RU2018104698A - Подложка, снабженная системой тонких слоев с термическими свойствами - Google Patents
Подложка, снабженная системой тонких слоев с термическими свойствами Download PDFInfo
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- RU2018104698A RU2018104698A RU2018104698A RU2018104698A RU2018104698A RU 2018104698 A RU2018104698 A RU 2018104698A RU 2018104698 A RU2018104698 A RU 2018104698A RU 2018104698 A RU2018104698 A RU 2018104698A RU 2018104698 A RU2018104698 A RU 2018104698A
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- Prior art keywords
- layer
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- functional
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- 239000000126 substance Substances 0.000 title 1
- 239000010410 layer Substances 0.000 claims 44
- 238000000576 coating method Methods 0.000 claims 18
- 239000011248 coating agent Substances 0.000 claims 15
- 239000000463 material Substances 0.000 claims 13
- 239000002346 layers by function Substances 0.000 claims 12
- 229910052751 metal Inorganic materials 0.000 claims 12
- 239000002184 metal Substances 0.000 claims 12
- 230000000087 stabilizing effect Effects 0.000 claims 9
- 230000000903 blocking effect Effects 0.000 claims 8
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims 6
- 230000004888 barrier function Effects 0.000 claims 5
- 239000011521 glass Substances 0.000 claims 5
- 230000003287 optical effect Effects 0.000 claims 5
- 239000000758 substrate Substances 0.000 claims 5
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims 3
- 239000011787 zinc oxide Substances 0.000 claims 3
- 239000011651 chromium Substances 0.000 claims 2
- 239000010955 niobium Substances 0.000 claims 2
- 229910052710 silicon Inorganic materials 0.000 claims 2
- 239000010703 silicon Substances 0.000 claims 2
- 239000010936 titanium Substances 0.000 claims 2
- 229910018072 Al 2 O 3 Inorganic materials 0.000 claims 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims 1
- 229910004298 SiO 2 Inorganic materials 0.000 claims 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 claims 1
- 229910052782 aluminium Inorganic materials 0.000 claims 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims 1
- 230000005540 biological transmission Effects 0.000 claims 1
- 229910052804 chromium Inorganic materials 0.000 claims 1
- VNNRSPGTAMTISX-UHFFFAOYSA-N chromium nickel Chemical compound [Cr].[Ni] VNNRSPGTAMTISX-UHFFFAOYSA-N 0.000 claims 1
- 239000005340 laminated glass Substances 0.000 claims 1
- 238000001755 magnetron sputter deposition Methods 0.000 claims 1
- 229910001092 metal group alloy Inorganic materials 0.000 claims 1
- 229910044991 metal oxide Inorganic materials 0.000 claims 1
- 150000004706 metal oxides Chemical class 0.000 claims 1
- 238000000034 method Methods 0.000 claims 1
- 229910001120 nichrome Inorganic materials 0.000 claims 1
- 229910052759 nickel Inorganic materials 0.000 claims 1
- 229910052758 niobium Inorganic materials 0.000 claims 1
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 claims 1
- 150000004767 nitrides Chemical class 0.000 claims 1
- 239000011241 protective layer Substances 0.000 claims 1
- -1 silicon nitrides Chemical class 0.000 claims 1
- 229910052709 silver Inorganic materials 0.000 claims 1
- 239000004332 silver Substances 0.000 claims 1
- 229910052719 titanium Inorganic materials 0.000 claims 1
Classifications
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- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B17/00—Layered products essentially comprising sheet glass, or glass, slag, or like fibres
- B32B17/06—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
- B32B17/10—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin
- B32B17/10005—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing
- B32B17/10165—Functional features of the laminated safety glass or glazing
- B32B17/10174—Coatings of a metallic or dielectric material on a constituent layer of glass or polymer
- B32B17/1022—Metallic coatings
- B32B17/10229—Metallic layers sandwiched by dielectric layers
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B7/00—Layered products characterised by the relation between layers; Layered products characterised by the relative orientation of features between layers, or by the relative values of a measurable parameter between layers, i.e. products comprising layers having different physical, chemical or physicochemical properties; Layered products characterised by the interconnection of layers
- B32B7/02—Physical, chemical or physicochemical properties
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- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/22—Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
- C03C17/225—Nitrides
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- C—CHEMISTRY; METALLURGY
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- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
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- C03C17/23—Oxides
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- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
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- C—CHEMISTRY; METALLURGY
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- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/0021—Reactive sputtering or evaporation
- C23C14/0036—Reactive sputtering
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- C—CHEMISTRY; METALLURGY
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- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
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- C23C14/3464—Sputtering using more than one target
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/30—Properties of the layers or laminate having particular thermal properties
- B32B2307/304—Insulating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/40—Properties of the layers or laminate having particular optical properties
- B32B2307/416—Reflective
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/24—Structurally defined web or sheet [e.g., overall dimension, etc.]
