SU23618A1 - The method of preparation of micanite - Google Patents
The method of preparation of micaniteInfo
- Publication number
- SU23618A1 SU23618A1 SU22429A SU22429A SU23618A1 SU 23618 A1 SU23618 A1 SU 23618A1 SU 22429 A SU22429 A SU 22429A SU 22429 A SU22429 A SU 22429A SU 23618 A1 SU23618 A1 SU 23618A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- micanite
- preparation
- resins
- reaction
- hydroxy
- Prior art date
Links
- 238000000034 method Methods 0.000 title description 7
- 238000002360 preparation method Methods 0.000 title description 2
- 239000011347 resin Substances 0.000 description 6
- 229920005989 resin Polymers 0.000 description 6
- -1 hydroxy aldehydes Chemical class 0.000 description 5
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000010445 mica Substances 0.000 description 2
- 229910052618 mica group Inorganic materials 0.000 description 2
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 1
- DCXXMTOCNZCJGO-UHFFFAOYSA-N Glycerol trioctadecanoate Natural products CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 1
- LGRFSURHDFAFJT-UHFFFAOYSA-N Phthalic anhydride Natural products C1=CC=C2C(=O)OC(=O)C2=C1 LGRFSURHDFAFJT-UHFFFAOYSA-N 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 239000010426 asphalt Substances 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- JHIWVOJDXOSYLW-UHFFFAOYSA-N butyl 2,2-difluorocyclopropane-1-carboxylate Chemical compound CCCCOC(=O)C1CC1(F)F JHIWVOJDXOSYLW-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical class OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Substances OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 150000001261 hydroxy acids Chemical class 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000025 natural resin Substances 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Silicates, Zeolites, And Molecular Sieves (AREA)
Description
В патенте № 11209 приведено описан-ие способа получени искусственных смол нагреванием многоатомных оксикислот , оксиальдегидов или оксикетонов в присутствии весьма незначительных количеств ароматических сульфокислот, как катализаторов. При этом участие нескольких компонентов дл реакции смолообразовани не вл етс об зательным . Каждое в отдельности оксисоединение , например глинокаль, глицерин, макнит, молочна и винио-лимонна кислота и т. д., при нагревании с 0,1-0,2% нафталин - В - сульфокислоты способно давать лосле сильной реакции, св занной с выделением большого количества воды, прозрачные, полутвердые и светлые смолы. Консинстенцию и другие свойства получаемых смол можно измен ть, ввод в реакцию несколько оксисоединений совместно или комбиниру оксисоединени с другими веществами , как-то: парафинами, нафталином, естественными смолами, растительными маслами, животными жирами, стеарином, елейном, пекали, асфальтами и т. п.Patent No. 11209 describes a process for producing synthetic resins by heating polyhydric hydroxy acids, hydroxy aldehydes or hydroxy ketones in the presence of very small amounts of aromatic sulfonic acids as catalysts. In this case, the involvement of several components for the gum reaction is not necessary. Individually, each oxo compound, such as alumina, glycerin, maknitol, lactic and vino-citric acid, etc., when heated with 0.1–0.2% naphthalene — B — sulfonic acid, can give a strong reaction to the elimination of large amounts of water, clear, semi-solid and light resin. The consistency and other properties of the resulting resins can be altered by entering into the reaction several oxo compounds together or combining the oxo compounds with other substances, such as paraffins, naphthalene, natural resins, vegetable oils, animal fats, stearin, oil, baking, asphalt, etc. P.
С.молы, полученные по вышеописанному способу, не представл ют собою конечного полимеризованного продукта и нуждаютс в дополнительном прогреве в течение 10-15 часов при 160°, после чего они приобретают нерастворимость, погодостойкость и твердость.The resins obtained by the above method do not represent the final polymerized product and need additional heating for 10-15 hours at 160 °, after which they acquire insolubility, weather resistance and hardness.
ЛГ. if.LH. if.
Получаемые подобным образом смолы , названные авторами „глипонами, па своим свойствам весьма близки к „глиптал м , запатентованным „General Electric Со.The resins obtained in a similar way, called by the authors „glypons, are very close in their properties to„ glyptal m, patented by „General Electric Co.
