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TW201303057A - Method for detecting effective power deviations in microwaves in plasma processing devices, and plasma processing device - Google Patents

Method for detecting effective power deviations in microwaves in plasma processing devices, and plasma processing device Download PDF

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Publication number
TW201303057A
TW201303057A TW101111241A TW101111241A TW201303057A TW 201303057 A TW201303057 A TW 201303057A TW 101111241 A TW101111241 A TW 101111241A TW 101111241 A TW101111241 A TW 101111241A TW 201303057 A TW201303057 A TW 201303057A
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microwave
plasma
plasma processing
processing container
processing apparatus
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TW101111241A
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Chinese (zh)
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Masaki Sano
Yoshinori Osaki
Jiro Katsuki
Koji Maekawa
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Tokyo Electron Ltd
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/32Gas-filled discharge tubes
    • H01J37/32009Arrangements for generation of plasma specially adapted for examination or treatment of objects, e.g. plasma sources
    • H01J37/32192Microwave generated discharge
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/32Gas-filled discharge tubes
    • H01J37/32009Arrangements for generation of plasma specially adapted for examination or treatment of objects, e.g. plasma sources
    • H01J37/32192Microwave generated discharge
    • H01J37/32266Means for controlling power transmitted to the plasma

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  • Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • Plasma & Fusion (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Plasma Technology (AREA)
  • Drying Of Semiconductors (AREA)

Abstract

This method finds effective power deviations in microwaves that arise among a plurality of plasma processing devices. Processing gas is supplied at a prescribed pressure to an evacuated processing vessel (12) and the vessel sealed. Microwaves are introduced into the sealed processing vessel at a prescribed electric power, and gas plasma for processing is generated. The change in the pressure in the processing vessel before plasma generation and the pressure in the processing vessel after plasma generation is measured, and the effective power deviation for the microwaves in the plasma processing device and the other plasma processing device is found on the basis of a correlative relation for the variation width for the pressure in another plasma processing device that is found in advance and forms a standard and the electric power for supplying the microwaves.

Description

電漿處理裝置中之微波實際功率的偏差量檢測方法及其電漿處理裝置 Method for detecting deviation of microwave actual power in plasma processing device and plasma processing device thereof

本發明關於一種在對被處理體進行電漿處理之電漿處理裝置中,檢測相異的複數電漿處理裝置間所產生之微波實際功率的偏差量之方法,以及電漿處理裝置。 The present invention relates to a method for detecting a deviation amount of actual microwave power generated between different plural plasma processing apparatuses in a plasma processing apparatus for plasma-treating a processed object, and a plasma processing apparatus.

在半導體元件的製造中,為了使用於以例如CMOS的閘極絕緣膜為首之各種用途,係進行矽氧化膜或矽氮化膜的形成。形成該矽氧化膜或矽氮化膜的方法已知有加熱矽基板來進行之熱氧化處理、熱氮化處理,或藉由電漿來對矽基板表面進行電漿處理之氮化處理或氧化處理之方法(例如專利文獻1)。 In the manufacture of a semiconductor element, in order to be used for various applications such as a gate insulating film of CMOS, formation of a tantalum oxide film or a tantalum nitride film is performed. A method of forming the tantalum oxide film or the tantalum nitride film is known as a thermal oxidation treatment, a thermal nitridation treatment by heating a tantalum substrate, or a nitriding treatment or oxidation by plasma treatment of a surface of a tantalum substrate by plasma. Method of treatment (for example, Patent Document 1).

上述電漿處理通常係在使用微波等來產生電漿之電漿處理裝置中進行。電漿處理裝置中係透過導波管、天線、介電體窗來將微波震盪器所產生之微波導入至處理容器,而生成包含有被供應至處理容器內的氧氣或氮氣之氣體的電漿。然後,藉由該氧氣的電漿或氮氣的電漿來對矽基板表面進行電漿處理,而於矽基板表面形成矽氧化膜或矽氮化膜。 The above plasma treatment is usually carried out in a plasma processing apparatus that uses microwaves or the like to generate plasma. In the plasma processing apparatus, the microwave generated by the microwave oscillator is introduced into the processing container through the waveguide, the antenna, and the dielectric window to generate a plasma containing the gas supplied to the oxygen or nitrogen in the processing container. . Then, the surface of the tantalum substrate is subjected to plasma treatment by plasma of the oxygen or plasma of nitrogen, and a tantalum oxide film or a tantalum nitride film is formed on the surface of the tantalum substrate.

專利文獻1:日本特開2003-115587號公報 Patent Document 1: Japanese Laid-Open Patent Publication No. 2003-115587

然而,上述般的電漿處理裝置縱使在相同條件下進行電漿處理,仍會有複數電漿處理裝置間形成於基 板表面之氧化膜的膜厚或氮濃度等有所差異之情事。如此地,若在裝置間發生電漿處理後的膜厚等有所差異,則會有產品品質上的問題。 However, in the above-described plasma processing apparatus, even if the plasma treatment is performed under the same conditions, a plurality of plasma processing apparatuses are formed in the base. The film thickness or nitrogen concentration of the oxide film on the surface of the plate varies. As described above, there is a problem in product quality if the film thickness or the like after the plasma treatment occurs between the devices.

上述裝置間差異的發生原因其中之一,推測為在對處理容器內供應微波的情況,會因該微波的經過路徑、電漿生成機構的組件、處理容器等的接合等之差異,而導致處理容器內電漿生成所消耗之微波的電功率,亦即微波的實際功率因某種原因而產生偏差。 One of the causes of the difference between the above-mentioned devices is presumed to be that the microwave is supplied to the processing container, and the processing is caused by the difference in the path of the microwave, the assembly of the plasma generating mechanism, the processing container, and the like. The electrical power of the microwaves generated by the plasma in the vessel, that is, the actual power of the microwaves, varies for some reason.

關於被供應至處理容器內之微波的電功率,可以電漿處理裝置所具備之控制部來進行監視,通常係依據該監視來控制微波的供應電功率。然而,即便是以控制部來監視,實際上,當微波被導入至處理容器內而生成電漿後,仍無法檢測電漿的微妙變化狀態,例如微波的電功率差異等。於是,上述裝置間所產生之電漿處理差異的原因便推測係因為導波管之後的天線部或介電體窗之微波傳播路徑中的尺寸公差、或裝置組裝時的組裝誤差,而導致微波傳播過程中的損失產生機差,因而便導致微波的實際功率產生差異。 The electric power supplied to the microwave in the processing container can be monitored by a control unit provided in the plasma processing apparatus, and the supply electric power of the microwave is usually controlled in accordance with the monitoring. However, even if it is monitored by the control unit, in fact, after the microwave is introduced into the processing container to generate plasma, it is impossible to detect a subtle change state of the plasma, such as a difference in electric power of the microwave. Therefore, the cause of the difference in plasma processing generated between the above devices is presumed to be due to dimensional tolerances in the microwave propagation path of the antenna portion or the dielectric window after the waveguide, or assembly errors during assembly of the device, resulting in microwaves. The loss in the propagation process creates a machine difference, which leads to a difference in the actual power of the microwave.

然而,由於並無定量地檢測微波的實際功率本身之方法,因此便無法求得實際功率的機差。於是,就目前來說便無法進行用以消除複數處理裝置間實際功率的機差之偏移(off-set)量調整,進而無法消除電漿處理裝置間電漿處理的差異。 However, since there is no method for quantitatively detecting the actual power of the microwave itself, the machine difference of the actual power cannot be obtained. Therefore, at present, the off-set amount adjustment for canceling the actual power between the complex processing devices cannot be performed, and the difference in plasma processing between the plasma processing devices cannot be eliminated.

本發明係鑑於上述問題點所發明者,其目的為求得電漿處理裝置間之微波實際功率的偏差量。 The present invention has been made in view of the above problems, and an object thereof is to obtain a deviation amount of microwave actual power between plasma processing apparatuses.

