TW201218961A - Method for producing chewing gum surface-coated with flavor substance - Google Patents
Method for producing chewing gum surface-coated with flavor substance Download PDFInfo
- Publication number
- TW201218961A TW201218961A TW100126786A TW100126786A TW201218961A TW 201218961 A TW201218961 A TW 201218961A TW 100126786 A TW100126786 A TW 100126786A TW 100126786 A TW100126786 A TW 100126786A TW 201218961 A TW201218961 A TW 201218961A
- Authority
- TW
- Taiwan
- Prior art keywords
- chewing gum
- powder
- flavor
- sugar
- coated
- Prior art date
Links
- 235000015218 chewing gum Nutrition 0.000 title claims abstract description 89
- 229940112822 chewing gum Drugs 0.000 title claims abstract description 84
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- 239000000126 substance Substances 0.000 title claims abstract description 36
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 16
- 239000000843 powder Substances 0.000 claims abstract description 77
- 239000011248 coating agent Substances 0.000 claims abstract description 60
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- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical group O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 230000001568 sexual effect Effects 0.000 description 1
- 235000019265 sodium DL-malate Nutrition 0.000 description 1
- HELHAJAZNSDZJO-OLXYHTOASA-L sodium L-tartrate Chemical compound [Na+].[Na+].[O-]C(=O)[C@H](O)[C@@H](O)C([O-])=O HELHAJAZNSDZJO-OLXYHTOASA-L 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 239000001509 sodium citrate Substances 0.000 description 1
- 229940005573 sodium fumarate Drugs 0.000 description 1
- 235000019294 sodium fumarate Nutrition 0.000 description 1
- 239000000176 sodium gluconate Substances 0.000 description 1
- 235000012207 sodium gluconate Nutrition 0.000 description 1
- 229940005574 sodium gluconate Drugs 0.000 description 1
- 239000001540 sodium lactate Substances 0.000 description 1
- 235000011088 sodium lactate Nutrition 0.000 description 1
- 229940005581 sodium lactate Drugs 0.000 description 1
- 239000001394 sodium malate Substances 0.000 description 1
- 229940074404 sodium succinate Drugs 0.000 description 1
- ZDQYSKICYIVCPN-UHFFFAOYSA-L sodium succinate (anhydrous) Chemical compound [Na+].[Na+].[O-]C(=O)CCC([O-])=O ZDQYSKICYIVCPN-UHFFFAOYSA-L 0.000 description 1
- 239000001433 sodium tartrate Substances 0.000 description 1
- 229960002167 sodium tartrate Drugs 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 229960002920 sorbitol Drugs 0.000 description 1
- 235000010356 sorbitol Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- BJIOGJUNALELMI-UHFFFAOYSA-N trans-isoeugenol Natural products COC1=CC(C=CC)=CC=C1O BJIOGJUNALELMI-UHFFFAOYSA-N 0.000 description 1
- 235000015870 tripotassium citrate Nutrition 0.000 description 1
- HRXKRNGNAMMEHJ-UHFFFAOYSA-K trisodium citrate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O HRXKRNGNAMMEHJ-UHFFFAOYSA-K 0.000 description 1
- 229940038773 trisodium citrate Drugs 0.000 description 1
- 235000019263 trisodium citrate Nutrition 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- 239000000811 xylitol Substances 0.000 description 1
- 235000010447 xylitol Nutrition 0.000 description 1
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 1
- 229960002675 xylitol Drugs 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G4/00—Chewing gum
- A23G4/02—Apparatus specially adapted for manufacture or treatment of chewing gum
- A23G4/025—Apparatus specially adapted for manufacture or treatment of chewing gum for coating or surface-finishing
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G4/00—Chewing gum
- A23G4/06—Chewing gum characterised by the composition containing organic or inorganic compounds
- A23G4/062—Products for covering, coating, finishing, decorating
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G4/00—Chewing gum
- A23G4/18—Chewing gum characterised by shape, structure or physical form, e.g. aerated products
- A23G4/20—Composite products, e.g. centre-filled, multi-layer, laminated
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Inorganic Chemistry (AREA)
- Confectionery (AREA)
- Medicinal Preparation (AREA)
Abstract
Description
201218961 六、發明說明: 【發明所屬之技術領域】 本發明係有關口香糖之製造方法,特別係有關於表面 塗佈香味物質之非糖衣口香糖之製造方法。 【先前技術】 口香糖係於橡膠基底中添加混合香味物質及軟化劑等 ,可供咀嚼享受其風味及食用感之糖果之總稱。 目前市售之口香糖依形狀大致可分爲2種。其一具有 以往之非糖衣之塊狀、長條狀等形狀。其二爲近年主流之 糖衣口香糖,於表面被覆糖類之粒狀或球狀的口香糖。 口香糖可藉由於將植物性樹脂、醋酸丙乙烯樹脂、酯 橡膠、聚異丁烯、碳酸鈣等加熱混合而製造之橡膠基底中 ’添加混合香味物質等橡膠原料而製造。再將混合後製造 之口香糖經壓延·裁斷·熟成步驟可達完成,但於糖衣口 香糖之製造步驟中,還要再加入於表面被覆添加香味成分 之糖衣層之步驟。 由於糖衣口香糖係自該被覆之糖衣層溶釋出香味,故 於開始咀嚼後才使香味表現,而具有自嚼食開始可享受其 風味之優點。反之,非糖衣口香糖則僅於與橡膠基底混合 時添加香味成分,一般而言香味成分未被添加於表面。因 此,自嚼食開始至香味釋放需花費一段時間。 專利文件1 :特開平6 - 1 5 3 8 0 4號公報 201218961 【發明內容】 [發明欲解決之課題] 本發明之課題係提供自嚼食開始即表現香味之非糖衣 口香糖之製造方法。 專利文件1係揭示一種藉由組合香料與乙醇後使其附 著於表面,可於開封時以及開始嚼食後表現香味之口香糖 。於製造口香糖時之壓延步驟中,爲了防止橡膠黏附於壓 延滾筒上’會於橡膠表面塗佈由粉糖等粉末所構成之防黏 粉,而專利文件1之口香糖,其防黏粉係使用組合經附著 香味成分之蔗糖粉末與乙醇者而製造。 然而’專利文件1之口香糖之製造方法,使蔗糖粉末 等吸附擔載因應需要而使其溶解於乙醇之香味成分,即將 與適當的乙醇粉末等混合之香料糖粉使用爲防黏粉,但存 在調製該香料糖粉需繁雜作業之問題。 [解決課題之手段] 有鑑於上述課題,本發明係有關包含藉由於橡膠基底 中加入砂糖·香料後再混合製成口香糖之步驟,以及於製 成之口香糖上塗佈防黏粉後進行壓延之步驟之非糖衣口香 糖之製造方法,於壓延口香糖之步驟中,其特徵爲將香味 物質塗佈於口香糖係與塗佈防黏粉獨立進行,且較佳係於 塗佈防黏粉之前,將香味物質塗佈於口香糖之非糖衣口香 糖之製造方法。