RU2017143921A - Гидрофобные полиолы - Google Patents
Гидрофобные полиолы Download PDFInfo
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- RU2017143921A RU2017143921A RU2017143921A RU2017143921A RU2017143921A RU 2017143921 A RU2017143921 A RU 2017143921A RU 2017143921 A RU2017143921 A RU 2017143921A RU 2017143921 A RU2017143921 A RU 2017143921A RU 2017143921 A RU2017143921 A RU 2017143921A
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- Prior art keywords
- butylene oxide
- composition according
- polyol based
- paragraphs
- mol
- Prior art date
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- 229920005862 polyol Polymers 0.000 title claims 14
- 150000003077 polyols Chemical class 0.000 title claims 14
- 230000002209 hydrophobic effect Effects 0.000 title 1
- 239000000203 mixture Substances 0.000 claims 13
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 claims 11
- 239000012948 isocyanate Substances 0.000 claims 9
- 150000002513 isocyanates Chemical class 0.000 claims 9
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims 5
- IQPQWNKOIGAROB-UHFFFAOYSA-N isocyanate group Chemical group [N-]=C=O IQPQWNKOIGAROB-UHFFFAOYSA-N 0.000 claims 2
- 229920002635 polyurethane Polymers 0.000 claims 2
- 239000004814 polyurethane Substances 0.000 claims 2
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims 1
- 239000000853 adhesive Substances 0.000 claims 1
- 230000001070 adhesive effect Effects 0.000 claims 1
- 125000002947 alkylene group Chemical group 0.000 claims 1
- 239000007795 chemical reaction product Substances 0.000 claims 1
- 239000011248 coating agent Substances 0.000 claims 1
- 238000000576 coating method Methods 0.000 claims 1
- 230000009477 glass transition Effects 0.000 claims 1
- 229920001451 polypropylene glycol Polymers 0.000 claims 1
- 239000000047 product Substances 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/30—Low-molecular-weight compounds
- C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
- C08G18/3203—Polyhydroxy compounds
- C08G18/3206—Polyhydroxy compounds aliphatic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
- C08G18/4804—Two or more polyethers of different physical or chemical nature
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
- C08G18/4804—Two or more polyethers of different physical or chemical nature
- C08G18/4808—Mixtures of two or more polyetherdiols
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
- C08G18/4854—Polyethers containing oxyalkylene groups having four carbon atoms in the alkylene group
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/65—Low-molecular-weight compounds having active hydrogen with high-molecular-weight compounds having active hydrogen
- C08G18/66—Compounds of groups C08G18/42, C08G18/48, or C08G18/52
- C08G18/6666—Compounds of group C08G18/48 or C08G18/52
- C08G18/667—Compounds of group C08G18/48 or C08G18/52 with compounds of group C08G18/32 or polyamines of C08G18/38
- C08G18/6674—Compounds of group C08G18/48 or C08G18/52 with compounds of group C08G18/32 or polyamines of C08G18/38 with compounds of group C08G18/3203
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/65—Low-molecular-weight compounds having active hydrogen with high-molecular-weight compounds having active hydrogen
- C08G18/66—Compounds of groups C08G18/42, C08G18/48, or C08G18/52
- C08G18/6666—Compounds of group C08G18/48 or C08G18/52
- C08G18/667—Compounds of group C08G18/48 or C08G18/52 with compounds of group C08G18/32 or polyamines of C08G18/38
- C08G18/6674—Compounds of group C08G18/48 or C08G18/52 with compounds of group C08G18/32 or polyamines of C08G18/38 with compounds of group C08G18/3203
- C08G18/6677—Compounds of group C08G18/48 or C08G18/52 with compounds of group C08G18/32 or polyamines of C08G18/38 with compounds of group C08G18/3203 having at least three hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
- C08G18/78—Nitrogen
- C08G18/79—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates
- C08G18/797—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates containing carbodiimide and/or uretone-imine groups
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/08—Polyurethanes from polyethers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J175/00—Adhesives based on polyureas or polyurethanes; Adhesives based on derivatives of such polymers
- C09J175/04—Polyurethanes
- C09J175/08—Polyurethanes from polyethers
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Polyurethanes Or Polyureas (AREA)
- Paints Or Removers (AREA)
- Adhesives Or Adhesive Processes (AREA)
Claims (13)
1. Отверждаемая композиция, включающая:
продукт реакции:
изоцианатного компонента, который включает один или несколько изоцианатов, причем изоцианатный индекс составляет от 90 до 150; и
способного реагировать с изоцианатом компонента, который включает смесь, содержащую от 5 мас.% до 95 мас.% первого полиола на основе бутиленоксида и от 5 мас.% до 95 мас.% второго полиола на основе бутиленоксида, причем первый полиол на основе бутиленоксида имеет среднечисленную молекулярную массу от 200 г/моль до 1000 г/моль и номинальное число гидроксильных групп от 2 до 6, второй полиол на основе бутиленоксида имеет среднечисленную молекулярную массу, составляющую более 1000 г/моль и менее 8000 г/моль, и номинальное число гидроксильных групп от 2 до 4, и смесь составляет по меньшей мере 50 мас.% относительно общей массы полиолов в реагирующем с изоцианатом компоненте.