為了達成上述目的,本發明之電漿處理裝置中之微波實際功率的偏差量檢測方法係在藉由微波電漿來處理被處理體之電漿處理裝置中,求得複數電漿處理裝置間所產生之微波實際功率的偏差量之方法;該電漿處理裝置具有:微波產生部,係產生微波;處理容器,係上面呈開口,而用以進行電漿處理;壓力測量機構,係測量該處理容器內的壓力;介電體窗,係氣密地封閉該處理容器的開口部;天線,係配置在該介電體窗的上面;導波管,係使該微波產生部所產生之微波朝該天線傳播並導入至該處理容器;氣體供應部,係對該處理容器內供應氣體;以及排氣部,係將該處理容器內排氣;其中,係使用該電漿處理裝置,而以特定壓力來將氣體供應至排氣後的該處理容器內並加以密閉;以特定電功率將微波導入至該處理容器內而生成該氣體的電漿;測量該電漿處理裝置中電漿生成前的處理容器內壓力與電漿生成後的處理容器內壓力之變化幅度;依據預先求得之作為基準的其他電漿處理裝置中壓力變化幅度與微波供應電功率的相關關係,來求得該電漿處理裝置與該其他電漿處理裝置之間之微波實際功率的偏差量。 In order to achieve the above object, the method for detecting the deviation of the actual power of the microwave in the plasma processing apparatus of the present invention is obtained by processing the plasma processing apparatus of the object to be processed by microwave plasma, and obtaining a plurality of plasma processing apparatuses. a method for generating a deviation amount of actual microwave power; the plasma processing device has: a microwave generating portion that generates microwaves; and a processing container that has an opening for performing plasma processing; and a pressure measuring mechanism that measures the processing a pressure in the container; a dielectric window that hermetically closes an opening of the processing container; an antenna disposed on the upper surface of the dielectric window; and a waveguide that causes the microwave generated by the microwave generating portion to face The antenna is propagated and introduced into the processing container; the gas supply portion supplies the gas into the processing container; and the exhaust portion is exhausted in the processing container; wherein the plasma processing device is used to specify Pressure to supply the gas to the treated container after the exhaust and to be sealed; introducing microwave into the processing container at a specific electric power to generate a plasma of the gas; measuring the The pressure in the processing vessel before the plasma generation in the slurry processing device and the pressure in the processing vessel after the plasma is generated; the pressure variation amplitude in the other plasma processing device based on the previously obtained reference is related to the microwave power supply A relationship is obtained to determine the amount of deviation of the actual microwave power between the plasma processing apparatus and the other plasma processing apparatus.

依據本發明,由於係在供應有處理氣體且被密閉 之處理容器生成電漿時測量處理容器內所產生之壓力變化的幅度,因此依據作為基準之其他電漿處理裝置中壓力變化幅度與微波供應電功率的相關關係,便可求得複數電漿處理裝置間之微波實際功率的偏差量。其結果,便可進行用以消除各處理裝置間所產生之微波實際功率的偏差之偏移量調整,從而可消除電漿處理裝置間的機差。 According to the present invention, since the system is supplied with a process gas and is sealed When the processing container generates the plasma, the magnitude of the pressure change generated in the processing container is measured, so that the complex plasma processing device can be obtained according to the correlation between the pressure variation amplitude and the microwave supply electric power in other plasma processing devices as a reference. The amount of deviation of the actual power of the microwave between. As a result, the offset adjustment for eliminating the deviation of the actual microwave power generated between the processing devices can be performed, and the machine difference between the plasma processing devices can be eliminated.

另一觀點之本發明電漿處理裝置係藉由微波電漿來處理被處理體,其具有:微波產生部,係產生微波;處理容器,係上面呈開口,而用以進行電漿處理;介電體窗,係供該微波穿透並導入至該處理容器內;蓋組件,係支撐該介電體窗並封閉該處理容器的開口;天線,係配置在該介電體窗的上面;介電體板,係配置在該天線的上面;覆蓋板,係配置為覆蓋該介電體板的上方;以及導波管,係連接於該覆蓋板,並將微波朝該天線傳播而導入至該處理容器;其中,該覆蓋板係具備有收容形成於其下面的該介電體板之凹陷部,並且該覆蓋板的外周緣部係具備有朝其外周方向突出所形成之外周突出部,與朝該外周突出部的下方突出所形成之下方突出部;另具備有:支撐於該蓋組件來支撐該覆蓋板的該外周突出部之L字型環狀固定組件、按壓該覆蓋板之該外周突出部的上面之環狀按壓組件、插通該按壓組件與該覆蓋板的外周突出部且固定在該固定組件之第1接合組件、以及插通該固定 組件且固定在該蓋組件之第2接合組件;該按壓組件的垂直部係形成為內周面會抵接於該覆蓋板的該外周突出部,且該按壓組件之垂直部的外周面會抵接於該固定組件的垂直部。 Another aspect of the present invention relates to a plasma processing apparatus for treating a processed object by microwave plasma, comprising: a microwave generating portion for generating microwaves; and a processing container having an opening for performing plasma processing; The electric window is for the microwave to penetrate and is introduced into the processing container; the cover assembly supports the dielectric window and closes the opening of the processing container; the antenna is disposed on the upper surface of the dielectric window; The electric board is disposed on the upper surface of the antenna; the cover board is disposed to cover the upper side of the dielectric board; and the waveguide is connected to the cover board, and the microwave is transmitted to the antenna to be introduced into the a processing container; wherein the cover plate is provided with a recessed portion for accommodating the dielectric plate formed on the lower surface thereof, and an outer peripheral edge portion of the cover plate is provided with an outer peripheral protrusion formed to protrude in an outer circumferential direction thereof, and And forming a lower protruding portion formed below the outer peripheral protruding portion; further comprising: an L-shaped annular fixing assembly supported by the cover assembly to support the outer peripheral protruding portion of the cover plate, and pressing the outer periphery of the cover plate Burst An upper annular pressing assembly of the upper portion, a first engaging component that is inserted into the pressing component and the outer peripheral protruding portion of the covering plate, and fixed to the fixing component, and inserted and fixed The assembly is fixed to the second joint assembly of the cover assembly; the vertical portion of the press assembly is formed such that the inner peripheral surface abuts against the outer peripheral protrusion of the cover plate, and the outer peripheral surface of the vertical portion of the pressing assembly abuts Connected to the vertical portion of the fixed assembly.

依據本發明,係在電漿處理(微波的實際功率)之不同的電漿處理裝置中,預先測量作為基準之電漿處理裝置的壓力與微波的功率,並由其結果來計算該微波功率的偏移(off-set),如此便可求得電漿處理裝置間之微波實際功率的偏差量。其結果,藉由測量有機差之電漿處理裝置的微波功率,並設定針對該測量結果之偏移值且加以使用,便可進行無機差的電漿處理。 According to the present invention, in the plasma processing apparatus of the plasma processing (the actual power of the microwave), the pressure of the plasma processing apparatus as the reference and the power of the microwave are measured in advance, and the microwave power is calculated from the result. Off-set, in this way, the amount of deviation of the actual microwave power between the plasma processing units can be determined. As a result, by measuring the microwave power of the organic poor plasma processing apparatus and setting the offset value for the measurement result and using it, the inorganic poor plasma treatment can be performed.

以下,參照圖式來加以說明本發明實施型態的一例。圖1係顯示本發明實施型態之電漿處理裝置1的概略結構。電漿處理裝置1具有處理容器12,該處理容器12係設置有用以保持矽基板(晶圓W)之晶圓保持台11。晶圓保持台11內部係設置有加熱器(未圖示),可將晶圓W加熱至特定溫度。處理容器12的底部係設置有將處理容器12的內部均勻地排氣之作為排氣部的排氣室13。排氣室13係連接有連通於真空幫浦等排氣裝置14之排氣管15。排氣管15係設置有閥體16,可藉由來自例如控制部17的訊號而進行開閉操作。 Hereinafter, an example of an embodiment of the present invention will be described with reference to the drawings. Fig. 1 is a view showing the schematic configuration of a plasma processing apparatus 1 according to an embodiment of the present invention. The plasma processing apparatus 1 has a processing container 12 provided with a wafer holding stage 11 for holding a silicon substrate (wafer W). A heater (not shown) is provided inside the wafer holding stage 11 to heat the wafer W to a specific temperature. The bottom of the processing container 12 is provided with an exhaust chamber 13 as an exhaust portion that uniformly exhausts the inside of the processing container 12. The exhaust chamber 13 is connected to an exhaust pipe 15 that communicates with an exhaust device 14 such as a vacuum pump. The exhaust pipe 15 is provided with a valve body 16 which can be opened and closed by a signal from, for example, the control unit 17.

