JPS561350A - Grafted chromatographic stationary phase or filler and its preparation - Google Patents
Grafted chromatographic stationary phase or filler and its preparationInfo
- Publication number
- JPS561350A JPS561350A JP7694079A JP7694079A JPS561350A JP S561350 A JPS561350 A JP S561350A JP 7694079 A JP7694079 A JP 7694079A JP 7694079 A JP7694079 A JP 7694079A JP S561350 A JPS561350 A JP S561350A
- Authority
- JP
- Japan
- Prior art keywords
- grafted
- filler
- stationary phase
- chromatographic stationary
- preferable
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 230000005526 G1 to G0 transition Effects 0.000 title abstract 2
- 239000000945 filler Substances 0.000 title abstract 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 5
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- 239000005909 Kieselgur Substances 0.000 abstract 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 125000003368 amide group Chemical group 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 239000000969 carrier Substances 0.000 abstract 1
- 239000011521 glass Substances 0.000 abstract 1
- 239000010453 quartz Substances 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 239000000741 silica gel Substances 0.000 abstract 1
- 229910002027 silica gel Inorganic materials 0.000 abstract 1
- 229910052710 silicon Inorganic materials 0.000 abstract 1
- 239000010703 silicon Substances 0.000 abstract 1
- 239000000377 silicon dioxide Substances 0.000 abstract 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Peptides Or Proteins (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
PURPOSE: To permit a chromatographic stationary phase or filler to be chemically stable and have various separation cabilities by allowing it to contain silicon graft having an optically active amide group.
CONSTITUTION: The N-acylamino acid residue containing asymmetric carbon is grafted into an inorganic carrier having the hydroxyl group on its surface. As the inorganic carrier having the hydroxyl group on its surface, such silica-containing carriers as silica gel, diatomaceous earth, glass, and quartz are preferable. The shape of the carrier can be either of spherical, crushed-shape, fibriform, bar-shaped, or hollow tube-shaped. However, for obtaining a highly efficient chromatogram, corpuscles having equal diameters or hollow tubes having a constant inside diameter are preferable.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7694079A JPS561350A (en) | 1979-06-20 | 1979-06-20 | Grafted chromatographic stationary phase or filler and its preparation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7694079A JPS561350A (en) | 1979-06-20 | 1979-06-20 | Grafted chromatographic stationary phase or filler and its preparation |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS561350A true JPS561350A (en) | 1981-01-09 |
| JPS6336466B2 JPS6336466B2 (en) | 1988-07-20 |
Family
ID=13619732
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP7694079A Granted JPS561350A (en) | 1979-06-20 | 1979-06-20 | Grafted chromatographic stationary phase or filler and its preparation |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS561350A (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1985000661A1 (en) * | 1983-07-20 | 1985-02-14 | Daicel Chemical Industries, Ltd. | Packing for use in separation |
| JPH01100451A (en) * | 1987-10-13 | 1989-04-18 | Shoji Hara | Separating agent |
| US6333426B1 (en) | 1992-12-03 | 2001-12-25 | Eka Nobel Ab | Chiral adsorbents and preparation thereof as well as compounds on which the absorbents are based and preparation of the compounds |
| WO2006069061A1 (en) * | 2004-12-21 | 2006-06-29 | Degussa Gmbh | Perfume delivery system |
| WO2006079089A1 (en) * | 2005-01-24 | 2006-07-27 | Degussa Gmbh | Perfume delivery system |
| CN103301822A (en) * | 2012-10-25 | 2013-09-18 | 中国人民解放军第四军医大学 | Polar liquid chromatogram filler and preparation method thereof |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6342378U (en) * | 1986-09-05 | 1988-03-19 | ||
| JPH0671092U (en) * | 1992-12-02 | 1994-10-04 | 顕造 宇梶 | Marumochi continuous cutting machine |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5381295A (en) * | 1976-12-27 | 1978-07-18 | Sumitomo Chemical Co | Grafted filler for chromatography and its manufacture |
| JPS5476587A (en) * | 1977-11-30 | 1979-06-19 | Sumitomo Chem Co Ltd | Optically active s-triazine derivative and method of separation and analysis of mirror-image isomer mixture having amino group using the same by gas-chromatography |
-
1979
- 1979-06-20 JP JP7694079A patent/JPS561350A/en active Granted
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5381295A (en) * | 1976-12-27 | 1978-07-18 | Sumitomo Chemical Co | Grafted filler for chromatography and its manufacture |
| JPS5476587A (en) * | 1977-11-30 | 1979-06-19 | Sumitomo Chem Co Ltd | Optically active s-triazine derivative and method of separation and analysis of mirror-image isomer mixture having amino group using the same by gas-chromatography |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1985000661A1 (en) * | 1983-07-20 | 1985-02-14 | Daicel Chemical Industries, Ltd. | Packing for use in separation |
| JPH01100451A (en) * | 1987-10-13 | 1989-04-18 | Shoji Hara | Separating agent |
| US6333426B1 (en) | 1992-12-03 | 2001-12-25 | Eka Nobel Ab | Chiral adsorbents and preparation thereof as well as compounds on which the absorbents are based and preparation of the compounds |
| WO2006069061A1 (en) * | 2004-12-21 | 2006-06-29 | Degussa Gmbh | Perfume delivery system |
| WO2006079089A1 (en) * | 2005-01-24 | 2006-07-27 | Degussa Gmbh | Perfume delivery system |
| CN103301822A (en) * | 2012-10-25 | 2013-09-18 | 中国人民解放军第四军医大学 | Polar liquid chromatogram filler and preparation method thereof |
| CN103301822B (en) * | 2012-10-25 | 2016-08-03 | 中国人民解放军第四军医大学 | A kind of polar liquid chromatogram filler and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6336466B2 (en) | 1988-07-20 |
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