。當使用技術級材料時，可將經濃縮之儲液加入噴霧溶液，因而施加溶液中丙酮與DMSO之最終濃度分別為16.2%與0.5%。
在含配方與技術級化合物之處理方面，將秤重之技術級材料量個別置於25 mL玻璃瓶，並以一定體積之97：3 v/v丙酮/DMSO溶解，以取得12X儲液，而測得之配方化合物量可個別置於25 mL玻璃瓶中，並以一定體積之1.5%(v/v)作物油濃縮物或水稀釋，以取得12X儲液。若受測化合物不易溶解，可加熱及/或超音波震盪該混合物。施加溶液之製備，係以適量之1.5%(v/v)作物油濃縮物之水性混合物或水，稀釋各適量儲液(例如，1 mL)，取得適當之最終濃度，因而最終之噴霧溶液含有1.25%(v/v)作物油濃縮物。視需要，將額外之水及/或97：3 v/v丙酮/DMSO加入個別施加溶液中，因而施加溶液中丙酮與DMSO之最終濃度相較後分別為8.1%與0.25%。
於施加前，所有儲液與施加溶液皆目視檢查其化合物相容性。以配備8002E噴嘴之懸吊式曼德爾(Mandel)履帶噴霧器，將噴霧溶液施加至植物材料，其經較準可於平均植物冠層高度上方18至20英吋(46至50 cm)之噴灑高度，以187 L/ha噴灑0.503 m2之施加面積。以溶劑空白配方於相同條件下噴灑對照組植物。
將處理組植物與對照組植物置於前述之溫室中，並以地下灌溉方式加水，以防受測化合物被洗出。大約3週後，以目視判斷受測植物之狀況，且相較於未處理組植物，並以0至100之百分比規模計分，其中0代表無損傷或生長抑制，而100代表完全死亡。
以科爾比方程式計算混合物之預期除草功效(Colby,S.R.1967.Calculation of the synergistic and antagonistic response of herbicide combinations.Weeds 15：20-22.)。
利用下列方程式計算含兩種活性成分A與B之混合物預期活性：預期值=A+B-(A x B/100)
A=混合物中使用相同濃度之活性成分A所觀察到之功效。
B=混合物中使用相同濃度之活性成分B所觀察到之功效。
受測化合物、所使用施加率、受測植物品種，以及實驗結果皆列於表1-9。
gae/ha=克酸當量/公頃
gai/ha=活性成分/公頃
Obs=觀察值
Exp=經由科爾比方程式計算之預期值
DAA=施加後天數
將欲檢測植物品種之雜草種子或小堅果種植於泥坑土中(泥漿)，其製備係以體積比1：1混合經切碎、未滅菌之礦質土壤(50.5百分比之粉砂、25.5百分比之黏土與24百分比之砂粒，伴隨pH值約7.6及約2.9百分比之有機質含量)與水。經製備之泥漿各以365 mL分裝至16盎司、表面積為86.59平方公分(cm2)之非穿孔型塑膠盆，各盆保留3公分之頂部空間。於種植或插秧前，泥漿進行隔夜乾燥。於塑膠穴盤中，以Sun Gro MetroMix® 306種植混合物種植稻米種子，其一般具有pH 6.0至6.8與約30%之有機質含量。於除草劑施加4日前，將第二或第三葉生長階段之幼苗，插秧至含840 mL泥漿之32-oz且表面積為86.59 cm2之非穿孔型塑膠盆中。塑膠盆頂部空間填上2.5至3 cm之水以形成稻田。當需要確保良好發芽率與健康之植物時，則進行殺菌劑處理及/或其他化學性或物理性處理。植物於溫室內生長4-22天，其中每日光照期約14小時，並於日間維持約29℃，夜間維持約26℃。以16盎司盆2 g與32盎司盆4 g之量添加營養物Osmocote®(19：6：12，N：P：K+微量營養物)。定期加水以
維持稻田浸水量，並視需要以懸吊式金屬鹵素1000瓦燈管提供輔助照明。當植物到達第一至第四真葉期時進行檢測。
所進行之處理係由4-胺基-3-氯-5-氟-6-(4-氯-2-氟-3-甲氧基-苯基)吡啶-2-羧酸(化合物A)之酸類或酯類，其每一者皆配製成SC、各種除草成分之單獨形式，與其結合物，組成。化合物A之形式係以酸當量為基礎施加。
經檢測之化合物A(式I化合物)之形式包括：
依據欲檢測之施加率、配方中活性成分濃度或酸當量、每盆每一成分施加體積為2 mL，每盆施加面積為86.59 cm2，計算各化合物或除草成分之處理需求量。
在配方化合物方面，將測得之量分別置於100或200 mL玻璃瓶，並以一定體積之1.25%(v/v)Agri-Dex®作物油濃縮物溶解，以取得各施加溶液。若受測化合物不易溶解，可加熱及/或超音波震盪該混合物。
在技術級化合物方面，將秤重之量分別置於100至200 mL玻璃瓶中，並以一定體積之丙酮溶解，以取得經濃縮儲液。若受測化合物不易溶解，可加熱及/或超音波震盪該混合物。以等體積之含2.5%(v/v)作物油濃縮物之水性混合物，稀釋所得之經濃縮儲液，因而最終之施加溶液含有1.25%(v/v)作物油濃縮物。
以移液器取適量之施加溶液，並單獨地與依序地注入稻田水層中，以完成施加。於相同條件下，以溶劑空白配方處理對照組植物。完成施加後，所有經處理植物材料皆接受相同濃度之丙酮與作物油濃縮物。
將處理組植物與對照組植物置於前述之溫室中，並視需要加水以維持稻田浸水量。大約3週後，以目視
判斷受測植物之狀況，相較於未處理組植物，並以0至100之百分比規模計分，其中0代表無損傷或生長抑制，而100代表完全死亡。
以科爾比方程式計算混合物之預期除草功效(Colby,S.R.1967.Calculation of the synergistic and antagonistic response of herbicide combinations.Weeds 15：20-22.)。
利用下列方程式計算含兩種活性成分A與B之混合物預期活性：預期值=A+B-(A x B/100)