處理容器12的上方係具有對應於晶圓保持台11上的晶圓W而開口之開口部。該開口部係配置有封閉該開口部,且對處理容器內供應微波之微波供應部2。微波供應部2係透過用以確保氣密性之O形環等密封材18,來支撐石英或Al2O3所構成的介電體窗19,且藉由具有開閉處理容器12的功能之蓋組件(Lid)50而被氣密地封閉。介電體窗19上(外側)係配置有天線20。該天線20係由具導電性的材質,例如銅、鋁、鎳等金屬製的薄圓板所構成,天線20表面係同心圓狀地形成有例如圖2所示之複數對的槽孔20a、20b,即所謂的輻射狀槽孔天線。各槽孔20a、20b為方形的貫穿溝槽,鄰接之槽孔20a、20b彼此係配設為相互呈直交而形成接近英文字母的「T」之文字。槽孔20a、20b的長度或配列間隔係依所供應之微波的波長而決定。 Above the processing container 12, there is an opening portion that opens corresponding to the wafer W on the wafer holding stage 11. The opening is provided with a microwave supply unit 2 that closes the opening and supplies microwaves into the processing container. The microwave supply unit 2 supports the dielectric window 19 made of quartz or Al 2 O 3 through a sealing material 18 such as an O-ring for ensuring airtightness, and has a function of opening and closing the processing container 12 The assembly (Lid) 50 is hermetically sealed. An antenna 20 is disposed on the outer side of the dielectric window 19 (outside). The antenna 20 is made of a conductive material, for example, a thin circular plate made of metal such as copper, aluminum or nickel. The surface of the antenna 20 is formed concentrically with, for example, a plurality of pairs of slots 20a as shown in FIG. 20b, a so-called radial slot antenna. Each of the slots 20a and 20b is a square through groove, and the adjacent slots 20a and 20b are arranged to be orthogonal to each other to form a letter of "T" close to the English letter. The length or arrangement spacing of the slots 20a, 20b is determined by the wavelength of the microwaves supplied.

天線20的上面如圖1所示,係配置有石英、氧化鋁、氮化鋁等所構成的介電體板(慢波板)21。該介電體板21係具有慢波板的功能。介電體板21上方係配置有覆蓋介電體板21之鋁等導電性覆蓋板22。又,天線20的外周部係卡合於覆蓋板22所設置。 As shown in FIG. 1, the upper surface of the antenna 20 is provided with a dielectric plate (slow wave plate) 21 made of quartz, alumina, aluminum nitride or the like. The dielectric body plate 21 has a function of a slow wave plate. A conductive cover plate 22 such as aluminum covering the dielectric plate 21 is disposed above the dielectric plate 21. Further, the outer peripheral portion of the antenna 20 is engaged with the cover plate 22.

覆蓋板22的內部係設置有供冷媒流通之冷媒流道22a。又,覆蓋板22的中央係連接有同軸導波管24。同軸導波管24的上端部係透過矩形導波管27及模式轉換機28而連接有作為微波產生部之微波產生裝置23。 Inside the cover plate 22, a refrigerant flow path 22a through which a refrigerant flows is provided. Further, a coaxial waveguide 24 is connected to the center of the cover plate 22. The upper end portion of the coaxial waveguide 24 is connected to the microwave generating device 23 as a microwave generating portion via the rectangular waveguide 27 and the mode converter 28.

微波產生裝置23係設置於處理容器12的外部,可產生例如2.45GHz的微波。又,微波產生裝置23係透過模式轉換機28而連接有阻抗匹配器25,以進行微波之阻抗的匹配。同軸導波管24係由外側導體24a與內側導體24b所構成,內側導體24b係連接於天線20。藉由此結構,則從微波產生裝置23所產生的微波便會在阻抗匹配器25、矩形導波管27、模式轉換機28及同軸導波管24內傳播,且以作為慢波板之介電體板21來被壓縮而波長變短後,來自天線20的圓偏波狀微波便會從介電體窗19被導入至處理容器12內。 The microwave generating device 23 is disposed outside the processing container 12 to generate a microwave of, for example, 2.45 GHz. Further, the microwave generating device 23 is connected to the mode converter 28 via the mode converter 28 to perform impedance matching of the microwaves. The coaxial waveguide 24 is composed of an outer conductor 24a and an inner conductor 24b, and an inner conductor 24b is connected to the antenna 20. With this configuration, the microwave generated from the microwave generating device 23 is propagated in the impedance matching unit 25, the rectangular waveguide 27, the mode converter 28, and the coaxial waveguide 24, and serves as a slow wave plate. When the electric body panel 21 is compressed and the wavelength is shortened, the circularly undulated microwave from the antenna 20 is introduced into the processing container 12 from the dielectric window 19.

又,阻抗匹配器25的上游側係設置有用以測量從微波產生裝置23所供應之微波的電功率之電功率測量機構26。電功率測量機構26係電連接於控制部17,其測量結果會被輸入至控制部17。 Further, the upstream side of the impedance matching unit 25 is provided with an electric power measuring mechanism 26 for measuring the electric power of the microwave supplied from the microwave generating device 23. The electric power measuring mechanism 26 is electrically connected to the control unit 17, and the measurement result is input to the control unit 17.

處理容器12上部的內周面係形成有用以供應電漿產生用氣體之氣體供應口30。氣體供應口30係沿著例如處理容器12的內周面而形成於複數部位處。氣體供應口30係連接有連通於例如處理容器12外部所設置的氣體供應部31之氣體供應管32。本實施型態之氣體供應部31係具有非活性氣體供應部33與氮氣供應部34,且透過各個閥體33a、34a、質流控制器33b、34b而連接於氣體供應口30。從氣體供應口30所供應之氣體的流量係受到質流控制器33b、34b的控 制。又,處理容器12的內周面除了氣體供應口30以外,亦設置有用以測量該處理容器12內的壓力之壓力測量機構35。壓力測量機構35係電連接於控制部17,其測量結果會被輸入至控制部17。此外,本實施型態中,係以在氣體供應部31儲存有稀有氣體之氬(Ar)氣,或使用於晶圓W的電漿氮化處理之氮氣的情況為例來加以說明。 The inner peripheral surface of the upper portion of the processing container 12 forms a gas supply port 30 for supplying a gas for plasma generation. The gas supply port 30 is formed at a plurality of locations along the inner circumferential surface of the processing container 12, for example. The gas supply port 30 is connected to a gas supply pipe 32 that communicates with, for example, the gas supply portion 31 provided outside the processing container 12. The gas supply unit 31 of the present embodiment has an inert gas supply unit 33 and a nitrogen gas supply unit 34, and is connected to the gas supply port 30 through the respective valve bodies 33a and 34a and the mass flow controllers 33b and 34b. The flow rate of the gas supplied from the gas supply port 30 is controlled by the mass flow controllers 33b, 34b. system. Further, in addition to the gas supply port 30, the inner peripheral surface of the processing container 12 is provided with a pressure measuring mechanism 35 for measuring the pressure in the processing container 12. The pressure measuring mechanism 35 is electrically connected to the control unit 17, and the measurement result is input to the control unit 17. Further, in the present embodiment, a case where argon (Ar) gas in which a rare gas is stored in the gas supply portion 31 or nitrogen gas which is used in plasma nitriding treatment of the wafer W will be described as an example.

處理容器12內之晶圓保持台11的周圍係設置有例如石英所構成的氣體隔板40,與用以支撐石英製氣體隔板40之鋁等金屬製支撐組件41。 A gas separator 40 made of, for example, quartz, and a metal support member 41 such as aluminum for supporting the quartz gas separator 40 are provided around the wafer holding stage 11 in the processing container 12.

以上的電漿處理裝置1係如上述般地設置有控制部17。控制部17為例如電腦,其係具有程式收納部(未圖示)。程式收納部亦收納有控制微波產生裝置23或閥體16等,來使電漿處理裝置1動作之程式。此外,該程式係記錄在例如電腦可讀取之硬碟(HD)、軟碟(FD)、光碟(CD)、磁光碟(MO)、記憶卡等可被電腦讀取的記憶媒體H,且可由該記憶媒體H被安裝至控制部17。 The above plasma processing apparatus 1 is provided with the control unit 17 as described above. The control unit 17 is, for example, a computer having a program storage unit (not shown). The program storage unit also stores a program for controlling the microwave processing device 23, the valve body 16, and the like to operate the plasma processing device 1. In addition, the program records a memory medium H that can be read by a computer, such as a computer readable hard disk (HD), a floppy disk (FD), a compact disk (CD), a magneto-optical disk (MO), a memory card, and the like. The memory unit H can be mounted to the control unit 17.

