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RU2010107984A - METHOD FOR REMOVING VANADIUM FROM VANADIUM CONTAINING RAW MATERIALS - Google Patents

METHOD FOR REMOVING VANADIUM FROM VANADIUM CONTAINING RAW MATERIALS Download PDF

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Publication number
RU2010107984A
RU2010107984A RU2010107984/02A RU2010107984A RU2010107984A RU 2010107984 A RU2010107984 A RU 2010107984A RU 2010107984/02 A RU2010107984/02 A RU 2010107984/02A RU 2010107984 A RU2010107984 A RU 2010107984A RU 2010107984 A RU2010107984 A RU 2010107984A
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RU
Russia
Prior art keywords
vanadium
pulp
ion exchanger
raw materials
desorption
Prior art date
Application number
RU2010107984/02A
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Russian (ru)
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RU2437946C2 (en
Inventor
Владиллен Александрович Козлов (KZ)
Владиллен Александрович Козлов
Индира Оразгалиевна Аймбетова (KZ)
Индира Оразгалиевна Аймбетова
Анатолий Александрович Карпов (RU)
Анатолий Александрович Карпов
Евгений Александрович Васин (RU)
Евгений Александрович Васин
Виталий Викторович Вдовин (RU)
Виталий Викторович Вдовин
Андрей Анатольевич Махнутин (RU)
Андрей Анатольевич Махнутин
Анна Аверьяновна Печенкина (RU)
Анна Аверьяновна Печенкина
Сергей Дмитриевич Сметанин (RU)
Сергей Дмитриевич Сметанин
Original Assignee
Владиллен Александрович Козлов (KZ)
Владиллен Александрович Козлов
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by Владиллен Александрович Козлов (KZ), Владиллен Александрович Козлов filed Critical Владиллен Александрович Козлов (KZ)
Priority to RU2010107984/02A priority Critical patent/RU2437946C2/en
Publication of RU2010107984A publication Critical patent/RU2010107984A/en
Application granted granted Critical
Publication of RU2437946C2 publication Critical patent/RU2437946C2/en

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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

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  • Treatment Of Water By Ion Exchange (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

1. Способ переработки ванадийсодержащего сырья, включающий подготовку сырья, окисление его в водной пульпе, выщелачивание кислотой и сорбцию ванадия из пульпы, отличающийся тем, что водную ванадиевую пульпу при Т:Ж=1:2 готовят из окисленного шлака или шлама обработкой кислотой от рН 11,5-7,5 до рН 4,5-4,0, а извлечение ванадия из огарка в раствор совмещают с противоточной сорбцией его из пульпы при рН 4,5-1,8 с последующей промывкой насыщенного ионита на дренаже и десорбцией ванадия со смолы. ! 2. Способ по п.1, отличающийся тем, что при выводе насыщенного ионита в пульпе поддерживают рН 4,5-4,0, а при вводе отреагированного ионита в пульпе рН 2,0-1,8. ! 3. Способ по п.1, отличающийся тем, что промывку насыщенного ионита осуществляют при содержании 350-650 кг V2O5 на тонну ионита 1%-ным раствором серной кислоты, а десорбцию ведут нитратом аммония 150-200 г/л при рН 7,5-8,5 в твердофазном режиме и рН 4,5-5,5 в объединенном десорбате в жидкофазном режиме. 1. A method of processing vanadium-containing raw materials, including the preparation of raw materials, its oxidation in an aqueous pulp, acid leaching and sorption of vanadium from the pulp, characterized in that the aqueous vanadium pulp at T: W = 1: 2 is prepared from oxidized slag or sludge by acid treatment from pH 11.5-7.5 to pH 4.5-4.0, and the extraction of vanadium from the cinder into the solution is combined with its countercurrent sorption from the pulp at pH 4.5-1.8, followed by washing the saturated ion exchanger on the drain and desorption of vanadium from resin. ! 2. The method according to claim 1, characterized in that when the saturated ion exchanger is removed in the pulp, the pH is maintained at 4.5-4.0, and when the reacted ion exchanger is introduced in the pulp, the pH is 2.0-1.8. ! 3. The method according to claim 1, characterized in that the saturated ion exchanger is washed with a content of 350-650 kg of V2O5 per ton of ion exchanger with a 1% solution of sulfuric acid, and desorption is carried out with ammonium nitrate 150-200 g / l at pH 7.5 -8.5 in solid phase mode and pH 4.5-5.5 in combined desorbate in liquid phase mode.