A=混合物中使用相同濃度之活性成分A所觀察到之功效。
B=混合物中使用相同濃度之活性成分B所觀察到之功效。
一些受測化合物、所使用施加率、受測植物品種，以及實驗結果皆列於表10-15。
於表面積103.2平方公分(cm2)之塑膠穴盤中，以Sun Gro MetroMix® 306種植混合物種植欲檢測植物品種之種子，其一般具有pH 6.0至6.8，與約30%之有機質含量。當需要確保良好發芽率與健康之植物時，則進行殺菌劑處理及/或其他化學性或物理性處理。植物於溫室內生長7-36天，其中每日光照期約14小時，並於日間維持約18℃且夜間維持約17℃。定期加入營養物與水，並視需要以懸吊式金屬鹵素1000瓦燈管提供輔助照明。當植物到達第二或第三真葉期時進行檢測。
所進行之處理係由4-胺基-3-氯-5-氟-6-(4-氯-2-氟-3-甲氧基-苯基)吡啶-2-羧酸(化合物A)之芐基酯，其配製成SC、第二種穀類除草劑之單獨形式，與其結合物，組成。
經檢測之化合物A(式I化合物)之形式包括：
其他除草成分之施加，係以活性成分為基礎，並包括乙醯乳酸合成酶(ALS)抑制性除草劑(磺醯胺化學級)，其中雙氟磺草胺之配方為Derby®，且啶磺草胺之配方為PowerFlex®。將經測量之4-胺基-3-氯-5-氟-6-(4-氯-2-氟-3-甲氧基-苯基)吡啶-2-羧酸(化合物A)之芐基酯，等分置於25毫升(mL)玻璃瓶中，並以一定量之1.25%(v/v)Agri-Dex®作物油濃縮物稀釋，以取得儲液。化合物之需求量係依據每公頃187公升(L/ha)之施加率，與12 mL之施加體積而定。第二種穀類除草劑之噴霧溶液與實驗化合物混合物之製備，係以儲液加入適量稀釋液中，以形成具有活性成分之12 mL噴霧溶液之二與三方組合物。以配備8002E噴嘴之懸吊式曼德爾履帶噴霧器，將配製之化合物施加至植物材料，其經較準可於平均植物冠層高度上方18英吋(46 cm)之噴灑高度，以187 L/ha噴灑至一施加面積0.503平方公尺(m2)。於相
同條件下，以溶劑空白配方噴灑對照組植物。
將處理組植物與對照組植物置於前述之溫室中，並以地下灌溉方式加水，以防受測化合物被洗出。於20-22天後，以目視判斷受測植物之狀況，且相較於未處理組植物，並以0至100之百分比規模計分，其中0代表無損傷且100代表完全死亡。
以科爾比方程式計算混合物之預期除草功效(Colby,S.R.1967.Calculation of the synergistic and antagonistic response of herbicide combinations.Weeds 15：20-22.)。
利用下列方程式計算含兩種活性成分A與B混合物之預期活性：預期值=A+B-(A x B/100)
A=混合物中使用相同濃度之活性成分A所觀察到之功效。
B=混合物中使用相同濃度之活性成分B所觀察到之功效。
受測化合物、所使用施加率、受測植物品種，以及實驗結果皆列於表16-18。
於哥倫比亞Tolima；希臘Thessaloniki；義大利
Ottobiano與Copiano；美國Greenville,MS與Eagle Lake,TX之田野條件下，進行多個出苗後之田野試驗；以及於日本Ryugasaki測試水注式處置。試驗地點皆位於直播稻米(栽培稻；Oryza sativa)之商業生產區，並以標準除草劑小區研究法進行，於日本除外，其田野試驗使用插秧稻米。出苗後之試驗區大小發生變化，由2 m(公尺)x 5 m改為3 m x 8 m(寬度x長度)，且每組4重複。水注試驗區之大小為2 x 2 m，且每組3重複。稻米作物以正常栽培方法進行施肥、播種、澆水、浸水與維護，以確保作物與雜草之良好生長。
出苗後田野試驗之所有處理皆以配備扇形噴嘴(80°或110°)之後背式壓縮空氣/氣體噴霧器進行施加，其經校準，以約200-400 kPa之噴嘴壓力，施加187至300 L/ha之噴灑體積。在日本，以水注方式進行各處理組之施加，其中各重複組皆以指定量之商業產品混入100 ml水中，並直接加入含作物與雜草之3 cm深水中。所進行之處理係由4-胺基-3-氯-5-氟-6-(4-氯-2-氟-3-甲氧基-苯基)吡啶-2-羧酸(化合物A)之芐基酯，其配製成SC(懸浮濃縮物)、各種除草成分之單獨形式，與其結合物，組成。
經檢測之化合物A(式I化合物)之形式包括：
以適當之產品配方比例將商業上購得之平速爛(Viper 20OD®(歐洲)、Grasp 240SC®(美國)與Wideattack 37.5SC®(日本))產品，混合於水中以達到所欲之比例，並依據單位施加面積(公頃)達到所欲之施加率。於施加15至56天後(DAA)，評估處理狀況並相較於未處理之對照組植物。目視之雜草控制係以0至100之百分比規模計分，其中0代表無損傷且100代表完全死亡。
所有的單獨產品與混合物之處理結果，皆為3至4個重複組之平均。試驗地點具有天然雜草族群。該雜草族群包括但不限於，闊葉信號草(寬葉臂形草或扁葉尾稃草，BRAPP)、莎草(異花莎草，CYPDI)、黃莎草(油莎草，CYPES)、義大利野間之多種稗屬物種(ECHSS)(經混合之ECHSS生物型)、亞馬遜千金子(類黍千金子(J.Presl)A.S.Hitchc.,LEFPA)，以及日本蘆葦(大井氏水莞(Roxb.)Palla,SCPJU)。
受測化合物、所使用施加率、受測植物品種，以及作物田野試驗之實驗結果皆列於表19-21。
CYPES 油莎草 黃莎草
ECHSS 稗屬
SCPJU 大井氏水莞 日本蘆葦
gae/ha=克酸當量/公頃