<第1實施型態> <First embodiment>

本實施型態之電漿處理裝置1係構成為如上所述,接下來,針對本實施型態之電漿處理裝置1中微波實際功率的偏差量檢測方法,說明其原理。 The plasma processing apparatus 1 of the present embodiment is configured as described above. Next, the principle of the method for detecting the deviation amount of the actual microwave power in the plasma processing apparatus 1 of the present embodiment will be described.

如上所述,縱使是以相同電功率來對相同結構的電漿處理裝置1供應微波而進行電漿處理的情況,在 複數電漿處理裝置1間形成於基板表面之氮化膜的膜厚或氮濃度等仍會有所差異。 As described above, even if the microwave processing is performed on the plasma processing apparatus 1 of the same structure with the same electric power, the plasma processing is performed. The film thickness or nitrogen concentration of the nitride film formed on the surface of the substrate between the plurality of plasma processing apparatuses 1 may vary.

針對此差異,使用與電漿處理裝置1相同結構的2台電漿處理裝置100、200,來進行以下的2種確認測試。 In response to this difference, the following two kinds of confirmation tests were performed using two plasma processing apparatuses 100 and 200 having the same configuration as that of the plasma processing apparatus 1.

首先,第1確認測試係確認2台電漿處理裝置100、200中電漿氮化處理的差異。在確認時,係將矽基板的晶圓W載置於晶圓保持台11,並以1400W~1700W的電功率範圍來對供應有氬氣與氮氣之處理容器12內供應微波,而對晶圓W進行電漿氮化處理。分別以2台電漿處理裝置100、200來進行該電漿氮化處理。圖3係顯示電漿氮化處理的結果。圖3中,橫軸為從微波產生裝置23所供應之微波的電功率,縱軸為藉由電漿氮化處理而形成於晶圓W表面之矽氮化膜的氮濃度,其係分別以A、B來表示2台電漿處理裝置100、200中電漿的供應電功率與氮濃度之相關關係之圖表。 First, the first confirmation test confirms the difference in plasma nitriding treatment in the two plasma processing apparatuses 100 and 200. At the time of confirmation, the wafer W of the germanium substrate is placed on the wafer holding stage 11, and microwaves are supplied to the processing container 12 supplied with argon gas and nitrogen gas in an electric power range of 1400 W to 1700 W, and the wafer W is applied. Plasma nitriding treatment is performed. The plasma nitriding treatment is performed by two plasma processing apparatuses 100 and 200, respectively. Figure 3 shows the results of the plasma nitriding treatment. In Fig. 3, the horizontal axis represents the electric power of the microwave supplied from the microwave generating device 23, and the vertical axis represents the nitrogen concentration of the tantalum nitride film formed on the surface of the wafer W by plasma nitriding treatment, which is respectively A. B shows a graph showing the correlation between the supplied electric power and the nitrogen concentration of the plasma in the two plasma processing apparatuses 100 and 200.

如圖3所示,可發現矽氮化膜的氮濃度在電漿電功率為1400W~1700W範圍的全部區域中,電漿處理裝置100所為者(圖3的圖形A)會較電漿處理裝置200所為者(圖3的圖形B)要來得高。 As shown in FIG. 3, it can be found that the nitrogen concentration of the tantalum nitride film is in the entire range of the plasma electric power of 1400 W to 1700 W, and the plasma processing apparatus 100 (the graph A of FIG. 3) is more than the plasma processing apparatus 200. The person (Figure B of Figure 3) is going to come high.

接著,第2確認測試係確認2台電漿處理裝置100、200中電漿電功率與處理容器12內的壓力之關係。第2確認測試中,係對已排氣狀態下的處理容器 12供應氬氣,並將處理容器12在內部壓力為240Pa之狀態下密閉後,以1400W~1700W的電功率範圍來對該處理容器12內供應微波而生成電漿。之後,測量藉由電漿生成而產生於處理容器12內之壓力變化的值。圖4係顯示第2確認測試的結果。圖4中,橫軸為從微波產生裝置23所供應之微波的電功率,縱軸為處理容器12內電漿生成前的壓力與電漿生成後的壓力之變化幅度,其係分別以C、D來表示2台電漿處理裝置100、200中電漿的電功率與壓力變化幅度之相關關係之圖表。 Next, the second confirmation test confirms the relationship between the electric power of the plasma in the two plasma processing apparatuses 100 and 200 and the pressure in the processing container 12. In the second confirmation test, the processing container in the exhausted state After the argon gas was supplied and the processing container 12 was sealed in a state where the internal pressure was 240 Pa, microwaves were supplied to the inside of the processing container 12 in an electric power range of 1400 W to 1700 W to generate a plasma. Thereafter, the value of the pressure change generated in the processing vessel 12 by the plasma generation is measured. Figure 4 shows the results of the second confirmation test. In Fig. 4, the horizontal axis represents the electric power of the microwave supplied from the microwave generating device 23, and the vertical axis represents the change range of the pressure before the plasma generation in the processing container 12 and the pressure after the plasma is generated, which are respectively C and D. A graph showing the correlation between the electric power of the plasma and the pressure change amplitude in the two plasma processing apparatuses 100 and 200.

如圖4所示,可發現處理容器12內的壓力變化幅度在電漿電功率為1400W~1700W範圍的全部區域中,電漿處理裝置100所為者(圖4的圖形C)會較電漿處理裝置200所為者(圖4的圖形D)要來得高。 As shown in FIG. 4, it can be found that the pressure variation range in the processing container 12 is in the entire range of the plasma electric power in the range of 1400 W to 1700 W, and the plasma processing apparatus 100 (the pattern C in FIG. 4) is more than the plasma processing apparatus. The 200 (Figure D of Figure 4) is coming high.

一般來說,電漿生成時處理容器12內的壓力係依存於微波的實際功率。於是,縱使是以相同電功率來對2台電漿處理裝置100、200供應微波,由處理容器12內的壓力變化幅度相異之圖4的結果,可得知仍會在電漿處理裝置100、200間產生微波實際功率的偏差。 In general, the pressure within the processing vessel 12 during plasma generation depends on the actual power of the microwave. Thus, even if microwaves are supplied to the two plasma processing apparatuses 100, 200 at the same electric power, the results of FIG. 4 differing in the magnitude of the pressure variation in the processing container 12, it is known that the plasma processing apparatus 100, 200 will still be present. The deviation of the actual power of the microwave is generated.

接著,為了調查壓力變化幅度與矽氮化膜的氮濃度之相關,便由圖3及圖4的結果製作了圖5所示之橫軸為壓力的變化幅度,縱軸為矽氮化膜的氮濃度的圖表。如圖5所示,不論是電漿處理裝置100所為之 電漿處理(圖5的圖形E)或電漿處理裝置200所為之電漿處理(圖5的圖形F),皆可發現壓力的變化幅度係與氮濃度大致相同。 Next, in order to investigate the correlation between the pressure change amplitude and the nitrogen concentration of the tantalum nitride film, the horizontal axis shown in FIG. 5 is the change width of the pressure, and the vertical axis is the tantalum nitride film. A chart of nitrogen concentration. As shown in FIG. 5, it is made by the plasma processing apparatus 100. The plasma treatment (pattern E of Fig. 5) or the plasma treatment of the plasma processing apparatus 200 (pattern F of Fig. 5) shows that the magnitude of the pressure change is substantially the same as the nitrogen concentration.

因此,若能由圖4所示之微波的供應電功率與處理容器12內的壓力變化幅度之相關關係,來求得2台電漿處理裝置100、200間的實際功率偏差量,便可對應於偏差量來設定微波供應電功率的偏移(off-set)。其結果,便可實質上消除2台電漿處理裝置100、200間的機差。 Therefore, if the actual power deviation between the two plasma processing apparatuses 100 and 200 can be obtained from the correlation between the supply electric power of the microwaves shown in FIG. 4 and the pressure variation range in the processing container 12, the deviation can be made. The amount is set to offset (off-set) of the microwave supply electric power. As a result, the difference between the two plasma processing apparatuses 100 and 200 can be substantially eliminated.

