JPH11128331A - Liquid aromatic composition - Google Patents
Liquid aromatic compositionInfo
- Publication number
- JPH11128331A JPH11128331A JP9297100A JP29710097A JPH11128331A JP H11128331 A JPH11128331 A JP H11128331A JP 9297100 A JP9297100 A JP 9297100A JP 29710097 A JP29710097 A JP 29710097A JP H11128331 A JPH11128331 A JP H11128331A
- Authority
- JP
- Japan
- Prior art keywords
- volatile silicone
- liquid
- fragrance
- aroma
- liquid fragrance
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000007788 liquid Substances 0.000 title claims abstract description 36
- 239000000203 mixture Substances 0.000 title claims description 23
- 125000003118 aryl group Chemical group 0.000 title abstract description 3
- 239000003205 fragrance Substances 0.000 claims abstract description 46
- 229920001296 polysiloxane Polymers 0.000 claims abstract description 18
- 239000004205 dimethyl polysiloxane Substances 0.000 claims abstract description 13
- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims abstract description 13
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims abstract description 13
- 150000001875 compounds Chemical class 0.000 claims description 13
- 239000002781 deodorant agent Substances 0.000 claims description 11
- 238000004332 deodorization Methods 0.000 abstract description 9
- 229920002545 silicone oil Polymers 0.000 abstract description 7
- 238000011156 evaluation Methods 0.000 abstract description 6
- 238000009792 diffusion process Methods 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 3
- 210000001072 colon Anatomy 0.000 abstract description 2
- 235000019568 aromas Nutrition 0.000 abstract 2
- 239000003795 chemical substances by application Substances 0.000 abstract 2
- 238000005259 measurement Methods 0.000 abstract 1
- 229930195733 hydrocarbon Natural products 0.000 description 10
- 150000002430 hydrocarbons Chemical class 0.000 description 8
- 239000007789 gas Substances 0.000 description 6
- 239000004215 Carbon black (E152) Substances 0.000 description 5
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 4
- LSDPWZHWYPCBBB-UHFFFAOYSA-N Methanethiol Chemical compound SC LSDPWZHWYPCBBB-UHFFFAOYSA-N 0.000 description 4
- 125000004122 cyclic group Chemical group 0.000 description 4
- 230000001877 deodorizing effect Effects 0.000 description 4
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 4
- 230000001953 sensory effect Effects 0.000 description 4
- MFKRHJVUCZRDTF-UHFFFAOYSA-N 3-methoxy-3-methylbutan-1-ol Chemical compound COC(C)(C)CCO MFKRHJVUCZRDTF-UHFFFAOYSA-N 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- -1 terpene hydrocarbons Chemical class 0.000 description 3
- GRWFGVWFFZKLTI-IUCAKERBSA-N (-)-α-pinene Chemical compound CC1=CC[C@@H]2C(C)(C)[C@H]1C2 GRWFGVWFFZKLTI-IUCAKERBSA-N 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- MOYAFQVGZZPNRA-UHFFFAOYSA-N Terpinolene Chemical compound CC(C)=C1CCC(C)=CC1 MOYAFQVGZZPNRA-UHFFFAOYSA-N 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- DIOQZVSQGTUSAI-UHFFFAOYSA-N decane Chemical compound CCCCCCCCCC DIOQZVSQGTUSAI-UHFFFAOYSA-N 0.000 description 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 2
- BKIMMITUMNQMOS-UHFFFAOYSA-N nonane Chemical compound CCCCCCCCC BKIMMITUMNQMOS-UHFFFAOYSA-N 0.000 description 2
- CFJYNSNXFXLKNS-UHFFFAOYSA-N p-menthane Chemical compound CC(C)C1CCC(C)CC1 CFJYNSNXFXLKNS-UHFFFAOYSA-N 0.000 description 2
- XOKSLPVRUOBDEW-UHFFFAOYSA-N pinane Chemical compound CC1CCC2C(C)(C)C1C2 XOKSLPVRUOBDEW-UHFFFAOYSA-N 0.000 description 2
