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RU2010126714A - METHOD FOR PRODUCING 1,4-DIAZABICYCLO [2.1.1] HEXAN - Google Patents

METHOD FOR PRODUCING 1,4-DIAZABICYCLO [2.1.1] HEXAN Download PDF

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Publication number
RU2010126714A
RU2010126714A RU2010126714/04A RU2010126714A RU2010126714A RU 2010126714 A RU2010126714 A RU 2010126714A RU 2010126714/04 A RU2010126714/04 A RU 2010126714/04A RU 2010126714 A RU2010126714 A RU 2010126714A RU 2010126714 A RU2010126714 A RU 2010126714A
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Russia
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diazabicyclo
bisamine
ethanediamine
hexan
producing
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RU2010126714/04A
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Russian (ru)
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RU2448968C2 (en
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Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
Елена Борисовна Рахимова (RU)
Елена Борисовна Рахимова
Инна Владимировна Васильева (RU)
Инна Владимировна Васильева
Внира Рахимовна Ахметова (RU)
Внира Рахимовна Ахметова
Асхат Габдрахманович Ибрагимов (RU)
Асхат Габдрахманович Ибрагимов
Любовь Федоровна Коржова (RU)
Любовь Федоровна Коржова
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Учреждение Российской академии наук ИНСТИТУТ НЕФТЕХИМИИ И КАТАЛИЗА РАН (RU)
Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран
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Priority to RU2010126714/04A priority Critical patent/RU2448968C2/en
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Abstract

Способ получения 1,4-диазабицикло[2.1.1]гексана общей формулы (1): ! ! отличающийся тем, что 1,2-этандиамин подвергают взаимодействию с N,N,N,N-тетраметилметандиамином (бисамин), взятыми в мольном соотношении 1,2-этандиамин:бисамин=10:(20-24) при температуре 40-60°C и атмосферном давлении в течение 1-3 ч. The method of obtaining 1,4-diazabicyclo [2.1.1] hexane of the general formula (1):! ! characterized in that 1,2-ethanediamine is reacted with N, N, N, N-tetramethylmethanediamine (bisamine) taken in a molar ratio of 1,2-ethanediamine: bisamine = 10: (20-24) at a temperature of 40-60 ° C and atmospheric pressure for 1-3 hours

Claims (1)

Способ получения 1,4-диазабицикло[2.1.1]гексана общей формулы (1):The method of obtaining 1,4-diazabicyclo [2.1.1] hexane of the general formula (1):
Figure 00000001
Figure 00000001
 отличающийся тем, что 1,2-этандиамин подвергают взаимодействию с N,N,N,N-тетраметилметандиамином (бисамин), взятыми в мольном соотношении 1,2-этандиамин:бисамин=10:(20-24) при температуре 40-60°C и атмосферном давлении в течение 1-3 ч. characterized in that 1,2-ethanediamine is reacted with N, N, N, N-tetramethylmethanediamine (bisamine) taken in a molar ratio of 1,2-ethanediamine: bisamine = 10: (20-24) at a temperature of 40-60 ° C and atmospheric pressure for 1-3 hours
RU2010126714/04A 2010-06-29 2010-06-29 Method of producing 1,4-diazabicyclo[2,1,1]hexane RU2448968C2 (en)

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RU2518490C2 (en) * 2012-09-27 2014-06-10 Федеральное Государственное Бюджетное Учреждение Науки Институт Нефтехимии И Катализа Ран Method of obtaining n, n'-bis[dimethylaminomethyl](thio)urea

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RU2160738C2 (en) * 1999-03-29 2000-12-20 ООО Научно-производственное предприятие "Новые технологии" Method of preparing 1,4-diazabiocyclo (2,2,2)octane

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