本發明係著眼於上述問題所發明者,接下來,針對本實施型態之求得微波實際功率的偏差量之方法來具體地加以說明。圖6係顯示本實施型態之微波實際功率的偏差量檢測方法的製程之流程圖。 The present invention has been made in view of the above problems, and the method of determining the amount of deviation of the actual microwave power in the present embodiment will be specifically described. Fig. 6 is a flow chart showing the process of the method for detecting the deviation amount of the actual power of the microwave in the present embodiment.

於複數電漿處理裝置100、200中,在求得微波實際功率的偏差量時,首先係在例如電漿處理裝置100中求得電漿的供應電功率與壓力變化幅度之相關關係。 In the plurality of plasma processing apparatuses 100 and 200, when the amount of deviation of the actual power of the microwave is obtained, first, for example, the plasma processing apparatus 100 determines the correlation between the supplied electric power of the plasma and the pressure change range.

求得相關關係時,首先係將處理容器12的內部排氣(圖6的步驟S1)。接著,經由氣體供應口30來對處理容器12內供應氬氣(圖6的步驟S2)。 When the correlation is obtained, first, the inside of the container 12 is exhausted (step S1 of Fig. 6). Next, argon gas is supplied into the processing container 12 via the gas supply port 30 (step S2 of FIG. 6).

之後,使處理容器12內的壓力成為例如240Pa後停止氬氣的供應並關閉閥體16,而在氬氣的壓力為240Pa之狀態下密閉處理容器12(圖6的步驟S3)。接著,以例如1400W~1700W的電功率範圍來對處理容 器12內供應微波而生成電漿(圖6的步驟S4)。此外,微波之供應電功率的監視係藉由電功率測量機構26而進行。 After that, the pressure in the processing container 12 is, for example, 240 Pa, and the supply of argon gas is stopped, and the valve body 16 is closed, and the processing container 12 is sealed in a state where the pressure of the argon gas is 240 Pa (step S3 in Fig. 6). Next, the processing capacity is performed with an electric power range of, for example, 1400 W to 1700 W. The microwave is supplied into the device 12 to generate plasma (step S4 of Fig. 6). Further, the monitoring of the supply electric power of the microwave is performed by the electric power measuring mechanism 26.

之後,測量因電漿生成而在處理容器12內所產生之壓力變化的幅度,來求得圖4的圖形C所示之電漿供應電功率與處理容器12內壓力的變化幅度之相關關係(圖6的步驟S5)。 Thereafter, the magnitude of the change in pressure generated in the processing vessel 12 due to plasma generation is measured to determine the correlation between the plasma supply electric power shown in the graph C of FIG. 4 and the variation range of the pressure in the processing container 12. Step S5) of 6.

接著,關於電漿處理裝置200亦與電漿處理裝置100同樣地,求得微波的供應電功率與處理容器12內的壓力變化幅度之相關關係。此情況下,係與上述電漿處理裝置100的情況同樣地將處理容器12的內部排氣(圖6的步驟S6),接著,對處理容器12內供應氬氣(圖6的步驟S7),而在處理容器12內的氬氣壓力為240Pa下密閉處理容器12(圖6的步驟S8)。然後,仍以1400W~1700W的電功率來對密閉後的處理容器12內供應微波而生成電漿(圖6的步驟S9),之後,測量因電漿生成而在處理容器12內所產生之壓力變化的幅度。藉以求得圖4的圖形D所示之電漿供應電功率與處理容器12內壓力的變化幅度之相關關係(圖6的步驟S10)。 Next, similarly to the plasma processing apparatus 100, the plasma processing apparatus 200 determines the correlation between the supply electric power of the microwave and the pressure variation range in the processing container 12. In this case, the inside of the processing container 12 is exhausted in the same manner as in the above-described plasma processing apparatus 100 (step S6 in FIG. 6), and then argon gas is supplied into the processing container 12 (step S7 in FIG. 6). On the other hand, the processing container 12 is hermetically sealed at a pressure of 240 Pa in the processing container 12 (step S8 of Fig. 6). Then, microwaves are supplied to the sealed processing container 12 at a power of 1400 W to 1700 W to generate plasma (step S9 of FIG. 6), and thereafter, pressure changes generated in the processing container 12 due to plasma generation are measured. Amplitude. The relationship between the electric power supplied to the plasma shown in the graph D of Fig. 4 and the magnitude of the change in the pressure in the processing container 12 is obtained (step S10 of Fig. 6).

然後,依據電漿處理裝置100的相關關係與電漿處理裝置200的相關關係,來求得電漿處理裝置100與電漿處理裝置200之間所產生之微波實際功率的偏差量(圖6的步驟S11)。具體來說,係由圖4的圖形D 來求得電漿處理裝置200中微波的供應電功率為例如1600W情況下之壓力變化幅度。此情況下的變化幅度大約為60.7Pa。然後,由圖4的圖形C來求得電漿處理裝置100中壓力的變化幅度同樣為60.7Pa情況下之電功率,其係為約1480W。由此可知,若以電漿處理裝置200為基準,則電漿處理裝置100中微波的實際功率係較電漿處理裝置200要高相當於微波的供應電功率120W之量。於是,在電漿處理裝置100中,只要使得從微波產生裝置23所供應之微波的設定偏移120W便可消除機差,而藉由電漿處理裝置100來進行相同於電漿處理裝置200之電漿處理。 Then, according to the correlation between the correlation between the plasma processing apparatus 100 and the plasma processing apparatus 200, the deviation amount of the actual microwave power generated between the plasma processing apparatus 100 and the plasma processing apparatus 200 is obtained (FIG. 6 Step S11). Specifically, it is represented by Figure D of Figure 4. The supply electric power of the microwave in the plasma processing apparatus 200 is determined to be, for example, a pressure variation range in the case of 1600 W. The magnitude of the change in this case is approximately 60.7 Pa. Then, from the graph C of FIG. 4, the electric power in the case where the pressure variation in the plasma processing apparatus 100 is also 60.7 Pa is obtained, which is about 1480 W. From this, it can be seen that, based on the plasma processing apparatus 200, the actual power of the microwave in the plasma processing apparatus 100 is higher than the plasma processing apparatus 200 by an amount equivalent to 120 W of the microwave supplying electric power. Therefore, in the plasma processing apparatus 100, the machine difference can be eliminated by shifting the setting of the microwave supplied from the microwave generating apparatus 23 by 120 W, and the same as the plasma processing apparatus 200 by the plasma processing apparatus 100. Plasma treatment.

依據以上的實施型態,由於係對電漿處理裝置100的處理容器12供應氬氣後密閉該處理容器12,且在該狀態下對處理容器12內供應微波而生成電漿時,測量處理容器12內所產生之壓力變化的幅度,因此依據預先求得之作為基準的電漿處理裝置200中壓力變化幅度與微波供應電功率的相關關係,便可求得電漿處理裝置100、200之間所產生之微波實際功率的偏差量。藉此,便可進行用以消除電漿處理裝置100、200間所產生之微波實際功率的偏差之微波功率的偏移調整,從而可消除電漿處理的機差。 According to the above embodiment, since the processing container 12 is sealed by supplying the argon gas to the processing container 12 of the plasma processing apparatus 100, and the microwave is generated in the processing container 12 in this state to generate plasma, the processing container is measured. The magnitude of the pressure change generated in the 12, so that the correlation between the pressure change amplitude and the microwave supply electric power in the plasma processing apparatus 200 based on the previously obtained reference can be obtained between the plasma processing apparatuses 100 and 200. The amount of deviation of the actual microwave power produced. Thereby, the offset adjustment of the microwave power for eliminating the variation of the actual microwave power generated between the plasma processing apparatuses 100 and 200 can be performed, and the machine difference of the plasma processing can be eliminated.