gai/ha=活性成分/公頃
Obs=觀察值
Exp=經由科爾比方程式計算之預期值
DAA=施加後天數
Claims (13)
- 一種協同性除草組成物，其包含一除草有效量之(a)式(I)化合物
- 如請求項1之組成物，其中(a)為式(I)化合物、式(I)化合物之C1-4烷基酯，或式(I)化合物之芐基酯。
- 如請求項1至2任一項之組成物，其中(b)為至少一個選自於由下列所構成之族群中的化合物，或者其農業上可接受之鹽類、羧酸、羧酸鹽或酯類：氯酯磺草胺-甲酯(cloransulam-methyl)、雙氯磺草胺(diclosulam)、雙氟磺草胺(florasulam)、唑嘧磺草胺(flumetsulam)、磺草唑胺(metosulam)、平速爛(penoxsulam)，以及啶磺草胺(pyroxsulam)。
- 如請求項1至3任一項之組成物，其更包含一農業上可接受之佐劑或載劑。
- 如請求項1至4任一項之組成物，其更包含一除草劑安全劑。
- 一種控制不良植被之方法，其包含以一除草有效量之(a)式(I)化合物
- 如請求項6之方法，其中(a)為式(I)化合物、式(I)化合物之C1-4烷基酯，或式(I)化合物之芐基酯。
- 如請求項6至7任一項之方法，其中(b)為至少一個選自於由下列所構成之族群中的化合物，或者其農業上可接受之鹽類、羧酸、羧酸鹽或酯類：氯酯磺草胺-甲酯、雙氯磺草胺、雙氟磺草胺、唑嘧磺草胺、磺草唑胺、平速爛，以及啶磺草胺。
- 如請求項6至8任一項之方法，其中該不良植被在經直播、湛水直播與插秧之稻米、穀類、小麥、大麥、燕麥、黑麥、高粱、玉蜀黍/玉米、甘蔗、向日葵、芸苔、油菜、甜菜、大豆、棉花、鳳梨、牧草、草地、牧場、休耕地、草皮、樹與藤園、水生植物、工業植被管理(IVM)或道路維護(ROW)中被控制。
- 如請求項6至9任一項之方法，其中(a)與(b)於雜草或作 物出苗前施加。
- 如請求項6至10任一項之方法，其中該不良植被在具草甘膦(glyphosate)-、5-烯醇丙酮基莽草酸-3-磷酸鹽(EPSP)合成酶抑制劑-、固殺草(glufosinate)-、麩胺醯胺酸合成酶抑制劑-、麥草畏(dicamba)-、苯氧基生長素-、吡啶基氧基生長素-、合成生長素-、生長素運輸抑制劑-、芳基氧基苯氧基丙酸酯-、環己烷二酮-、苯基吡唑啉-、乙醯輔酶A羧化酶(ACCase)抑制劑-、咪唑啉酮-、磺醯基脲-、嘧啶基硫代苯甲酸酯-、三唑并嘧啶-、磺醯基胺基羰基三唑酮-、乙醯乳酸合成酶(ALS)或乙醯羥酸合成酶(AHAS)抑制劑-、4-羥基苯基-丙酮酸二氧酶(HPPD)抑制劑-、八氫番茄紅素去飽和酶(phytoene desaturase)抑制劑-、類胡蘿蔔素生合成抑制劑-、原紫質原(protoporphyrinogen)氧化酶(PPO)抑制劑-、纖維素生合成抑制劑-、有絲分裂抑制劑-、微管抑制劑-、極長鏈脂肪酸抑制劑-、脂肪酸與脂質生合成抑制劑-、光合系統I抑制劑-、光合系統II抑制劑-、三嗪-，或溴苯腈(bromoxynil)-耐受性之作物中被控制。
- 如請求項11之方法，其中該耐受性作物具有多個或複合性狀，對於多種除草劑或多重作用模式具有耐受性。
- 如請求項6至12之方法，其中該不良植被包含具除草劑抗性或耐受性之雜草。
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| Application Number | Priority Date | Filing Date | Title |
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| US201261675037P | 2012-07-24 | 2012-07-24 | |
| US61/675,037 | 2012-07-24 | ||
| US13/832,978 US8906825B2 (en) | 2012-07-24 | 2013-03-15 | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and triazolopyrimidine sulfonamides |
| US13/832,978 | 2013-03-15 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW102126125A TWI662896B (zh) | 2012-07-24 | 2013-07-22 | 包含４－胺基－３－氯－５－氟－６－（４－氯－２－氟－３－甲氧基苯基）吡啶－２－羧酸或其衍生物以及三唑并嘧啶磺醯胺之除草組成物 |
Country Status (31)
| Country | Link |
|---|---|
| US (1) | US8906825B2 (zh) |
| EP (1) | EP2877007B1 (zh) |
| JP (1) | JP6255398B2 (zh) |
| KR (1) | KR102089384B1 (zh) |
| CN (1) | CN104602528B (zh) |
| AR (1) | AR091892A1 (zh) |
| AU (1) | AU2013293303B2 (zh) |
| BR (1) | BR102013018646B8 (zh) |
| CA (1) | CA2880088C (zh) |
| CL (1) | CL2015000164A1 (zh) |
| CO (1) | CO7200268A2 (zh) |
