RU2018139094A - Синтез цеолита типа aei - Google Patents
Синтез цеолита типа aei Download PDFInfo
- Publication number
- RU2018139094A RU2018139094A RU2018139094A RU2018139094A RU2018139094A RU 2018139094 A RU2018139094 A RU 2018139094A RU 2018139094 A RU2018139094 A RU 2018139094A RU 2018139094 A RU2018139094 A RU 2018139094A RU 2018139094 A RU2018139094 A RU 2018139094A
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- RU
- Russia
- Prior art keywords
- porous oxide
- coating
- aluminosilicate
- crystals
- oxide coating
- Prior art date
Links
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 title claims 17
- 229910021536 Zeolite Inorganic materials 0.000 title claims 10
- 239000010457 zeolite Substances 0.000 title claims 10
- 230000015572 biosynthetic process Effects 0.000 title claims 4
- 238000003786 synthesis reaction Methods 0.000 title claims 4
- 239000011248 coating agent Substances 0.000 claims 10
- 238000000576 coating method Methods 0.000 claims 10
- 239000013078 crystal Substances 0.000 claims 9
- 229910000323 aluminium silicate Inorganic materials 0.000 claims 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims 4
- 229910052723 transition metal Inorganic materials 0.000 claims 3
- 150000003624 transition metals Chemical class 0.000 claims 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims 2
- 150000002500 ions Chemical class 0.000 claims 2
- 239000000377 silicon dioxide Substances 0.000 claims 2
- JPVYNHNXODAKFH-UHFFFAOYSA-N Cu2+ Chemical compound [Cu+2] JPVYNHNXODAKFH-UHFFFAOYSA-N 0.000 claims 1
- 229910017052 cobalt Inorganic materials 0.000 claims 1
- 239000010941 cobalt Substances 0.000 claims 1
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims 1
- 229910001431 copper ion Inorganic materials 0.000 claims 1
- 229910052742 iron Inorganic materials 0.000 claims 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 229910052759 nickel Inorganic materials 0.000 claims 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/04—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof using at least one organic template directing agent, e.g. an ionic quaternary ammonium compound or an aminated compound
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
- B01J29/72—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65 containing iron group metals, noble metals or copper
- B01J29/76—Iron group metals or copper
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
- B01J29/78—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65 containing arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
- C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/54—Particles characterised by their aspect ratio, i.e. the ratio of sizes in the longest to the shortest dimension
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Crystallography & Structural Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Catalysts (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
Claims (10)
1. Покрытие из пористого оксида, включающее кристаллы AEI цеолита, имеющие среднее аспектовое отношение (L/D) менее чем или равное 3.
2. Покрытие из пористого оксида по п.1, где кристаллы алюмосиликатного AEI цеолита имеют среднее аспектовое отношение (L/D) менее чем или равное 2.
3. Покрытие из пористого оксида по п.1, где кристаллы алюмосиликатного AEI цеолита имеют средний размер кристалла от примерно 0,05 до примерно 5 мкм.
4. Покрытие из пористого оксида по п.1, где кристаллы алюмосиликатного AEI цеолита имеют средний размер кристалла от примерно 1 до примерно 1,5 мкм.
5. Покрытие из пористого оксида по п.1, где кристаллы алюмосиликатного AEI цеолита имеют соотношение диоксида кремния к оксиду алюминия от примерно 10 до примерно 35.
6. Покрытие из пористого оксида по п.1, где кристаллы алюмосиликатного AEI цеолита имеют соотношение диоксида кремния к оксиду алюминия от примерно 15 до примерно 25.
7. Покрытие из пористого оксида по п.1, где кристаллы алюмосиликатного AEI цеолита содержат обменные ионы одного или нескольких переходных металлов после синтеза.
8. Покрытие из пористого оксида по п.7, где переходные металлы включают, по меньшей мере, один металл, выбранный из группы, состоящей из марганеца, железа, кобальта, никеля и их смеси.
