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RU2016129970A - Вспененная масса фенольной смолы и способ ее получения - Google Patents

Вспененная масса фенольной смолы и способ ее получения Download PDF

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Publication number
RU2016129970A
RU2016129970A RU2016129970A RU2016129970A RU2016129970A RU 2016129970 A RU2016129970 A RU 2016129970A RU 2016129970 A RU2016129970 A RU 2016129970A RU 2016129970 A RU2016129970 A RU 2016129970A RU 2016129970 A RU2016129970 A RU 2016129970A
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Russia
Prior art keywords
phenolic resin
less
average molecular
molecular weight
thermal conductivity
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RU2016129970A
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English (en)
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RU2658066C2 (ru
RU2016129970A3 (ru
Inventor
Масато ХАМАДЗИМА
Сигеми МУКАИЯМА
Йосихито ФУКАСАВА
Ацуси КУМАДА
Original Assignee
Асахи Касеи Констракшн Матириалс Корпорейшн
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Publication of RU2016129970A publication Critical patent/RU2016129970A/ru
Publication of RU2016129970A3 publication Critical patent/RU2016129970A3/ru
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    • C08J2201/02—Foams characterised by the foaming process characterised by mechanical pre- or post-treatments
    • C08J2201/026—Crosslinking before of after foaming
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2203/00—Foams characterized by the expanding agent
    • C08J2203/14—Saturated hydrocarbons, e.g. butane; Unspecified hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2203/00—Foams characterized by the expanding agent
    • C08J2203/16—Unsaturated hydrocarbons
    • C08J2203/162—Halogenated unsaturated hydrocarbons, e.g. H2C=CF2
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2203/00—Foams characterized by the expanding agent
    • C08J2203/18—Binary blends of expanding agents
    • C08J2203/182—Binary blends of expanding agents of physical blowing agents, e.g. acetone and butane
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2205/00—Foams characterised by their properties
    • C08J2205/04—Foams characterised by their properties characterised by the foam pores
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
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    • C08J2205/00—Foams characterised by their properties
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    • C08J2205/044—Micropores, i.e. average diameter being between 0,1 micrometer and 0,1 millimeter
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    • C08J2205/00—Foams characterised by their properties
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    • C08J2205/052—Closed cells, i.e. more than 50% of the pores are closed
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    • C08J2361/00—Characterised by the use of condensation polymers of aldehydes or ketones; Derivatives of such polymers
    • C08J2361/04—Condensation polymers of aldehydes or ketones with phenols only
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    • C08J2361/04—Condensation polymers of aldehydes or ketones with phenols only
    • C08J2361/06—Condensation polymers of aldehydes or ketones with phenols only of aldehydes with phenols
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  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
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Claims (13)

1. Пена из фенольной смолы, содержащая фенольную смолу и вспенивающий агент, содержащий, по меньшей мере, одно соединение из хлорированного гидрофторолефина или нехлорированного гидрофторолефина,
имеющая плотность 10 кг/м3 или более и 150 кг/м3 или менее,
имеющая теплопроводность при температуре окружающей среды 10°C 0,0175 Вт/м⋅К или менее и
имеющая теплопроводность при температуре окружающей среды 23°C 0,0185 Вт/м⋅К или менее.
2. Пена из фенольной смолы по п.1, имеющая кислородный индекс 28об.% или более.
3. Пена из фенольной смолы по п.1 или 2, имеющая теплопроводность при температуре окружающей среды 10°C 0,0185 Вт/м⋅К или менее после выдерживания в атмосфере при температуре 110°C в течение 14 дней.
4. Пена из фенольной смолы по любому из пп.1-3, имеющая долю закрытых ячеек 90% или более, средний диаметр ячеек 50 мкм или более и 200 мкм или менее и долю площади пустот 0,2% или менее.
5. Пена из фенольной смолы по любому из пп.1-4, где вспенивающий агент содержит, по меньшей мере, один олефин, выбранный из группы, состоящей из 1-хлор-3,3,3-трифторпропена, 1,3,3,3-тетрафтор-1-пропена, 2,3,3,3-тетрафтор-1-пропена и 1,1,1,4,4,4-гексафтор-2-бутена.
6. Способ получения пены из фенольной смолы, включающий стадию вспенивания и отверждения вспениваемой композиции фенольной смолы, содержащей фенольную смолу, поверхностно-активное вещество, катализатор отверждения и вспенивающий агент на лицевом материале,
где вспенивающий агент содержит, по меньшей мере, одно соединение из хлорированного гидрофторолефина или нехлорированного гидрофторолефина,
средневзвешенная молекулярная масса Mw фенольной смолы составляет 400 или более и 3000 или менее,
отношение средневзвешенной молекулярной массы Mw к среднечисленной молекулярной массе Mn фенольной смолы, Mw/Mn, составляет 1,5 или более и 6,0 или менее и средневзвешенная молекулярная масса Mw и среднечисленная молекулярная масса Mn представляют собой значения, определяемые с помощью гель-проникающей хроматографии.
7. Способ по п.6, где вспениваемая композиция фенольной смолы представляет собой смесь, содержащую исходные материалы фенольной смолы, содержащие фенольную смолу и воду, поверхностно-активное вещество, катализатор отверждения и вспенивающий агент, и доля влажности исходных материалов фенольной смолы составляет 1% масс или более и 20% масс или менее по отношению к массе материала фенольной смолы.
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