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PH12012000062A1 - Preparation of pectin and polyphenolic compositions from mango peels - Google Patents

Preparation of pectin and polyphenolic compositions from mango peels

Info

Publication number
PH12012000062A1
PH12012000062A1 PH1/2012/000062A PH12012000062A PH12012000062A1 PH 12012000062 A1 PH12012000062 A1 PH 12012000062A1 PH 12012000062 A PH12012000062 A PH 12012000062A PH 12012000062 A1 PH12012000062 A1 PH 12012000062A1
Authority
PH
Philippines
Prior art keywords
pectin
preparation
improved process
mango
recovery
Prior art date
Application number
PH1/2012/000062A
Inventor
Francis Dave C Siacor
Evelyn B Taboada
Original Assignee
Univ Of San Carlos
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Univ Of San Carlos filed Critical Univ Of San Carlos
Priority to PH1/2012/000062A priority Critical patent/PH12012000062A1/en
Priority to PCT/PH2013/000009 priority patent/WO2013141723A1/en
Priority to PH12017000214A priority patent/PH12017000214A1/en
Priority to PH12017000213A priority patent/PH12017000213A1/en
Publication of PH12012000062A1 publication Critical patent/PH12012000062A1/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08BPOLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B37/00Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
    • C08B37/0006Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid
    • C08B37/0045Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid alpha-D-Galacturonans, e.g. methyl ester of (alpha-1,4)-linked D-galacturonic acid units, i.e. pectin, or hydrolysis product of methyl ester of alpha-1,4-linked D-galacturonic acid units, i.e. pectinic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23BPRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
    • A23B2/00Preservation of foods or foodstuffs, in general
    • A23B2/70Preservation of foods or foodstuffs, in general by treatment with chemicals
    • A23B2/725Preservation of foods or foodstuffs, in general by treatment with chemicals in the form of liquids or solids
    • A23B2/729Organic compounds; Microorganisms; Enzymes
    • A23B2/733Compounds of undetermined constitution obtained from animals or plants
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K10/00Animal feeding-stuffs
    • A23K10/30Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
    • A23K10/37Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from waste material
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/10Organic substances
    • A23K20/111Aromatic compounds
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/10Organic substances
    • A23K20/163Sugars; Polysaccharides
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L19/00Products from fruits or vegetables; Preparation or treatment thereof
    • A23L19/03Products from fruits or vegetables; Preparation or treatment thereof consisting of whole pieces or fragments without mashing the original pieces
    • A23L19/07Fruit waste products, e.g. from citrus peel or seeds
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L29/00Foods or foodstuffs containing additives; Preparation or treatment thereof
    • A23L29/20Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
    • A23L29/206Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of vegetable origin
    • A23L29/231Pectin; Derivatives thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/105Plant extracts, their artificial duplicates or their derivatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00Medicinal preparations containing organic active ingredients
    • A61K31/70Carbohydrates; Sugars; Derivatives thereof
    • A61K31/715Polysaccharides, i.e. having more than five saccharide radicals attached to each other by glycosidic linkages; Derivatives thereof, e.g. ethers, esters
    • A61K31/732Pectin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/22Anacardiaceae (Sumac family), e.g. smoketree, sumac or poison oak
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08BPOLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B37/00Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
    • C08B37/0003General processes for their isolation or fractionation, e.g. purification or extraction from biomass
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L5/00Compositions of polysaccharides or of their derivatives not provided for in groups C08L1/00 or C08L3/00
    • C08L5/06Pectin; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/10General cosmetic use
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P60/00Technologies relating to agriculture, livestock or agroalimentary industries
    • Y02P60/80Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
    • Y02P60/87Re-use of by-products of food processing for fodder production

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Polymers & Plastics (AREA)
  • General Health & Medical Sciences (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Mycology (AREA)
  • Molecular Biology (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • Botany (AREA)
  • Biotechnology (AREA)
  • Zoology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Epidemiology (AREA)
  • Materials Engineering (AREA)
  • Biochemistry (AREA)
  • Animal Husbandry (AREA)
  • Microbiology (AREA)
  • Nutrition Science (AREA)
  • Birds (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Medical Informatics (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Dispersion Chemistry (AREA)
  • Dermatology (AREA)
  • Sustainable Development (AREA)
  • Physiology (AREA)
  • Wood Science & Technology (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Preparation Of Fruits And Vegetables (AREA)