以上的實施型態雖係針對電漿處理裝置100與電漿處理裝置200兩者,而在例如1400W~1700W的微波電功率範圍下測量壓力變化幅度,但針對電漿處理 裝置100,只要在1400W~1700W的任意範圍內,僅測量1點的壓力變化幅度即可。其係因為針對電漿處理裝置100,只要測量例如微波的電功率為1600W情況下的壓力變化,便可求得與作為基準之電漿處理裝置200之間的微波實際功率偏差量係相當於微波之供應電功率的120W量。此外,以電漿處理裝置100、200的何者為基準當然可任意決定。實際上,較佳係使用例如已使用於產品的生產之電漿處理裝置,亦即已經知道處理後的氮濃度之裝置為基準。 The above embodiment is directed to both the plasma processing apparatus 100 and the plasma processing apparatus 200, and measures the pressure variation range in a microwave electric power range of, for example, 1400 W to 1700 W, but for plasma processing. The device 100 only needs to measure the pressure change width at one point in any range of 1400 W to 1700 W. For the plasma processing apparatus 100, as long as the pressure change in the case where the electric power of the microwave is 1600 W is measured, the actual power deviation between the microwave and the plasma processing apparatus 200 as the reference can be determined to be equivalent to the microwave. Supply 120W of electric power. Further, it is of course arbitrarily determined based on which of the plasma processing apparatuses 100 and 200 is used as a reference. In practice, it is preferred to use, for example, a plasma processing apparatus that has been used in the production of a product, that is, a device that already knows the nitrogen concentration after treatment.

又,以上的實施型態雖係在電漿處理裝置100中以特定的微波功率生成電漿,藉此來測量處理容器12內所產生之壓力變化幅度,並由作為基準之電漿處理裝置200的功率與壓力之相關關係來求得機差,但例如在進行電漿氮化處理時已預先決定所欲氮濃度的情況,亦可由圖5的圖形E來直接求得對應於該所欲氮濃度之微波的供應電功率。具體來說,例如電漿氮化處理中的氮濃度為13%之情況下,由圖5的圖形E可得知只要使此時的處理容器12內壓力變化幅度為大約62Pa即可。於是,只要在電漿處理裝置100中以240Pa來將氬氣導入至處理容器12內,接著使所供應之微波的電功率變化來求得壓力測量機構35的測量值會成為62Pa情況下之電功率,便可在電漿處理裝置100中直接求得用以使氮濃度成為13%的微波功率。此情況下,由於係直接求得用以獲得目標氮濃度之微 波電功率,因此可更加精密地使電漿處理裝置100、200間之處理結果為一致。 Further, in the above embodiment, the plasma processing apparatus 100 generates plasma at a specific microwave power, thereby measuring the pressure variation range generated in the processing container 12, and the plasma processing apparatus 200 as a reference. The relationship between the power and the pressure is used to determine the machine difference. For example, when the plasma nitriding treatment is performed, the desired nitrogen concentration is determined in advance, and the pattern E corresponding to the desired nitrogen can be directly obtained. The supply power of the microwave of the concentration. Specifically, for example, when the nitrogen concentration in the plasma nitriding treatment is 13%, it can be seen from the graph E of FIG. 5 that the pressure change range in the processing container 12 at this time is about 62 Pa. Then, as long as the argon gas is introduced into the processing container 12 at 240 Pa in the plasma processing apparatus 100, and then the electric power of the supplied microwave is changed, the electric power of the measurement value of the pressure measuring mechanism 35 becomes 62 Pa. The microwave power for making the nitrogen concentration 13% can be directly obtained in the plasma processing apparatus 100. In this case, it is directly obtained to obtain the target nitrogen concentration. Since the wave power is used, the processing results between the plasma processing apparatuses 100 and 200 can be made more precise.

<第2實施型態> <Second embodiment>

此外,以上的實施型態雖係針對消除複數電漿處理裝置100、200間之微波實際功率的偏差之方法加以說明,但縱使是單一的電漿處理裝置1,當維修保養等將電漿處理裝置1分解再組裝後的情況,亦會因組裝誤差而在維修保養前後有微波的實際功率發生偏差之情況。 Further, although the above embodiment is described with respect to a method of eliminating the variation in the actual microwave power between the plurality of plasma processing apparatuses 100 and 200, even if it is a single plasma processing apparatus 1, the plasma is treated as a maintenance or the like. When the device 1 is disassembled and reassembled, the actual power of the microwave may be deviated before and after maintenance due to assembly errors.

為了降低上述組裝誤差,一有效方法係在維修保養前後,以不改變天線20或介電體窗19相對於處理容器12的相對位置之方式來構成電漿處理裝置1。以下,針對其具體結構加以說明。 In order to reduce the above assembly error, an effective method is to form the plasma processing apparatus 1 in a manner that does not change the relative position of the antenna 20 or the dielectric window 19 with respect to the processing container 12 before and after maintenance. Hereinafter, the specific structure will be described.

圖7係顯示電漿處理裝置1之處理容器12上部的蓋組件50、介電體窗19、天線20、介電體板(慢波板)21及覆蓋板22附近的結構之部分概略縱剖視圖。此外,以下的說明以外的結構由於與上述說明相同,故省略說明。 Fig. 7 is a partial longitudinal cross-sectional view showing the structure of the lid assembly 50, the dielectric window 19, the antenna 20, the dielectric plate (slow wave plate) 21, and the vicinity of the cover plate 22 in the upper portion of the processing container 12 of the plasma processing apparatus 1. . In addition, since the structure other than the following description is the same as that of the above description, description is abbreviate|omitted.

介電體窗19係透過O形環等密封組件(未圖示)而氣密地被支撐在從蓋組件50的內周面朝內側段差狀地突出而設置之支撐部50a的上面。介電體窗19上面係配置有天線20。天線20的上面係配置有介電體板21。 The dielectric window 19 is airtightly supported by a sealing member (not shown) such as an O-ring, and is supported on the upper surface of the support portion 50a which is provided to protrude inward from the inner circumferential surface of the lid assembly 50. An antenna 20 is disposed on the upper surface of the dielectric window 19. A dielectric plate 21 is disposed on the upper surface of the antenna 20.

對應於覆蓋天線20及作為慢波板之介電體板21 般之覆蓋板22的下面位置處係形成有覆蓋板22的外周部朝向下方突出之下方突出部22b,且形成有朝上方凹陷之凹陷部22c。介電體板21係密接於該凹陷部22c而被加以收納。又,覆蓋板22的外周緣部之高度方向的中央附近係形成有朝外周方向突出之外周突出部22d。 Corresponding to the cover antenna 20 and the dielectric plate 21 as a slow wave plate In the lower position of the cover plate 22, a lower protruding portion 22b that protrudes downward from the outer peripheral portion of the cover plate 22 is formed, and a recessed portion 22c that is recessed upward is formed. The dielectric plate 21 is in close contact with the recessed portion 22c and housed therein. Further, in the vicinity of the center in the height direction of the outer peripheral edge portion of the cover plate 22, the outer peripheral projection portion 22d is formed to protrude in the outer circumferential direction.

蓋組件50的上面50b係藉由於鉛直方向貫穿該固定組件51的垂直部51a之螺栓等接合組件52而固定有剖面形狀呈略L字型之圓環狀固定組件51。 The upper surface 50b of the cap assembly 50 is fixed to the annular fixing member 51 having a substantially L-shaped cross-sectional shape by a joint assembly 52 such as a bolt penetrating through the vertical portion 51a of the fixing member 51 in the vertical direction.

覆蓋板22之外周突出部22d的下面係被支撐在固定組件51的上面。外周突出部22d的上面外周部係密接有剖面形狀呈L字形而90度往左旋轉之略L字型的圓環狀按壓組件53,並從按壓組件53的水平部53a的上面貫穿按壓組件53、外周突出部22d,而以螺栓等接合組件54來將介電體窗19、天線20、介電體板21一起固定在覆蓋板22。又,按壓組件53的垂直部53b係構成為內周面會抵接於覆蓋板22的外周突出部22d,且該垂直部53b的外周面會抵接於固定組件51的垂直部51a。又,藉由在覆蓋板22之下方突出部22b的外周面與固定組件51的內周面之間形成有環狀間隙(餘隙),便可在維修保養時容易進行中心校正。於是,便可藉由固定組件51的垂直部51a來防止覆蓋板22及按壓組件53往水平方向移動。與此同時,可使介電體窗19、天線20、介電體板21及覆蓋板(冷卻 板)22自對位。於是,維修保養前後之處理容器12與天線20等的相對位置便不會改變。因此,藉由使得電漿處理裝置1之處理容器12的上端部附近成為圖7的結構,便可在維修保養前後將微波實際功率的偏差抑制在最小限度。 The lower surface of the outer peripheral projection 22d of the cover panel 22 is supported on the upper surface of the fixing assembly 51. The outer peripheral portion of the outer peripheral protruding portion 22d is in close contact with a substantially L-shaped annular pressing member 53 having an L-shaped cross section and 90 degrees to the left, and passes through the pressing member 53 from the upper surface of the horizontal portion 53a of the pressing unit 53. The outer peripheral portion 22d is fixed to the cover plate 22 by the dielectric member 19, the antenna 20, and the dielectric plate 21 by a bonding member 54 such as a bolt. Further, the vertical portion 53b of the pressing unit 53 is configured such that the inner peripheral surface abuts against the outer peripheral protruding portion 22d of the cover plate 22, and the outer peripheral surface of the vertical portion 53b abuts against the vertical portion 51a of the fixing unit 51. Further, by forming an annular gap (recess) between the outer peripheral surface of the lower protruding portion 22b of the cover plate 22 and the inner peripheral surface of the fixing unit 51, center correction can be easily performed at the time of maintenance. Thus, the cover plate 22 and the pressing member 53 can be prevented from moving in the horizontal direction by the vertical portion 51a of the fixing member 51. At the same time, the dielectric window 19, the antenna 20, the dielectric plate 21, and the cover plate can be cooled (cooled) Board) 22 self-alignment. Therefore, the relative positions of the processing container 12 before and after the maintenance, the antenna 20, and the like do not change. Therefore, by making the vicinity of the upper end portion of the processing container 12 of the plasma processing apparatus 1 into the configuration of FIG. 7, the variation in the actual power of the microwave can be minimized before and after the maintenance.

