KR900004677A - "β-알라닌이아세트산 또는 이 화합물의 알칼리금속염 이나 암모늄염의 제법" - Google Patents
"β-알라닌이아세트산 또는 이 화합물의 알칼리금속염 이나 암모늄염의 제법" Download PDFInfo
- Publication number
- KR900004677A KR900004677A KR1019890012714A KR890012714A KR900004677A KR 900004677 A KR900004677 A KR 900004677A KR 1019890012714 A KR1019890012714 A KR 1019890012714A KR 890012714 A KR890012714 A KR 890012714A KR 900004677 A KR900004677 A KR 900004677A
- Authority
- KR
- South Korea
- Prior art keywords
- alkali metal
- preparation
- acid
- diacetic acid
- alanine diacetic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- UWRBFYBQPCJRRL-UHFFFAOYSA-N 3-[bis(carboxymethyl)amino]propanoic acid Chemical compound OC(=O)CCN(CC(O)=O)CC(O)=O UWRBFYBQPCJRRL-UHFFFAOYSA-N 0.000 title claims abstract 7
- 150000003863 ammonium salts Chemical class 0.000 title claims abstract 7
- 229910052783 alkali metal Inorganic materials 0.000 title claims abstract 6
- -1 alkali metal salt Chemical class 0.000 title claims 2
- 150000001875 compounds Chemical class 0.000 title claims 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract 4
- 150000001340 alkali metals Chemical class 0.000 claims abstract 4
- 239000012736 aqueous medium Substances 0.000 claims abstract 4
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims abstract 3
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract 3
- 239000002585 base Substances 0.000 claims abstract 3
- 239000002609 medium Substances 0.000 claims abstract 3
- 150000001412 amines Chemical class 0.000 claims abstract 2
- 229910021529 ammonia Inorganic materials 0.000 claims abstract 2
- 238000000034 method Methods 0.000 claims 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims 2
- WDJHALXBUFZDSR-UHFFFAOYSA-N acetoacetic acid Chemical compound CC(=O)CC(O)=O WDJHALXBUFZDSR-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- TVMUHOAONWHJBV-UHFFFAOYSA-N dehydroglycine Chemical compound OC(=O)C=N TVMUHOAONWHJBV-UHFFFAOYSA-N 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 229910052757 nitrogen Inorganic materials 0.000 claims 1
- NBZBKCUXIYYUSX-UHFFFAOYSA-N iminodiacetic acid Chemical compound OC(=O)CNCC(O)=O NBZBKCUXIYYUSX-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B26—HAND CUTTING TOOLS; CUTTING; SEVERING
- B26F—PERFORATING; PUNCHING; CUTTING-OUT; STAMPING-OUT; SEVERING BY MEANS OTHER THAN CUTTING
- B26F1/00—Perforating; Punching; Cutting-out; Stamping-out; Apparatus therefor
- B26F1/38—Cutting-out; Stamping-out
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/14—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Forests & Forestry (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Indole Compounds (AREA)
Abstract
Description
Claims (4)
- a) β-알라닌이아세트산(Ia)의 제조를 위하여 이미노이아세트산과 아크릴산을 비염기성 수용성 매질에서 서로 반응시키고 및 b) β-알아닌이아세트산의 알칼리금속염이나 암모늄염(Ib)의 제조를 위하여 이미노이아세트산과 아크릴산을 알칼리수용성 매질에서 또는 질소염기를 함유하는 수용성 매질에서 서로 반응시키고, 또는 비염기성 매질에서 형성된 (Ia)를 알칼리금속염기, 암모니아 또는 아민을 사용하여 (Ib)로 전환시킴을 특징으로 하는 β-알라닌이아세트산(Ia) 또는 이 화합물의 알칼리금속염이나 암모늄염(Ib)의 제조 방법.
- 제1항에 있어서, 그 반응을 70 내지 100℃의 온도에서 수행함을 특징으로 하는 방법.
- 제1항에 있어서, 구현예(a)의 경우에 그 반응을 pH 0 내지 1에서 수행함을 특징으로 하는 방법.