- 235000007586 terpenes Nutrition 0.000 description 2
- IFNXAMCERSVZCV-UHFFFAOYSA-L zinc;2-ethylhexanoate Chemical compound [Zn+2].CCCCC(CC)C([O-])=O.CCCCC(CC)C([O-])=O IFNXAMCERSVZCV-UHFFFAOYSA-L 0.000 description 2
- YKFLAYDHMOASIY-UHFFFAOYSA-N γ-terpinene Chemical compound CC(C)C1=CCC(C)=CC1 YKFLAYDHMOASIY-UHFFFAOYSA-N 0.000 description 2
- WTARULDDTDQWMU-RKDXNWHRSA-N (+)-β-pinene Chemical compound C1[C@H]2C(C)(C)[C@@H]1CCC2=C WTARULDDTDQWMU-RKDXNWHRSA-N 0.000 description 1
- WTARULDDTDQWMU-IUCAKERBSA-N (-)-Nopinene Natural products C1[C@@H]2C(C)(C)[C@H]1CCC2=C WTARULDDTDQWMU-IUCAKERBSA-N 0.000 description 1
- XMGQYMWWDOXHJM-SNVBAGLBSA-N (-)-α-limonene Chemical compound CC(=C)[C@H]1CCC(C)=CC1 XMGQYMWWDOXHJM-SNVBAGLBSA-N 0.000 description 1
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
- CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 description 1
- WTARULDDTDQWMU-UHFFFAOYSA-N Pseudopinene Natural products C1C2C(C)(C)C1CCC2=C WTARULDDTDQWMU-UHFFFAOYSA-N 0.000 description 1
- LCTONWCANYUPML-UHFFFAOYSA-M Pyruvate Chemical compound CC(=O)C([O-])=O LCTONWCANYUPML-UHFFFAOYSA-M 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 239000006096 absorbing agent Substances 0.000 description 1
- 125000002015 acyclic group Chemical group 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- XCPQUQHBVVXMRQ-UHFFFAOYSA-N alpha-Fenchene Natural products C1CC2C(=C)CC1C2(C)C XCPQUQHBVVXMRQ-UHFFFAOYSA-N 0.000 description 1
- MVNCAPSFBDBCGF-UHFFFAOYSA-N alpha-pinene Natural products CC1=CCC23C1CC2C3(C)C MVNCAPSFBDBCGF-UHFFFAOYSA-N 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 229930006722 beta-pinene Natural products 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- XXJWXESWEXIICW-UHFFFAOYSA-N diethylene glycol monoethyl ether Chemical compound CCOCCOCCO XXJWXESWEXIICW-UHFFFAOYSA-N 0.000 description 1
- 229940075557 diethylene glycol monoethyl ether Drugs 0.000 description 1
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 description 1
- SNRUBQQJIBEYMU-UHFFFAOYSA-N dodecane Chemical compound CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- LCWMKIHBLJLORW-UHFFFAOYSA-N gamma-carene Natural products C1CC(=C)CC2C(C)(C)C21 LCWMKIHBLJLORW-UHFFFAOYSA-N 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 229940094933 n-dodecane Drugs 0.000 description 1
- 230000009965 odorless effect Effects 0.000 description 1
- 229930004008 p-menthane Natural products 0.000 description 1
- 229930006728 pinane Natural products 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- GRWFGVWFFZKLTI-UHFFFAOYSA-N rac-alpha-Pinene Natural products CC1=CCC2C(C)(C)C1C2 GRWFGVWFFZKLTI-UHFFFAOYSA-N 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 239000012488 sample solution Substances 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- RSJKGSCJYJTIGS-UHFFFAOYSA-N undecane Chemical compound CCCCCCCCCCC RSJKGSCJYJTIGS-UHFFFAOYSA-N 0.000 description 1
- GAWWVVGZMLGEIW-GNNYBVKZSA-L zinc ricinoleate Chemical compound [Zn+2].CCCCCC[C@@H](O)C\C=C/CCCCCCCC([O-])=O.CCCCCC[C@@H](O)C\C=C/CCCCCCCC([O-])=O GAWWVVGZMLGEIW-GNNYBVKZSA-L 0.000 description 1
- 229940100530 zinc ricinoleate Drugs 0.000 description 1
Landscapes
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
- Fats And Perfumes (AREA)
Abstract
Description
【０００１】[0001]
【発明の属する技術分野】本発明は、香りの拡散性の良
い液体芳香剤組成物に関する。BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a liquid fragrance composition having good scent diffusibility.