9. Покрытие из пористого оксида по п.7, где количество обменных ионов одного или нескольких переходных металлов после синтеза составляет от примерно 0,1 до примерно 10 мас.%.
10. Покрытие из пористого оксида по п.1, где алюмосиликатный цеолит содержит от примерно 0,5 до примерно 5 мас.% обменных ионов меди после синтеза из расчета на общий вес цеолита.
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201361898155P | 2013-10-31 | 2013-10-31 | |
| US61/898,155 | 2013-10-31 | ||
| US201361907615P | 2013-11-22 | 2013-11-22 | |
| US61/907,615 | 2013-11-22 |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2016121171A Division RU2672744C2 (ru) | 2013-10-31 | 2014-10-31 | Синтез цеолита типа aei |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| RU2018139094A true RU2018139094A (ru) | 2019-03-04 |
| RU2018139094A3 RU2018139094A3 (ru) | 2021-07-29 |
| RU2764725C2 RU2764725C2 (ru) | 2022-01-19 |
Family
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Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2018139094A RU2764725C2 (ru) | 2013-10-31 | 2014-10-31 | Синтез цеолита типа aei |
| RU2016121171A RU2672744C2 (ru) | 2013-10-31 | 2014-10-31 | Синтез цеолита типа aei |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2016121171A RU2672744C2 (ru) | 2013-10-31 | 2014-10-31 | Синтез цеолита типа aei |
Country Status (10)
| Country | Link |
|---|---|
| US (2) | US9919296B2 (ru) |
| EP (2) | EP3878813A1 (ru) |
| JP (2) | JP6513652B2 (ru) |
| KR (1) | KR102298258B1 (ru) |
| CN (4) | CN108439426A (ru) |
| BR (1) | BR112016009688B1 (ru) |
| DE (1) | DE102014115865A1 (ru) |
| GB (1) | GB2521909B (ru) |
| RU (2) | RU2764725C2 (ru) |
| WO (1) | WO2015063501A1 (ru) |
Families Citing this family (38)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP6513652B2 (ja) * | 2013-10-31 | 2019-05-15 | ジョンソン、マッセイ、パブリック、リミテッド、カンパニーＪｏｈｎｓｏｎ Ｍａｔｔｈｅｙ Ｐｕｂｌｉｃ Ｌｉｍｉｔｅｄ Ｃｏｍｐａｎｙ | Ａｅｉゼオライトの合成 |
| JP6318990B2 (ja) * | 2014-08-29 | 2018-05-09 | 東ソー株式会社 | Ａｅｉ型ゼオライトの製造方法 |
| US10399858B2 (en) | 2014-11-03 | 2019-09-03 | California Institute Of Technology | Producing zeolite SSZ-39 using isomeric mixtures of organic structure directing agents |
| CN107074569B (zh) * | 2014-11-21 | 2019-09-13 | 三菱化学株式会社 | Aei型沸石、其制造方法和其用途 |
| CA2979346C (en) | 2015-03-15 | 2021-03-23 | Sachem, Inc. | Structure directing agent for improved synthesis of zeolites |
| WO2017026484A1 (ja) * | 2015-08-13 | 2017-02-16 | 東ソー株式会社 | Ａｅｉ型ゼオライトの製造方法 |
| JP2017036204A (ja) * | 2015-08-13 | 2017-02-16 | 東ソー株式会社 | Ａｅｉ型ゼオライトの製造方法 |
| JP6759833B2 (ja) * | 2015-08-19 | 2020-09-23 | 東ソー株式会社 | Ａｅｉ型ゼオライトの製造方法 |
| JP6834250B2 (ja) * | 2015-09-01 | 2021-02-24 | 東ソー株式会社 | Ａｅｉ型ゼオライトの製造方法 |
| EP3374316B1 (en) * | 2015-11-11 | 2021-01-27 | Johnson Matthey Public Limited Company | Aluminosilicate aei zeolite preparation |
| JP6769107B2 (ja) * | 2016-05-19 | 2020-10-14 | 三菱ケミカル株式会社 | Ａｅｉ型ゼオライトの製造方法 |