2. Композиция по п. 1, в которой первый полиол на основе бутиленоксида содержит от 75 мас.% до 100 мас.% бутиленоксида по отношению к общей массе алкиленоксидов и имеет номинальное число гидроксильных групп 3.
3. Композиция по п. 1 или 2, в которой второй полиол на основе бутиленоксида представляет собой полиоксибутилен-полиоксипропиленовый полиол, имеющий номинальное число гидроксильных групп 2, или полиоксибутилен-полиоксиэтиленовый полиол, имеющий номинальное число гидроксильных групп 2.
4. Композиция по любому из пп. 1-3, в которой второй полиол на основе бутиленоксида имеет среднечисленную молекулярную массу от 1500 г/моль до 3000 г/моль.
5. Композиция по любому из пп. 1-4, в которой отношение массового процентного содержания первого полиола на основе бутиленоксида в реагирующем с изоцианатом компоненте к массовому процентному содержанию второго полиола на основе бутиленоксида в реагирующем с изоцианатом компоненте находится в диапазоне от 0,1 до 3,5.
6. Композиция по п. 5, в которой, когда указанное отношение находится у верхнего предела диапазона от 0,1 до 3,5, отвержденный продукт отверждаемой композиции имеет повышенную прочность при растяжении, меньшее относительное удлинение при разрыве, повышенный расчетный модуль упругости и повышенную температуру стеклования по сравнению со случаем, в котором указанное отношение находится у нижнего предела диапазона от 0,1 до 3,5, причем нижний предел диапазона не превышает верхний предел диапазона.
7. Композиция по любому из пп. 1-6, в котором способный реагировать с изоцианатом компонент дополнительно включает простой полиэфирполиол, не представляющий собой первый и второй полиолы на основе бутиленоксида.
8. Композиция по любому из пп. 1-7, в котором изоцианатный компонент включает от 20 мас.% до 100 мас.%, по отношению к общей массе изоцианатного компонента, одного или нескольких содержащих концевые изоцианатные группы форполимеров, имеющих содержание изоцианатных групп от 1 мас.% до 35 мас.%.
9. Адгезив на полиуретановой основе, включающий отверждаемую композицию по любому из пп. 1-8.
10. Покрытие на полиуретановой основе, включающее отверждаемую композицию по любому из пп. 1-8.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201562169071P | 2015-06-01 | 2015-06-01 | |
| US62/169,071 | 2015-06-01 | ||
| PCT/US2016/034564 WO2016196258A1 (en) | 2015-06-01 | 2016-05-27 | Hydrophobic Polyols |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| RU2017143921A true RU2017143921A (ru) | 2019-06-17 |
| RU2017143921A3 RU2017143921A3 (ru) | 2019-11-19 |
| RU2719440C2 RU2719440C2 (ru) | 2020-04-17 |
Family
ID=56118041
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2017143921A RU2719440C2 (ru) | 2015-06-01 | 2016-05-27 | Гидрофобные полиолы |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US10487171B2 (ru) |
| EP (1) | EP3303433B1 (ru) |
| JP (1) | JP6845161B2 (ru) |
| CN (1) | CN107690446B (ru) |
| BR (1) | BR112017024681B1 (ru) |
| RU (1) | RU2719440C2 (ru) |
| WO (1) | WO2016196258A1 (ru) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109312049A (zh) * | 2016-05-26 | 2019-02-05 | 康宁光电通信有限责任公司 | 用于包覆模制覆盖光纤电缆的材料配方 |
| US20200317850A1 (en) * | 2016-05-31 | 2020-10-08 | Dow Global Technologies Llc | Low cathodic disbondment coating compositions |
| WO2019149634A1 (de) * | 2018-01-31 | 2019-08-08 | Basf Se | Verbundelement mit verbesserten eigenschaften |
| KR102668892B1 (ko) * | 2018-04-02 | 2024-05-29 | 디디피 스페셜티 일렉트로닉 머티리얼즈 유에스, 엘엘씨 | 2-성분 폴리우레탄 접착제 조성물 |