201218961 VI. Description of the Invention: [Technical Field of the Invention] The present invention relates to a method for producing a chewing gum, and more particularly to a method for producing a non-sugar-coated chewing gum having a surface-coated aroma. [Prior Art] Chewing gum is a general term for adding a flavoring substance and a softening agent to a rubber base, which can be chewed to enjoy its flavor and taste. Currently, commercially available chewing gums can be roughly classified into two types according to their shapes. One of them has a shape such as a block shape or a long strip shape of a conventional non-sugar coat. The second is the mainstream sugar-coated chewing gum in recent years, which is coated with granulated or spherical chewing gum of sugar. The chewing gum can be produced by adding a rubber raw material such as a mixed flavoring material to a rubber base produced by heating and mixing a vegetable resin, a vinyl acetate resin, an ester rubber, a polyisobutylene or a calcium carbonate. Further, the chewing gum produced by mixing can be subjected to a calendering, cutting, and aging step, but in the step of producing the sugar-coated chewing gum, a step of coating the sugar-coated layer with the flavor component added to the surface is further added. Since the sugar-coated chewing gum dissolves the flavor from the coated sugar-coated layer, the flavor is expressed after the chewing is started, and the flavor is enjoyed from the beginning of chewing. Conversely, non-sugar-coated chewing gum adds a flavor component only when mixed with a rubber substrate. Generally, the flavor component is not added to the surface. Therefore, it takes a while from the start of chewing to the release of flavor. Patent Document 1: Japanese Laid-Open Patent Publication No. Hei. No. Hei. No. Hei. No. Hei. No. Hei. No. Hei. No. Hei. Patent Document 1 discloses a chewing gum which can be attached to a surface by combining a fragrance with ethanol, which can be expressed at the time of opening and after starting to chew. In the calendering step in the manufacture of chewing gum, in order to prevent the rubber from adhering to the calendering drum, an anti-adhesive powder composed of powder such as powdered sugar is applied to the rubber surface, and the chewing gum of Patent Document 1 has a combination of anti-adhesive powder. It is produced by attaching a sucrose powder of a flavor component to ethanol. However, in the method of producing the chewing gum of the patent document 1, the sucrose powder or the like is dissolved in the flavor component of ethanol as needed, that is, the flavored sugar powder mixed with an appropriate ethanol powder or the like is used as an anti-stick powder, but exists. The problem of complicated work is required to prepare the flavored sugar powder. [Means for Solving the Problem] In view of the above problems, the present invention relates to a step of preparing a chewing gum by adding a sugar and a flavor to a rubber base, and applying the anti-stick powder to the prepared chewing gum for calendering. The method for producing a non-sugar-coated chewing gum, in the step of rolling the chewing gum, characterized in that the application of the aroma substance to the chewing gum system and the application of the anti-adhesive powder are carried out independently, and preferably before the application of the anti-adhesive powder, the fragrance is A method for producing a non-sugar-coated chewing gum in which a substance is applied to a chewing gum.
S -6- 201218961 [發明的效果] 藉由使用本發明之製造方法,可以較簡便之裝置,容 易地製造具優異之香味表現之非糖衣Q香糖。另外,依據 本發明之方法製造之非糖衣口香糖,由於表面塗佈有充分 量之香味物質,自嚼食開始即可表現香味。 圖1係表示一般市售之非糖衣口香糖製造方法之一例 〇 於第1步驟(製造橡膠基底步驟)中,首先,加熱混 合以植物性樹脂爲首之原料而製造橡廖基底。植物性樹脂 係使用將人心果(Sapodilla)之樹的樹液熬煮並凝固之天 然膠乳等。另外亦使用醋酸丙乙烯、酯橡膠、聚異丁烯、 碳酸鈣等。該等原料可僅使用一種,亦可混合2種以上橡 膠基底原料。 於第2步驟(混合步驟)中,以混合機將香味料及軟 化劑等橡膠原料與第1步驟所製造之橡膠基底混合,製作 柔軟且呈固狀之口香糖。香味料可使用單糖類、雙糖類、 寡糖類、糖醇類以及高甜度甜味料等甜味料、精油、香辛 料萃取物、合成香料等香料等。其他橡膠原料可使用酸味 料等及增黏劑等。該等原料亦可僅添加一種,亦可添加2 種以上後混合。於其後再以擠壓機將口香糖再次攪合並使 其均勻,呈薄片狀壓出。 於第3步驟(壓延步驟)中,將第2步驟製造並自擠壓 機壓出之薄片狀的口香糖,以壓延滾筒進行壓延。此時, 爲不使口香糖黏著於壓延滾筒,預先於壓出之口香糖上以 -7- 201218961 麵粉灑粉器塗佈粉糖等粉末狀之防黏粉。防黏粉可因應狀 況使用粉糖、澱粉、甘露糖醇等。另外,壓延步驟可爲使 口香糖成爲最終製品之厚度,分數階段進行。 經壓延步驟之口香糖,依最終商品型態而有所不同’ 但一般係經下述步驟加工爲市售口香糖之形式。首先’於 第4步驟(裁斷步驟)中以裁斷機裁斷爲略正方形時’可 再以附縱向刀刃之滾筒,加入分割線以可分斷爲具有期望 長度之長方狀。加上分割線之口香糖於第5步驟(熟成步 驟)中冷卻熟成,再於第6步驟(包裝·捆包步驟)中’ 自分割線部分分離切斷,將呈長方形狀之口香糖薄片設置 於包裝機,以包裝機具備之刀刃裁斷爲期望的單片的尺寸 ,進行包裝·捆包。 本發明之特徵係於上述第3壓延步驟中,包含於進行 壓延之前於口香糖上塗佈香味物質之步驟。將香味物質塗 佈於口香糖係與塗佈防黏粉獨立進行,而於壓延步驟分爲 數階段進行時,可於任一階段前進行塗佈,但較佳係於塗 佈防黏粉之前,將香味物質塗佈於口香糖。該構成係如圖 2所示,自擠壓機壓出之薄片狀橡膠之表面形成有香味物》 質之層,進而於其上形成防黏粉之層而成。圖2係表示僅 於單面塗佈香味物質與防黏粉之狀態,但亦可於薄片狀W 橡膠之兩面塗佈香味物質以及防黏粉。由於本發明係於該 狀態下使香味物質與薄片狀之橡膠一同藉由壓延滾筒進行 壓延,香味物質被壓附於橡膠表面,而具有香味物質對橡 膠表面附著性高之優點。 -8- 201218961 於第3步驟之壓延步驟中,並未特別限定塗佈於口香 糖之香味物質’亦可使用甜味料、香料、酸味料等任一種 。可僅使用該等之一種,亦可組合2種以上使用。亦可含 有其他的著色料及咖啡因等。塗佈的香味物質可爲與第2 步驟之混合步驟中’混合於橡膠基底之香味料等相同者, 亦可塗佈其他物質。但塗佈液體狀之香味物質時,由於會 出現防黏粉吸收水份後,可能會黏著於壓延滾筒上,以及 於移動時香味物質會被輸送帶等吸附而脫落之可能性,塗 佈之香味物質以粉末狀爲佳。 甜味料可舉出葡萄糖、果糖等單糖類、麥芽糖、乳糖 、庶糖等雙糖類、寡糖、水飴、山梨糖醇、甘露糖醇、木 糖醇、麥芽糖醇、紅藻糖醇、還原巴拉金糖、還原水飴等 糖醇、醋磺內酯鉀及阿斯巴甜等高甜度甜味料,粉末果汁 等。 香料可舉出胡椒薄荷油、荷蘭薄荷油、橘子油、檸檬 油、葡萄柚油、萊姆油、薰衣草油、茉莉花油、鼠尾草油 、月桂油 '洋甘菊油、巴西利油、香菜油、登蔻油、肉桂 油、生薑油、芄妥油、天竺葵油、牛膝草油、鳶尾油、印 蒿油、欖香脂油等精油類、辣椒橙、香草萃取物等香辛料 萃取物、1-薄荷醇、香芹酮、丁香酚、異丁香酚、酯類、 紫羅蘭酮、香草醛、乙基香草醛、麥芽酚等合成香料等。 酸味料可舉出己二酸、衣康酸、檸檬酸、檸檬酸鉀、 檸檬酸三鉀、檸檬酸三鈉、葡萄糖酸-5-內酯、葡萄糖酸 、葡萄糖酸鉀、葡萄糖酸鈉、琥珀酸、琥珀酸鈉、琥珀酸 -9- 201218961 二鈉、醋酸鈉、DL-酒石酸、L-酒石酸、DL-酒石酸鈉、 L·酒石酸鈉、乳酸、乳酸鈉、冰醋酸、植酸、富馬酸、富 馬酸鈉、DL-蘋果酸、DL·蘋果酸鈉以及磷酸等。 另外,爲使香味物質更容易附著於橡膠上,可於塗佈 香味物質前,以水或乙醇等醇類濡濕薄片狀橡膠表面。 並未特別限定塗佈香味物質之方法。若爲可全面塗佈 薄片狀橡膠則爲佳,例如以與防黏粉相同之方法,使用麵 粉灑粉器等撒落香味物質而進行塗佈。 香味物質之塗佈量依所塗佈之香味物質種類而異,而 以相對於口香糖之重量比爲〇.〇1〜3.00%爲佳,〇.〇5〜 1.00%更佳。例如塗佈之香味物質爲薄荷醇粉末香料時, 以 0 · 0 1 〜3.0 0 % 爲佳,0.0 5 〜1 · 0 0 % 亦佳,0.2 5 〜0.5 0 % 更 佳。薄荷醇粉末香料之塗佈量低於0.01 %以下時,自開始 嚼食口香糖時幾乎無法感覺到香味的擴散,而塗佈量高於 3.0 0%以上時,自開始嚼食口香糖時感覺薄荷醇的苦味過 強。 另外,塗佈之香味物質爲胡椒薄荷粉末香料時,以 0.01〜2.00%爲佳,0.05〜1.00%更佳。胡椒薄荷粉末香料 之塗佈量低於〇 . 〇 1 %以下時,自開始嚼食口香糖時幾乎無 法感覺到香味的擴散,而塗佈量高於2.0 0 %以上時,自開 始嚼食口香糖時感覺來自胡椒薄荷的苦澀味過強。 進而,塗佈之香味物質爲檸檬粉末果汁時,以0.01〜 3.00%爲佳,0.05〜1.00%更佳。檸檬粉末果汁之塗佈量低 於0.0 1 %以下時,自開始嚼食口香糖時幾乎無法感覺到香 -10- 201218961 味的擴散,而塗佈量高於3.00 %以上時 糖時感覺來自檸檬果汁粉末的酸味、溫 塗佈之香味物質爲富馬酸時,以I 0.05 〜1.00% 更佳,0.25 〜0.50 % 最佳。 於0.01 %以下時,自開始嚼食口香糖時 味的擴散,而塗佈量高於3.00 %以上時 糖時感覺酸味過強,且香味平衡顯著地 進而,塗佈之香味物質爲檸檬粉讳 2.00%爲佳,0.05 〜1.00 % 更佳,〇.25-粉末香料之塗佈量低於0 · 0 1 %以下時, 時幾乎無法感覺到香味的擴散,而塗f彳 時,自開始嚼食口香糖時感覺苦澀味過, 本發明相對於以往之口香糖製造步 中附加將香味物質塗佈於口香糖係與塗 之步驟而可達成。因此,無需大幅修改 低成本導入。另外,所塗佈之香味物質 依據本發明之方法所製造之口香 瞬間塗佈於表面的香味物質即溶出於 嚼食時,即可表現強烈的香味。 【實施方式】 [實施例1] 使用2 0重量%之天然膠乳等天然 ,自開始嚼食口香 味過強。 1.0 1 〜3 · 0 0 % 爲佳, 富馬酸之塗佈量低 幾乎無法感覺到香 ,自開始嚼食口香 崩解。 香料時,以0.0 1〜 0.50%最佳。檸檬 自開始嚼食口香糖 ί量高於2.0 0 %以上 強。 驟,僅於壓延步驟 佈防黏粉獨立進行 現有設備,且可以 種類亦可容易變更 ,由於在含入口中 液中,而可自開始 脂、20重量%之醋 -11 - 201218961 酸丙乙烯樹脂、15重量%之酯橡膠、10重量%之聚異丁烯 、20重量%之蠟、5重量%之單酸甘油酯、1〇重量%之碳酸 鈣,並根據一般之製造法製造橡膠基底。 