KR830005165A - 알킬 설폰의 제조방법 - Google Patents
알킬 설폰의 제조방법 Download PDFInfo
- Publication number
- KR830005165A KR830005165A KR1019810000751A KR810000751A KR830005165A KR 830005165 A KR830005165 A KR 830005165A KR 1019810000751 A KR1019810000751 A KR 1019810000751A KR 810000751 A KR810000751 A KR 810000751A KR 830005165 A KR830005165 A KR 830005165A
- Authority
- KR
- South Korea
- Prior art keywords
- och
- nitrogen
- methyl
- carbons
- formula
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- 238000000034 method Methods 0.000 title claims 3
- -1 alkyl sulfone Chemical class 0.000 title 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims 12
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 8
- 229910052757 nitrogen Inorganic materials 0.000 claims 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical group [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims 4
- 150000001875 compounds Chemical class 0.000 claims 4
- 239000001301 oxygen Substances 0.000 claims 4
- 229910052760 oxygen Inorganic materials 0.000 claims 4
- 125000003342 alkenyl group Chemical group 0.000 claims 3
- 125000000217 alkyl group Chemical group 0.000 claims 3
- 125000001511 cyclopentyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C1([H])[H] 0.000 claims 3
- 125000004186 cyclopropylmethyl group Chemical group [H]C([H])(*)C1([H])C([H])([H])C1([H])[H] 0.000 claims 3
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims 3
- ICSNLGPSRYBMBD-UHFFFAOYSA-N 2-aminopyridine Chemical compound NC1=CC=CC=N1 ICSNLGPSRYBMBD-UHFFFAOYSA-N 0.000 claims 2
- MGWGWNFMUOTEHG-UHFFFAOYSA-N 4-(3,5-dimethylphenyl)-1,3-thiazol-2-amine Chemical compound CC1=CC(C)=CC(C=2N=C(N)SC=2)=C1 MGWGWNFMUOTEHG-UHFFFAOYSA-N 0.000 claims 2
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims 2
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 claims 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical group [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims 2
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 claims 2
- 229910052794 bromium Inorganic materials 0.000 claims 2
- 239000000460 chlorine Substances 0.000 claims 2
- 229910052801 chlorine Inorganic materials 0.000 claims 2
- 239000011737 fluorine Substances 0.000 claims 2
- 229910052731 fluorine Inorganic materials 0.000 claims 2
- 239000001257 hydrogen Substances 0.000 claims 2
- 229910052739 hydrogen Inorganic materials 0.000 claims 2
- 150000002431 hydrogen Chemical class 0.000 claims 2
- JCXJVPUVTGWSNB-UHFFFAOYSA-N nitrogen dioxide Inorganic materials O=[N]=O JCXJVPUVTGWSNB-UHFFFAOYSA-N 0.000 claims 2
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims 2
- 229910052717 sulfur Chemical group 0.000 claims 2
- 239000011593 sulfur Chemical group 0.000 claims 2
- KCZIUKYAJJEIQG-UHFFFAOYSA-N 1,3,5-triazin-2-amine Chemical compound NC1=NC=NC=N1 KCZIUKYAJJEIQG-UHFFFAOYSA-N 0.000 claims 1
- NHQDETIJWKXCTC-UHFFFAOYSA-N 3-chloroperbenzoic acid Chemical compound OOC(=O)C1=CC=CC(Cl)=C1 NHQDETIJWKXCTC-UHFFFAOYSA-N 0.000 claims 1
- 239000003054 catalyst Substances 0.000 claims 1
- 150000002540 isothiocyanates Chemical class 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 229910017464 nitrogen compound Inorganic materials 0.000 claims 1
- 150000002830 nitrogen compounds Chemical class 0.000 claims 1
- 230000001590 oxidative effect Effects 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
- BUXTXUBQAKIQKS-UHFFFAOYSA-N sulfuryl diisocyanate Chemical compound O=C=NS(=O)(=O)N=C=O BUXTXUBQAKIQKS-UHFFFAOYSA-N 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D239/00—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings
- C07D239/02—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings
- C07D239/24—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members
- C07D239/28—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, directly attached to ring carbon atoms
- C07D239/32—One oxygen, sulfur or nitrogen atom
- C07D239/42—One nitrogen atom
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D401/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
- C07D401/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
- C07D401/12—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings linked by a chain containing hetero atoms as chain links
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Plural Heterocyclic Compounds (AREA)
- Pyridine Compounds (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (3)
- 일반식(Ⅲ)의 2-아미노피리딘 또는 2-아미노-1,3,5-트리아진을 적당히 치환된 일반식(Ⅱ)의 설포닐 이소시아네이트 또는 이소티오시아네이트와 반응시켜 일반식(Ⅰ)의 화합물 및 그의 염을 제조하는 방법.상기 구조식에서R1은 R3SO2또는 R3S이고R3는 탄소수 1내지 4의 알킬, 탄소수 3내지 4의 알케닐, 사이클로펜틸 또는 사이클로프로필메틸이고R2는 수소, 불소, 염소, 브롬, 메틸, OCH3, CF3, 이산화질소, CN이고n은 0.1 또는 2의 정수이고W가 산소 또는 유황이고T가 CH 또는 질소이고Z가 CH 또는 질소이고X는 메틸, 에틸, OCH3, OC2H5또는 CH2OCH3이고Y는 메틸 또는 OCH3이다.