【０００２】[0002]
【従来の技術】従来、液体芳香剤として、油性の香料
を、油性の基剤に溶解したものが使用されている。この
基剤としては、通常イソパラフィン系炭化水素が使用さ
れている（特公昭５７−５０５０４号公報参照）。しか
しながら、イソパラフィン系炭化水素の基剤は、香りの
拡散性が悪い、特有の基剤臭を有する等の欠点がある。2. Description of the Related Art Conventionally, a liquid fragrance in which an oily fragrance is dissolved in an oily base has been used. As this base, an isoparaffinic hydrocarbon is usually used (see Japanese Patent Publication No. 57-50504). However, the bases of isoparaffinic hydrocarbons have drawbacks such as poor diffusibility of fragrance and a peculiar base odor.
【０００３】[0003]
【発明が解決しようとする課題】本発明の目的は、香り
の拡散性の良い液体芳香剤を提供することにある。SUMMARY OF THE INVENTION An object of the present invention is to provide a liquid fragrance having a good scent diffusion property.
【０００４】[0004]
【課題を解決するための手段】本発明によれば、揮発性
シリコーン化合物及び香料を含む液体芳香剤組成物が提
供される。According to the present invention, there is provided a liquid fragrance composition comprising a volatile silicone compound and a fragrance.
【０００５】また、本発明によれば、揮発性シリコーン
化合物が式（１）で示される構造を有するジメチルポリ
シロキサン及び／又は式（２）で示される構造を有する
ジメチルポリシロキサンFurther, according to the present invention, the volatile silicone compound is a dimethylpolysiloxane having a structure represented by the formula (1) and / or a dimethylpolysiloxane having a structure represented by the formula (2)
【０００６】[0006]
【化２】 Embedded image
【０００７】（但し、式中ｍは１から６の整数、ｎは４
から６の整数）からなる前記液体芳香剤組成物が提供さ
れる。(Where m is an integer of 1 to 6 and n is 4
Wherein said liquid fragrance composition comprises:
【０００８】さらに、本発明によれば、消臭剤をさらに
含むことを特徴とする前記液体芳香剤組成物が提供され
る。Further, according to the present invention, there is provided the liquid fragrance composition, further comprising a deodorant.
【０００９】[0009]
【発明の実施の形態】本発明の液体芳香剤組成物は、基
剤として、揮発性シリコーン化合物を含む。DESCRIPTION OF THE PREFERRED EMBODIMENTS The liquid fragrance composition of the present invention contains a volatile silicone compound as a base.
【００１０】前記揮発性シリコーン化合物としては、前
記式（１）で示される構造を有するジメチルポリシロキ
サン（以下非環状ジメチルポリシロキサンと称す）及び
／又は式（２）に示される構造を有するジメチルポリシ
ロキサン（以下環状ジメチルポリシロキサンと称す）を
好ましく挙げることができる。As the volatile silicone compound, dimethylpolysiloxane having a structure represented by the formula (1) (hereinafter referred to as acyclic dimethylpolysiloxane) and / or dimethylpolysiloxane having a structure represented by the formula (2) Siloxane (hereinafter referred to as cyclic dimethylpolysiloxane) can be preferably exemplified.
【００１１】前記式（１）中、ｍの値は１〜６、好まし
くは１〜４である。また、前記式（２）中、ｎの値は４
〜６、好ましくは４〜５である。ｍ又はｎの値を６以下
とすることにより、本発明の効果を得るのに十分な揮発
性を得ることができる。In the above formula (1), the value of m is 1 to 6, preferably 1 to 4. In the above equation (2), the value of n is 4
-6, preferably 4-5. By setting the value of m or n to 6 or less, sufficient volatility for obtaining the effect of the present invention can be obtained.