| DK (1) | DK2877007T3 (zh) |
| ES (1) | ES2724213T3 (zh) |
| FR (1) | FR23C1009I2 (zh) |
| HK (1) | HK1209588A1 (zh) |
| IL (1) | IL236860B (zh) |
| IN (1) | IN2015DN01387A (zh) |
| MX (1) | MX376864B (zh) |
| MY (1) | MY172122A (zh) |
| NZ (1) | NZ704889A (zh) |
| PE (2) | PE20150983A1 (zh) |
| PH (1) | PH12015500143A1 (zh) |
| PL (1) | PL2877007T3 (zh) |
| PT (1) | PT2877007T (zh) |
| RU (2) | RU2017128209A (zh) |
| SA (1) | SA113340740B1 (zh) |
| TW (1) | TWI662896B (zh) |
| UA (1) | UA114110C2 (zh) |
| UY (1) | UY34938A (zh) |
| WO (1) | WO2014018390A1 (zh) |
| ZA (1) | ZA201501135B (zh) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104604892A (zh) * | 2014-12-22 | 2015-05-13 | 广东中迅农科股份有限公司 | 含有氟氯吡啶酯和唑草酮以及啶磺草胺的除草组合物 |
Families Citing this family (33)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PL2514314T3 (pl) | 2007-08-27 | 2017-08-31 | Dow Agrosciences Llc | Synergistyczna kompozycja chwastobójcza zawierająca pewne kwasy pirydynokarboksylowe oraz pewne herbicydy stosowane w uprawie zbóż i ryżu |
| US8889591B2 (en) | 2012-07-24 | 2014-11-18 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl)pyridine-2-carboxylic acid or a derivative thereof and bromobutide, daimuron, oxaziclomefone or pyributicarb |
| US8916499B2 (en) | 2012-07-24 | 2014-12-23 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and a protoporphyrinogen oxidase inhibitor |
| US8809232B2 (en) * | 2012-07-24 | 2014-08-19 | Dow Agroscience Llc | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and halosulfuron, pyrazosulfuron and esprocarb |
| US8912121B2 (en) | 2012-07-24 | 2014-12-16 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl)pyridine-2-carboxylic acid or a derivative thereof and certain PS II inhibitors |
| US8846570B2 (en) | 2012-07-24 | 2014-09-30 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl)pyridine-2-carboxylic acid or a derivative thereof and microtubule inhibiting herbicides |
| US8912120B2 (en) | 2012-07-24 | 2014-12-16 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and synthetic auxin herbicides |
| US8841233B2 (en) * | 2012-07-24 | 2014-09-23 | Dow Agrosciences Llc | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and 4-hydroxyphenyl-pyruvate dioxygenase (HPPD) inhibitors |
| US8883682B2 (en) | 2012-07-24 | 2014-11-11 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl)pyridine-2-carboxylic acid or a derivative thereof and auxin transport inhibitors |
