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KR970027203A - Rubber compositions based on functionalized diene polymers having silica and silanol terminal functional groups - Google Patents

Rubber compositions based on functionalized diene polymers having silica and silanol terminal functional groups Download PDF

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Publication number
KR970027203A
KR970027203A KR1019960051967A KR19960051967A KR970027203A KR 970027203 A KR970027203 A KR 970027203A KR 1019960051967 A KR1019960051967 A KR 1019960051967A KR 19960051967 A KR19960051967 A KR 19960051967A KR 970027203 A KR970027203 A KR 970027203A
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KR
South Korea
Prior art keywords
silica
diene polymer
composition
silanol
polysiloxane block
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KR1019960051967A
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Korean (ko)
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KR100474449B1 (en
Inventor
쟝-릭 까비오쉬
제라르 라보즈
Original Assignee
이벨 로베르
꽁빠니 제네랄 데 제따블리스망 미쉐린-미쉐린에 꽁빠니
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Publication of KR970027203A publication Critical patent/KR970027203A/en
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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B60—VEHICLES IN GENERAL
    • B60C—VEHICLE TYRES; TYRE INFLATION; TYRE CHANGING; CONNECTING VALVES TO INFLATABLE ELASTIC BODIES IN GENERAL; DEVICES OR ARRANGEMENTS RELATED TO TYRES
    • B60C1/00—Tyres characterised by the chemical composition or the physical arrangement or mixture of the composition
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L53/00—Compositions of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B60—VEHICLES IN GENERAL
    • B60C—VEHICLE TYRES; TYRE INFLATION; TYRE CHANGING; CONNECTING VALVES TO INFLATABLE ELASTIC BODIES IN GENERAL; DEVICES OR ARRANGEMENTS RELATED TO TYRES
    • B60C1/00—Tyres characterised by the chemical composition or the physical arrangement or mixture of the composition
    • B60C1/0016—Compositions of the tread
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/42—Block-or graft-polymers containing polysiloxane sequences
    • C08G77/442—Block-or graft-polymers containing polysiloxane sequences containing vinyl polymer sequences
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L19/00—Compositions of rubbers not provided for in groups C08L7/00 - C08L17/00
    • C08L19/006—Rubber characterised by functional groups, e.g. telechelic diene polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
    • C08L83/10—Block- or graft-copolymers containing polysiloxane sequences
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02T—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO TRANSPORTATION
    • Y02T10/00—Road transport of goods or passengers
    • Y02T10/80—Technologies aiming to reduce greenhouse gasses emissions common to all road transportation technologies
    • Y02T10/86—Optimisation of rolling resistance, e.g. weight reduction 

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Tires In General (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)

Abstract

본 발명은 실리카를 주강화 충전제로서 포함하고 실란올 작용 그룹 또는 실란을 말단을 갖는 폴리실록산 블록을 쇄 말단으로서 갖는 디엔 중합체가 1종 이상을 포함하는 고무 조성물에 관한 것으로서, 이 조성물은 히스테레시스가 적어 구름 저항이 적은 타이어의 트레드로서 사용하기에 특히 적합하다.The present invention relates to a rubber composition comprising silica as a main strengthening filler and at least one diene polymer having a silanol functional group or a silane-terminated polysiloxane block as the chain end, wherein the composition is hysteresis free. It is particularly suitable for use as a tread for tires with low rolling resistance.

Description

실리카와 실란올 말단 작용 그룹을 갖는 작용화된 디엔 중합체를 기재로 하는 고무 조성물Rubber compositions based on functionalized diene polymers having silica and silanol terminal functional groups

본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음Since this is an open matter, no full text was included.