再以製造之橡膠基底爲基礎,依表1所示一般之組成 以混合機進行混合,製造口香糖。 表1 橡膠基底 20份 砂糖 60份 葡萄糖 5份 水飴 12份 甘油 1份 胡椒薄荷香料 1份 薄荷醇 1份 製成之口香糖再使用擠壓機進行再混練。經再混練後 自擠壓機壓出之薄片狀的橡膠寬度爲54cm,高度平均爲 2-93cm,橫截面平均爲158cm2。而被壓出之橡膠量平均爲 6 7.2 kg/ 分。 截斷自擠壓機壓出之薄片狀的橡膠的左右兩端,再以 麵粉灑粉器撒落塗佈薄荷醇粉末香料。撒落塗佈之薄荷醇 粉末香料組成係薄荷醇:賦形劑=20 : 80。之後,再撒落 塗佈作爲防黏粉之適量的砂糖。S -6-201218961 [Effects of the Invention] By using the production method of the present invention, it is possible to easily produce a non-sugar-coated chewing gum having an excellent flavor performance by a simple apparatus. Further, the non-sugar-coated chewing gum produced by the method of the present invention exhibits aroma from the beginning of chewing because a sufficient amount of aroma is applied to the surface. Fig. 1 is a view showing an example of a method for producing a non-sugar-coated chewing gum which is generally commercially available. In the first step (step of producing a rubber substrate), first, a rubber-based substrate is produced by heating and mixing a raw material such as a vegetable resin. The vegetable resin is a natural latex which is cooked and solidified by the sap of the tree of the Sapodilla. Further, vinyl acetate, ester rubber, polyisobutylene, calcium carbonate or the like is also used. These materials may be used alone or in combination of two or more kinds of rubber base materials. In the second step (mixing step), a rubber material such as a flavoring material and a softening agent is mixed with a rubber base produced in the first step by a mixer to produce a soft and solid chewing gum. As the flavoring material, a sweetener such as a monosaccharide, a disaccharide, an oligosaccharide, a sugar alcohol, or a high-intensity sweetener, a fragrance such as an essential oil, a spice extract, or a synthetic fragrance can be used. Other rubber materials such as sour materials and tackifiers can be used. These raw materials may be added alone or in combination of two or more. Thereafter, the chewing gum was again stirred by an extruder to make it uniform, and it was extruded in the form of a sheet. In the third step (calendering step), the sheet-like chewing gum which was produced in the second step and pressed out from the extruder was calendered by a calender roll. At this time, in order to prevent the gum from sticking to the calender roll, a powdery anti-adhesive powder such as powdered sugar is applied to the pressed chewing gum by a -7-201218961 flour duster. Anti-adhesive powder can be used in accordance with the condition of powdered sugar, starch, mannitol and the like. Alternatively, the calendering step can be carried out in a fractional stage to make the chewing gum the thickness of the final product. The chewing gum in the calendering step varies depending on the final commercial form', but is generally processed into the form of a commercially available chewing gum by the following procedure. First, in the fourth step (cutting step), when the cutting machine is cut into a square shape, the roller having the longitudinal blade can be added, and the dividing line can be added to be divided into a rectangular shape having a desired length. The chewing gum of the dividing line is cooled and matured in the fifth step (cooking step), and then separated and cut off from the dividing line in the sixth step (packaging and packing step), and the rectangular chewing gum sheet is set in the packaging machine. The packaging and packaging are carried out by cutting the blade with the size of the desired single piece. The present invention is characterized in that in the third calendering step, the step of applying a flavoring substance to the chewing gum before calendering is included. Applying the aroma substance to the chewing gum system separately from applying the anti-sticking powder, and when the calendering step is carried out in several stages, the coating may be performed before any stage, but preferably before applying the anti-adhesive powder, The aroma is applied to the chewing gum. This configuration is as shown in Fig. 2. The surface of the flaky rubber extruded from the extruder is formed with a layer of aroma and a layer of anti-adhesive powder formed thereon. Fig. 2 shows a state in which the aroma substance and the anti-adhesive powder are applied only on one side, but the aroma substance and the anti-adhesive powder may be applied to both sides of the sheet-like W rubber. Since the present invention is such that the aroma substance is calendered together with the sheet-like rubber by the calender roll in this state, the aroma substance is pressed against the rubber surface, and the aroma substance has an advantage of high adhesion to the rubber surface. -8-201218961 In the rolling step of the third step, the flavoring substance applied to the chewing gum is not particularly limited, and any of sweeteners, flavors, and sour materials may be used. These may be used alone or in combination of two or more. It can also contain other coloring materials and caffeine. The applied aroma substance may be the same as the flavoring material mixed in the rubber base in the mixing step of the second step, or may be coated with other substances. However, when a liquid-like aroma substance is applied, since the anti-adhesive powder absorbs moisture, it may adhere to the calender roll, and the aroma substance may be adsorbed and peeled off by the conveyor belt during the movement, and coated. The aroma substance is preferably in the form of a powder. Examples of the sweetener include monosaccharides such as glucose and fructose, disaccharides such as maltose, lactose, and sucrose, oligosaccharides, leeches, sorbitol, mannitol, xylitol, maltitol, erythritol, and reduction of para Gold sugar, reduced water sputum and other sugar alcohols, potassium acesulfame lactone and high-sweet sweeteners such as aspartame, powdered juice, etc. Spices include peppermint oil, menthol