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RU2013130865A - METHOD FOR APPLICATION ON A CARRYING SURFACE OF COATINGS WITH A POROUS METALLORGANIC STRUCTURE - Google Patents

METHOD FOR APPLICATION ON A CARRYING SURFACE OF COATINGS WITH A POROUS METALLORGANIC STRUCTURE Download PDF

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Publication number
RU2013130865A
RU2013130865A RU2013130865/04A RU2013130865A RU2013130865A RU 2013130865 A RU2013130865 A RU 2013130865A RU 2013130865/04 A RU2013130865/04 A RU 2013130865/04A RU 2013130865 A RU2013130865 A RU 2013130865A RU 2013130865 A RU2013130865 A RU 2013130865A
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layer
solutions
spraying
bearing surface
solution
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RU2013130865/04A
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Russian (ru)
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Мануэла ГААБ
Андреа ВЕБЕР
Милан КОСТУР
Ульрих Мюллер
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Басф Се
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
    • C07F5/06—Aluminium compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/22—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by diffusion
    • B01D53/228—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by diffusion characterised by specific membranes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0079—Manufacture of membranes comprising organic and inorganic components
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/14—Dynamic membranes
    • B01D69/141—Heterogeneous membranes, e.g. containing dispersed material; Mixed matrix membranes
    • B01D69/147—Heterogeneous membranes, e.g. containing dispersed material; Mixed matrix membranes containing embedded adsorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/14—Dynamic membranes
    • B01D69/141—Heterogeneous membranes, e.g. containing dispersed material; Mixed matrix membranes
    • B01D69/148—Organic/inorganic mixed matrix membranes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
    • B01D71/02—Inorganic material
    • B01D71/022—Metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • B01J20/223—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material containing metals, e.g. organo-metallic compounds, coordination complexes
    • B01J20/226—Coordination polymers, e.g. metal-organic frameworks [MOF], zeolitic imidazolate frameworks [ZIF]
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28023—Fibres or filaments
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3242—Layers with a functional group, e.g. an affinity material, a ligand, a reactant or a complexing group
    • B01J20/3244—Non-macromolecular compounds
    • B01J20/3265—Non-macromolecular compounds with an organic functional group containing a metal, e.g. a metal affinity ligand
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic Table
    • C07F3/02—Magnesium compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic Table
    • C07F3/04—Calcium compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic Table
    • C07F3/06—Zinc compounds
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H19/00—Coated paper; Coating material
    • D21H19/02—Metal coatings
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H19/00—Coated paper; Coating material
    • D21H19/10—Coatings without pigments
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H25/00—After-treatment of paper not provided for in groups D21H17/00 - D21H23/00
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/20—Organic adsorbents
    • B01D2253/204—Metal organic frameworks (MOF's)

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Dispersion Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Fertilizers (AREA)

Abstract

1. Способ нанесения на не менее чем часть несущей поверхности покрытия с пористой с металлорганической структурой, которая состоит из не менее чем одного не менее чем бидентатного органического соединения, связанного с не менее чем одним ионом металла, при этом способ включает стадии:(а) обрызгивание не менее чем части несущей поверхности первым раствором, включающим не менее чем один ион металла,(б) обрызгивание не менее чем части несущей поверхности вторым раствором, включающим не менее чем одно не менее чем бидентатное органическое соединение,при этом стадию (б) осуществляют перед стадией а), после нее или одновременно с ней и получают слой с пористой металлорганической структурой.2. Способ по п.1, где слой сушат.3. Способ по п.2, где слой сушат при не менее чем 150°C.4. Способ по п.1 или 2, где обрызгивание первым, вторым или обоими растворами проводят в барабане для обрызгивания.5. Способ по п.1 или 2, где первый, второй раствор или оба раствора находятся при комнатной температуре.6. Способ по п.1 или 2, где первый, второй раствор или оба раствора представляют собой водные растворы.7. Способ по п.1 или 2, где несущая поверхность представлена волокнистой или вспененной поверхностью.8. Способ по п.1 или 2, где не менее чем один ион металла выбирают из группы, включающей металлы магний, кальций, алюминий и цинк.9. Способ по п.1 или 2, где не менее чем одно не менее чем бидентатное органическое соединение является производным дикарбоновой, трикарбоновой или тетракарбоновой кислоты.10. Способ по п.1 или 2, где слой с пористой металлорганической структурой имеет массу в пределах от 0,1 г/мдо 100 г/м.1. A method of applying on at least a part of the bearing surface of a coating with a porous organometallic structure, which consists of at least one at least bidentate organic compound associated with at least one metal ion, the method comprising the steps: (a) spraying at least part of the bearing surface with a first solution containing at least one metal ion, (b) spraying at least part of the bearing surface with a second solution containing at least one at least one bidentate organic compound, while step (b) is carried out before, after or simultaneously with stage a), a layer with a porous organometallic structure is obtained. 2. The method of claim 1, wherein the layer is dried. The method according to claim 2, wherein the layer is dried at not less than 150 ° C. 4. The method of claim 1 or 2, wherein spraying with the first, second, or both solutions is carried out in a sprinkler drum. The method according to claim 1 or 2, wherein the first solution, the second solution, or both solutions are at room temperature. The method of claim 1 or 2, wherein the first, second, or both solutions are aqueous solutions. The method according to claim 1 or 2, wherein the supporting surface is a fibrous or foamed surface. The method according to claim 1 or 2, wherein at least one metal ion is selected from the group consisting of the metals magnesium, calcium, aluminum and zinc. The method according to claim 1 or 2, wherein at least one at least one bidentate organic compound is a derivative of a dicarboxylic, tricarboxylic or tetracarboxylic acid. The method according to claim 1 or 2, wherein the porous organometallic layer has a weight in the range from 0.1 g / m to 100 g / m.