【００１２】前記非環状ジメチルポリシロキサン又は前
記環状ジメチルポリシロキサンは、ｍ又はｎの値が前記
範囲内である各種のものの混合物であってもよく、また
ｍ又はｎの値が前記範囲内のうち一つの値のもののみを
実質的に含む単一成分のものであってもよい。単一成分
のものを単独で用いた場合は、揮散速度の一定した液体
芳香剤組成物を得ることができる。The non-cyclic dimethylpolysiloxane or the cyclic dimethylpolysiloxane may be a mixture of various kinds in which the value of m or n is within the above-mentioned range, and the value of m or n may be any of those in the above range. It may be a single component substantially containing only one value. When a single component is used alone, a liquid fragrance composition having a constant volatilization rate can be obtained.
【００１３】これらの揮発性シリコーン化合物は、通常
無色透明、無臭の液体である。These volatile silicone compounds are usually colorless, transparent and odorless liquids.
【００１４】本発明の液体芳香剤組成物中の前記揮発性
シリコーン化合物の含有割合は、４０重量％以上、好ま
しくは６０重量％以上であることが望ましい。揮発性シ
リコーン化合物の含有割合を４０重量％以上とすること
により、本発明の効果を得るのに十分な揮発性を得るこ
とができる。The content of the volatile silicone compound in the liquid fragrance composition of the present invention is preferably at least 40% by weight, more preferably at least 60% by weight. By setting the content of the volatile silicone compound to 40% by weight or more, sufficient volatility for obtaining the effects of the present invention can be obtained.
【００１５】本発明の液体芳香剤組成物は、香料を含
む。The liquid fragrance composition of the present invention contains a fragrance.
【００１６】前記香料としては、特に限定されないが、
前記揮発性シリコーン化合物中に０．０１重量％以上の
割合で溶解することができる各種の香料を挙げることが
できる。The fragrance is not particularly limited,
Various flavors that can be dissolved in the volatile silicone compound at a rate of 0.01% by weight or more can be given.
【００１７】本発明の液体芳香剤組成物中の前記香料の
含有割合は、０．０１〜４０重量％、好ましくは０．１
〜３０重量％であることが望ましい。The content of the fragrance in the liquid fragrance composition of the present invention is 0.01 to 40% by weight, preferably 0.1 to 40% by weight.
It is desirably about 30% by weight.
【００１８】本発明の液体芳香剤組成物は、前記香料に
加え、消臭剤をさらに含むことができる。前記消臭剤と
しては、前記揮発性シリコーン化合物に可溶であれば特
に限定されないが、ピルビン酸エステル類、メタアクリ
ル酸エステル類、２−エチルヘキサン酸亜鉛、リシノー
ル酸亜鉛等の各種の油溶性消臭剤を挙げることができ
る。The liquid fragrance composition of the present invention may further contain a deodorant in addition to the above-mentioned fragrance. The deodorant is not particularly limited as long as it is soluble in the volatile silicone compound, and various oil-soluble substances such as pyruvate, methacrylate, zinc 2-ethylhexanoate, and zinc ricinoleate are used. Deodorants can be mentioned.
【００１９】本発明の液体芳香剤組成物中の前記消臭剤
の含有割合は、０．０１〜４０重量％、好ましくは０．
１〜３０重量％であることが望ましい。The content of the deodorant in the liquid fragrance composition of the present invention is 0.01 to 40% by weight, preferably 0.1 to 40% by weight.
Desirably, it is 1 to 30% by weight.
【００２０】本発明の液体芳香剤組成物は、前記揮発性
シリコーン化合物、香料、消臭剤の他に、液体芳香剤組
成物の揮散速度を調整する、消臭剤の消臭効果を高める
等の目的で、他の有機成分を適宜配合することができ
る。The liquid fragrance composition of the present invention controls the volatilization rate of the liquid fragrance composition, enhances the deodorizing effect of the deodorant, etc., in addition to the volatile silicone compound, fragrance and deodorant. For the purpose of the above, other organic components can be appropriately blended.
