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SE8007141L - PROCEDURE FOR PREPARING PENICILLANIC ACID DERIVATIVES - Google Patents

PROCEDURE FOR PREPARING PENICILLANIC ACID DERIVATIVES

Info

Publication number
SE8007141L
SE8007141L SE8007141A SE8007141A SE8007141L SE 8007141 L SE8007141 L SE 8007141L SE 8007141 A SE8007141 A SE 8007141A SE 8007141 A SE8007141 A SE 8007141A SE 8007141 L SE8007141 L SE 8007141L
Authority
SE
Sweden
Prior art keywords
carboxy group
acid derivatives
penicillanic acid
procedure
antibiotics
Prior art date
Application number
SE8007141A
Other languages
Swedish (sv)
Other versions
SE449613B (en
Inventor
I S Vangedal
Original Assignee
Leo Pharm Prod Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Leo Pharm Prod Ltd filed Critical Leo Pharm Prod Ltd
Publication of SE8007141L publication Critical patent/SE8007141L/en
Publication of SE449613B publication Critical patent/SE449613B/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D499/00Heterocyclic compounds containing 4-thia-1-azabicyclo [3.2.0] heptane ring systems, i.e. compounds containing a ring system of the formula:, e.g. penicillins, penems; Such ring systems being further condensed, e.g. 2,3-condensed with an oxygen-, nitrogen- or sulfur-containing hetero ring

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Cephalosporin Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Compounds of the formula I <IMAGE> in which R1 stands for hydrogen, alkyl, alkoxy, halogen, or trifluoromethyl, and R2 stands for a carboxy group or for a protected carboxy group, in particular an esterified carboxy group; or, if appropriate, a salt thereof, are obtained by oxidising the corresponding penicillanic acid derivatives or their sulfoxides with hydrogen peroxide in the presence of a tungsten or molybdenum catalyst. This process eliminates secondary degradative oxidative side reactions and simplifies the isolation and purification of the product, thus providing high yields and thereby being particularly suited for large scale production. The compounds of formula I, depending upon the meanings of R1 and R2, are of value as beta -lactamase inhibitors and/or antibiotics, and/or as intermediates in the production of antibiotics and/or beta -lactamase inhibitors.
SE8007141A 1979-10-11 1980-10-10 PROCEDURE FOR PREPARING 1,1-DIOXOPENICILLANIC ACID DERIVATIVES SE449613B (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB7935284 1979-10-11
GB7942062 1979-12-05

Publications (2)

Publication Number Publication Date
SE8007141L true SE8007141L (en) 1981-04-12
SE449613B SE449613B (en) 1987-05-11

Family

ID=26273161

Family Applications (1)

Application Number Title Priority Date Filing Date
SE8007141A SE449613B (en) 1979-10-11 1980-10-10 PROCEDURE FOR PREPARING 1,1-DIOXOPENICILLANIC ACID DERIVATIVES

Country Status (11)

Country Link
CA (1) CA1142174A (en)
CH (1) CH646174A5 (en)
DE (1) DE3037896A1 (en)
DK (1) DK154085C (en)
FR (1) FR2467210A1 (en)
GB (1) GB2059960B (en)
IE (1) IE50650B1 (en)
IT (1) IT1132938B (en)
LU (1) LU82842A1 (en)
NL (1) NL8005626A (en)
SE (1) SE449613B (en)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4331599A (en) * 1981-02-02 1982-05-25 Pfizer Inc. Sparingly water-soluble salts of penicillanic acid 1,1-dioxide
US4381263A (en) * 1981-03-23 1983-04-26 Pfizer Inc. Process for the preparation of penicillanic acid esters
IN159362B (en) * 1981-03-23 1987-05-09 Pfizer
US4502988A (en) * 1983-08-08 1985-03-05 Eli Lilly And Company Oxidation process
GB2206579B (en) * 1987-07-10 1991-05-29 Erba Farmitalia 6a and 6b-(substituted methyl)-penicillanic acid derivatives
CN102977120B (en) * 2012-12-14 2015-05-27 江西富祥药业股份有限公司 Method for preparing and crystallizing sulbactam pivoxyl

Also Published As

Publication number Publication date
IT8025223A0 (en) 1980-10-09
DK154085C (en) 1989-02-27
IT1132938B (en) 1986-07-09
DE3037896A1 (en) 1981-04-23
IE801963L (en) 1981-04-11
GB2059960B (en) 1983-10-19
LU82842A1 (en) 1981-06-04
NL8005626A (en) 1981-04-14
DK424080A (en) 1981-04-12
FR2467210B1 (en) 1983-08-19
IE50650B1 (en) 1986-06-11
DK154085B (en) 1988-10-10
CA1142174A (en) 1983-03-01
SE449613B (en) 1987-05-11
CH646174A5 (en) 1984-11-15
GB2059960A (en) 1981-04-29
FR2467210A1 (en) 1981-04-17

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