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RU2014123620A - Self-emulsifying polyolefin compositions - Google Patents

Self-emulsifying polyolefin compositions Download PDF

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RU2014123620A
RU2014123620A RU2014123620/04A RU2014123620A RU2014123620A RU 2014123620 A RU2014123620 A RU 2014123620A RU 2014123620/04 A RU2014123620/04 A RU 2014123620/04A RU 2014123620 A RU2014123620 A RU 2014123620A RU 2014123620 A RU2014123620 A RU 2014123620A
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polyolefin
water
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Райнер Добрава
Дитер БЕКХ
Раджан К. ПАНАНДИКЕР
Джули МЕНКХАУС
Франк ХЮЛЬСКЕТТЕР
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Басф Се
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8105—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • A61K8/8111—Homopolymers or copolymers of aliphatic olefines, e.g. polyethylene, polyisobutene; Compositions of derivatives of such polymers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/8164—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a carboxyl radical, and containing at least one other carboxyl radical in the molecule, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers, e.g. poly (methyl vinyl ether-co-maleic anhydride)
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    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
    • C09K23/003—Organic compounds containing only carbon and hydrogen
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0008—Detergent materials or soaps characterised by their shape or physical properties aqueous liquid non soap compositions
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    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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    • A61K2800/594—Mixtures of polymers
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
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    • C11D3/37—Polymers
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3749—Polyolefins; Halogenated polyolefins; Natural or synthetic rubber; Polyarylolefins or halogenated polyarylolefins
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3757—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions
    • C11D3/3765—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions in liquid compositions

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Abstract

1. Самоэмульгируемая композиция, содержащаяa) полиолефин(ы) в количестве от 5 до 90 мас. %b) полимерный эмульгатор(ы) Pв количестве от 5 до 90 мас. %c) масло(а) Oв количестве от 0 до 40 мас. %d) поверхностно-активное вещество(а) Sв количестве от 5 до 40 мас. %e) добавку(и) Aв количестве от 0 до 10 мас. %f) воду в количестве от 0 до 8 мас. %на основе общей массы композиции,где вода не является непрерывной фазой композиции,где массовое отношение полиолефина(ов) к Pи Sнаходится в интервале от 4:1 до 1:3, и массовое отношение Pк Sвыше 1.25.2. Самоэмульгируемая композиция по п. 1, где компоненты независимо друг от друга присутствуют в количествах:a) полиолефин(ы) в количестве от 20 до 70 мас. %b) полимерный эмульгатор(ы) Pв количестве от 10 до 50 мас. %c) масло(а) Oв количестве от 0 до 40 мас. %d) поверхностно-активное вещество(а) Sв количестве от 5 до 30 мас. %e) добавка(и) Aв количестве от 0 до 10 мас. %f) вода в количестве от 0 до 8 мас. %на основе общей массы композиции,где вода не является непрерывной фазой композиции,где массовое отношение полиолефина(ов) к Pи Sнаходится в интервале от 4:1 до 1:3, и массовое отношение Pк Sвыше 1.25.3. Самоэмульгируемая композиция по п. 1, где компоненты независимо друг от друга присутствуют в количествах:a) полиолефин(ы) в количестве от 30 до 60 мас. %b) полимерный эмульгатор(ы) Pв количестве от 20 до 45 мас. %c) масло(а) Oв количестве от 0,1 до 30 мас. %d) поверхностно-активное вещество(а) Sв количестве от 5 до 25 мас. %e) добавка(и) Aв количестве от 0,1 до 10 мас. %f) вода в количестве от 0 до 8 мас. %на основе общей массы композиции,где вода не является непрерывной фазой композиции,где массовое отношение полиолефина(ов) к Pи Sнаходится в интервале от 4:1 до 1:3, и массовое отношение Pк Sвыше 1.25.4. С�1. Self-emulsifiable composition containing a) polyolefin(s) in an amount of from 5 to 90 wt. %b) polymeric emulsifier(s) P in an amount of from 5 to 90 wt. %c) oil(s) O in an amount of from 0 to 40 wt. %d) surfactant(s) S in an amount