【００２１】前記他の有機成分としては、アルコール
類、グリコールモノエーテル類、ｎ−パラフィン系炭化
水素、イソパラフィン系炭化水素、テルペン系炭化水素
等を挙げることができる。前記アルコール類としては、
メタノール、エタノール、イソプロピルアルコール等が
挙げられる。前記グリコールモノエーテル類としては、
ジエチレングリコールモノエチルエーテル、３−メチル
−３−メトキシブタノール等が挙げられる。前記ｎ−パ
ラフィン系炭化水素としては、ｎ−ノナン、ｎ−デカ
ン、ｎ−ウンデカン、ｎ−ドデカン等が挙げられる。前
記イソパラフィン系炭化水素としては、炭素数８から１
４までのイソパラフィン系炭化水素が挙げられる。前記
テルペン系炭化水素としては、α−ピネン、β−ピネ
ン、α−リモネン、ｌ−リモネン、ジペンテン、ターピ
ノーレン、ピナン、ｐ−メンタン、ｌ−ｐ−メンテン、
γ−テルピネン等が挙げられる。Examples of the other organic components include alcohols, glycol monoethers, n-paraffinic hydrocarbons, isoparaffinic hydrocarbons, terpene hydrocarbons and the like. As the alcohols,
Examples include methanol, ethanol, and isopropyl alcohol. As the glycol monoethers,
Examples thereof include diethylene glycol monoethyl ether and 3-methyl-3-methoxybutanol. Examples of the n-paraffinic hydrocarbon include n-nonane, n-decane, n-undecane, n-dodecane and the like. The isoparaffinic hydrocarbon may have 8 to 1 carbon atoms.
Up to 4 isoparaffinic hydrocarbons. Examples of the terpene hydrocarbon include α-pinene, β-pinene, α-limonene, l-limonene, dipentene, terpinolene, pinane, p-menthane, l-p-menthene,
γ-terpinene and the like.
【００２２】本発明の液体芳香剤組成物中の前記他の有
機成分の含有割合は、特に限定されないが、１重量％以
上５９．９９重量％以下の含有割合で混合することが好
ましい。The content ratio of the other organic components in the liquid fragrance composition of the present invention is not particularly limited, but it is preferable that the other organic components are mixed at a content ratio of 1% by weight or more and 59.99% by weight or less.
【００２３】本発明の液体芳香剤組成物は、前記他の有
機成分の他に、さらに、酸化防止剤、防腐剤、紫外線吸
収剤、油溶性色素等の通常の添加剤を含むことができ
る。The liquid fragrance composition of the present invention may further contain ordinary additives such as antioxidants, preservatives, ultraviolet absorbers and oil-soluble dyes, in addition to the above-mentioned other organic components.
【００２４】本発明の液体芳香剤組成物の用途として
は、特に限定されないが、室内の芳香消臭、自動車内の
芳香消臭、トイレ内の芳香消臭、げた箱内の芳香消臭、
台所回りの芳香消臭、浴室内の芳香消臭等に使用するこ
とができる。The use of the liquid fragrance composition of the present invention is not particularly limited, but may include deodorization in a room, deodorization in a car, deodorization in a toilet, deodorization in a box,
It can be used for aroma deodorization around the kitchen, aroma deodorization in the bathroom, etc.
【００２５】[0025]
【発明の効果】本発明の液体芳香剤組成物は、基剤とし
て揮発性シリコーン化合物を含むため、香りの拡散性の
強い液体芳香剤組成物とすることができる。Since the liquid fragrance composition of the present invention contains a volatile silicone compound as a base, it can be a liquid fragrance composition having a strong scent diffusion property.
【００２６】[0026]
【実施例】以下実施例によりさらに詳細に説明するが、
本発明はこれらに限定されるものではない。The present invention will be described in more detail with reference to the following examples.
The present invention is not limited to these.
【００２７】[0027]
【実施例１】（液体芳香剤の官能評価） 揮発性シリコーン油（ジメチルポリシロキサン）Ｘ−２
１−３０３１（商品名、信越化学工業（株）製）９０ｇ
及び香料（コロンの香り）１０ｇを混合し、液体芳香剤
を調製し、その５ｇを５ｃｍ×５ｃｍ、厚さ３ｍｍの濾
紙に含浸させ、内容積２ｍ3の官能評価室内に３０分間
放置した後、香りの強さを５段階評価法にて評価した。
結果を表１に示す。Example 1 (Sensory evaluation of liquid fragrance) Volatile silicone oil (dimethylpolysiloxane) X-2
1-3031 (trade name, manufactured by Shin-Etsu Chemical Co., Ltd.) 90 g
And flavoring were mixed 10g (fragrance colon), the liquid fragrance is prepared, its 5g of 5 cm × 5 cm, was impregnated into a filter paper having a thickness of 3 mm, allowed to stand for 30 minutes in a sensory evaluation room having an inner volume of 2m 3, The intensity of the scent was evaluated by a five-point evaluation method.