Claims (14)

1종 이상의 작용화된 디엔 중합체와 강화 충전제로서의 실리카를 포함하는 가황성 고무 조성물로서, 작용화된 디엔 중합체가 실란올 작용 그룹 또는 실란올 말단을 갖는 폴리실록산 블록을 쇄 말단으로서 갖는 디엔 중합체이고 실리카가 주성분으로서 존재하는 가황성 고무 조성물.A vulcanizable rubber composition comprising at least one functionalized diene polymer and silica as a reinforcing filler, wherein the functionalized diene polymer is a diene polymer having a polysiloxane block as chain end having a silanol functional group or silanol end and the silica is Vulcanizable rubber composition present as a main component. 제1항에 있어서, 실란올 말단을 갖는 폴리실록산 블록의 화학식이 다음과 같은 조성물.The composition of claim 1 wherein the formula of the polysiloxane block having silanol ends is as follows. [-(SiR1R2O)x-H] (1)[-(SiR 1 R 2 O) x -H] (1) 위의 화학식(1)에서, R1과 R2는 동일하거나 상이하면 탄소수 1 내지 10의 알킬, 사이클로알킬, 아릴, 알크아릴, 아르알킬 또는 비닐 그룹이고, x는 1 내지 1500의 정수이다.In formula (1) above, R 1 and R 2 are the same or different alkyl, cycloalkyl, aryl, alkaryl, aralkyl or vinyl group having 1 to 10 carbon atoms, and x is an integer of 1 to 1500. 제2항에 있어서, R1과 R2가 탄소수 1내지 5의 알킬 그룹, 바람직하게는 메틸 그룹인 조성물.The composition of claim 2 wherein R 1 and R 2 are alkyl groups of 1 to 5 carbon atoms, preferably methyl groups. 제1항에 있어서, 디엔 중합체가 부타디엔-스티렌 또는 부타디엔-수티렌-이소프렌 공중합체인 조성물.The composition of claim 1, wherein the diene polymer is butadiene-styrene or butadiene-sutirene-isoprene copolymer. 제4항에 있어서, 폴리부타디엔 및/또는 부타디엔-이소프렌 공중합체 및/또는 천연 고무를 추가로 포함하는 조성물.The composition of claim 4 further comprising polybutadiene and / or butadiene-isoprene copolymer and / or natural rubber. 제1항에 있어서, 강화 충전제가 전부 실리카로 구성되는 조성물.The composition of claim 1, wherein the reinforcing fillers are all composed of silica. 제1항에 있어서, 강화 충전제가 실리카와 부성분으로서의 카본 블랙을 포함하는 조성물.The composition of claim 1 wherein the reinforcing filler comprises silica and carbon black as a minor component. 제1항에 있어서, 실리카가 CTAB 표면적이 450㎡/g 이하이고 BET 표면적이 450㎡/g이하인 고분산성 침강 실리카인 조성물.The composition of claim 1 wherein the silica is a highly dispersible precipitated silica having a CTAB surface area of 450 m 2 / g or less and a BET surface area of 450 m 2 / g or less. 제8항에 있어서, 실리카가 BET 비표면적/CTAB 비표면적의 비가 1 이상 1.2 이하인 조성물.The composition of claim 8, wherein the silica has a ratio of BET specific surface area / CTAB specific surface area of 1 to 1.2. 1종 이상의 작용화된 디엔 중합체와 강화 충전제로서의 실리카를 포함하는 가황성 고무 조성물을 포함하는 구름 저항이 적은 타이어로서, 작용화된 디엔 중합체가 실란을 작용 그룹 또는 실란을 말단을 갖는 폴리실록산 블록을 쇄 말단으로서 갖는 디엔 중합체이고 실리카가 주성분으로서 존재하는 타이어.A low rolling resistance tire comprising a vulcanizable rubber composition comprising at least one functionalized diene polymer and silica as a reinforcing filler, wherein the functionalized diene polymer chains a polysiloxane block having a silane functional group or silane end A tire in which a diene polymer as a terminal is present and silica is present as a main component. 제10항에 있어서, 조성물이 트레드에 사용되는 타이어.The tire of claim 10, wherein the composition is used for a tread. 제1종 이상의 작용화된 디엔 중합체와 강화 충전제로서의 실리카를 포함하는 가황성 고무 조성물로 이루어진 타이어 트레드로서, 작용화된 디엔 중합체가 실란올 작용 그룹 또는 실란올 말단을 갖는 폴리실록산 블록을 쇄 말단으로서 갖는 디엔 중합체이고 실리카가 중성분으로서 존재하는 타이어 트레드.A tire tread consisting of a vulcanizable rubber composition comprising at least one functionalized diene polymer and silica as reinforcing filler, wherein the functionalized diene polymer has, as chain end, a polysiloxane block having silanol functional groups or silanol ends Tire tread with diene polymer and silica present as a heavy component. 