oil, orange oil, lemon oil, grapefruit oil, lime oil, lavender oil, jasmine oil, sage oil, bay oil 'chamomile oil, perilla oil, coriander oil, Essential oils such as eucalyptus oil, cinnamon oil, ginger oil, eucalyptus oil, geranium oil, hyssop oil, iris oil, artemisia oil, eucalyptus oil, pepper orange, vanilla extract, etc., 1- Synthetic flavors such as menthol, carvone, eugenol, isoeugenol, esters, ionone, vanillin, ethyl vanillin, maltol, and the like. Examples of the sour material include adipic acid, itaconic acid, citric acid, potassium citrate, tripotassium citrate, trisodium citrate, glucono-5-lactone, gluconic acid, potassium gluconate, sodium gluconate, and amber. Acid, sodium succinate, succinic acid-9- 201218961 disodium, sodium acetate, DL-tartaric acid, L-tartaric acid, DL-sodium tartrate, sodium L-tartrate, lactic acid, sodium lactate, glacial acetic acid, phytic acid, fumaric acid, Sodium fumarate, DL-malic acid, DL·sodium malate, and phosphoric acid. Further, in order to make the aroma substance more easily adhere to the rubber, the surface of the sheet-like rubber may be wetted with an alcohol such as water or ethanol before the application of the flavoring material. The method of applying the aroma substance is not particularly limited. It is preferable to apply the flaky rubber in a full-scale manner, for example, by applying a scented substance such as a flour powder squeegee in the same manner as the anti-adhesive powder. The coating amount of the aroma substance varies depending on the type of the aroma substance to be applied, and the weight ratio with respect to the chewing gum is preferably 〇1 to 3.00%, more preferably 〇5 1.00%. For example, when the aroma substance to be coated is a menthol powder flavor, it is preferably 0·0 1 to 3.0 0%, preferably 0.0 5 to 1 · 0 0 %, more preferably 0.2 5 to 0.5 0 %. When the coating amount of the menthol powder flavor is less than 0.01%, the diffusion of the flavor is hardly felt when the chewing gum is started to be chewed, and when the coating amount is more than 3.0% or more, the menthol is felt when the chewing gum is started. The bitterness is too strong. Further, when the applied aroma is a peppermint powder flavor, it is preferably 0.01 to 2.00%, more preferably 0.05 to 1.00%. When the amount of the peppermint powder flavor is less than 〇. 〇1% or less, the spread of the flavor is hardly felt when the chewing gum is started, and when the coating amount is higher than 2.0%, the chewing gum is started. I feel that the bitter taste from peppermint is too strong. Further, when the aroma substance to be applied is lemon powder juice, it is preferably 0.01 to 3.00%, more preferably 0.05 to 1.00%. When the coating amount of the lemon powder juice is less than 0.01% or less, the spread of the fragrant -10-201218961 taste is hardly felt when the chewing gum is started, and when the coating amount is higher than 3.00%, the sugar is felt from the lemon juice. When the acidity of the powder and the warm coating of the aroma are fumaric acid, it is preferably from 0.05 to 1.00%, and most preferably from 0.25 to 0.50%. When it is 0.01% or less, the taste spreads when chewing gum is started, and when the coating amount is more than 3.00%, the sugar taste is too strong, and the flavor balance is remarkably further, and the applied aroma is lemon powder 2.00 % is better, 0.05 to 1.00% is better. When the coating amount of 〇.25-powder flavor is less than 0 · 0 1%, the diffusion of the fragrance is hardly felt, and when the coating is applied, the food is chewed. The chewing gum feels bitter and tastes. The present invention can be achieved by adding a flavoring substance to the chewing gum system and coating step in the conventional chewing gum manufacturing step. Therefore, there is no need to significantly modify the low cost import. Further, the applied aroma substance The mouth fragrance produced by the method of the present invention, when the aroma substance applied to the surface instantaneously is dissolved in the chew, can express a strong fragrance. [Embodiment] [Example 1] Naturally, 20% by weight of natural latex or the like was used, and the chewing taste was too strong since the beginning. 1.0 1 〜3 · 0 0 % is preferable, the coating amount of fumaric acid is low, and the fragrant taste is hardly felt, and the chewing gum is disintegrated since the beginning. When the fragrance is used, it is preferably 0.01 to 0.50%. Lemon Since the beginning of chewing gum, the amount is higher than 2.0 0%. In the calendering step, the existing equipment can be independently disposed, and the type can be easily changed. Since the liquid is contained in the inlet, the self-starting fat, 20% by weight of vinegar-11 - 201218961 acid propylene vinyl resin, 15% by weight of ester rubber, 10% by weight of polyisobutylene, 20% by weight of wax, 5% by weight of monoglyceride, and 1% by weight of calcium carbonate, and a rubber substrate was produced according to a general production method. Further, based on the manufactured rubber substrate, the mixture was mixed by a mixer according to the general composition shown in Table 1 to produce a chewing gum. Table 1 Rubber base 20 parts Sugar 60 parts Glucose 5 parts Water 饴 12 parts Glycerin 1 part Peppermint spice 1 part Menthol 1 part The chewing gum was re-mixed using an extruder. After re-kneading, the flaky rubber extruded from the extruder has a width of 54 cm, an average height of 2-93 cm, and an average cross-section of 158 cm 2 . The amount of rubber that was extruded was an average of 6 7.2 kg/min. The left and right ends of the flaky rubber extruded from the extruder were cut off, and the menthol powder fragrance was applied by a flour sprinkler. Sprinkled coated menthol Powder flavor composition menthol: Excipient = 20: 80. After that, the appropriate amount of granulated sugar is applied as a release powder.