Table 1 shows the results.
【００２８】[0028]
【実施例２】（液体芳香剤の官能評価） シリコーン油としてＸ−２１−３０３１の代わりに、環
状シリコーン油 ＳＨ２４４（商品名、東レダウコーニ
ングシリコーン（株）製）を用いた他は、実施例１と同
様に液体芳香剤を調製し、香りの強さを評価した。結果
を表１に示す。[Example 2] (Sensory evaluation of liquid fragrance) Except that a cyclic silicone oil SH244 (trade name, manufactured by Toray Dow Corning Silicone Co., Ltd.) was used instead of X-21-3031 as the silicone oil. A liquid fragrance was prepared in the same manner as in Example 1, and the intensity of the fragrance was evaluated. Table 1 shows the results.
【００２９】[0029]
【比較例１】（液体芳香剤の官能評価） シリコーン油 Ｘ−２１−３０３１の代わりに、ＩＰソ
ルベント１６２０（商品名、イソパラフィン系炭化水
素、出光石油化学（株）製）を用いた他は、実施例１と
同様に液体芳香剤を調製し、香りの強さを評価した。結
果を表１に示す。Comparative Example 1 (Sensory evaluation of liquid fragrance) Instead of using silicone oil X-21-3031, IP Solvent 1620 (trade name, isoparaffin hydrocarbon, manufactured by Idemitsu Petrochemical Co., Ltd.) was used. A liquid fragrance was prepared in the same manner as in Example 1, and the intensity of the fragrance was evaluated. Table 1 shows the results.
【００３０】[0030]
【表１】 [Table 1]
【００３１】[0031]
【実施例３】（液体芳香消臭剤の消臭効果試験） 揮発性シリコーン油 Ｘ−２１−３０３１を８３．０
ｇ、３−メチル−３−メトキシブタノール１０．０ｇ、
消臭剤として２−エチルヘキサン酸亜鉛２．０ｇ、及び
香料（森の香り）５．０ｇを混合し、液体芳香消臭剤を
調製し、これを被検試料として、アンモニア臭、硫化水
素臭及びメチルメルカプタン臭に対する消臭効果を下記
の方法により測定した。Example 3 (Deodorizing effect test of liquid aromatic deodorant) 83.0 of volatile silicone oil X-21-3031
g, 3-methyl-3-methoxybutanol 10.0 g,
Liquid deodorant was prepared by mixing 2.0 g of zinc 2-ethylhexanoate as a deodorant and 5.0 g of a fragrance (forest fragrance). And the deodorizing effect on methyl mercaptan odor was measured by the following method.
【００３２】消臭効果試験 ５ｃｍ×５ｃｍ、厚さ３ｍｍの濾紙に被検試料溶液５ｇ
を含浸させ、これを１リットル三角フラスコに入れた
後、臭気ガスとしてアンモニア、硫化水素又はメチルメ
ルカプタンを注入し、コック付きガラス管を備えたシリ
コン栓で密封し、１時間後のガス濃度を北川式ガス検知
管で測定した。また、コントロールとして、揮発性シリ
コーン油 Ｘ−２１−３０３１を８５．０ｇ、３−メチ
ル−３−メトキシブタノール１０．０ｇ、及び香料（森
の香り）５．０ｇを混合して調製した試料について同様
に操作し、ガス濃度を測定し、下記に示す式により消臭
率を求めた。結果を表２に示す。 Deodorizing effect test 5 g of a test sample solution was placed on a filter paper of 5 cm × 5 cm and 3 mm thick.
And put it in a 1-liter Erlenmeyer flask, inject ammonia, hydrogen sulfide or methyl mercaptan as an odor gas, seal with a silicon stopper equipped with a glass tube with a cock, and after 1 hour, measure the gas concentration by Kitagawa It was measured with a gas detector tube. As a control, the same applies to a sample prepared by mixing 85.0 g of volatile silicone oil X-21-3031, 10.0 g of 3-methyl-3-methoxybutanol, and 5.0 g of fragrance (forest scent). , The gas concentration was measured, and the deodorization rate was determined by the following equation. Table 2 shows the results.
