KR860004001A - 할로겐화 3,3-디메틸-5-헥센-2-온의 제조방법 - Google Patents
할로겐화 3,3-디메틸-5-헥센-2-온의 제조방법 Download PDFInfo
- Publication number
- KR860004001A KR860004001A KR1019850008421A KR850008421A KR860004001A KR 860004001 A KR860004001 A KR 860004001A KR 1019850008421 A KR1019850008421 A KR 1019850008421A KR 850008421 A KR850008421 A KR 850008421A KR 860004001 A KR860004001 A KR 860004001A
- Authority
- KR
- South Korea
- Prior art keywords
- bromine
- chlorine
- process according
- fluorine
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/20—Unsaturated compounds containing keto groups bound to acyclic carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/20—Unsaturated compounds containing keto groups bound to acyclic carbon atoms
- C07C49/227—Unsaturated compounds containing keto groups bound to acyclic carbon atoms containing halogen
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
- C07C45/67—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
- C07C45/68—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Description
Claims (8)
- 하기 일반식(II)의 아세트산 에스테르를, 수성 할로겐수소산의 존재하에 필요시 추가의 불활성희석제의 존재하에 하기 일반식(III)의 2-메틸부탄-3-온과 반응시킴을 특징으로 하여 하기 일반식(I)의 할로겐화 3,3,-디메틸-5-헥센-2-온을 제조하는 방법.상기식에서, X는 할로겐을 나타내고, Y는 할로겐 또는 트리할로게노알킬을 나타내며, Hal은 염소 또는 브롬을 나타낸다.
- 제1항에 있어서, X가 불소, 염소 또는 브롬이고, Y가 불소, 염소, 브롬 또는 할로게노-C1-C4-알킬이며, Hal이 염소 또는 브롬인 일반식(I)화합물의 제조방법.
- 제1항에 있어서, X가 불소, 염소 또는 브롬이고, Y가 불소, 염소, 브롬 또는 트리플루오로 메틸이며, Hal이 염소 또는 브롬인 일반식(I) 화합물의 제조방법
- 제1항 내지 3항중 어느한 항에 있어서, 추가의 불활성 용매의 부재하에 반응을 수행하는 방법.
- 제1항 내지 4항중 어느한 항에 있어서, 과량의 염산 또는 브롬화수소산의 존재하에 반응을 수행하는 방법.
- 제1항 내지 5항중 어느한 항에 있어서, 0 내지 100℃에서 반응을 수행하는 방법.
- 제1항 내지 6항중 어느한 항에 있어서, 30 내지 80℃에서 반응을 수행하는 방법.
- 제1항 내지 7항중 어느한 항에 있어서, 출발물질(II) 및 (III)을 등몰량으로 사용하는 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEP3441370.7 | 1984-11-13 | ||
| DE19843441370 DE3441370A1 (de) | 1984-11-13 | 1984-11-13 | Verfahren zur herstellung von halogenierten 3,3-dimethyl-5-hexen-2-onen |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR860004001A true KR860004001A (ko) | 1986-06-16 |
| KR920003102B1 KR920003102B1 (ko) | 1992-04-18 |
Family
ID=6250130
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019850008421A Expired KR920003102B1 (ko) | 1984-11-13 | 1985-11-12 | 할로겐화 3,3-디메틸-5-헥센-2-온의 제조방법 |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US4602117A (ko) |
| EP (1) | EP0187216B1 (ko) |
| JP (1) | JPS61122240A (ko) |
| KR (1) | KR920003102B1 (ko) |
| AT (1) | ATE33821T1 (ko) |
| CA (1) | CA1241344A (ko) |
| DE (2) | DE3441370A1 (ko) |
| DK (1) | DK170330B1 (ko) |
| HU (1) | HU202179B (ko) |
| IL (1) | IL77002A (ko) |
| ZA (1) | ZA858665B (ko) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3802273A1 (de) * | 1988-01-27 | 1989-08-03 | Basf Ag | 3,3-dimethyl-hex-5-en-2-onderivate, verfahren zu ihrer herstellung und ihre verwendung |
| US6225506B1 (en) * | 1999-12-13 | 2001-05-01 | Boulder Scientific Company | Synthesis of alkene-2-ones |
| US7793068B2 (en) * | 2005-12-21 | 2010-09-07 | Sandisk Corporation | Dual mode access for non-volatile storage devices |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2482066A (en) * | 1946-10-19 | 1949-09-13 | Eastman Kodak Co | Acetylation of compounds containing a-co-(ch2)x-co-group |
| US3337634A (en) * | 1963-05-07 | 1967-08-22 | Eastman Kodak Co | Allenic ketones and process for their preparation |
| DE1768099A1 (de) * | 1968-03-30 | 1971-02-11 | Basf Ag | Verfahren zur Herstellung von Alk-1-en-5-onen und Alk-1-en-5-alen |