其次,將薄片狀的橡膠以壓延滾筒經過4階段進行壓 延。經壓延之口香糖厚度爲1 .67mm。經壓延步驟之口香 糖可依照一般的製法裁斷爲板狀橡膠之形狀爲7.20cm XNext, the flaky rubber was rolled in four stages by a calender roll. The calendered chewing gum has a thickness of 1.67 mm. The chewing gum of the calendering step can be cut into a shape of a plate rubber of 7.20 cm X according to a general method.
S -12- 201218961 1.90cm之長方形。 薄荷醇粉末香料之塗佈量係如下述表2所示,可使其 於相對於橡膠重量爲0 · 0 0 5 %〜3 · 5 0 %之間變化。針對製作 之各口香糖,採用訓練有素之專門受試員進行與香味表現 有關之綜合性的官能評價,並將評價結果示於表2。表中 記號係具下述之意義。 ◎:具非常優異之香味擴散,且全體香味的平衡佳, 極佳。 〇:具優異之香味擴散,且全體香味的平衡亦佳。 △:稍缺乏香味擴散,或全體香味的平衡不佳。 X:欠缺香味擴散,或全體香味的平衡不佳》 表2 實施例1中塗佈薄荷醇粉末香料之口香糖之官能評價結果 塗佈量(%) 官能評價 備考 0.005 X 未感覺豳效果。 0.01 △ 具有涼感擴散效果。但效果微弱。 0.05 〇 初咀嚼即有清涼感。 0.25 ◎ 具清爽的擴散感。適度的平衡感。 0.50 ◎ 效果大。咀嚼瞬間即有清涼感擴散。 1.00 〇 含入口中瞬間。即有清涼感擴散彳曰伴隨稍稍的苦味。 3.00 Δ 效果大但苦味亦強。 3.50 X 具衝撃感俏苦味過強。 自表2可得知薄荷醇粉末香料之塗佈量相對於橡膠重 量爲0.0 0 5 %時’幾乎未感受到塗佈薄荷醇粉末香料之效果 。而塗佈量爲0.01 %時,雖然效果微弱但自開始嚼食時香 -13- 201218961 味擴散即增加,可發現塗佈薄荷醇粉末香料之效果。 0.05 %〜1.0 0%時自開始嚼食即具優異的香味擴散效果 全體香味的平衡亦佳。特別於塗佈0.25%或0.50%時, 擴散效果極佳,且全體香味的平衡佳,爲極佳之結果 於塗佈量爲3.00%時,雖可自開始嚼食即感受到非常 的香味擴散效果,但亦出現來自薄荷醇強烈的苦味, 成全體香味的平衡欠佳之結果。塗佈量爲3 · 5 0%時, 過強而不適於嚼食。 因此,塗佈之香味物質爲薄荷醇粉末香料時,試 果爲塗佈量以0.01〜3.00%爲佳,0.05〜1.00%亦佳, 〜0.50%最佳。 [實施例2 ] 以實施例1製造之橡膠基底爲基礎,依表1所示一 組成以混合機進行混合,與實施例1相同製造口香糖 使用擠壓機進行再混練。截斷自擠壓機壓出之薄片狀 膠的左右兩端,再以麵粉灑粉器撒落塗佈胡椒薄荷粉 料。胡椒薄荷粉末香料組成係賦形劑(阿拉伯橡膠等 香料成分=8 5 : 1 5。之後,與實施例1相同,撒落塗佈 粉後進行壓延·裁斷。 胡椒薄荷粉末香料之塗佈量係如下述表3所示’ 其於相對於橡膠重量爲0.005%〜2.50%之間變化。針 作之各口香糖,與實施例1相同’採用訓練有素之專 試員進行與香味表現有關之綜合性的官能評價’並將 塗佈 ,且 香味 。而 強烈 而造 苦味 驗結 0.25 般之 ,再 的橡 末香 ): 防黏 可使 對製 門受 評價S -12- 201218961 1.90cm rectangle. The coating amount of the menthol powder flavor is as shown in the following Table 2, and it can be changed from 0. 0.05% to 3.50% with respect to the weight of the rubber. For each of the produced chewing gums, a well-trained and specialized test subject was used to perform a comprehensive functional evaluation related to the expression of the fragrance, and the evaluation results are shown in Table 2. The symbols in the table have the following meanings. ◎: It has a very good fragrance spread, and the balance of the whole fragrance is excellent and excellent. 〇: The fragrance is excellent, and the balance of the whole fragrance is also good. △: A slight lack of fragrance spread, or the balance of the entire fragrance is not good. X: lack of fragrance diffusion, or poor balance of the entire fragrance. Table 2 Functional evaluation results of the chewing gum coated with menthol powder flavor in Example 1. Coating amount (%) Functional evaluation Preparation 0.005 X No sensation effect. 0.01 △ has a cool diffusion effect. But the effect is weak. 0.05 〇 There is a cool feeling when chewing at the beginning. 0.25 ◎ With a refreshing sense of diffusion. Moderate balance. 0.50 ◎ The effect is large. At the moment of chewing, there is a cooling sensation. 1.00 〇 Contains an instant in the entrance. That is, there is a cooling sensation, accompanied by a slight bitterness. 3.00 Δ The effect is large but the bitterness is also strong. 3.50 X has a strong taste and is too bitter. It can be seen from Table 2 that when the coating amount of the menthol powder flavor is 0.055% with respect to the weight of the rubber, the effect of coating the menthol powder flavor is hardly felt. When the coating amount was 0.01%, although the effect was weak, the flavor spread was increased from the start of chewing, and the effect of coating the menthol powder flavor was found. 0.05%~1.0 0% When you start chewing, you will have an excellent fragrance diffusion effect. The balance of the whole fragrance is also good. Especially when coating 0.25% or 0.50%, the diffusion effect is excellent, and the balance of the whole fragrance is good. It is an excellent result. When the coating amount is 3.00%, although the chewing is started, the fragrance is very diffused. The effect, but also the strong bitterness from menthol, the result of a poor balance of the overall fragrance. When the coating amount is 3 · 50%, it is too strong to be chewy. Therefore, when the applied aroma substance is a menthol powder flavor, the coating amount is preferably 0.01 to 3.00%, more preferably 0.05 to 1.00%, and most preferably 0.50%. [Example 2] Based on the rubber substrate produced in Example 1, a composition was mixed by a mixer according to the composition shown in Table 1, and the chewing gum was produced in the same manner as in Example 1 and re-kneaded using an extruder. The left and right ends of the flaky rubber extruded from the extruder were cut off, and the peppermint powder was spread by a flour sprinkler. The peppermint powder flavor composition is an excipient (a fragrance component such as Arabian rubber = 85:15. Thereafter, in the same manner as in Example 1, the coating powder is sprinkled and then rolled and cut. The coating amount of the peppermint powder flavor is As shown in the following Table 3, it varies between 0.005% and 2.50% with respect to the weight of the rubber. Each chewing gum is the same as in the first embodiment. A well-trained tester is used to perform the synthesis related to the fragrance performance. Sexual faculty evaluation 'will be coated and scented. Strong and bitter taste will be checked 0.25, then the scent of the oak): Anti-adhesive can evaluate the door