此外,從同軸導波管24往鉛直方向傳播之微波在被導入至天線20時,亦會在介電體板21內朝向外周方向傳播。於是,微波便會從微波供應部2外周部之固定組件51的接合部溢漏而發生損失。較佳係將該等損失抑制在最小限度。此情況下,例如圖7所示,藉由分別在較接合組件54要靠處理容器12內側之位置處、覆蓋板22之外周突出部22d的上面與按壓組件53的下面之接合面、外周突出部22d的下面與固定組件51的上面之接合面、以及固定組件51的下面與蓋組件50的上面部之接合面設置有金屬製的圓環狀微波遮蔽組件60,便可防止在介電體板21內往外周方向傳播之微波溢漏至外部。遮蔽組件60係使用金屬製的螺旋遮蔽環等。此外,亦可如圖7所示般,遮蔽組件60亦可設置於較接合組件54要靠處理容器外側之位置處。此情況下,為了防止微波從覆蓋板22、固定組件51、按壓組件53及接合組件54的接觸面溢漏,較佳係分別在較接合組件54要靠外側且為外周突出部22d的上面與按壓組件53之水平部53a的下面之接合面,以及按壓組件53之垂直部53b的下端部與固定 組件51的上面之接合面配置有遮蔽組件60。 Further, when the microwave propagating from the coaxial waveguide 24 in the vertical direction is introduced into the antenna 20, it also propagates in the outer peripheral direction in the dielectric plate 21. Then, the microwave leaks from the joint portion of the fixing member 51 at the outer peripheral portion of the microwave supply portion 2, and the loss occurs. It is preferred to minimize these losses. In this case, for example, as shown in Fig. 7, the outer surface of the outer peripheral projection portion 22d of the cover plate 22 and the lower surface of the pressing member 53 and the outer peripheral portion are respectively protruded at a position where the joint assembly 54 is to be inside the processing container 12, respectively. A joint surface of the lower portion of the portion 22d and the upper surface of the fixing member 51, and a joint surface of the lower surface of the fixing member 51 and the upper surface portion of the lid assembly 50 are provided with a metal annular microwave shielding member 60 to prevent the dielectric body. The microwave propagating in the outer peripheral direction of the board 21 overflows to the outside. The shielding unit 60 is a metal spiral shielding ring or the like. In addition, as shown in FIG. 7, the shielding assembly 60 may also be disposed at a position closer to the outer side of the processing container than the engaging assembly 54. In this case, in order to prevent the microwave from leaking from the contact faces of the cover plate 22, the fixing member 51, the pressing member 53, and the engaging member 54, it is preferable to respectively be on the outer side of the engaging member 54 and on the outer peripheral portion 22d. The lower surface of the horizontal portion 53a of the pressing member 53 and the lower end portion of the vertical portion 53b of the pressing member 53 are fixed and fixed. The upper joint surface of the assembly 51 is provided with a shield assembly 60.

以上,雖已說明本發明之較佳實施型態,但本發明未限定於上述範例,而亦可適用於其他的微波電漿裝置,例如ECR電漿裝置、表面波電漿裝置等。又,本發明所屬技術領域中具通常知識者,應當可在申請專利範圍所記載之技術思想範疇內,思及各種變化例或修正例,且可明瞭該等當然亦屬於本發明之技術範圍。 Although the preferred embodiments of the present invention have been described above, the present invention is not limited to the above examples, and can be applied to other microwave plasma devices, such as ECR plasma devices, surface wave plasma devices, and the like. Further, those skilled in the art to which the present invention pertains may be able to make various modifications or alterations within the scope of the technical scope of the invention, and it is obvious that these are also within the technical scope of the present invention.

1‧‧‧電漿處理裝置 1‧‧‧Plastic processing unit

2‧‧‧微波供應部 2‧‧‧Microwave Supply Department

11‧‧‧晶圓保持台 11‧‧‧ Wafer Holder

12‧‧‧處理容器 12‧‧‧Processing container

13‧‧‧排氣室 13‧‧‧Exhaust chamber

17‧‧‧控制部 17‧‧‧Control Department

18‧‧‧密封材 18‧‧‧ Sealing material

19‧‧‧介電體窗 19‧‧‧Dielectric window

20‧‧‧天線 20‧‧‧Antenna

21‧‧‧介電體板(慢波板) 21‧‧‧Dielectric board (slow wave board)

22‧‧‧覆蓋板 22‧‧‧ Covering board

23‧‧‧微波產生裝置 23‧‧‧Microwave generating device

24‧‧‧同軸導波管 24‧‧‧ coaxial waveguide

27‧‧‧矩形導波管 27‧‧‧Rectangular waveguide

28‧‧‧模式轉換器 28‧‧‧Mode Converter

30‧‧‧氣體供應口 30‧‧‧ gas supply port

31‧‧‧氣體供應部 31‧‧‧ Gas Supply Department

32‧‧‧氣體供應管 32‧‧‧ gas supply pipe

33‧‧‧非活性氣體供應部 33‧‧‧Inactive Gas Supply Department

34‧‧‧氮氣供應部 34‧‧‧Nitrogen Supply Department

35‧‧‧壓力測量機構 35‧‧‧Pressure measuring agency

40‧‧‧隔板 40‧‧‧Baffle

41‧‧‧支撐組件 41‧‧‧Support components

50‧‧‧蓋組件(Lid) 50‧‧‧Cover assembly (Lid)

51‧‧‧固定組件 51‧‧‧Fixed components

52‧‧‧接合組件 52‧‧‧ Engagement components

53‧‧‧按壓組件 53‧‧‧ Pressing components

60‧‧‧遮蔽組件 60‧‧‧shading components

W‧‧‧晶圓 W‧‧‧ wafer

圖1係顯示實施本發明之電漿處理裝置的一結構例之概略縱剖視圖。 Fig. 1 is a schematic longitudinal cross-sectional view showing a configuration example of a plasma processing apparatus embodying the present invention.

圖2係顯示本實施型態之電漿處理裝置中所使用之天線的型態之俯視圖。 Fig. 2 is a plan view showing the form of an antenna used in the plasma processing apparatus of the present embodiment.

圖3係顯示電漿處理裝置中電漿的供應電功率與氮濃度之相關關係之圖表。 Fig. 3 is a graph showing the correlation between the supplied electric power and the nitrogen concentration of the plasma in the plasma processing apparatus.

圖4係顯示電漿處理裝置中電漿的電功率與壓力的變化幅度之相關關係之圖表。 Fig. 4 is a graph showing the correlation between the electric power of the plasma in the plasma processing apparatus and the magnitude of change in pressure.

圖5係顯示電漿處理裝置中氮濃度與壓力變化幅度的相關關係之圖表。 Fig. 5 is a graph showing the correlation between the nitrogen concentration and the magnitude of pressure change in the plasma processing apparatus.

圖6為求得微波實際功率的偏差量之步驟流程圖。 Figure 6 is a flow chart showing the steps of determining the amount of deviation of the actual power of the microwave.