of 5 to 40 wt. %e) additive(s) A in an amount of from 0 to 10 wt. %f) water in an amount of from 0 to 8 wt. % based on the total weight of the composition, where water is not a continuous phase of the composition, where the mass ratio of polyolefin(s) to P and S is in the range from 4:1 to 1:3, and the mass ratio of P to S is greater than 1.25.2. Self-emulsifiable composition according to claim 1, where the components are independently present in amounts of: a) polyolefin(s) in an amount of 20 to 70 wt. %b) polymeric emulsifier(s) P in an amount of from 10 to 50 wt. %c) oil(s) O in an amount of from 0 to 40 wt. %d) surfactant(s) S in an amount of 5 to 30 wt. %e) additive(s) A in an amount of from 0 to 10 wt. %f) water in an amount of from 0 to 8 wt. % based on the total weight of the composition, where water is not a continuous phase of the composition, where the mass ratio of polyolefin(s) to P and S is in the range from 4:1 to 1:3, and the mass ratio of P to S is greater than 1.25.3. Self-emulsifiable composition according to claim 1, where the components are independently present in amounts of: a) polyolefin(s) in an amount of from 30 to 60 wt. %b) polymeric emulsifier(s) P in an amount of from 20 to 45 wt. %c) oil(s) O in an amount of from 0.1 to 30 wt. %d) surfactant(s) S in an amount of 5 to 25 wt. %e) additive(s) A in an amount of from 0.1 to 10 wt. %f) water in an amount of from 0 to 8 wt. % based on the total weight of the composition, where water is not the continuous phase of the composition, where the weight ratio of polyolefin(s) to P and S is in the range of 4:1 to 1:3, and the weight ratio of P to S is greater than 1.25.4. C�

Claims (14)

1. Самоэмульгируемая композиция, содержащая1. Self-emulsifiable composition containing a) полиолефин(ы) в количестве от 5 до 90 мас. %a) polyolefin (s) in an amount of from 5 to 90 wt. % b) полимерный эмульгатор(ы) Px в количестве от 5 до 90 мас. %b) a polymer emulsifier (s) P x in an amount of from 5 to 90 wt. % c) масло(а) Ox в количестве от 0 до 40 мас. %c) oil (a) O x in an amount of from 0 to 40 wt. % d) поверхностно-активное вещество(а) Sx в количестве от 5 до 40 мас. %d) surfactant (a) S x in an amount of from 5 to 40 wt. % e) добавку(и) Ax в количестве от 0 до 10 мас. %e) additive (s) A x in an amount of from 0 to 10 wt. % f) воду в количестве от 0 до 8 мас. %f) water in an amount of from 0 to 8 wt. % на основе общей массы композиции,based on the total weight of the composition, где вода не является непрерывной фазой композиции,where water is not a continuous phase of the composition, где массовое отношение полиолефина(ов) к Px и Sx находится в интервале от 4:1 до 1:3, и массовое отношение Px к Sx выше 1.25.where the mass ratio of polyolefin (s) to P x and S x is in the range from 4: 1 to 1: 3, and the mass ratio of P x to S x is above 1.25. 2. Самоэмульгируемая композиция по п. 1, где компоненты независимо друг от друга присутствуют в количествах:2. Self-emulsifiable composition according to claim 1, where the components are independently present in amounts of: a) полиолефин(ы) в количестве от 20 до 70 мас. %a) polyolefin (s) in an amount of from 20 to 70 wt. % b) полимерный эмульгатор(ы) Px в количестве от 10 до 50 мас. %b) a polymer emulsifier (s) P x in an amount of from 10 to 50 wt. % c) масло(а) Ox в количестве от 0 до 40 мас. %c) oil (a) O x in an amount of from 0 to 40 wt. % d) поверхностно-активное вещество(а) Sx в количестве от 5 до 30 мас. %d) surfactant (a) S x in an amount of from 5 to 30 wt. % e) добавка(и) Ax в количестве от 0 до 10 мас. %e) additive (s) A x in an amount of from 0 to 10 wt. % f) вода в количестве от 0 до 8 мас. %f) water in an amount of from 0 to 8 wt. % на основе общей массы композиции,based on the total weight of the composition, где вода не является непрерывной фазой композиции,where water is not a continuous phase of the composition, где массовое отношение полиолефина(ов) к Px и Sx находится в интервале от 4:1 до 1:3, и массовое отношение Px к Sx выше 1.25.where the mass ratio of polyolefin (s) to P x and S x is in the range from 4: 1 to 1: 3, and the mass ratio of P x to S x is above 1.25. 