S -14- 201218961 結果不於表3'。 表3 實施例2中塗f 市胡椒薄荷粉末香料之口香糖之官能評價結果 __ 塗佈量(%) 官能評價 備考 __ 0.005 X 幾乎未感覺到效果。 _- 0.01 Δ 稍感覺胡椒薄荷般的擴散效果。但效果微弱。__ 0.05 〇 初咀嚼即有胡椒薄:荷般的擴散效果。 ___- 0.25 ◎ 咀嚼瞬間即具有胡椒薄荷,清涼感的擴散效果 0.50 〇 效果大。具有醇厚度之胡椒薄荷的擴散效果。__ 1.00 〇 含入口中瞬間即有胡椒薄荷擴散。仴伴隨&許苦雜迷_1__ 2.00 Δ 效果大但苦澀味強。 __- 2.50 X 具衝撃感但苦澀味過強。 ____ 自表3可得知胡椒薄荷粉末香料之塗佈量相對於橡膠 重量爲0.00 5 %時,幾乎未感受到塗佈胡椒薄荷粉末香料之 效果》而塗佈量爲0.01 %時,雖然效果微弱但自開始嚼食 時香味擴散即增加,可發現塗佈胡椒薄荷粉末香料之效果 。塗佈0·〇5%〜1.00%時自開始嚼食即具優異的胡椒薄荷香 味擴散效果,且全體香味的平衡亦佳。塗佈量2.00%時, 雖可自開始嚼食即感受到非常強烈的香味擴散效果,但亦 出現來自胡椒薄荷強烈的苦澀味,而造成全體香味的平衡 欠佳之結果。塗佈量爲2.5 0 %時,苦澀味過強而不適於嚼 食。 因此’塗佈之香味物質爲胡椒薄荷粉末香料時,試驗 結果爲塗佈量以0 · 0 1〜2.0 0 %爲佳,〇 . 0 S〜1 . 0 0 %亦佳。 -15- 201218961 [實施例3 ] 以實施例1製造之橡膠基底爲基礎,依表4所示一般之 組成以混合機進行混合製造口香糖’再使用擠壓機進行再 混練。 表4 橡膠基底 20份 砂糖 60份 葡萄糖 5份 酸味料 1份 水飴 12份 甘油 1份 檸檬香料 1份 再混練後,截斷自擠壓機壓出之薄片狀的橡膠的左右 兩端,再以麵粉灑粉器撒落塗佈檸檬粉末果汁。檸檬粉末 果汁之組成係環糊精:檸檬濃縮果汁=75 : 25,濃縮果汁 之濃縮倍率爲3.5倍。之後,與實施例1相同’撒落塗佈防 黏粉後進行壓延·裁斷。 檸檬粉末果汁之塗佈量係如下述表5所示’可使其於 相對於橡膠重量爲〇 . 〇 〇 5 %〜3 · 5 0 %之間變化。針對製作之 各口香糖,與實施例1相同,採用訓練有素之專門受試員 進行與香味表現有關之綜合性的官能評價,並將評價結果 示於表5。S -14- 201218961 The result is not shown in Table 3'. Table 3 Functional evaluation results of the chewing gum of the f pepper peppermint powder flavor in Example 2 __ Coating amount (%) Functional evaluation Remarks __ 0.005 X The effect was hardly felt. _- 0.01 Δ A little peppermint-like diffusion effect. But the effect is weak. __ 0.05 初 At the beginning of chewing, there is a thin pepper: a diffusion effect like a lotus. ___- 0.25 ◎ It has peppermint at the moment of chewing, and the diffusion effect of coolness is 0.50 〇. The diffusion effect of peppermint with an alcohol thickness. __ 1.00 胡椒 Instantly peppermint spreads in the mouth.仴 Companion & 苦苦杂_1__ 2.00 Δ The effect is large but bitter and strong. __- 2.50 X has a sense of rush but bitter taste is too strong. ____ From Table 3, it can be seen that when the coating amount of the peppermint powder flavor is 0.005% with respect to the weight of the rubber, the effect of applying the peppermint powder flavor is hardly felt, and the coating amount is 0.01%, although the effect is weak. However, since the spread of the fragrance is increased from the start of chewing, the effect of coating the peppermint powder flavor can be found. When the coating is applied from 0% to 5% to 1.00%, it is excellent in the spread of peppermint flavor and the balance of the whole fragrance. When the coating amount is 2.00%, a very strong flavor diffusion effect can be felt from the start of chewing, but a strong bitterness from peppermint is also caused, resulting in a poor balance of the overall fragrance. When the coating amount is 2.5%, the bitter taste is too strong to be chewy. Therefore, when the coated aroma is a peppermint powder flavor, the test result is preferably 0. 0 1 to 2.0 0%, and 〇 0 S~1. 0 0 % is also preferable. -15-201218961 [Example 3] Based on the rubber substrate produced in Example 1, a mixture of a chewing gum was prepared by a mixer in accordance with the general composition shown in Table 4, and re-kneading was carried out using an extruder. Table 4 Rubber base 20 parts sugar 60 parts glucose 5 parts sour material 1 part water mash 12 parts glycerin 1 part lemon spice 1 part and then kneaded, cut off the left and right ends of the flaky rubber extruded from the extruder, and then flour The duster is spread to coat the lemon powder juice. Lemon powder The composition of the juice is cyclodextrin: lemon concentrated juice = 75: 25, concentrated juice is 3.5 times concentrated. Thereafter, in the same manner as in Example 1, the anti-adhesive powder was applied by being dropped, and then rolling and cutting were performed. The coating amount of the lemon powder juice is as shown in the following Table 5, which can be changed from 〇 〇 5 % to 3 · 50 % with respect to the weight of the rubber. For each of the produced chewing gums, a comprehensive functional evaluation relating to the expression of the flavor was carried out by using a trained and specialized tester in the same manner as in Example 1, and the evaluation results are shown in Table 5.