| US3655768A (en) * | 1968-11-13 | 1972-04-11 | Basf Ag | Production of alk-1-en-6-ones |
| EP0095047B1 (de) * | 1982-05-05 | 1985-11-27 | Bayer Ag | Verfahren zur Herstellung von 3-vinylsubstituierten 2,2-Dimethylcyclopropan-1-carbonsäuren bzw. ihren Estern und neue Zwischenprodukte dafür |
-
1984
- 1984-11-13 DE DE19843441370 patent/DE3441370A1/de not_active Withdrawn
-
1985
- 1985-11-02 DE DE8585113942T patent/DE3562366D1/de not_active Expired
- 1985-11-02 AT AT85113942T patent/ATE33821T1/de not_active IP Right Cessation
- 1985-11-02 EP EP85113942A patent/EP0187216B1/de not_active Expired
- 1985-11-06 US US06/795,683 patent/US4602117A/en not_active Expired - Lifetime
- 1985-11-08 CA CA000494956A patent/CA1241344A/en not_active Expired
- 1985-11-11 JP JP60250995A patent/JPS61122240A/ja active Granted
- 1985-11-11 IL IL77002A patent/IL77002A/xx not_active IP Right Cessation
- 1985-11-12 KR KR1019850008421A patent/KR920003102B1/ko not_active Expired
- 1985-11-12 ZA ZA858665A patent/ZA858665B/xx unknown
- 1985-11-12 HU HU854318A patent/HU202179B/hu not_active IP Right Cessation
- 1985-11-12 DK DK521785A patent/DK170330B1/da not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| EP0187216A3 (en) | 1987-05-13 |
| KR920003102B1 (ko) | 1992-04-18 |
| CA1241344A (en) | 1988-08-30 |
| DE3441370A1 (de) | 1986-05-22 |
| HUT38891A (en) | 1986-07-28 |
| ATE33821T1 (de) | 1988-05-15 |
| EP0187216A2 (de) | 1986-07-16 |
| DK170330B1 (da) | 1995-08-07 |
| EP0187216B1 (de) | 1988-04-27 |
| JPS61122240A (ja) | 1986-06-10 |
| IL77002A0 (en) | 1986-04-29 |
| US4602117A (en) | 1986-07-22 |
| HU202179B (en) | 1991-02-28 |
| DK521785A (da) | 1986-05-14 |
| DK521785D0 (da) | 1985-11-12 |
| IL77002A (en) | 1989-03-31 |
| DE3562366D1 (en) | 1988-06-01 |
| ZA858665B (en) | 1986-07-30 |
| JPH0572895B2 (ko) | 1993-10-13 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| KR880011151A (ko) | 티아제핀 화합물의 제조방법 | |
| KR880003927A (ko) | 2-클로로-5-클로로 메틸티아졸의 제조방법 | |
| KR860004052A (ko) | 살진균성 아졸 화합물의 제조방법 | |
| KR840004756A (ko) | 항 정신질환제의 제조방법 | |
| KR840000541A (ko) | N-디히드로티아졸릴-3-퀴놀린 카복사미드 유도체의 제조방법 | |
| KR840003610A (ko) | 요소 유도체의 제조방법 | |
| KR860004001A (ko) | 할로겐화 3,3-디메틸-5-헥센-2-온의 제조방법 | |
| KR860002446A (ko) | 2,4-디클로로-5-플루오로-벤조산의 제조방법 | |
| KR840005139A (ko) | 피라졸로피리딘 유도체의 제조방법 | |
| KR900701746A (ko) | 2-할로-4-알킬술포닐벤조산의 제조방법 | |
| KR890014459A (ko) | 4-할로-3-옥소-2-알콕시이미노부티르산 에스테르의 제조방법 | |
| KR840003627A (ko) | 4-피페라지닐-4-페닐 퀴나졸린 유도체의 제조방법 | |
| KR900009616A (ko) | 5-아미노-1,2,4-트리아졸-3-설폰아미드의 제조방법 | |
| KR850003392A (ko) | 광학적으로 균일한 아제티디논의 제조방법 | |
| KR860002474A (ko) | 치환된 페닐술포닐아졸의 제조방법 | |
| KR890014434A (ko) | 할로겐-함유 방향족 화합물의 제조방법 | |
| KR910011845A (ko) | 2-푸릴피리미딘 유도체의 제조방법 | |
| KR860000295A (ko) | 옥시캄 유도체의 제조방법 | |
| KR860002454A (ko) | 살리실아미드 유도체의 제조방법 | |
| KR860002473A (ko) | 4-메틸-5-티오포름아미디노메틸이미다졸 디하이드로클로라이드의 제조방법 | |
| KR880012505A (ko) | 신규 염소화 방법 | |
| KR880000418A (ko) | 4-치환-2-머캅토-벤조 티아졸 유도체의 제조방법 | |
| KR880001636A (ko) | 벤즈이미다졸 유도체의 제조 방법 | |
| KR850001158A (ko) | 할로게노 알킬 카밤산 에스테르의 제조방법 | |
| KR880005097A (ko) | O-아릴-n'-피리미딘-2-일 이소우레아의 제조방법 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PA0109 | Patent application |
St.27 status event code: A-0-1-A10-A12-nap-PA0109 |
|
| R17-X000 | Change to representative recorded |
St.27 status event code: A-3-3-R10-R17-oth-X000 |
|
| PG1501 | Laying open of application |
St.27 status event code: A-1-1-Q10-Q12-nap-PG1501 |
|
| A201 | Request for examination | ||
| PA0201 | Request for examination |
St.27 status event code: A-1-2-D10-D11-exm-PA0201 |