| US8791048B2 (en) * | 2012-07-24 | 2014-07-29 | Dow Agrosciences Llc | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and clomazone |
| US8871681B2 (en) * | 2012-07-24 | 2014-10-28 | Dow Agrosciences Llc | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and certain sulfonylureas |
| US9644469B2 (en) | 2012-07-24 | 2017-05-09 | Dow Agrosciences Llc | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and VLCFA and lipid synthesis inhibiting herbicides |
| US8796177B2 (en) * | 2012-07-24 | 2014-08-05 | Dow Agrosciences Llc | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl)pyridine-2-carboxylic acid or a derivative thereof and acetyl-CoA carboxylase (ACCase) inhibitors |
| US8906826B2 (en) | 2012-07-24 | 2014-12-09 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and imidazolinones |
| US8901035B2 (en) | 2012-07-24 | 2014-12-02 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and cellulose biosynthesis inhibitor herbicides |
| US8871680B2 (en) * | 2012-07-24 | 2014-10-28 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and a di-methoxy-pyrimidine and derivatives thereof |
| US20140031224A1 (en) * | 2012-07-24 | 2014-01-30 | Dow Agrosciences Llc | Safened herbicidal compositions including 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl)pyridine-2-carboxylic acid or a derivative thereof for use in rice |
| US8895470B2 (en) | 2012-07-24 | 2014-11-25 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and glyphosate or glufosinate |
| RU2658667C2 (ru) * | 2013-03-15 | 2018-06-22 | ДАУ АГРОСАЙЕНСИЗ ЭлЭлСи | Гербицидно-антидотные композиции, включающие 4-амино-3-хлор-5-фтор-6-(4-хлор-2-фтор-3-метоксифенил)пиридин-2-карбоновую кислоту или ее производное, для применения в кукурузе (маисе) |
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| CN104585189B (zh) * | 2014-12-22 | 2018-02-06 | 广东中迅农科股份有限公司 | 含有氟氯吡啶酯和吡草醚以及啶磺草胺的除草组合物 |
| EA026986B1 (ru) * | 2015-02-17 | 2017-06-30 | Акционерное общество "Щелково Агрохим" | Гербицидная композиция для защиты посевов кукурузы |
| WO2017044556A1 (en) * | 2015-09-08 | 2017-03-16 | Dow Agrosciences Llc | Herbicidal compositions containing 4-amino-3-chloro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof, a triazolopyrimidine sulfonamide herbicide or a derivative thereof, and glyphosate or a derivative thereof |