S -16- 201218961 表5 實施例3中塗佈檸檬粉末果汁之口香糖之官能評僭結果 塗佈量(%) 官能評價 備考 0.005 X 未感覺到效果。 0.01 Δ 衝擊感低。僅能感覺果汁感之程度。 0.05 〇 衝擊感稍低但檸檬果汁感擴散。 0.25 〇 初咀嚼瞬即可“覺檸檬果汁感。 0.50 ◎ 具檸檬果汁感。具適度的平衡。 1.00 〇 含入口中瞬間即可感覺果汁感。具醇厚香味。 3.00 Λ 具衝撃感但酸味澀味強。 3.50 X 具衝撃感但酸味澀味過強。 自表5可得知檸檬粉末果汁之塗佈量相對於橡膠重量 爲0.00 5 %時,幾乎未感受到塗佈檸檬粉末果汁之效果。而 塗佈量爲0.01%時,雖然效果微弱但自開始嚼食時香味擴 散即增加,可發現塗佈檸檬粉末果汁之效果。塗佈0.05% 〜1.00%時自開始嚼食即具優異的檸檬香味擴散效果,且 全體香味的平衡亦佳。塗佈量3.00%時,雖可自開始嚼食 即感受到非常強烈的香味擴散效果,但亦出現來自檸檬果 汁強烈的酸味、澀味,而造成全體香味的平衡欠佳之結果 。塗佈量爲3.50%時,酸味、澀味過強而不適於嚼食。 因此,塗佈之香味物質爲檸檬粉末果汁時,試驗結果 爲塗佈量以0.0 1〜3.0 0 %爲佳,0.0 5〜1.0 0 %亦佳。 [實施例4] 以實施例1製造之橡膠基底爲基礎,依表4所示一般之 組成以混合機進行混合,與實施例1相同製造口香糖,再 -17- 201218961 使用擠壓機進行再混練。再混練後,截斷自擠壓機壓出之 薄片狀的橡膠的左右兩端’再以麵粉灑粉器撒落塗佈富馬 酸。富馬酸純度爲99%以上,粒度爲100 mesh pass ( 95% )。之後,與實施例1相同,撒落塗佈防黏粉後進行壓延 •裁斷。 富馬酸之塗佈量係如下述表6所示,可使其於相對於 橡膠重量爲0.005%〜3.50%之間變化。針對製作之各口香 糖,與實施例1相同採用訓練有素之專門受試員進行與香 味表現有關之綜合性的官能評價,並將評價結果示於表6 表6 實施例4中塗佈富馬酸之口香糖之官能評價結果 塗佈量(%) 官能評價 備考 0.005 X 未感覺到效果。 0.01 △ 衝撃感低。僅有感覺之程度。 0.05 〇 初咀嚼即有酸味感。 0.25 ◎ 初咀嚼即有酸味感。酸味具醇厚度。 0.50 ◎ 初咀嚼即有酸味感。衝擊感大 1.00 〇 含入口中瞬間酸味感擴散。刺激感稍強。 3.00 Δ 具衝擊感但酸味稍強。 3.50 X 具衝撃感但酸味過強。 自表6可得知富馬酸之塗佈量相對於橡膠重量爲 0.00 5 %時,幾乎未感受到塗佈富馬酸之效果。而塗佈量爲 0.0 1 %時,雖然效果微弱但自開始嚼食時香味擴散即增加 ,可發現塗佈富馬酸之效果。在塗佈〇·〇5%〜1.00 %之場合S -16- 201218961 Table 5 Functional evaluation results of chewing gum coated with lemon powder juice in Example 3. Coating amount (%) Functional evaluation Remarks 0.005 X No effect was felt. 0.01 Δ Low impact. Only feel the degree of juice feeling. 0.05 〇 The impact is slightly lower but the lemon juice is spread. 0.25 〇 咀 咀 咀 即可 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 3.50 X has a squeaking sensation but a too strong sour taste. From Table 5, it can be seen that when the coating amount of the lemon powder juice is 0.005% relative to the weight of the rubber, the effect of applying the lemon powder juice is hardly felt. When the coating amount is 0.01%, although the effect is weak, the flavor spread is increased from the start of chewing, and the effect of applying the lemon powder juice can be found. When the coating is 0.05% to 1.00%, the lemon flavor is excellent since the start of chewing. The diffusion effect is good, and the balance of the whole fragrance is also good. When the coating amount is 3.00%, although a very strong flavor diffusion effect can be felt from the beginning of chewing, there is also a strong sourness and astringency from the lemon juice, which causes the whole The result of poor balance of the fragrance. When the coating amount is 3.50%, the sour taste and the astringency are too strong to be chewed. Therefore, when the applied aroma is lemon powder juice, the test result is the coating amount. 0.0 1 to 3.0 0% is preferably 0.0 5 to 1.0%. [Example 4] Based on the rubber substrate produced in Example 1, the mixture was mixed by a general machine according to the general composition shown in Table 4, and was carried out. Example 1 was made of the same chewing gum, and then -17-201218961 was re-kneaded using an extruder. After re-mixing, the left and right ends of the flaky rubber extruded from the extruder were cut off and then spread by a flour sprinkler. Fumaric acid. The purity of fumaric acid was 99% or more, and the particle size was 100 mesh pass (95%). Thereafter, in the same manner as in Example 1, the anti-adhesive powder was applied and rolled, and then subjected to calendering and cutting. The amount can be changed from 0.005% to 3.50% with respect to the weight of the rubber as shown in the following Table 6. For each of the produced chewing gums, the trained tester and the fragrance were used in the same manner as in Example 1. The comprehensive functional evaluation was performed, and the evaluation results are shown in Table 6. Table 6 Functional evaluation results of the fumaric acid-coated chewing gum in Example 4 Coating amount (%) Functional evaluation preparation 0.005 X No effect was observed. 0.01 △ The feeling of rushing is low. Only the degree of sensation. 0.05 〇 At the beginning of chewing, there is a sour taste. 0.25 ◎ The initial chew has a sour taste. The sour taste has an alcoholic thickness. 0.50 ◎ The initial chew has a sour taste. The impact is 1.00 〇. The instant sour taste spreads in the mouth. The stimulation is slightly stronger. 3.00 Δ It has a strong impact but a slightly strong acidity. 3.50 X has a strong scent but a too strong acidity. From Table 6, it can be seen that when the coating amount of fumaric acid is 0.005% relative to the weight of the rubber, almost no coating of fumaric acid is felt. When the coating amount is 0.01%, the effect of coating fumaric acid can be found, although the effect is weak, but the fragrance diffusion increases from the start of chewing. In the case of coating 〇·〇 5%~1.00%
S -18- 201218961 ,自開始嚼食時酸味感之擴散佳,且全體香味均衡上亦有 良好結果。特別於塗佈0.25%或0.50%時,酸味擴散效果極 佳,且全體香味的平衡佳,爲極佳之結果。塗佈量爲 3.0 0%時,雖可自開始嚼食即感受到非常強烈的香味擴散 效果,但亦感受到相當強烈的酸味,而造成全體香味的平 衡欠佳之結果。塗佈量爲3.50%時,酸味過強而不適於嚼 食。 因此,塗佈之香味物質爲富馬酸時,試驗結果爲塗佈 量以 0 · 0 1 〜3.0 0 % 爲佳,0 · 0 5 〜1 · 0 0 % 亦佳,0 · 2 5 % 〜0.5 0 % 最佳。 [實施例5] 以實施例1製造之橡膠基底爲基礎,依表4所示一般之 組成以混合機進行混合,與實施例1相同製造口香糖,再 使用擠壓機進行再混練。截斷自擠壓機壓出之薄片狀的橡 膠的左右兩端,再以麵粉灑粉器撒落塗佈檸檬粉末香料。 檸檬粉末香料組成係賦形劑(阿拉伯橡膠等):香料成分 =8 5 : 1 5。之後,與實施例1相同,撒落塗佈防黏粉後進行 壓延·裁斷。 檸檬粉末香料之塗佈量係如下述表7所示,可使其於 相對於橡膠重量爲0.005%〜2.50%之間變化。針對製作之 各口香糖,與實施例1相同,採用訓練有素之專門受試員 進行與香味表現有關之綜合性的官能評價,並將評價結果 示於表7。 -19- 201218961 表7 實施例5中塗佈檸檬粉末香; 科之口香糖之官能評價結果 塗佈量(%) 官能評價 備考 0.005 X 未感覺到效果。 0.01 Δ 衝擊感低。僅能感覺檸檬味被強化。 0.05 〇 初咀嚼即有檸檬感擴散。但效果微弱。 0.25 ◎ 初咀嚼即有檸檬果汁感。 0.50 ◎ 衝擊感大。檸檬感具醇厚度。 1.00 〇 含入口中瞬間即有檸檬感擴散。但刺激稍強。 2.00 Δ 具衝撃感但苦澀味稍強。 2.50 X 具衝撃感但苦澀味渦強。 自表7可得知檸檬粉末香料之塗佈量相對於橡膠重量 爲0.00 5 %時,幾乎未感受到塗佈檸檬粉末香料之效果。而 塗佈量爲0 · 0 1 %時,雖然效果微弱但自開始嚼食時香味擴 散即增加,可發現塗佈檸檬粉末香料之效果。塗佈0.05% 〜1.0 0%時自開始嚼食即具優異的檸檬香味擴散效果,且 全體香味的平衡亦佳。特別於塗佈0.25%或0.50%時,檸檬 香味擴散效果極佳,且全體香味的平衡佳,爲極佳之結果 。塗佈量2.00%時,雖可自開始嚼食即感受到非常強烈的 香味擴散效果,但亦出現強烈的苦澀味,而造成全體香味 的平衡欠佳之結果。塗佈量爲2.5 0%時,苦澀味過強而不 適於嚼食。 