Claims (3)

1. Способ переработки ванадийсодержащего сырья, включающий подготовку сырья, окисление его в водной пульпе, выщелачивание кислотой и сорбцию ванадия из пульпы, отличающийся тем, что водную ванадиевую пульпу при Т:Ж=1:2 готовят из окисленного шлака или шлама обработкой кислотой от рН 11,5-7,5 до рН 4,5-4,0, а извлечение ванадия из огарка в раствор совмещают с противоточной сорбцией его из пульпы при рН 4,5-1,8 с последующей промывкой насыщенного ионита на дренаже и десорбцией ванадия со смолы.1. A method of processing vanadium-containing raw materials, including the preparation of raw materials, its oxidation in aqueous pulp, acid leaching and sorption of vanadium from the pulp, characterized in that the aqueous vanadium pulp at T: W = 1: 2 is prepared from oxidized slag or sludge by acid treatment from pH 11.5-7.5 to pH 4.5-4.0, and the extraction of vanadium from the cinder in the solution is combined with countercurrent sorption of it from the pulp at pH 4.5-1.8, followed by washing of the saturated ion exchanger on the drainage and desorption of vanadium from the resin. 2. Способ по п.1, отличающийся тем, что при выводе насыщенного ионита в пульпе поддерживают рН 4,5-4,0, а при вводе отреагированного ионита в пульпе рН 2,0-1,8.2. The method according to claim 1, characterized in that when the saturated ion exchanger is withdrawn in the pulp, a pH of 4.5-4.0 is maintained, and when the reacted ion exchanger is introduced into the pulp, the pH is 2.0-1.8. 3. Способ по п.1, отличающийся тем, что промывку насыщенного ионита осуществляют при содержании 350-650 кг V2O5 на тонну ионита 1%-ным раствором серной кислоты, а десорбцию ведут нитратом аммония 150-200 г/л при рН 7,5-8,5 в твердофазном режиме и рН 4,5-5,5 в объединенном десорбате в жидкофазном режиме. 3. The method according to claim 1, characterized in that the washing of the saturated ion exchanger is carried out at a content of 350-650 kg of V 2 O 5 per ton of ion exchanger with 1% sulfuric acid solution, and desorption is carried out with ammonium nitrate 150-200 g / l at pH 7.5-8.5 in the solid state mode and pH 4.5-5.5 in the combined desorbate in the liquid phase mode.
RU2010107984/02A 2010-03-05 2010-03-05 Procedure for processing vanadium containing raw material RU2437946C2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
RU2010107984/02A RU2437946C2 (en) 2010-03-05 2010-03-05 Procedure for processing vanadium containing raw material

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Application Number Priority Date Filing Date Title
RU2010107984/02A RU2437946C2 (en) 2010-03-05 2010-03-05 Procedure for processing vanadium containing raw material

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RU2010107984A true RU2010107984A (en) 2011-09-10
RU2437946C2 RU2437946C2 (en) 2011-12-27

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115011818A (en) * 2022-06-15 2022-09-06 上海寰泰绿钒科技有限公司 Method for extracting vanadium from stone coal

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109182768A (en) * 2018-10-25 2019-01-11 攀钢集团攀枝花钢铁研究院有限公司 The method of vanadium and chromium is separated from vanadium chromium slag

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2545105A1 (en) * 1983-04-27 1984-11-02 Pechiney Uranium High-temperature pretreatment of uraniferous, vanadiferous or molybdeniferous ores containing clayey gangue by means of an alkaline aqueous solution
RU2118389C1 (en) * 1997-07-30 1998-08-27 Акционерное общество открытого типа "Ванадий-Тулачермет" Method of isolating vanadium
AT408454B (en) * 1999-03-18 2001-12-27 Treibacher Ind Ag METHOD FOR OXIDATING VANADIUM
RU2211253C2 (en) * 2001-10-11 2003-08-27 Государственное унитарное предприятие "Всероссийский научно-исследовательский институт химической технологии" Method for extraction of uranium, molybdenum and vanadium
RU2193072C1 (en) * 2001-11-28 2002-11-20 Открытое акционерное общество "Ванадий-Тула" Method of extraction of vanadium

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115011818A (en) * 2022-06-15 2022-09-06 上海寰泰绿钒科技有限公司 Method for extracting vanadium from stone coal

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Effective date: 20140306