- 제1항에 있어서, 구현예(b)의 경우에 그 반응을 pH 7 내지 9에서 수행함을 특징으로 하는 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3829859A DE3829859A1 (de) | 1988-09-02 | 1988-09-02 | Verfahren zur herstellung von ss-alanindiessigsaeure oder ihren alkalimetall- oder ammoniumsalzen |
| DEP3829859.7 | 1988-09-02 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| KR900004677A true KR900004677A (ko) | 1990-04-12 |
Family
ID=6362159
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019890012714A Ceased KR900004677A (ko) | 1988-09-02 | 1989-09-02 | "β-알라닌이아세트산 또는 이 화합물의 알칼리금속염 이나 암모늄염의 제법" |
Country Status (9)
| Country | Link |
|---|---|
| US (2) | US5068416A (ko) |
| EP (1) | EP0356972B2 (ko) |
| JP (1) | JPH02101054A (ko) |
| KR (1) | KR900004677A (ko) |
| AT (1) | ATE98218T1 (ko) |
| AU (1) | AU611586B2 (ko) |
| CA (1) | CA1316937C (ko) |
| DE (2) | DE3829859A1 (ko) |
| ES (1) | ES2046408T5 (ko) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3829847A1 (de) * | 1988-09-02 | 1990-03-15 | Basf Ag | Wasch- und reinigungsmittel |
| DE4039922A1 (de) * | 1990-12-14 | 1992-06-17 | Basf Ag | Verfahren zur herstellung von (beta)-alanindiessigsaeure und ihren alkalimetallsalzen |
| GB9116684D0 (en) * | 1991-08-02 | 1991-09-18 | Exxon Chemical Patents Inc | Corrosion inhibitors |
| US5362412A (en) * | 1991-04-17 | 1994-11-08 | Hampshire Chemical Corp. | Biodegradable bleach stabilizers for detergents |
| GB9114012D0 (en) * | 1991-06-28 | 1991-08-14 | Exxon Chemical Patents Inc | Amine adducts as corrosion inhibitors |
| DE4216560A1 (de) * | 1992-05-20 | 1993-11-25 | Basf Ag | Verfahren zur Herstellung von µ-Alanindiessigsäure oder ihren Alkalimetall- oder Ammoniumsalzen |
| US5481018A (en) * | 1995-03-31 | 1996-01-02 | The Dow Chemical Company | Amino nitrile intermediate for the preparation of alanine diacetic acid |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2195974A (en) * | 1936-05-19 | 1940-04-02 | Ig Farbenindustrie Ag | Process of producing new amino-carboxylic acids |
| US3260745A (en) * | 1962-04-18 | 1966-07-12 | Socony Mobil Oil Co Inc | N-t-alkyl-beta-amino propionic acids |
| CH621999A5 (ko) * | 1976-06-24 | 1981-03-13 | Ciba Geigy Ag | |
| IT1137492B (it) * | 1981-05-26 | 1986-09-10 | Maria Curti | Composti ad attivita' gaba simile,procedimento per prepararli e composizioni farmaceutiche che li comprendono |
| EP0265818B1 (de) * | 1986-10-27 | 1994-09-28 | Chemische Fabrik Stockhausen GmbH | Verfahren zur Herstellung von N,N-disubstituierten Beta-Aminopropionsäuren und ihre Verwendung zur Hydrophobierung von Leder und Pelzen |
-
1988
- 1988-09-02 DE DE3829859A patent/DE3829859A1/de not_active Withdrawn
-
1989
- 1989-08-17 US US07/394,816 patent/US5068416A/en not_active Expired - Lifetime
- 1989-08-21 CA CA000608864A patent/CA1316937C/en not_active Expired - Fee Related
- 1989-08-29 EP EP89115869A patent/EP0356972B2/de not_active Expired - Lifetime
- 1989-08-29 ES ES89115869T patent/ES2046408T5/es not_active Expired - Lifetime
- 1989-08-29 AT AT89115869T patent/ATE98218T1/de not_active IP Right Cessation
- 1989-08-29 DE DE89115869T patent/DE58906358D1/de not_active Expired - Lifetime
- 1989-09-01 AU AU40954/89A patent/AU611586B2/en not_active Ceased
- 1989-09-01 JP JP1224760A patent/JPH02101054A/ja active Pending
- 1989-09-02 KR KR1019890012714A patent/KR900004677A/ko not_active Ceased
-
1991
- 1991-03-25 US US07/674,149 patent/US5130476A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| JPH02101054A (ja) | 1990-04-12 |
| DE58906358D1 (de) | 1994-01-20 |
| CA1316937C (en) | 1993-04-27 |
| DE3829859A1 (de) | 1990-03-22 |
| AU4095489A (en) | 1990-03-08 |
| US5068416A (en) | 1991-11-26 |
| ATE98218T1 (de) | 1993-12-15 |
| EP0356972A2 (de) | 1990-03-07 |
| US5130476A (en) | 1992-07-14 |
| EP0356972B1 (de) | 1993-12-08 |
| AU611586B2 (en) | 1991-06-13 |
| EP0356972A3 (de) | 1991-10-09 |
| EP0356972B2 (de) | 1997-04-02 |
| ES2046408T5 (es) | 1997-05-16 |
| ES2046408T3 (es) | 1994-02-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PA0109 | Patent application |
Patent event code: PA01091R01D Comment text: Patent Application Patent event date: 19890902 |
|
| PG1501 | Laying open of application | ||
| A201 | Request for examination | ||
| PA0201 | Request for examination |
Patent event code: PA02012R01D Patent event date: 19940719 Comment text: Request for Examination of Application Patent event code: PA02011R01I Patent event date: 19890902 Comment text: Patent Application |
|
| E902 | Notification of reason for refusal | ||
| PE0902 | Notice of grounds for rejection |
Comment text: Notification of reason for refusal Patent event date: 19971126 Patent event code: PE09021S01D |
|
| E601 | Decision to refuse application | ||
| PE0601 | Decision on rejection of patent |
Patent event date: 19980317 Comment text: Decision to Refuse Application Patent event code: PE06012S01D Patent event date: 19971126 Comment text: Notification of reason for refusal Patent event code: PE06011S01I |