3. Самоэмульгируемая композиция по п. 1, где компоненты независимо друг от друга присутствуют в количествах:3. The self-emulsifying composition according to claim 1, where the components are independently present in amounts of: a) полиолефин(ы) в количестве от 30 до 60 мас. %a) polyolefin (s) in an amount of from 30 to 60 wt. % b) полимерный эмульгатор(ы) Px в количестве от 20 до 45 мас. %b) a polymer emulsifier (s) P x in an amount of from 20 to 45 wt. % c) масло(а) Ox в количестве от 0,1 до 30 мас. %c) oil (a) O x in an amount of from 0.1 to 30 wt. % d) поверхностно-активное вещество(а) Sx в количестве от 5 до 25 мас. %d) surfactant (a) S x in an amount of from 5 to 25 wt. % e) добавка(и) Ax в количестве от 0,1 до 10 мас. %e) additive (s) A x in an amount of from 0.1 to 10 wt. % f) вода в количестве от 0 до 8 мас. %f) water in an amount of from 0 to 8 wt. % на основе общей массы композиции,based on the total weight of the composition, где вода не является непрерывной фазой композиции,where water is not a continuous phase of the composition, где массовое отношение полиолефина(ов) к Px и Sx находится в интервале от 4:1 до 1:3, и массовое отношение Px к Sx выше 1.25.where the mass ratio of polyolefin (s) to P x and S x is in the range from 4: 1 to 1: 3, and the mass ratio of P x to S x is above 1.25. 4. Самоэмульгируемая композиция по п. 1, где компоненты независимо друг от друга присутствуют в количествах:4. The self-emulsifying composition of claim 1, wherein the components are independently present in amounts of: a) полиолефин(ы) в количестве от 40 до 50 мас. %a) polyolefin (s) in an amount of from 40 to 50 wt. % b) полимерный эмульгатор(ы) Px в количестве от 25 до 40 мас. %b) a polymer emulsifier (s) P x in an amount of from 25 to 40 wt. % c) масло(а) Ox в количестве от 5 до 15 мас. %c) oil (a) O x in an amount of from 5 to 15 wt. % d) поверхностно-активное вещество(а) Sx в количестве от 5 до 15 мас. %d) surfactant (a) S x in an amount of from 5 to 15 wt. % e) добавка(и) Ax в количестве от 2 до 8 мас. %e) additive (s) A x in an amount of from 2 to 8 wt. % f) вода в количестве от 0 до 8 мас. %f) water in an amount of from 0 to 8 wt. % на основе общей массы композиции,based on the total weight of the composition, где вода не является непрерывной фазой композиции,where water is not a continuous phase of the composition, где массовое отношение полиолефина(ов) к Px и Sx находится в интервале от 4:1 до 1:3, и массовое отношение Px к Sx выше 1.25.where the mass ratio of polyolefin (s) to P x and S x is in the range from 4: 1 to 1: 3, and the mass ratio of P x to S x is above 1.25. 5. Самоэмульгируемая композиция по любому одному из пп. 1-4, где композицией является композиция без содержания воды.5. The self-emulsifying composition according to any one of paragraphs. 1-4, where the composition is a composition without water content. 6. Самоэмульгируемая композиция по любому одному из пп. 1-4, где композицией является композиция с уменьшенным содержанием воды.6. The self-emulsifying composition according to any one of paragraphs. 1-4, where the composition is a composition with a reduced water content. 7. Самоэмульгируемая композиция по любому одному из пп. 1-4, где полиолефин(ы) выбирается/выбираются из группы, содержащей: полиэтилен, полипропилен, полибутилен и полиизобутен.7. The self-emulsifying composition according to any one of paragraphs. 1-4, where the polyolefin (s) is selected / selected from the group consisting of: polyethylene, polypropylene, polybutylene and polyisobutene. 8. Самоэмульгируемая композиция по любому одному из пп. 1-4, где полимерный эмульгатор(ы) Px выбирается/выбираются из группы, содержащей:8. The self-emulsifying composition according to any one of paragraphs. 1-4, where the polymer emulsifier (s) P x is selected / selected from the group consisting of: P1) полиизобутеновые производные, где P1 представляет собой полиизобутенамин, полиизобутен янтарный ангидрид, сополимер полиизобутен янтарного ангидрида с полиалкиленгликолем, сополимер полиизобутен янтарного ангидрида с олигоамином или с алкоксилатом олигоамина,P1) polyisobutene derivatives, where P1 is polyisobutenamine, polyisobutene succinic anhydride, a copolymer of polyisobutene succinic anhydride with polyalkylene glycol, a copolymer of polyisobutene succinic anhydride with oligoamine or oligoamine alkoxylate, P2) полимерные катионные эмульгаторы, где P2 является результатом полимеризации:P2) polymer cationic emulsifiers, where P2 is the result of polymerization: A2) одного или более катионных этиленненасыщенных мономеровA 2 ) one or more cationic ethylenically unsaturated monomers B2) одного или более линейных или разветвленных алкил(мет)акрилатов,B 2 ) one or more linear or branched alkyl (meth) acrylates, C2) от 0 до 30 масс. % одной или более C3-C8 моноэтиленненасыщенных карбоновых кислот,C 2 ) from 0 to 30 mass. % of one or more C 3 -C 8 monoethylenically unsaturated carboxylic acids, P3) являющиеся сополимерами полиалкилена(ов) формулы 3P 3 ) being copolymers of polyalkylene (s) of formula 3