- Y10T428/24942—Structurally defined web or sheet [e.g., overall dimension, etc.] including components having same physical characteristic in differing degree
- Y10T428/2495—Thickness [relative or absolute]
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/24—Structurally defined web or sheet [e.g., overall dimension, etc.]
- Y10T428/24942—Structurally defined web or sheet [e.g., overall dimension, etc.] including components having same physical characteristic in differing degree
- Y10T428/2495—Thickness [relative or absolute]
- Y10T428/24967—Absolute thicknesses specified
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Claims (38)
1. Материал, содержащий прозрачную подложку, покрытую системой тонких слоев, содержащей последовательно, начиная от подложки, чередование трех функциональных металлических слоев на основе серебра, обозначенных, считая от подложки, как первый, второй и третий функциональные слои, и чередование четырех диэлектрических покрытий, обозначенных, считая от подложки, как M1, M2, M3 и M4, причем каждое диэлектрическое покрытие содержит по меньшей мере один диэлектрический слой, так что каждый функциональный металлический слой расположен между двумя диэлектрическими покрытиями, отличающийся тем, что:
- толщина первого функционального слоя меньше толщины второго функционального слоя,
- толщина первого функционального слоя меньше толщины третьего функционального слоя,
- диэлектрические покрытия M1 и M2 имеют оптические толщины Eo1 и Eo2, соответственно, которые удовлетворяют следующему соотношению: Eo2<1,1·Eo1.
2. Материал по п. 1, отличающийся тем, что отношение толщины третьего функционального металлического слоя к толщине второго функционального слоя составляет от 0,90 до 1,10, включая граничные значения.
3. Материал по одному из предыдущих пунктов, отличающийся тем, что три функциональных металлических слоя удовлетворяют следующим условиям:
- толщина первого функционального металлического слоя составляет от 6 до 12 нм,
- толщина второго функционального металлического слоя составляет от 13 до 20 нм,
- толщина третьего функционального металлического слоя составляет от 13 до 20 нм.
4. Материал по любому из предыдущих пунктов, отличающийся тем, что система тонких слоев дополнительно содержит по меньшей мере один блокирующий слой, находящийся в контакте с функциональным слоем, выбранный из металлических слоев на основе металла или металлического сплава, металлонитридных слоев, металлоксидных слоев и металлооксинитридных слоев с одним или несколькими элементами, выбранными из титана, никеля, хрома и ниобия, такой как слой Ti, TiN, TiOx, Nb, NbN, Ni, NiN, Cr, CrN, NiCr, NiCrN.
5. Материал по предыдущему пункту, отличающийся тем, что полная толщина всех блокирующих слоев, находящихся в контакте с функциональными слоями, составляет от 0,1 до 2 нм, включая граничные значения.
6. Материал по одному из предыдущих пунктов, отличающийся тем, что диэлектрические покрытия удовлетворяют следующим условиям:
- оптическая толщина первого диэлектрического покрытия M1 составляет от 85 до 150 нм,
- оптическая толщина второго диэлектрического покрытия M2 составляет от 80 до 150 нм,
- оптическая толщина третьего диэлектрического покрытия M3 составляет от 135 до 220 нм,
- оптическая толщина четвертого диэлектрического покрытия M4 составляет от 65 до 120 нм.
7. Материал по любому из предыдущих пунктов, отличающийся тем, что каждое диэлектрическое покрытие содержит по меньшей мере один диэлектрический слой с функцией барьера на основе соединений кремния и/или алюминия, выбранных из оксидов, таких, как SiO2 и Al2O3, нитридов кремния Si3N4 и AlN и оксинитридов SiOxNy и AlOxNy.