【００３３】 消臭率（％）＝（（ｃ−ｓ）／ｃ）×１００ ｓ：試験容器中の臭気ガス濃度（ｐｐｍ） ｃ：コントロール容器中の臭気ガス濃度（ｐｐｍ）Deodorization rate (%) = ((cs) / c) × 100 s: Odor gas concentration in test container (ppm) c: Odor gas concentration in control container (ppm)
【００３４】[0034]
【表２】 [Table 2]
───────────────────────────────────────────────────── フロントページの続き (72)発明者 島田 光男 大阪府大阪市東淀川区東淡路１−６−27 大洋香料株式会社研究所内 ────────────────────────────────────────────────── ─── Continued from the front page (72) Mitsuo Shimada Inventor, 1-27-27 Higashiawaji, Higashiyodogawa-ku, Osaka-shi, Osaka
Claims (3)
液体芳香剤組成物。1. A liquid fragrance composition comprising a volatile silicone compound and a fragrance.
される構造を有するジメチルポリシロキサン及び／又は
式（２）で示される構造を有するジメチルポリシロキサ
ン 【化１】 （但し、式中ｍは１から６の整数、ｎは４から６の整
数）からなる請求項１記載の液体芳香剤組成物。2. A dimethylpolysiloxane in which the volatile silicone compound has a structure represented by the formula (1) and / or a dimethylpolysiloxane having a structure represented by the formula (2): The liquid fragrance composition according to claim 1, wherein m is an integer of 1 to 6, and n is an integer of 4 to 6.
求項１又は２記載の液体芳香剤組成物。3. The liquid fragrance composition according to claim 1, further comprising a deodorant.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP9297100A JPH11128331A (en) | 1997-10-29 | 1997-10-29 | Liquid aromatic composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP9297100A JPH11128331A (en) | 1997-10-29 | 1997-10-29 | Liquid aromatic composition |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPH11128331A true JPH11128331A (en) | 1999-05-18 |
Family
ID=17842212
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP9297100A Pending JPH11128331A (en) | 1997-10-29 | 1997-10-29 | Liquid aromatic composition |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH11128331A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004087225A1 (en) * | 2003-04-04 | 2004-10-14 | Robert Mcbride Limited | Air modifiying agent dispenser |
| US6808684B2 (en) * | 2002-04-05 | 2004-10-26 | International Flavors & Fragrance Inc. | Fragrance material |
| US6861031B2 (en) * | 2002-04-05 | 2005-03-01 | International Flavors & Fragrances Inc. | Fragrance material |
| EP3205331A1 (en) * | 2016-02-10 | 2017-08-16 | Henkel IP & Holding GmbH | Diminishing gel compositions and associated methods |
| CN110746201A (en) * | 2019-12-02 | 2020-02-04 | 佛山欧神诺陶瓷有限公司 | Building ceramic tile fragrance slow-release agent and preparation method thereof |
-
1997
- 1997-10-29 JP JP9297100A patent/JPH11128331A/en active Pending
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6808684B2 (en) * | 2002-04-05 | 2004-10-26 | International Flavors & Fragrance Inc. | Fragrance material |
| US6861031B2 (en) * | 2002-04-05 | 2005-03-01 | International Flavors & Fragrances Inc. | Fragrance material |
| US7172998B2 (en) | 2002-04-05 | 2007-02-06 | International Flavors & Fragrances Inc. | Fragrance material |
| WO2004087225A1 (en) * | 2003-04-04 | 2004-10-14 | Robert Mcbride Limited | Air modifiying agent dispenser |
| EP3205331A1 (en) * | 2016-02-10 | 2017-08-16 | Henkel IP & Holding GmbH | Diminishing gel compositions and associated methods |
| US10258707B2 (en) | 2016-02-10 | 2019-04-16 | Henkel IP & Holding GmbH | Diminishing gel compositions and associated methods |
| CN110746201A (en) * | 2019-12-02 | 2020-02-04 | 佛山欧神诺陶瓷有限公司 | Building ceramic tile fragrance slow-release agent and preparation method thereof |
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