Abstract

This invention relates to an improved process in the recovery and preparation of pectin and polyphenolic compositions from mango peels. In this improved process, the pectin-containing material is subjected to acid-hydrolysis to extract pectin, then separation of the filtrate containing the pectin material by a simple settling-decantation-filtration step, and recovery of the pectin material by alcoholic precipitation-mixing-and-settling step. The pectin precipitate is further dried and milled to obtain the pectin-powder. The improved process is characterized by its pectin yield of 30% or greater. The pectin obtained herein is further characterized by its galacturonic acid content of 70% or higher and degree of esterification of 65% or greater, as it employs the defatted mango peel powder.
PH1/2012/000062A 2012-03-22 2012-03-22 Preparation of pectin and polyphenolic compositions from mango peels PH12012000062A1 (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
PH1/2012/000062A PH12012000062A1 (en) 2012-03-22 2012-03-22 Preparation of pectin and polyphenolic compositions from mango peels
PCT/PH2013/000009 WO2013141723A1 (en) 2012-03-22 2013-03-15 Preparation of pectin and polyphenolic compositions from mango peels
PH12017000214A PH12017000214A1 (en) 2012-03-22 2017-07-21 Process for the manufacture of spent mango peel powder
PH12017000213A PH12017000213A1 (en) 2012-03-22 2017-07-21 Preparation of pectin from mango peels

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PH1/2012/000062A PH12012000062A1 (en) 2012-03-22 2012-03-22 Preparation of pectin and polyphenolic compositions from mango peels

Publications (1)

Publication Number Publication Date
PH12012000062A1 true PH12012000062A1 (en) 2020-10-19

Family

ID=48366549

Family Applications (3)

Application Number Title Priority Date Filing Date
PH1/2012/000062A PH12012000062A1 (en) 2012-03-22 2012-03-22 Preparation of pectin and polyphenolic compositions from mango peels
PH12017000214A PH12017000214A1 (en) 2012-03-22 2017-07-21 Process for the manufacture of spent mango peel powder
PH12017000213A PH12017000213A1 (en) 2012-03-22 2017-07-21 Preparation of pectin from mango peels

Family Applications After (2)

Application Number Title Priority Date Filing Date
PH12017000214A PH12017000214A1 (en) 2012-03-22 2017-07-21 Process for the manufacture of spent mango peel powder
PH12017000213A PH12017000213A1 (en) 2012-03-22 2017-07-21 Preparation of pectin from mango peels

Country Status (2)

Country Link
PH (3) PH12012000062A1 (en)
WO (1) WO2013141723A1 (en)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2515515B1 (en) * 2013-04-29 2015-11-02 Galina IGNATYEVA Manufacturing method of achromatic pectin, modified fiber and pectin and standardized pectin
CN105998109B (en) * 2016-06-24 2020-08-04 贺州学院 A kind of mango pit polyphenol extract and preparation method thereof
CN106138130B (en) * 2016-07-26 2020-08-04 贺州学院 Mango seed flavone extract and preparation method thereof
CN109874963A (en) * 2019-04-12 2019-06-14 倪震丹 A kind of Apples paper and preparation method thereof
CN112914012B (en) * 2021-01-29 2023-09-15 广西壮族自治区农业科学院 A method for extracting bonded aroma substances from mango peel and its application
CN113024616A (en) * 2021-03-22 2021-06-25 贺州学院 Preparation method of mango seed tannic acid

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5626901A (en) 1979-08-10 1981-03-16 Takuo Sakai Preparation of pectin from plant tissue
US5071970A (en) 1988-11-23 1991-12-10 University Of Florida Process for producing pectin with a high-to-medium methoxyl content from beet pulp
US6143346A (en) 1993-12-02 2000-11-07 Hercules Incorporated Pectin process and composition
CA2128293C (en) 1993-12-06 2002-09-03 Masayuki Tanabe Fruit polyphenols and medicinal compositions containing them
GB2342921A (en) 1998-10-24 2000-04-26 Zylepsis Ltd Demethoxylation of pectins, plant extracts containing PME and the uses thereof
US6143337A (en) 1999-04-30 2000-11-07 The United States Of America As Represented By The Secretary Of Agriculture Extraction of pectin by microwave heating under pressure
DK1233988T3 (en) 1999-11-22 2007-07-30 Philip G Crandall Isolation of pectin from soybeans
FR2820738B1 (en) 2001-02-15 2003-05-16 Agronomique Inst Nat Rech PROCESS FOR THE EXTRACTION, FRACTIONATION AND PURIFICATION OF POLYPHENOLIC COMPOUNDS FROM SORTING GAPS OF FRESH PLANTS USING A HIGH-YIELD ADSORPTION AND ELUTING RESIN
EP1877448A2 (en) 2005-03-09 2008-01-16 Cargill, Incorporated Process for obtaining pectin

Also Published As

Publication number Publication date
PH12017000214A1 (en) 2017-11-27
PH12017000213A1 (en) 2019-02-11
WO2013141723A1 (en) 2013-09-26

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