8. Материал по любому из предыдущих пунктов, отличающийся тем, что каждое диэлектрическое покрытие содержит по меньшей мере один диэлектрический слой со стабилизирующей функцией на основе кристаллического оксида, в частности, на основе оксида цинка, необязательно легированного по меньшей мере одним другим элементом, таким как алюминий.
9. Материал по любому из предыдущих пунктов, отличающийся тем, что каждый функциональный слой находится выше диэлектрического покрытия, верхний слой которого является диэлектрическим слоем со стабилизирующей функцией, предпочтительно на основе оксида цинка, и/или ниже диэлектрического покрытия, нижний слой которого является диэлектрическим слоем со стабилизирующей функцией, предпочтительно на основе оксида цинка.
10. Материал по любому из предыдущих пунктов, отличающийся тем, что он содержит систему тонких слоев, содержащую, начиная от прозрачной подложки:
- первое диэлектрическое покрытие, содержащее по меньшей мере один диэлектрический слой с функцией барьера и диэлектрический слой со стабилизирующей функцией,
- необязательно, блокирующий слой,
- первый функциональный слой,
- необязательно, блокирующий слой,
- второе диэлектрическое покрытие, содержащее по меньшей мере один нижний диэлектрический слой со стабилизирующей функцией, диэлектрический слой с функцией барьера и верхний диэлектрический слой со стабилизирующей функцией,
- необязательно, блокирующий слой,
- второй функциональный слой,
- необязательно, блокирующий слой,
- третье диэлектрическое покрытие, содержащее по меньшей мере один нижний диэлектрический слой со стабилизирующей функцией, диэлектрический слой с функцией барьера и верхний диэлектрический слой со стабилизирующей функцией,
- необязательно, блокирующий слой,
- третий функциональный слой,
- необязательно, блокирующий слой,
- четвертое диэлектрическое покрытие, содержащее по меньшей мере один диэлектрический слой со стабилизирующей функцией, диэлектрический слой с функцией барьера и, необязательно, защитный слой.
11. Материал по любому из предыдущих пунктов, отличающийся тем, что он имеет светопропускание ниже 60,0% и/или отражение света с наружной стороны больше или равное 20,0%.
12. Способ получения материала по одному из предыдущих пунктов, в котором слои системы слоев осаждают методом магнетронного распыления.
13. Стекло, содержащее по меньшей мере один материал по одному из предыдущих п.п. 1-11.
14. Стекло по предыдущему пункту, отличающееся тем, что система тонких слоев расположена в стекле так, что падающий снаружи свет проходит сначала через первое диэлектрическое покрытие, прежде чем пройти через первый функциональный металлический слой.
15. Стекло по любому из пунктов 13 или 14, отличающееся тем, что оно имеет вид монолитного остекления, многослойного стекла или стеклопакета, в частности, однокамерного или двухкамерного стеклопакета.