| EP3386306A4 (en) * | 2015-12-08 | 2019-07-10 | Dow AgroSciences LLC | HERBICIDAL COMPOSITIONS WITH 4-AMIN-3-CHLOR-6 (4-CHLORO-2-FLUORO-3-METHOXYPHENYL) PYRIDINE-2-CARBOXYLIC ACID, FLORASULAM AND PYROXSULAM OR DERIVATIVES THEREOF |
| CN106234391A (zh) * | 2016-08-04 | 2016-12-21 | 北京燕化永乐生物科技股份有限公司 | 一种复配除草剂 |
| CN111820228A (zh) * | 2019-04-19 | 2020-10-27 | 江苏省农垦生物化学有限公司 | 一种组合除草剂及生产方法 |
| CN114586798A (zh) * | 2021-04-02 | 2022-06-07 | 江苏富田农化有限公司 | 一种除杂草组合物及其除草剂 |
| CN115707382A (zh) * | 2021-08-20 | 2023-02-21 | 佛山市盈辉作物科学有限公司 | 一种含五氟磺草胺、丙草胺和氯氟吡啶酯的除草组合物 |
| WO2023114652A1 (en) | 2021-12-16 | 2023-06-22 | Corteva Agriscience Llc | Method of applying a composition comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof |
| WO2023192088A1 (en) * | 2022-03-29 | 2023-10-05 | Corteva Agriscience Llc | A method of weed control in sugar beet |
| CN115735930B (zh) * | 2022-12-28 | 2024-01-30 | 安徽众邦生物工程有限公司 | 一种含氯氟吡啶酯、五氟磺草胺和异恶草松的除草组合物 |
| CN115777714B (zh) * | 2022-12-28 | 2024-06-28 | 安徽众邦生物工程有限公司 | 一种含氯氟吡啶酯、五氟磺草胺和丙草胺的除草组合物 |
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| US20080234130A1 (en) | 2005-08-24 | 2008-09-25 | Pioneer Hi-Bred International, Inc. | Compositions providing tolerance to multiple herbicides and methods of use thereof |
| RU2428416C2 (ru) | 2006-01-13 | 2011-09-10 | Дау Агросайенсиз Ллс | 6-(полизамещенный арил)-4-аминопиколинаты и их применение в качестве гербицидов |
| PL2514314T3 (pl) | 2007-08-27 | 2017-08-31 | Dow Agrosciences Llc | Synergistyczna kompozycja chwastobójcza zawierająca pewne kwasy pirydynokarboksylowe oraz pewne herbicydy stosowane w uprawie zbóż i ryżu |
| EP2191719A1 (de) | 2008-11-29 | 2010-06-02 | Bayer CropScience AG | Herbizid-Safener-Kombination |
| WO2011043876A1 (en) | 2009-10-07 | 2011-04-14 | Dow Agrosciences Llc | Synergistic fungicidal composition containing 5-fluorocytosine for fungal control in cereals |
| PL2555615T3 (pl) | 2010-02-19 | 2014-09-30 | Dow Agrosciences Llc | Synergistyczna herbicydowo/fungicydowa kompozycja zawierająca kwas 4-amino-3-chloro-6-(4-chloro-2-fluoro-3-metoksyfenylo)pirydyno-2-karboksylowy oraz fungicyd |
| UA109797C2 (uk) | 2010-11-05 | 2015-10-12 | Спосіб боротьби з бур'янами, що мають стійкість до гербіцидів на основі феноксіалканових кислот, за допомогою 4-аміно-3-хлор-6-(4-хлор-2-фтор-3-метоксифеніл)піридин-2-карбонової кислоти і її солей або складних ефірів | |