В журнале „Агд Mittelungen за окт брь 1927 г. (№ 10. S. 415-416) сообщаетс о весьма успешном применении в последнее врем „глипталей дл изготовлени миканита. В предлагаемом изобретении приготовление миканита производитс следующим образом: мелко расщепленные листочки слюды проклеиваютс с.молою („глипоны).The journal Mittelungen Agde for October 1927 (No. 10. S. 415-416) reported on the very recent successful use of glyptals for the manufacture of micanite. In the present invention, the preparation of micanite is carried out as follows: finely split mica sheets are glued to the molar (glipons).
Проклеенна стопа листочков прессуетс под небольщим давлением и затем прогреваетс 15-20 часов при температуре, близкой к 180°.The glued foot of the leaflets is pressed under low pressure and then warms up for 15–20 hours at a temperature close to 180 °.
Преимуществом этого способа изобретатели считают именно то, что дл его приготовлени не требуетс фталевого ангидрида (примен ющегос пра глиптальном способе), отсутствующего у нас на рынке.The advantage of this method is that the inventors believe that it does not require the use of phthalic anhydride (using the correct glyptal method), which is absent from the market.
Предмет изобретени .The subject matter of the invention.
Способ приготовлени миканита путем проклеивани слюды смолами, отличающийс тем, что в качестве св зующего вещества примен ют смолу,, полученную по способу, изложенному в патенте № 11209.A method for preparing micanite by sizing mica with resins, characterized in that resin used in the process described in patent No. 11209 is used as a binder.
1ИИ. «Печатный TfjK1and. "Printed TfjK
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU22429A SU23618A1 (en) | 1928-01-05 | 1928-01-05 | The method of preparation of micanite |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU22429A SU23618A1 (en) | 1928-01-05 | 1928-01-05 | The method of preparation of micanite |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU23618A1 true SU23618A1 (en) | 1931-10-31 |
Family
ID=48342119
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU22429A SU23618A1 (en) | 1928-01-05 | 1928-01-05 | The method of preparation of micanite |
Country Status (1)
| Country | Link |
|---|---|
| SU (1) | SU23618A1 (en) |
-
1928
- 1928-01-05 SU SU22429A patent/SU23618A1/en active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| SU23618A1 (en) | The method of preparation of micanite | |
| CH342753A (en) | Process for the preparation of a stable solution of a curable condensation product from melamine, thiourea and formaldehyde | |
| DE635926C (en) | Process for the production of stand oils with wood oil character | |
| SU6822A1 (en) | The method of obtaining non-melting and insoluble condensation products of phenols with aldehydes | |
| SU48305A1 (en) | The method of obtaining resinous condensation products | |
| SU51730A1 (en) | The method of obtaining artificial resin | |
| DE356224C (en) | Process for the preparation of resinous condensation products | |
| DE733679C (en) | Process for the production of cation-exchanging synthetic resins based on phenol | |
| DE884424C (en) | Process for the production of curable synthetic resins | |
| US1736757A (en) | Reaction products of a natural resin-phenolic resinous material and method of making same | |
| SU27789A1 (en) | The method of producing glyptal resins | |
| GB160482A (en) | Process for the treatment of wood or other substances containing cellulose for the purpose of obtaining cellulose and artificial resin, asphalt, lac and the like | |
| DE968543C (en) | Cation exchanger | |
| SU11209A1 (en) | The method of obtaining artificial resin | |
| SU62782A1 (en) | The method of obtaining thermosetting artificial resin | |
| SU39901A1 (en) | Lacquer manufacturing method | |
| SU61851A1 (en) | The method of obtaining cast transparent artificial resin | |
| DE438228C (en) | Process for the distillation of raw coal | |
| DE609729C (en) | Process for the production of curable, meltable condensation products from aromatic amines and aldehydes, which are soluble in organic solvents | |
| DE858703C (en) | Process for the manufacture of tanning agents | |
| DE710770C (en) | Process for the production of resinous condensation products | |
| SU18348A1 (en) | Method for purification of condensation products of phenols with aldehydes | |
| DE715288C (en) | Process for the production of synthetic resins | |
| SU5145A1 (en) | The method of obtaining synthetic resins | |
| DE721060C (en) | Process for the preparation of resinous condensation products |