圖7係顯示處理容器上部的結構的概略之縱剖視圖。 Fig. 7 is a schematic longitudinal cross-sectional view showing the structure of the upper portion of the processing container.

S1‧‧‧將處理容器12內排氣 S1‧‧‧ will treat the exhaust in the container 12

S2‧‧‧供應氬氣 S2‧‧‧ supply of argon

S3‧‧‧將密閉處理容器12(240Pa) S3‧‧‧Closed processing container 12 (240Pa)

S4‧‧‧供應微波、生成電漿 S4‧‧‧Supply microwave, generate plasma

S5‧‧‧計算壓力-電功率之相關關係 S5‧‧‧ Calculate the correlation between pressure and electric power

S6‧‧‧將處理容器12內排氣 S6‧‧‧ will treat the exhaust in the container 12

S7‧‧‧供應氬氣 S7‧‧‧ supplies argon

S8‧‧‧將密閉處理容器12(240Pa) S8‧‧‧Closed processing container 12 (240Pa)

S9‧‧‧供應微波、生成電漿 S9‧‧‧Supply microwave, generate plasma

S10‧‧‧計算壓力-電功率之相關關係 S10‧‧‧ Calculate the correlation between pressure and electric power

S11‧‧‧計算微波實際功率的偏差量 S11‧‧‧ Calculate the deviation of the actual power of the microwave

Claims (5)

一種電漿處理裝置中之微波實際功率的偏差量檢測方法,係在藉由微波電漿來處理被處理體之電漿處理裝置中,檢測複數電漿處理裝置間所產生之微波實際功率的偏差量之方法;該電漿處理裝置具有:微波產生部,係產生微波;處理容器,係上面呈開口,而用以進行電漿處理;壓力測量機構,係測量該處理容器內的壓力;介電體窗,係氣密地封閉該處理容器的開口部;天線,係配置在該介電體窗的上面;導波管,係使該微波產生部所產生之微波朝該天線傳播並導入至該處理容器;氣體供應部,係對該處理容器內供應氣體;以及排氣部,係將該處理容器內排氣;其中,係使用該電漿處理裝置,而以特定壓力來將氣體供應至排氣後的該處理容器內並加以密閉;以特定電功率將微波導入至該處理容器內而生成該氣體的電漿;測量該電漿處理裝置中電漿生成前的處理容器內壓力與電漿生成後的處理容器內壓力之變化幅度;依據預先求得之作為基準的其他電漿處理裝置中壓力變化幅度與微波供應電功率的相關關係,來求得該電漿處理裝置與該其他電漿處理裝置之間之微波實 際功率的偏差量。 A method for detecting the deviation of the actual power of the microwave in the plasma processing apparatus is for detecting the deviation of the actual power of the microwave generated between the plurality of plasma processing apparatuses in the plasma processing apparatus for treating the object to be processed by microwave plasma The plasma processing device has a microwave generating portion for generating microwaves, a processing container having an opening for performing plasma processing, and a pressure measuring mechanism for measuring a pressure in the processing container; a body window that hermetically closes an opening of the processing container; an antenna disposed on an upper surface of the dielectric window; and a waveguide that causes the microwave generated by the microwave generating portion to propagate toward the antenna and is introduced into the window a processing unit; a gas supply unit for supplying a gas into the processing container; and an exhaust unit for exhausting the inside of the processing container; wherein the plasma processing device is used to supply the gas to the discharge at a specific pressure After the gas is sealed in the processing container; the microwave is introduced into the processing container at a specific electric power to generate a plasma of the gas; and the plasma is measured in the plasma processing device The magnitude of the change in the pressure in the front processing vessel and the pressure in the processing vessel after the plasma is generated; and the correlation between the pressure variation amplitude and the microwave power supply in the other plasma processing apparatus as a reference obtained in advance Microwave between the slurry processing device and the other plasma processing device The amount of deviation of the power. 如申請專利範圍第1項之電漿處理裝置中之微波實際功率的偏差量檢測方法,其中該作為基準之其他電漿處理裝置係已使用於產品的生產之電漿處理裝置。 A method for detecting a deviation amount of microwave actual power in a plasma processing apparatus according to the first aspect of the invention, wherein the other plasma processing apparatus as a reference has been used in a plasma processing apparatus for production of a product. 一種電漿處理裝置,係藉由微波電漿來處理被處理體,其具有:微波產生部,係產生微波;處理容器,係上面呈開口,而用以進行電漿處理;介電體窗,係供該微波穿透並導入至該處理容器內;蓋組件,係支撐該介電體窗並封閉該處理容器的開口;天線,係配置在該介電體窗的上面;介電體板,係配置在該天線的上面;覆蓋板,係配置為覆蓋該介電體板的上方;以及導波管,係連接於該覆蓋板,並將微波朝該天線傳播而導入至該處理容器;其中,該覆蓋板係具備有收容形成於其下面的該介電體板之凹陷部,並且該覆蓋板的外周緣部係具備有朝其外周方向突出所形成之外周突出部,與朝該外周突出部的下方突出所形成之下方突出部;另具備有:支撐於該蓋組件來支撐該覆蓋板的該外周突出部之L字型環狀固定組件、按壓該覆蓋板之 該外周突出部的上面之環狀按壓組件、插通該按壓組件與該覆蓋板的外周突出部且固定在該固定組件之第1接合組件、以及插通該固定組件且固定在該蓋組件之第2接合組件;該按壓組件的垂直部係形成為內周面會抵接於該覆蓋板的該外周突出部,且該按壓組件之垂直部的外周面會抵接於該固定組件的垂直部。 A plasma processing apparatus for treating a processed object by microwave plasma, comprising: a microwave generating portion for generating microwaves; and a processing container having an opening for performing plasma processing; a dielectric window; The microwave is penetrated and introduced into the processing container; the cover assembly supports the dielectric window and closes the opening of the processing container; the antenna is disposed on the upper surface of the dielectric window; the dielectric plate, Arranging on the top of the antenna; a cover plate configured to cover the upper portion of the dielectric plate; and a waveguide connected to the cover plate and propagating the microwave toward the antenna for introduction into the processing container; The cover plate is provided with a recessed portion for accommodating the dielectric plate formed on the lower surface thereof, and the outer peripheral edge portion of the cover plate is provided with an outer peripheral protrusion formed to protrude toward the outer circumferential direction thereof, and protrudes toward the outer periphery a lower protruding portion formed on a lower portion of the portion; and an L-shaped annular fixing member supported on the cover assembly to support the outer peripheral protruding portion of the cover plate, and pressing the cover plate An upper annular pressing assembly of the outer peripheral protruding portion, a first engaging component inserted into the pressing component and the outer peripheral protruding portion of the covering plate, and fixed to the fixing component, and inserted into the fixing component and fixed to the cover assembly a second joint assembly; the vertical portion of the press assembly is formed such that an inner peripheral surface abuts against the outer peripheral protrusion of the cover plate, and an outer peripheral surface of the vertical portion of the pressing assembly abuts a vertical portion of the fixing assembly . 如申請專利範圍第3項之電漿處理裝置,其中較該接合組件要靠處理容器內側的位置處、該冷卻板之外周突出部的上面與按壓組件之水平部的下面之間的位置處、該下方突出部的下面與該固定組件的上面之間的位置處、以及固定組件的下面與處理容器的上面部之間的位置處係分別設置有圓環狀微波遮蔽組件。 A plasma processing apparatus according to claim 3, wherein the joint assembly is located at a position on the inner side of the processing container, at a position between an upper surface of the outer peripheral portion of the cooling plate and a lower portion of the horizontal portion of the pressing member, An annular microwave shielding assembly is disposed at a position between a lower surface of the lower protruding portion and an upper surface of the fixing member, and a position between a lower surface of the fixing assembly and an upper surface portion of the processing container. 如申請專利範圍第3或4項之電漿處理裝置,其係具有形成於該覆蓋板之該下方突出部的外周面與該固定組件的內周面之間隙。 A plasma processing apparatus according to claim 3 or 4, which has a gap formed between an outer peripheral surface of the lower protruding portion of the cover sheet and an inner peripheral surface of the fixing member.
TW101111241A 2011-03-31 2012-03-30 Method for detecting effective power deviations in microwaves in plasma processing devices, and plasma processing device TW201303057A (en)

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