Claims (10)

1. Способ нанесения на не менее чем часть несущей поверхности покрытия с пористой с металлорганической структурой, которая состоит из не менее чем одного не менее чем бидентатного органического соединения, связанного с не менее чем одним ионом металла, при этом способ включает стадии:1. The method of applying to at least part of the bearing surface of the coating with a porous with an organometallic structure, which consists of at least one at least one bidentate organic compound associated with at least one metal ion, the method includes the steps of: (а) обрызгивание не менее чем части несущей поверхности первым раствором, включающим не менее чем один ион металла,(a) spraying at least part of the bearing surface with a first solution comprising at least one metal ion, (б) обрызгивание не менее чем части несущей поверхности вторым раствором, включающим не менее чем одно не менее чем бидентатное органическое соединение,(b) spraying at least a part of the bearing surface with a second solution comprising at least one not less than a bidentate organic compound, при этом стадию (б) осуществляют перед стадией а), после нее или одновременно с ней и получают слой с пористой металлорганической структурой.wherein stage (b) is carried out before stage a), after it, or simultaneously with it, a layer with a porous organometallic structure is obtained. 2. Способ по п.1, где слой сушат.2. The method according to claim 1, where the layer is dried. 3. Способ по п.2, где слой сушат при не менее чем 150°C.3. The method according to claim 2, where the layer is dried at not less than 150 ° C. 4. Способ по п.1 или 2, где обрызгивание первым, вторым или обоими растворами проводят в барабане для обрызгивания.4. The method according to claim 1 or 2, where the spraying of the first, second or both solutions is carried out in a spraying drum. 5. Способ по п.1 или 2, где первый, второй раствор или оба раствора находятся при комнатной температуре.5. The method according to claim 1 or 2, where the first, second solution or both solutions are at room temperature. 6. Способ по п.1 или 2, где первый, второй раствор или оба раствора представляют собой водные растворы.6. The method according to claim 1 or 2, where the first, second solution, or both solutions are aqueous solutions. 7. Способ по п.1 или 2, где несущая поверхность представлена волокнистой или вспененной поверхностью.7. The method according to claim 1 or 2, where the bearing surface is a fibrous or foamed surface. 8. Способ по п.1 или 2, где не менее чем один ион металла выбирают из группы, включающей металлы магний, кальций, алюминий и цинк.8. The method according to claim 1 or 2, where at least one metal ion is selected from the group comprising metals magnesium, calcium, aluminum and zinc. 9. Способ по п.1 или 2, где не менее чем одно не менее чем бидентатное органическое соединение является производным дикарбоновой, трикарбоновой или тетракарбоновой кислоты.9. The method according to claim 1 or 2, where at least one at least one bidentate organic compound is a derivative of a dicarboxylic, tricarboxylic or tetracarboxylic acid. 10. Способ по п.1 или 2, где слой с пористой металлорганической структурой имеет массу в пределах от 0,1 г/м2 до 100 г/м2. 10. The method according to claim 1 or 2, where the layer with a porous organometallic structure has a mass in the range from 0.1 g / m 2 to 100 g / m 2 .
RU2013130865/04A 2010-12-07 2011-12-05 METHOD FOR APPLICATION ON A CARRYING SURFACE OF COATINGS WITH A POROUS METALLORGANIC STRUCTURE RU2013130865A (en)

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EP10193902 2010-12-07
EP10193902.3 2010-12-07
PCT/IB2011/055446 WO2012077030A1 (en) 2010-12-07 2011-12-05 Process for coating support surface with porous metal-organic framework

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EP (1) EP2649081A4 (en)
JP (1) JP2014500143A (en)
KR (1) KR20130135882A (en)
CN (1) CN103249738A (en)
AU (1) AU2011340166A1 (en)
BR (1) BR112013012870A2 (en)
CA (1) CA2818825A1 (en)
MX (1) MX2013006021A (en)
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KR20130135882A (en) 2013-12-11
EP2649081A1 (en) 2013-10-16
BR112013012870A2 (en) 2016-09-06
MX2013006021A (en) 2013-07-29
WO2012077030A1 (en) 2012-06-14
CN103249738A (en) 2013-08-14
AU2011340166A1 (en) 2013-06-13
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