SU64700A1 - The method of obtaining therapeutic balm - Google Patents
The method of obtaining therapeutic balmInfo
- Publication number
- SU64700A1 SU64700A1 SU4769A SU4769A SU64700A1 SU 64700 A1 SU64700 A1 SU 64700A1 SU 4769 A SU4769 A SU 4769A SU 4769 A SU4769 A SU 4769A SU 64700 A1 SU64700 A1 SU 64700A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- resin
- fir
- obtaining therapeutic
- balm
- obtaining
- Prior art date
Links
- 230000001225 therapeutic effect Effects 0.000 title description 4
- 238000000034 method Methods 0.000 title description 3
- 241000021559 Dicerandra Species 0.000 title 1
- 235000010654 Melissa officinalis Nutrition 0.000 title 1
- 239000000865 liniment Substances 0.000 title 1
- 239000011347 resin Substances 0.000 description 10
- 229920005989 resin Polymers 0.000 description 10
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 238000004821 distillation Methods 0.000 description 3
- 235000007173 Abies balsamea Nutrition 0.000 description 2
- 239000004857 Balsam Substances 0.000 description 2
- 244000018716 Impatiens biflora Species 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 150000002989 phenols Chemical class 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 229910021578 Iron(III) chloride Inorganic materials 0.000 description 1
- 241000218657 Picea Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
- 235000019438 castor oil Nutrition 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000010645 fir oil Substances 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 235000021588 free fatty acids Nutrition 0.000 description 1
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 1
- 239000010446 mirabilite Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 150000008442 polyphenolic compounds Chemical class 0.000 description 1
- 235000013824 polyphenols Nutrition 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000010079 rubber tapping Methods 0.000 description 1
- RSIJVJUOQBWMIM-UHFFFAOYSA-L sodium sulfate decahydrate Chemical compound O.O.O.O.O.O.O.O.O.O.[Na+].[Na+].[O-]S([O-])(=O)=O RSIJVJUOQBWMIM-UHFFFAOYSA-L 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
Landscapes
- Cosmetics (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Description
Предлагаемый способ получени лечебного бальзама из живицы пихты заключаетс в том, что живицу раствор ют в органическом растворителе, отфильтрованный раствор промывают водой дл удалени фенолов и свободных жирных кислот, затем отгон ют растворитель и легколетучке терпены и полученный продукт раствор ют в очищенном касторовом масле.The proposed method of obtaining a therapeutic balsam from the fir resin is that the resin is dissolved in an organic solvent, the filtered solution is washed with water to remove phenols and free fatty acids, then the solvent and the volatile terpenes are distilled off and the resulting product is dissolved in purified castor oil.
Исходным сырьем дл получени лечебного бальзама вл етс пихтова живица, полученна подсочкой , или экстракционным путем , требующа последовательного применени специальных методов очистки, облагораживани , удалени из нее раздражающих и прижигающих примесей и концентрировани до оптимальной дл лечебных целей консистенции.The raw material for obtaining a therapeutic balsam is spruce resin obtained by tapping or extraction, requiring the sequential use of special methods of cleaning, refining, removing irritating and cauterizing impurities from it, and concentrating to the optimum consistency for therapeutic purposes.
В результате такой обработки химический состав пихтовой живицы измен етс вместе с ее физическими свойствами (в зкость, удельный вес и пр.)Технологическа схема переработки пихтовой живицы складываетс из следующих операций:As a result of this treatment, the chemical composition of fir resin is changed along with its physical properties (viscosity, specific gravity, etc.). The technological scheme for processing fir fir resin consists of the following operations:
1) Растворение живицы в серном эфире, пихтовом масле, или в продукте отгона пихтовой живицы с паром -в пихтовом терпентине .1) Dissolving the resin in sulfuric ether, fir oil, or in the product of the distillate fir fir resin with steam, in fir firings.
2)Фильтраци полученного подвижного раствора через фильтр Шотта NO 4, фильтровальную бумагу или фильтровальную диагональ; здесь удал ютс все механические примеси.2) Filtration of the resulting mobile solution through a Schott NO 4 filter, filter paper or filter diagonal; here all mechanical impurities are removed.
3)Промывка фильтрованного раствора дестиллированной водой 1 : 1 п тикратно или более до полного исчезновени кислой реакции на лакмус и окраски с хлорным железом на фенолы; промывкой удал ютс водорастворимые кислоты и полифенолы.3) Rinse the filtered solution with distilled water 1: 1 for 5 or more times until the acidic reaction to litmus is completely disappeared and stained with ferric chloride for phenols; water-soluble acids and polyphenols are removed by washing.
4)Декантаци или разделение на делительной воронке раствора живицы от промывной воды и осушение раствора живицы свежепрокаленной глауберовой солью или хлористым кальцием.4) Decanting or separating the solution of resin from the washing water on a separating funnel and drying the solution of the resin of freshly rolled Glauber's salt or calcium chloride.
5)Отгонка растворител из живицы , причем дл серного эфира отгонка вначале (в течение двух часов) ведетс без включени вакуума на вод ной бане с приемным холодильником, улавливающим и охлаждающим пары эфира, затем включаетс вакуум-разрежение и дальнейша отгонка идет при разрежении в 15-20 мм ртутного столба при темпера5) Distillation of the solvent from the resin; moreover, for sulfuric ether, the distillation is first (within two hours) carried out without switching on the vacuum in a water bath with a suction cooler, which catches and cools the ether vapor, then vacuum suction is started and further distillation takes place at a vacuum of 15 -20 mmHg at tempera
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU4769A SU64700A1 (en) | 1942-05-21 | 1942-05-21 | The method of obtaining therapeutic balm |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU4769A SU64700A1 (en) | 1942-05-21 | 1942-05-21 | The method of obtaining therapeutic balm |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU64700A1 true SU64700A1 (en) | 1944-11-30 |
Family
ID=48245360
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU4769A SU64700A1 (en) | 1942-05-21 | 1942-05-21 | The method of obtaining therapeutic balm |
Country Status (1)
| Country | Link |
|---|---|
| SU (1) | SU64700A1 (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2116067C1 (en) * | 1996-04-30 | 1998-07-27 | Иван Семенович Парфенов | Preparation containing essential or turpentine oil and a method of its preparing |
| RU2140278C1 (en) * | 1998-01-26 | 1999-10-27 | Жлудов Владимир Мелентьевич | Method of fir balsam "olesya" producing |
-
1942
- 1942-05-21 SU SU4769A patent/SU64700A1/en active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2116067C1 (en) * | 1996-04-30 | 1998-07-27 | Иван Семенович Парфенов | Preparation containing essential or turpentine oil and a method of its preparing |
| RU2140278C1 (en) * | 1998-01-26 | 1999-10-27 | Жлудов Владимир Мелентьевич | Method of fir balsam "olesya" producing |
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