|
| P11-X000 | Amendment of application requested |
St.27 status event code: A-2-2-P10-P11-nap-X000 |
|
| P13-X000 | Application amended |
St.27 status event code: A-2-2-P10-P13-nap-X000 |
|
| PA0201 | Request for examination |
St.27 status event code: A-1-2-D10-D11-exm-PA0201 |
|
| E902 | Notification of reason for refusal | ||
| PE0902 | Notice of grounds for rejection |
St.27 status event code: A-1-2-D10-D21-exm-PE0902 |
|
| P11-X000 | Amendment of application requested |
St.27 status event code: A-2-2-P10-P11-nap-X000 |
|
| P13-X000 | Application amended |
St.27 status event code: A-2-2-P10-P13-nap-X000 |
|
| G160 | Decision to publish patent application | ||
| PG1605 | Publication of application before grant of patent |
St.27 status event code: A-2-2-Q10-Q13-nap-PG1605 |
|
| E701 | Decision to grant or registration of patent right | ||
| PE0701 | Decision of registration |
St.27 status event code: A-1-2-D10-D22-exm-PE0701 |
|
| GRNT | Written decision to grant | ||
| PR0701 | Registration of establishment |
St.27 status event code: A-2-4-F10-F11-exm-PR0701 |
|
| PR1002 | Payment of registration fee |
St.27 status event code: A-2-2-U10-U11-oth-PR1002 Fee payment year number: 1 |
|
| PR1001 | Payment of annual fee |
St.27 status event code: A-4-4-U10-U11-oth-PR1001 Fee payment year number: 4 |
|
| PR1001 | Payment of annual fee |
St.27 status event code: A-4-4-U10-U11-oth-PR1001 Fee payment year number: 5 |
|
| PR1001 | Payment of annual fee |
St.27 status event code: A-4-4-U10-U11-oth-PR1001 Fee payment year number: 6 |
|
| PR1001 | Payment of annual fee |
St.27 status event code: A-4-4-U10-U11-oth-PR1001 Fee payment year number: 7 |
|
| R18-X000 | Changes to party contact information recorded |
St.27 status event code: A-5-5-R10-R18-oth-X000 |
|
| R18-X000 | Changes to party contact information recorded |
St.27 status event code: A-5-5-R10-R18-oth-X000 |
|
| R18-X000 | Changes to party contact information recorded |
St.27 status event code: A-5-5-R10-R18-oth-X000 |
|
| PN2301 | Change of applicant |
St.27 status event code: A-5-5-R10-R13-asn-PN2301 St.27 status event code: A-5-5-R10-R11-asn-PN2301 |
|
| PR1001 | Payment of annual fee |
St.27 status event code: A-4-4-U10-U11-oth-PR1001 Fee payment year number: 8 |
|
| FPAY | Annual fee payment |
Payment date: 20000330 Year of fee payment: 9 |
|
| PR1001 | Payment of annual fee |
St.27 status event code: A-4-4-U10-U11-oth-PR1001 Fee payment year number: 9 |
|
| R18-X000 | Changes to party contact information recorded |
St.27 status event code: A-5-5-R10-R18-oth-X000 |
|
| R18-X000 | Changes to party contact information recorded |
St.27 status event code: A-5-5-R10-R18-oth-X000 |
|
| LAPS | Lapse due to unpaid annual fee | ||
| PC1903 | Unpaid annual fee |
St.27 status event code: A-4-4-U10-U13-oth-PC1903 Not in force date: 20010419 Payment event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE |
|
| PC1903 | Unpaid annual fee |
St.27 status event code: N-4-6-H10-H13-oth-PC1903 Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE Not in force date: 20010419 |
|
| R18-X000 | Changes to party contact information recorded |
St.27 status event code: A-5-5-R10-R18-oth-X000 |
|
| R18-X000 | Changes to party contact information recorded |
St.27 status event code: A-5-5-R10-R18-oth-X000 |
|
| R18-X000 | Changes to party contact information recorded |
St.27 status event code: A-5-5-R10-R18-oth-X000 |
|
| P22-X000 | Classification modified |
St.27 status event code: A-4-4-P10-P22-nap-X000 |