| TWI596088B (zh) | 2011-01-25 | 2017-08-21 | 陶氏農業科學公司 | ４－胺基－６－（經取代的苯基）吡啶甲酸酯及６－胺基－２－（經取代的苯基）－４－嘧啶羧酸酯之芳烷酯以及其等作為除草劑之用途 |
| BR102012027933A2 (pt) | 2011-11-01 | 2015-11-17 | Dow Agrosciences Llc | composições pesticidas estáveis |
| US8871680B2 (en) | 2012-07-24 | 2014-10-28 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and a di-methoxy-pyrimidine and derivatives thereof |
| US8916499B2 (en) | 2012-07-24 | 2014-12-23 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and a protoporphyrinogen oxidase inhibitor |
| US8895470B2 (en) | 2012-07-24 | 2014-11-25 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and glyphosate or glufosinate |
| US8883682B2 (en) | 2012-07-24 | 2014-11-11 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl)pyridine-2-carboxylic acid or a derivative thereof and auxin transport inhibitors |
| US8912121B2 (en) | 2012-07-24 | 2014-12-16 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl)pyridine-2-carboxylic acid or a derivative thereof and certain PS II inhibitors |
| US8846570B2 (en) | 2012-07-24 | 2014-09-30 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl)pyridine-2-carboxylic acid or a derivative thereof and microtubule inhibiting herbicides |
| US9644469B2 (en) | 2012-07-24 | 2017-05-09 | Dow Agrosciences Llc | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and VLCFA and lipid synthesis inhibiting herbicides |
| US8889591B2 (en) | 2012-07-24 | 2014-11-18 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl)pyridine-2-carboxylic acid or a derivative thereof and bromobutide, daimuron, oxaziclomefone or pyributicarb |
| US8871681B2 (en) | 2012-07-24 | 2014-10-28 | Dow Agrosciences Llc | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and certain sulfonylureas |
| US8901035B2 (en) | 2012-07-24 | 2014-12-02 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and cellulose biosynthesis inhibitor herbicides |
| US8841233B2 (en) | 2012-07-24 | 2014-09-23 | Dow Agrosciences Llc | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and 4-hydroxyphenyl-pyruvate dioxygenase (HPPD) inhibitors |
| US8906826B2 (en) | 2012-07-24 | 2014-12-09 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and imidazolinones |
| US8912120B2 (en) | 2012-07-24 | 2014-12-16 | Dow Agrosciences, Llc. | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and synthetic auxin herbicides |
