RU2008114571A - METHOD FOR QUANTITATIVE DETERMINATION OF HESPERIDIN BY DIFFERENTIAL VOLTAMPEROMETRY METHOD - Google Patents
METHOD FOR QUANTITATIVE DETERMINATION OF HESPERIDIN BY DIFFERENTIAL VOLTAMPEROMETRY METHOD Download PDFInfo
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- RU2008114571A RU2008114571A RU2008114571/15A RU2008114571A RU2008114571A RU 2008114571 A RU2008114571 A RU 2008114571A RU 2008114571/15 A RU2008114571/15 A RU 2008114571/15A RU 2008114571 A RU2008114571 A RU 2008114571A RU 2008114571 A RU2008114571 A RU 2008114571A
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- hesperidin
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- quantitative determination
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Abstract
Способ количественного определения гесперидина, включающий перевод гесперидина из пробы в раствор и вольтамперометрическое определение с использованием индикаторного стеклоуглеродного электрода, отличающийся тем, что используют дифференциальную вольтамперометрию, при этом накопление гесперидина в перемешиваемом растворе проводят в течение 60÷120 с при потенциале электролиза (-0,6÷-0,8) В относительно насыщенного хлоридсеребряного электрода на фоне 0,1 н двузамещенного гидрофосфата натрия с последующей регистрацией анодных пиков в дифференциальном режиме съемки вольтамперограмм при скорости развертки потенциала 20÷30 мВ/с, и концентрацию гесперидина определяют по высоте пика в диапазоне потенциалов от 0,35 до 0,45 В методом добавок аттестованных смесей.A method for the quantitative determination of hesperidin, including the transfer of hesperidin from a sample to a solution and voltammetric determination using an indicator glassy carbon electrode, characterized in that differential voltammetry is used, while the accumulation of hesperidin in a stirred solution is carried out for 60 ÷ 120 s at an electrolysis potential (-0, 6 ÷ -0.8) In a relatively saturated silver chloride electrode against a background of 0.1 n disubstituted sodium hydrogen phosphate, followed by registration of the anode peaks in diff differential voltammograms shooting mode, when the potential sweep rate of 20 ÷ 30 mV / s, and the concentration of hesperidin is determined by the peak height in the potential range of from 0.35 to 0.45 by addition certified mixtures.
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| Application Number | Priority Date | Filing Date | Title |
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| RU2008114571/15A RU2381502C2 (en) | 2008-04-14 | 2008-04-14 | Method for quantitative determination of hesperedin using differential voltammetry method |
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| Application Number | Priority Date | Filing Date | Title |
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| RU2008114571/15A RU2381502C2 (en) | 2008-04-14 | 2008-04-14 | Method for quantitative determination of hesperedin using differential voltammetry method |
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| RU2008114571A true RU2008114571A (en) | 2009-10-20 |
| RU2381502C2 RU2381502C2 (en) | 2010-02-10 |
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| RU2008114571/15A RU2381502C2 (en) | 2008-04-14 | 2008-04-14 | Method for quantitative determination of hesperedin using differential voltammetry method |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2447444C1 (en) * | 2010-10-12 | 2012-04-10 | Российская Федерация, От Имени Которой Выступает Министерство Образования И Науки Российской Федерации | Method for determining total content of thiol antioxidants in plant objects by cathodic voltammetry |
| CN115791916A (en) * | 2022-10-27 | 2023-03-14 | 广东省农业科学院果树研究所 | Probe type electrochemical detection device and preparation method and application thereof |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2441224C1 (en) * | 2010-10-12 | 2012-01-27 | Российская Федерация, От Имени Которой Выступает Министерство Образования И Науки Российской Федерации | Voltammetric method for quantitative determination of total content of flavonoids in plant material |
| RU2504761C1 (en) * | 2012-07-12 | 2014-01-20 | Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Национальный исследовательский Томский политехнический университет" | Method for quantitative determination of nickel by stripping voltammetry on organo-modified electrode |
| CN103575820B (en) * | 2012-08-01 | 2016-08-10 | 天士力制药集团股份有限公司 | The analysis method of 5 kinds of flavonoid glycosides and application in pharmacokinetics thereof in blood plasma |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100213895B1 (en) * | 1996-10-14 | 1999-08-02 | 박원훈 | A composition for preventing and treating cardiovascular diseases comprising citrus peel extract, hesperidin or naringin isolated therefrom |
| RU2194987C2 (en) * | 2000-05-26 | 2002-12-20 | Научно-исследовательский институт кардиологии Томского научного центра СО РАМН | Method for determining catecholamine quantity in urine |
| RU2246722C1 (en) * | 2003-11-06 | 2005-02-20 | Научно-исследовательский институт кардиологии Томского научного центра Сибирского отделения Академии медицинских наук | Inversion voltampermetric method of determining concentration of amiodarone (cordarone) |
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2008
- 2008-04-14 RU RU2008114571/15A patent/RU2381502C2/en not_active IP Right Cessation
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2447444C1 (en) * | 2010-10-12 | 2012-04-10 | Российская Федерация, От Имени Которой Выступает Министерство Образования И Науки Российской Федерации | Method for determining total content of thiol antioxidants in plant objects by cathodic voltammetry |
| CN115791916A (en) * | 2022-10-27 | 2023-03-14 | 广东省农业科学院果树研究所 | Probe type electrochemical detection device and preparation method and application thereof |
| CN115791916B (en) * | 2022-10-27 | 2023-11-24 | 广东省农业科学院果树研究所 | Probe type electrochemical detection device and preparation method and application thereof |
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| Publication number | Publication date |
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| RU2381502C2 (en) | 2010-02-10 |
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Effective date: 20100415 |