제1종 이상의 디엔 단량체를 촉매의 존재하에 중합시켜 리빙 디엔 중합체를 수득하고, 이를 1종 이상의 유기 실란과 반응시키고, 용매를 증기로 스트리핑시켜 실란올 작용 그룹 또는 실란올 말단을 갖는 폴리실록산 블록을 쇄 말단으로서 갖는 디엔 중합체를 회수한 다음 건조시킴을 포함하여, 실란올 작용 그룹 또는 실란올 말단을 갖는 폴리실록산 블록을 쇄 말단으로서 갖는 디엔 중합체를 수득하는 방법.Polymerizing at least one diene monomer in the presence of a catalyst to obtain a living diene polymer, reacting it with at least one organic silane, and stripping the solvent with steam to chain polysiloxane blocks with silanol functional groups or silanol ends. A process for obtaining a diene polymer having as a chain end a polysiloxane block having a silanol functional group or silanol end, including recovering the diene polymer having as a terminal and then drying. Six 말단(여기서, x는 할로겐 원자이다)을 갖는 디엔 중합체에 디리티 오폴리실록산 또는 디소디오폴리실록산을 그라프트시키고, 그라프트 생성물을 양자 공여 화합물과 반응시킨 다음, 용매를 증기로 스트리핑시켜 실란올 말단을 갖는 폴리실록산 블록을 내포하는 불록 공중합체를 회수하고 건조시킴을 포함하여, 실란올 말단을 갖는 폴리실록산 블록을 쇄 말단으로서 갖는 디엔 공중합체를 제조하는 방법.A diene polymer having six ends (where x is a halogen atom) is grafted to a diity oppolysiloxane or disodiopolysiloxane, the graft product is reacted with a proton donor compound, and the solvent is stripped with vapor to give silanol ends. A method for producing a diene copolymer having as the chain end a polysiloxane block having a silanol end, including recovering and drying the block copolymer containing the polysiloxane block having a. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.※ Note: The disclosure is based on the initial application.
KR1019960051967A 1995-11-07 1996-11-05 Rubber compositions based on functionalized diene polymers with silica and silanol terminal functional groups Expired - Lifetime KR100474449B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR9513249A FR2740778A1 (en) 1995-11-07 1995-11-07 SILICA-BASED RUBBER COMPOSITION AND FUNCTIONALIZED DIENE POLYMER HAVING TERMINAL SILANOL FUNCTION
FR9513249 1995-11-07

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KR970027203A true KR970027203A (en) 1997-06-24
KR100474449B1 KR100474449B1 (en) 2005-08-10

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US (1) US6013718A (en)
EP (1) EP0778311B1 (en)
JP (1) JP3693769B2 (en)
KR (1) KR100474449B1 (en)
CN (1) CN1105750C (en)
AT (1) ATE189244T1 (en)
AU (1) AU712080B2 (en)
BR (1) BR9605443A (en)
CA (1) CA2189363C (en)
DE (1) DE69606382T2 (en)
ES (1) ES2141431T3 (en)
FR (1) FR2740778A1 (en)

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US6013718A (en) 2000-01-11
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CA2189363C (en) 2007-06-26
CN1105750C (en) 2003-04-16
DE69606382D1 (en) 2000-03-02
EP0778311A1 (en) 1997-06-11
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MX9605368A (en) 1997-10-31
ATE189244T1 (en) 2000-02-15
ES2141431T3 (en) 2000-03-16
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AU712080B2 (en) 1999-10-28
BR9605443A (en) 1998-08-04

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