| US8796177B2 (en) | 2012-07-24 | 2014-08-05 | Dow Agrosciences Llc | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl)pyridine-2-carboxylic acid or a derivative thereof and acetyl-CoA carboxylase (ACCase) inhibitors |
| US8809232B2 (en) | 2012-07-24 | 2014-08-19 | Dow Agroscience Llc | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and halosulfuron, pyrazosulfuron and esprocarb |
| US8791048B2 (en) | 2012-07-24 | 2014-07-29 | Dow Agrosciences Llc | Herbicidal compositions comprising 4-amino-3-chloro-5-fluoro-6-(4-chloro-2-fluoro-3-methoxyphenyl) pyridine-2-carboxylic acid or a derivative thereof and clomazone |
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2013
- 2013-03-15 US US13/832,978 patent/US8906825B2/en active Active
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- 2013-07-19 PE PE2015000075A patent/PE20150983A1/es not_active Application Discontinuation
- 2013-07-19 PE PE2019001024A patent/PE20191302A1/es unknown
- 2013-07-19 IN IN1387DEN2015 patent/IN2015DN01387A/en unknown
- 2013-07-19 RU RU2017128209A patent/RU2017128209A/ru not_active Application Discontinuation
- 2013-07-19 NZ NZ704889A patent/NZ704889A/en not_active IP Right Cessation
- 2013-07-19 JP JP2015524336A patent/JP6255398B2/ja active Active
- 2013-07-19 CN CN201380045690.6A patent/CN104602528B/zh active Active
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- 2013-07-19 UA UAA201501577A patent/UA114110C2/uk unknown
- 2013-07-19 WO PCT/US2013/051289 patent/WO2014018390A1/en not_active Ceased
- 2013-07-19 KR KR1020157004625A patent/KR102089384B1/ko active Active
- 2013-07-19 EP EP13822211.2A patent/EP2877007B1/en active Active
- 2013-07-19 PL PL13822211T patent/PL2877007T3/pl unknown
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- 2013-07-19 RU RU2015105953A patent/RU2629217C2/ru active
- 2013-07-19 DK DK13822211.2T patent/DK2877007T3/en active
- 2013-07-19 MX MX2015001142A patent/MX376864B/es active IP Right Grant
- 2013-07-22 BR BR102013018646A patent/BR102013018646B8/pt active IP Right Grant
- 2013-07-22 TW TW102126125A patent/TWI662896B/zh active
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- 2013-07-24 AR ARP130102637A patent/AR091892A1/es active IP Right Grant
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104604892A (zh) * | 2014-12-22 | 2015-05-13 | 广东中迅农科股份有限公司 | 含有氟氯吡啶酯和唑草酮以及啶磺草胺的除草组合物 |
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