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RU2015120312A - AMMONIA SYNTHESIS REACTOR WITH SEPARATED FLOW AND TUBULAR NOZZLE - Google Patents

AMMONIA SYNTHESIS REACTOR WITH SEPARATED FLOW AND TUBULAR NOZZLE Download PDF

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Publication number
RU2015120312A
RU2015120312A RU2015120312A RU2015120312A RU2015120312A RU 2015120312 A RU2015120312 A RU 2015120312A RU 2015120312 A RU2015120312 A RU 2015120312A RU 2015120312 A RU2015120312 A RU 2015120312A RU 2015120312 A RU2015120312 A RU 2015120312A
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RU
Russia
Prior art keywords
catalyst
reactor
tubes
coolant
layers
Prior art date
Application number
RU2015120312A
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Russian (ru)
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RU2608092C2 (en
Inventor
Дмитрий Александрович Блохин
Original Assignee
Дмитрий Александрович Блохин
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Application filed by Дмитрий Александрович Блохин filed Critical Дмитрий Александрович Блохин
Priority to RU2015120312A priority Critical patent/RU2608092C2/en
Publication of RU2015120312A publication Critical patent/RU2015120312A/en
Application granted granted Critical
Publication of RU2608092C2 publication Critical patent/RU2608092C2/en

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/02Preparation, purification or separation of ammonia
    • C01C1/04Preparation of ammonia by synthesis in the gas phase

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  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)

Abstract

1. Реактор синтеза аммиака, в котором синтез-газ, содержащий азот и водород, разделен на два или более основных потока, каждый из которых подается в механически изолированную реакционную зону, причем охлаждение реакционных зон осуществляется с помощью теплообменных трубок, находящихся в слое катализатора, а движение газа через слои катализатора и охлаждающего вещества через теплообменные трубки, расположенные в катализаторе, осуществляется преимущественно вертикально.2. Реактор по п. 1, в котором в каждой реакционной зоне могут присутствовать два или боле слоев катализатора.3. Реактор по п. 2, в котором по крайней мере один слой катализатора снабжен теплоотводящими трубками.4. Реактор по п. 1, в котором катализатор располагается внутри трубок, а охлаждающее вещество подается в межтрубное пространство.5. Способ реконструкции существующего аппарата с получением реактора, описанного в пп. 1-4.1. An ammonia synthesis reactor in which the synthesis gas containing nitrogen and hydrogen is divided into two or more main streams, each of which is supplied to a mechanically isolated reaction zone, and the reaction zones are cooled using heat transfer tubes located in the catalyst layer, and the movement of gas through the layers of the catalyst and the coolant through the heat exchange tubes located in the catalyst is carried out mainly vertically. 2. The reactor according to claim 1, wherein in each reaction zone two or more catalyst layers may be present. The reactor of claim 2, wherein at least one catalyst bed is provided with heat sink tubes. The reactor according to claim 1, in which the catalyst is located inside the tubes, and the coolant is fed into the annulus. A method of reconstructing an existing apparatus to obtain the reactor described in paragraphs. 1-4.

Claims (5)

1. Реактор синтеза аммиака, в котором синтез-газ, содержащий азот и водород, разделен на два или более основных потока, каждый из которых подается в механически изолированную реакционную зону, причем охлаждение реакционных зон осуществляется с помощью теплообменных трубок, находящихся в слое катализатора, а движение газа через слои катализатора и охлаждающего вещества через теплообменные трубки, расположенные в катализаторе, осуществляется преимущественно вертикально.1. An ammonia synthesis reactor in which the synthesis gas containing nitrogen and hydrogen is divided into two or more main streams, each of which is supplied to a mechanically isolated reaction zone, and the reaction zones are cooled using heat transfer tubes located in the catalyst layer, and the movement of gas through the layers of the catalyst and coolant through the heat exchange tubes located in the catalyst is carried out mainly vertically. 2. Реактор по п. 1, в котором в каждой реакционной зоне могут присутствовать два или боле слоев катализатора.2. The reactor according to claim 1, in which in each reaction zone may be present two or more layers of catalyst. 3. Реактор по п. 2, в котором по крайней мере один слой катализатора снабжен теплоотводящими трубками.3. The reactor according to claim 2, in which at least one catalyst bed is provided with heat sink tubes. 4. Реактор по п. 1, в котором катализатор располагается внутри трубок, а охлаждающее вещество подается в межтрубное пространство.4. The reactor according to claim 1, in which the catalyst is located inside the tubes, and the coolant is fed into the annulus. 5. Способ реконструкции существующего аппарата с получением реактора, описанного в пп. 1-4. 5. A method of reconstructing an existing apparatus to obtain the reactor described in paragraphs. 1-4.
RU2015120312A 2015-05-29 2015-05-29 Ammonia synthesis reactor with split-flow and tubular nozzle RU2608092C2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
RU2015120312A RU2608092C2 (en) 2015-05-29 2015-05-29 Ammonia synthesis reactor with split-flow and tubular nozzle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
RU2015120312A RU2608092C2 (en) 2015-05-29 2015-05-29 Ammonia synthesis reactor with split-flow and tubular nozzle

Publications (2)

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RU2015120312A true RU2015120312A (en) 2016-12-20
RU2608092C2 RU2608092C2 (en) 2017-01-13

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RU2015120312A RU2608092C2 (en) 2015-05-29 2015-05-29 Ammonia synthesis reactor with split-flow and tubular nozzle

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107055570A (en) * 2017-03-21 2017-08-18 武汉金中石化工程有限公司 Low-pressure synthetic ammonia equipment and low-pressure synthetic ammonia method

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AR113649A1 (en) 2017-12-20 2020-05-27 Haldor Topsoe As COOLED AXIAL FLOW CONVERTER

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4372920A (en) * 1979-07-13 1983-02-08 Ammonia Casale S.A. Axial-radial reactor for heterogeneous synthesis
DE10116150A1 (en) * 2001-03-31 2002-10-10 Mg Technologies Ag Process for the catalytic generation of ammonia from synthesis gas
US7081230B2 (en) * 2002-11-15 2006-07-25 Kellogg Brown & Root Llc Split-flow, vertical ammonia converter
US8197785B2 (en) * 2008-02-27 2012-06-12 Kellogg Brown & Root Llc Split flow contactor

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107055570A (en) * 2017-03-21 2017-08-18 武汉金中石化工程有限公司 Low-pressure synthetic ammonia equipment and low-pressure synthetic ammonia method

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Publication number Publication date
RU2608092C2 (en) 2017-01-13

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MM4A The patent is invalid due to non-payment of fees

Effective date: 20170530