| CN108473328B (zh) * | 2016-05-25 | 2021-12-07 | 环球油品公司 | 高电荷密度金属磷酸盐分子筛 |
| EP3519357A1 (en) * | 2016-09-30 | 2019-08-07 | Johnson Matthey Public Limited Company | Synthesis of aei and cu-aei zeolites |
| US10737252B2 (en) * | 2016-09-30 | 2020-08-11 | Johnson Matthey Public Limited Company | High silica AEI zeolite |
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| CA3067708C (en) | 2017-06-19 | 2022-10-04 | Sachem, Inc. | Process for ssz-39 synthesis using modified reaction composition |
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| CN109384246B (zh) * | 2017-08-10 | 2021-06-25 | 中触媒新材料股份有限公司 | 一种aei结构分子筛及其制备方法和应用 |
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| JP7502275B2 (ja) * | 2018-09-11 | 2024-06-18 | ビーエーエスエフ コーポレーション | 骨格型ａｅｉを有するゼオライト材料の製造方法 |
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-
2014
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- 2014-10-31 CN CN201810458635.4A patent/CN108439426A/zh active Pending
- 2014-10-31 RU RU2018139094A patent/RU2764725C2/ru active
- 2014-10-31 US US14/529,647 patent/US9919296B2/en active Active
- 2014-10-31 RU RU2016121171A patent/RU2672744C2/ru active
- 2014-10-31 DE DE201410115865 patent/DE102014115865A1/de active Pending
- 2014-10-31 KR KR1020167014174A patent/KR102298258B1/ko not_active Expired - Fee Related
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- 2014-10-31 CN CN202110107855.4A patent/CN112939011B/zh active Active
- 2014-10-31 EP EP21165655.8A patent/EP3878813A1/en active Pending
- 2014-10-31 BR BR112016009688-6A patent/BR112016009688B1/pt not_active IP Right Cessation
- 2014-10-31 WO PCT/GB2014/053242 patent/WO2015063501A1/en not_active Ceased
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Also Published As
| Publication number | Publication date |
|---|---|
| JP2019147735A (ja) | 2019-09-05 |
| DE102014115865A1 (de) | 2015-04-30 |
| KR20160075758A (ko) | 2016-06-29 |
| CN112939010B (zh) | 2024-01-09 |
| JP6513652B2 (ja) | 2019-05-15 |
| US20180193824A1 (en) | 2018-07-12 |
| CN104591204A (zh) | 2015-05-06 |
| US9919296B2 (en) | 2018-03-20 |
| EP3063093B1 (en) | 2021-06-16 |
| BR112016009688A2 (ru) | 2017-08-01 |
| GB201419427D0 (en) | 2014-12-17 |
| KR102298258B1 (ko) | 2021-09-07 |
| BR112016009688B1 (pt) | 2021-11-16 |
| JP6836620B2 (ja) | 2021-03-03 |
| CN112939010A (zh) | 2021-06-11 |
| US20150118150A1 (en) | 2015-04-30 |
| JP2016538217A (ja) | 2016-12-08 |
| EP3063093A1 (en) | 2016-09-07 |
| GB2521909B (en) | 2018-05-09 |
| US10940466B2 (en) | 2021-03-09 |
| RU2764725C2 (ru) | 2022-01-19 |
| CN112939011A (zh) | 2021-06-11 |
| GB2521909A (en) | 2015-07-08 |
| RU2016121171A (ru) | 2017-12-05 |
| RU2672744C2 (ru) | 2018-11-19 |
| RU2018139094A3 (ru) | 2021-07-29 |
| CN108439426A (zh) | 2018-08-24 |
| WO2015063501A1 (en) | 2015-05-07 |
| EP3878813A1 (en) | 2021-09-15 |
| CN112939011B (zh) | 2025-02-11 |
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