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| FR1556483 | 2015-07-08 | ||
| FR1556483A FR3038598B1 (fr) | 2015-07-08 | 2015-07-08 | Substrat muni d'un empilement a proprietes thermiques |
| PCT/FR2016/051653 WO2017006030A1 (fr) | 2015-07-08 | 2016-06-30 | Substrat muni d'un empilement a proprietes thermiques |
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| RU2018104698A true RU2018104698A (ru) | 2019-08-08 |
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| EP (1) | EP3319917B1 (ru) |
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| US10196735B2 (en) * | 2017-03-03 | 2019-02-05 | Guardian Glass, LLC | Coated article having low-E coating with IR reflecting layer(s) and doped titanium oxide dielectric layer(s) and method of making same |
| KR102082424B1 (ko) * | 2017-07-25 | 2020-02-27 | 주식회사 케이씨씨 | 저방사 유리 |
| WO2019050193A1 (ko) * | 2017-09-08 | 2019-03-14 | (주)엘지하우시스 | 창호용 기능성 건축 자재 |
| FR3072957B1 (fr) * | 2017-10-30 | 2019-10-18 | Saint-Gobain Glass France | Substrat muni d'un empilement a proprietes thermiques |
| FR3078653B1 (fr) * | 2018-03-08 | 2023-10-27 | Saint Gobain | Materiau muni d'un empilement a proprietes thermiques |
| FR3084356A1 (fr) | 2018-07-26 | 2020-01-31 | Saint-Gobain Glass France | Materiau comprenant un substrat muni d'un empilement a proprietes thermiques. |
| FR3086285A1 (fr) * | 2018-09-20 | 2020-03-27 | Saint-Gobain Glass France | Materiau a proprietes optiques et esthetiques |
| KR102659107B1 (ko) * | 2018-12-31 | 2024-04-18 | 쌩-고벵 글래스 프랑스 | 다층 박막이 구비된 투명 기판 및 이를 포함하는 다중 글레이징 유닛 |
| KR102894085B1 (ko) | 2019-03-28 | 2025-12-02 | 비트로 플랫 글래스 엘엘씨 | 가열가능한 차량 전면 유리 |
| JP7723670B2 (ja) | 2020-02-14 | 2025-08-14 | ビトロ フラット グラス エルエルシー | 低シート抵抗コーティング |
| FR3121675B1 (fr) * | 2021-04-12 | 2023-12-29 | Saint Gobain | Substrat muni d’un empilement a proprietes thermiques |
| EP4092571B1 (en) | 2021-05-20 | 2025-08-06 | Litesentry LLC | Method to classify quench patterns of heat-treated coated mineral glasses and predict the optical visibility thereof |
| CN114940589B (zh) * | 2022-06-30 | 2024-09-24 | 长兴旗滨节能玻璃有限公司 | 增透超保温玻璃 |
| EP4328570A1 (en) | 2022-08-25 | 2024-02-28 | Saint-Gobain Glass France | Method to classify quench patterns of insulating glazing units and predict the optical visibility thereof |
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| US2478817A (en) * | 1943-07-03 | 1949-08-09 | Libbey Owens Ford Glass Co | Method of forming surface films by vapor coating and the article resulting therefrom |
| FR2736632B1 (fr) * | 1995-07-12 | 1997-10-24 | Saint Gobain Vitrage | Vitrage muni d'une couche conductrice et/ou bas-emissive |
| FR2748743B1 (fr) * | 1996-05-14 | 1998-06-19 | Saint Gobain Vitrage | Vitrage a revetement antireflet |
| FR2942794B1 (fr) * | 2009-03-09 | 2011-02-18 | Saint Gobain | Substrat muni d'un empilement a proprietes thermiques comportant des couches a haut indice de refraction |
| BE1019345A3 (fr) * | 2010-05-25 | 2012-06-05 | Agc Glass Europe | Vitrage de controle solaire a faible facteur solaire. |
| CN202175621U (zh) * | 2011-07-11 | 2012-03-28 | 信义节能玻璃（芜湖）有限公司 | 一种三银low-e镀膜玻璃 |
| FR2985724B1 (fr) * | 2012-01-16 | 2014-03-07 | Saint Gobain | Substrat muni d'un empilement a proprietes thermiques comportant quatre couches fonctionnelles metalliques. |
| FR3005048B1 (fr) * | 2013-04-30 | 2020-09-25 | Saint Gobain | Substrat muni d'un empilement a proprietes thermiques |
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| BR112017027581B1 (pt) | 2022-12-13 |
| BR112017027581A2 (pt) | 2018-08-28 |
| FR3038598B1 (fr) | 2017-07-21 |
| RU2018104698A3 (ru) | 2019-10-09 |
| FR3038598A1 (fr) | 2017-01-13 |
| US20180194677A1 (en) | 2018-07-12 |
| MX2017016712A (es) | 2018-03-09 |
| CN107810170A (zh) | 2018-03-16 |
| EP3319917A1 (fr) | 2018-05-16 |
| WO2017006030A1 (fr) | 2017-01-12 |
| EP3319917B1 (fr) | 2024-11-13 |
| CO2017013531A2 (es) | 2018-03-20 |
| RU2708304C2 (ru) | 2019-12-05 |
| KR20180028435A (ko) | 2018-03-16 |
| US10815147B2 (en) | 2020-10-27 |
| KR102592541B1 (ko) | 2023-10-23 |
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