因此,塗佈之香味物質爲檸檬粉末香料時,試驗結果 爲塗佈量以〇 · 〇 1〜2 · 0 0 %爲佳,〇 . 〇 5〜1 . 0 0 %亦佳’ 0 _ 2 5 % 〜0.5 0%時可獲得期望之結果。S -18- 201218961, the spread of sourness is good when starting to chew, and the overall fragrance has good results. Especially when the coating is 0.25% or 0.50%, the acid taste diffusion effect is excellent, and the balance of the entire fragrance is excellent, which is an excellent result. When the coating amount is 3.0 0%, a very strong flavor diffusion effect can be felt from the start of chewing, but a strong acid taste is also felt, resulting in a poor balance of the entire fragrance. When the coating amount is 3.50%, the sourness is too strong to be suitable for chewing. Therefore, when the applied aroma is fumaric acid, the test result is preferably 0. 0 1 to 3.0 0 %, 0 · 0 5 〜1 · 0 0 % is also good, 0 · 2 5 % 〜 0.5 0 % is the best. [Example 5] Based on the rubber substrate produced in Example 1, the composition was mixed by a mixer according to the general composition shown in Table 4, and the chewing gum was produced in the same manner as in Example 1, and then re-kneaded using an extruder. The left and right ends of the flaky rubber extruded from the extruder were cut off, and the lemon powder flavor was spread by a flour sprinkler. Lemon powder flavor composition excipient (arab rubber, etc.): perfume ingredient = 8 5 : 15 . Thereafter, in the same manner as in Example 1, the anti-adhesive powder was applied by dropping, and then rolling and cutting were performed. The coating amount of the lemon powder flavor is as shown in the following Table 7, and it can be changed from 0.005% to 2.50% with respect to the weight of the rubber. For each of the produced chewing gums, a comprehensive sensory evaluation relating to the expression of the flavor was carried out by using a trained and specialized tester in the same manner as in Example 1, and the evaluation results are shown in Table 7. -19- 201218961 Table 7 Coating of lemon powder in Example 5; Functional evaluation result of chewing gum of the group Coating amount (%) Functional evaluation Remarks 0.005 X No effect was felt. 0.01 Δ Low impact. Only the lemon flavor can be felt to be strengthened. 0.05 〇 At the beginning of chewing, there is a lemony spread. But the effect is weak. 0.25 ◎ At the beginning of chewing, there is a lemon juice feeling. 0.50 ◎ Large impact. Lemon has an alcoholic thickness. 1.00 柠檬 Instantly there is a lemony spread in the mouth. But the stimulus is slightly stronger. 2.00 Δ has a sense of sputum but a bitter taste. 2.50 X has a rushing sensation but a bitter taste vortex. It can be seen from Table 7 that when the coating amount of the lemon powder flavor is 0.005% with respect to the weight of the rubber, the effect of applying the lemon powder flavor is hardly felt. On the other hand, when the coating amount was 0 · 0 1%, although the effect was weak, the fragrance spread was increased from the start of chewing, and the effect of applying the lemon powder flavor was found. When applying 0.05% to 1.00%, it is excellent in the spread of lemon flavor since the start of chewing, and the balance of the whole fragrance is also good. Especially when coating 0.25% or 0.50%, the lemon flavor is excellent in diffusion and the balance of the whole fragrance is excellent, which is an excellent result. When the coating amount is 2.00%, a very strong flavor spread effect can be felt from the start of chewing, but a strong bitterness is also exhibited, resulting in a poor balance of the entire fragrance. When the coating amount is 2.50%, the bitter taste is too strong to be suitable for chewing. Therefore, when the applied aroma is lemon powder flavor, the test result is preferably 〇· 〇1~2 · 0 0 %, 〇. 〇5~1 . 0 0 %也佳' 0 _ 2 5 The desired result is obtained when % ~ 0.5 0%.
S -20- 201218961 【圖式簡單說明】 [圖1]表示一般市售之非糖衣口香糖製造方法之流程 圖。 [圖2]表示本發明塗佈香味物質與防黏粉之模式圖。 -21 -S -20- 201218961 [Simplified description of the drawings] [Fig. 1] shows a flow chart of a method for producing a non-sugar-coated chewing gum which is generally commercially available. Fig. 2 is a schematic view showing the application of the fragrance substance and the anti-adhesive powder of the present invention. -twenty one -
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| JPS4849962A (en) * | 1971-10-26 | 1973-07-14 | ||
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| FI760471A7 (en) * | 1975-03-19 | 1976-09-20 | Life Savers Inc | |
| IE50130B1 (en) * | 1979-10-04 | 1986-02-19 | Warner Lambert Co | Aspartame-sweetened chewing gum and method of producing same |
| US4562076A (en) * | 1982-12-27 | 1985-12-31 | Wm. Wrigley Jr. Company | Chewing gum with coating of thaumatin or monellin and method |
| JPH06153804A (en) | 1992-11-25 | 1994-06-03 | Lotte Co Ltd | Chewing gum |
| JP3801818B2 (en) * | 1999-09-22 | 2006-07-26 | カネボウ株式会社 | Flavor expression chewing gum |
| JP2003000157A (en) * | 2001-06-26 | 2003-01-07 | Freunt Ind Co Ltd | Particle-adhered food and method for producing the same |
| JP2011505142A (en) * | 2007-11-29 | 2011-02-24 | キャドバリー アダムス ユーエスエー エルエルシー | Fine particle coating |
-
2010
- 2010-07-30 JP JP2010172089A patent/JP2012029639A/en active Pending
-
2011
- 2011-07-26 WO PCT/JP2011/004189 patent/WO2012014440A1/en not_active Ceased
- 2011-07-26 KR KR1020187030513A patent/KR102015239B1/en active Active
- 2011-07-26 KR KR1020137004987A patent/KR20130137141A/en not_active Ceased
- 2011-07-28 TW TW100126786A patent/TWI620507B/en active
Also Published As
| Publication number | Publication date |
|---|---|
| KR102015239B1 (en) | 2019-08-27 |
| JP2012029639A (en) | 2012-02-16 |
| KR20130137141A (en) | 2013-12-16 |
| WO2012014440A1 (en) | 2012-02-02 |
| KR20180119690A (en) | 2018-11-02 |
| TWI620507B (en) | 2018-04-11 |
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