| US11072725B2 (en) | 2018-12-19 | 2021-07-27 | Crosslink Technology, Inc. | Polyurethane compositions for coating |
| HUE072667T2 (hu) | 2021-07-13 | 2025-12-28 | Akzo Nobel Coatings Int Bv | Egykomponensû, nedvességre keményedõ ragasztókészítmény |
| AU2022311498B2 (en) | 2021-07-13 | 2024-02-15 | Akzo Nobel Coatings International B.V. | One-component moisture-curable adhesive composition |
| CN114133552B (zh) * | 2021-11-30 | 2023-12-12 | 山东一诺威新材料有限公司 | 疏水型聚醚多元醇及其制备方法 |
| CN115260439B (zh) * | 2022-08-11 | 2023-09-22 | 山东一诺威新材料有限公司 | 汽车漆面保护膜用超疏水型聚氨酯材料及其制备方法 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4687788A (en) | 1982-10-08 | 1987-08-18 | The Dow Chemical Company | Dimensionally stable urethane elastomers |
| EP0136396B1 (de) * | 1983-09-20 | 1987-08-12 | Th. Goldschmidt AG | Verwendung ausgewählter Polyetherole und Polyisocyanate zur Herstellung von Klebmitteln auf Polyurethanbasis |
| US4745170A (en) | 1985-07-25 | 1988-05-17 | The Dow Chemical Company | Polyurethane elastomers from EO/BO polyether polyols |
| DE4104199A1 (de) | 1991-02-12 | 1992-08-13 | Basf Ag | Verfahren zur herstellung von polyurethan-elastomeren und hierfuer geeignete mischungen aus polyoxybutylen-polyoxyalkylen-glykolen und glycidylverbindungen |
| DE4132015A1 (de) * | 1991-09-26 | 1993-04-01 | Basf Ag | Thermoplastische polyurethan-elastomere mit einem geringen organischen kohlenstoffabgabewert, verfahren zu ihrer herstellung und ihre verwendung |
| US6103850A (en) | 1995-12-29 | 2000-08-15 | Basf Corporation | Sealants made using low unsaturation polyoxyalkylene polyether polyols |
| US6127443A (en) * | 1998-11-06 | 2000-10-03 | Bayer Antwerp N.V. | Energy management polyurethane rigid foams with high recovery |
| US6855765B2 (en) | 2001-12-12 | 2005-02-15 | National University Of Singapore | Heat and hot water resistant polyurethane sealant |
| BR112013021243A2 (pt) * | 2011-03-08 | 2020-10-27 | Basf Se | processo para a produção de espumas rígidas de poliuretano, espuma rígida de poliuretano, e, uso de uma espuma rígida de poliuretano |
| WO2012158664A2 (en) | 2011-05-16 | 2012-11-22 | Ashland Inc. | Two part polyurea-urethane adhesive with elevated high temperature storage modulus |
| DK3052539T3 (en) * | 2013-10-02 | 2017-10-16 | Dow Global Technologies Llc | Sprayable polyurethane based protective coating |
| DK3149100T3 (da) | 2014-05-30 | 2020-06-15 | Dow Global Technologies Llc | Hydrofobe polyoler til forseglingsanvendelser |
-
2016
- 2016-05-27 JP JP2017562266A patent/JP6845161B2/ja active Active
- 2016-05-27 BR BR112017024681-3A patent/BR112017024681B1/pt active IP Right Grant
- 2016-05-27 US US15/577,903 patent/US10487171B2/en active Active
- 2016-05-27 CN CN201680029268.5A patent/CN107690446B/zh active Active
- 2016-05-27 WO PCT/US2016/034564 patent/WO2016196258A1/en not_active Ceased
- 2016-05-27 EP EP16728515.4A patent/EP3303433B1/en active Active
- 2016-05-27 RU RU2017143921A patent/RU2719440C2/ru active
Also Published As
| Publication number | Publication date |
|---|---|
| US20180162988A1 (en) | 2018-06-14 |
| RU2719440C2 (ru) | 2020-04-17 |
| RU2017143921A3 (ru) | 2019-11-19 |
| JP6845161B2 (ja) | 2021-03-17 |
| BR112017024681B1 (pt) | 2021-12-14 |
| EP3303433A1 (en) | 2018-04-11 |
| EP3303433B1 (en) | 2021-02-17 |
| CN107690446B (zh) | 2021-02-26 |
| WO2016196258A1 (en) | 2016-12-08 |
| CN107690446A (zh) | 2018-02-13 |
| JP2018522965A (ja) | 2018-08-16 |
| BR112017024681A2 (pt) | 2018-07-24 |
| US10487171B2 (en) | 2019-11-26 |
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