- R1이 SR3이고 W가 산소인 일반식(Ia)의 화합물을 m-클로로과벤조산으로 산화시켜 R1이 SOR3이고 W가 산소인 일반식(Ib)의 화합물을 제조하는 방법.상기 구조식에서R3는 탄소수 1내지 4의 알킬, 탄소수 3내지 4의 알케닐, 사이클로펜틸 또는 사이클로프로필메틸이고R2는 수소, 불소, 염소, 브롬, 메틸, OCH3, CF3, 이산화질소, CN 또는 아미노이고T가 CH 또는 질소이고Z가 CH 또는 질소이고X는 메틸, 에틸, OCH3, OC2H5또는 CH2OCH3이고Y는 메틸, 또는 OCH3이다.
- 상용하는 질소화합물을 촉매로 환원시켜 R2가 아미노인 일반식(Ⅰ)화합물을 제조하는 방법.상기 구조식에서R1은 R3S[O]n이고R3는 탄소수 1내지 4의 알킬, 탄소수 3내지 4의 알케닐, 사이클로펜틸 또는 사이클로프로필메틸이고n은 0,1 또는 2의 정수이고W는 산소 또는 유황이고T는 CH 또는 질소이고Z가 CH 또는 질소이고X는 메틸, 에틸, OCH3, OC2H5또는 CH2OCH3이고Y는 메틸 또는 OCH3이다.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US12817680A | 1980-03-07 | 1980-03-07 | |
| US128176 | 1993-09-29 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| KR830005165A true KR830005165A (ko) | 1983-08-03 |
Family
ID=22434023
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019810000751A Ceased KR830005165A (ko) | 1980-03-07 | 1981-03-07 | 알킬 설폰의 제조방법 |
Country Status (5)
| Country | Link |
|---|---|
| JP (1) | JPS56139466A (ko) |
| KR (1) | KR830005165A (ko) |
| CA (1) | CA1189073A (ko) |
| PH (1) | PH17301A (ko) |
| ZA (1) | ZA811484B (ko) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4618363A (en) * | 1982-01-25 | 1986-10-21 | Ciba-Geigy Corporation | N-phenylsulfonyl-N'-triazinylureas |
| ZA836639B (en) * | 1982-09-08 | 1984-05-30 | Ciba Geigy Ag | Novel sulfonylureas |
| JPS6036386A (ja) * | 1983-08-05 | 1985-02-25 | 東芝セラミツクス株式会社 | スラデイングノズル用充填材 |
| JP2546200B2 (ja) * | 1991-02-20 | 1996-10-23 | 東ソー株式会社 | 田植前湛水下水田除草用水性懸濁製剤および散布方法 |
| JP5468289B2 (ja) * | 2008-04-18 | 2014-04-09 | 石原産業株式会社 | ピリミジン系化合物の製造方法 |
-
1981
- 1981-03-05 PH PH25317A patent/PH17301A/en unknown
- 1981-03-05 ZA ZA00811484A patent/ZA811484B/xx unknown
- 1981-03-05 JP JP3063181A patent/JPS56139466A/ja active Pending
- 1981-03-05 CA CA000372421A patent/CA1189073A/en not_active Expired
- 1981-03-07 KR KR1019810000751A patent/KR830005165A/ko not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| JPS56139466A (en) | 1981-10-30 |
| CA1189073A (en) | 1985-06-18 |
| PH17301A (en) | 1984-07-18 |
| ZA811484B (en) | 1982-10-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PA0109 | Patent application |
Patent event code: PA01091R01D Comment text: Patent Application Patent event date: 19810307 |
|
| PG1501 | Laying open of application | ||
| PE0902 | Notice of grounds for rejection |
Comment text: Notification of reason for refusal Patent event date: 19840319 Patent event code: PE09021S01D |
|
| PE0601 | Decision on rejection of patent |
Patent event date: 19840831 Comment text: Decision to Refuse Application Patent event code: PE06012S01D Patent event date: 19840319 Comment text: Notification of reason for refusal Patent event code: PE06011S01I |