Figure 00000001
Figure 00000001
 где R*=H, CH3,where R * = H, CH 3 , R=H, метил,R = H, methyl, R′=H, метил,R ′ = H, methyl, n=1-200,n = 1-200, с моноэтиленненасыщенными мономерами.with monoethylenically unsaturated monomers. 9. Самоэмульгируемая композиция по любому одному из пп. 1-4, где полимер(ы) Px выбирается/выбираются из группы, содержащей:9. The self-emulsifying composition according to any one of paragraphs. 1-4, where the polymer (s) P x is selected / selected from the group consisting of: P1) полиизобутеновые производные, где P1 представляет собой полиизобутенамин, полиизобутен янтарный ангидрид, сополимер полиизобутен янтарного ангидрида с полиалкиленгликолем,P1) polyisobutene derivatives, where P1 is polyisobutenamine, polyisobutene succinic anhydride, a copolymer of polyisobutene succinic anhydride with polyalkylene glycol, P2) полимерные катионные эмульгаторы, где P2 является результатом полимеризации:P2) polymer cationic emulsifiers, where P2 is the result of polymerization: A2) диаллилдиметиламмония хлорида,A2) diallyldimethylammonium chloride, B2) одного или более линейных или разветвленных алкил(мет)акрилатов,B2) one or more linear or branched alkyl (meth) acrylates, C2) от 0 до 30 масс. % акриловой кислоты.C2) from 0 to 30 mass. % acrylic acid. P3) являющиеся сополимерами полиалкилена(ов) формулы 3P3) being copolymers of polyalkylene (s) of formula 3
Figure 00000002
Figure 00000002
 где R*=H, CH3, where R * = H, CH 3 , R=H, метил,R = H, methyl, R′=H, метил,R ′ = H, methyl, n=1-200,n = 1-200, с моноэтиленненасыщенными мономерами.with monoethylenically unsaturated monomers. 10. Самоэмульгируемая композиция по любому одному из пп. 1-4, где масло(а) Ox выбирается/выбираются из группы, содержащей:10. The self-emulsifying composition according to any one of paragraphs. 1-4, where the oil (a) O x is selected / selected from the group consisting of: c1) минеральные масла, имеющие точку кипения при атмосферном давлении 150°C или вышеc1) mineral oils having a boiling point at atmospheric pressure of 150 ° C or higher c2) сложные эфиры C10-C26-карбоновых кислот и C8-C24-спиртов и c2) esters of C 10 -C 26 carboxylic acids and C 8 -C 24 alcohols; and с3) силиконовые масла.c3) silicone oils. 11. Самоэмульгируемая композиция по любому одному из пп. 1-4, где поверхностно-активное вещество(а) Sx выбирается/выбираются из группы, содержащей:11. The self-emulsifying composition according to any one of paragraphs. 1-4, where the surfactant (a) S x is selected / selected from the group consisting of: d1) неионные поверхностно-активные вещества,d1) nonionic surfactants, d2) анионные поверхностно-активные вещества; иd2) anionic surfactants; and d3) катионные поверхностно-активные вещества.d3) cationic surfactants. 12. Самоэмульгируемая композиция по любому одному из пп. 1-4, которая имеет содержание органического растворителя менее 50 мг/кг композиции.12. The self-emulsifying composition according to any one of paragraphs. 1-4, which has an organic solvent content of less than 50 mg / kg of the composition. 13. Применение эмульсии по пп. 1-12 в химических технических применениях, в косметических средствах, для защиты растений, получения и обработки бумаги, текстиля и кожи, в композиции клеев, красителей и пигментов, в покрытиях, для фармацевтических применений, в строительстве, для обработки древесины.13. The use of the emulsion according to paragraphs. 1-12 in chemical technical applications, in cosmetics, for plant protection, the preparation and processing of paper, textiles and leather, in the composition of adhesives, dyes and pigments, in coatings, for pharmaceutical applications, in construction, for wood processing. 14. Применение эмульсии по пп. 1-12 для мытья автомобилей, в моющих композициях для стирки, в очищающих средствах для твердых поверхностей, в жидкостях для автоматического мытья посуды и в жидкостях для мытья посуды. 14. The use of the emulsion according to paragraphs. 1-12 for washing cars, in detergent compositions for washing, in detergents for hard surfaces, in liquids for automatic washing dishes and in liquids for washing dishes.
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